CN106333384B - A kind of mixed type tobacco molecular distillation light component electronic cigarette liquid and preparation method thereof - Google Patents
A kind of mixed type tobacco molecular distillation light component electronic cigarette liquid and preparation method thereof Download PDFInfo
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- CN106333384B CN106333384B CN201610934054.4A CN201610934054A CN106333384B CN 106333384 B CN106333384 B CN 106333384B CN 201610934054 A CN201610934054 A CN 201610934054A CN 106333384 B CN106333384 B CN 106333384B
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- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 196
- 241000208125 Nicotiana Species 0.000 title claims abstract description 189
- 238000000199 molecular distillation Methods 0.000 title claims abstract description 75
- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 28
- 239000007788 liquid Substances 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 239000000284 extract Substances 0.000 claims abstract description 155
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 32
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 12
- 235000016068 Berberis vulgaris Nutrition 0.000 claims abstract description 11
- 241000335053 Beta vulgaris Species 0.000 claims abstract description 11
- 244000241838 Lycium barbarum Species 0.000 claims abstract description 11
- 235000015459 Lycium barbarum Nutrition 0.000 claims abstract description 11
- 235000015468 Lycium chinense Nutrition 0.000 claims abstract description 11
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 11
- 235000001453 Glycyrrhiza echinata Nutrition 0.000 claims abstract description 10
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 claims abstract description 10
- 235000017382 Glycyrrhiza lepidota Nutrition 0.000 claims abstract description 10
- 229940010454 licorice Drugs 0.000 claims abstract description 10
- 239000002562 thickening agent Substances 0.000 claims abstract description 10
- 235000011187 glycerol Nutrition 0.000 claims abstract description 9
- 239000003381 stabilizer Substances 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 7
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 7
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical class CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims abstract 5
- 235000019437 butane-1,3-diol Nutrition 0.000 claims abstract 3
- 235000019504 cigarettes Nutrition 0.000 claims description 32
- 235000013599 spices Nutrition 0.000 claims description 25
- 239000002994 raw material Substances 0.000 claims description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 13
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 11
- 239000000706 filtrate Substances 0.000 claims description 7
- AXPZIVKEZRHGAS-UHFFFAOYSA-N 3-benzyl-5-[(2-nitrophenoxy)methyl]oxolan-2-one Chemical compound [O-][N+](=O)C1=CC=CC=C1OCC1OC(=O)C(CC=2C=CC=CC=2)C1 AXPZIVKEZRHGAS-UHFFFAOYSA-N 0.000 claims description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 6
- 239000011734 sodium Substances 0.000 claims description 6
- 229910052708 sodium Inorganic materials 0.000 claims description 6
- 244000303040 Glycyrrhiza glabra Species 0.000 claims description 5
- 229920002907 Guar gum Polymers 0.000 claims description 5
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 5
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 5
- 238000004821 distillation Methods 0.000 claims description 5
- 239000000665 guar gum Substances 0.000 claims description 5
- 235000010417 guar gum Nutrition 0.000 claims description 5
- 229960002154 guar gum Drugs 0.000 claims description 5
- 102000004169 proteins and genes Human genes 0.000 claims description 5
- 108090000623 proteins and genes Proteins 0.000 claims description 5
- 235000010413 sodium alginate Nutrition 0.000 claims description 5
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims description 5
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims description 5
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 4
- 239000000661 sodium alginate Substances 0.000 claims description 4
- 229940005550 sodium alginate Drugs 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 229940058015 1,3-butylene glycol Drugs 0.000 claims 2
- 238000002242 deionisation method Methods 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 9
- 239000002304 perfume Substances 0.000 abstract description 7
- 240000004670 Glycyrrhiza echinata Species 0.000 abstract 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 15
- 239000000779 smoke Substances 0.000 description 15
- 244000061176 Nicotiana tabacum Species 0.000 description 7
- 230000000391 smoking effect Effects 0.000 description 7
- 206010011224 Cough Diseases 0.000 description 4
- 241000202807 Glycyrrhiza Species 0.000 description 4
- 238000001514 detection method Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 210000000697 sensory organ Anatomy 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 244000303965 Cyamopsis psoralioides Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 239000008896 Opium Substances 0.000 description 1
- 208000004224 Opium Dependence Diseases 0.000 description 1
- 201000007100 Pharyngitis Diseases 0.000 description 1
- 206010036790 Productive cough Diseases 0.000 description 1
- 206010044302 Tracheitis Diseases 0.000 description 1
- 244000126002 Ziziphus vulgaris Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 206010006451 bronchitis Diseases 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 239000000469 ethanolic extract Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 229960001027 opium Drugs 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000002685 pulmonary effect Effects 0.000 description 1
- 208000023504 respiratory system disease Diseases 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 208000024794 sputum Diseases 0.000 description 1
- 210000003802 sputum Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A24F47/002—
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention provides a kind of mixed type tobacco molecular distillation light component electronic cigarette liquid and preparation method thereof.The electronics tobacco tar is that thickener and stabilizer are added after deionized water is heated, it is sufficiently stirred for, then adds mixed type tobacco molecular distillation light component and be uniformly mixing to obtain mixed liquor, then by natural flavouring essence for tobacco, glycerine and 1,3 butanediols are added in mixed liquor, and stirring at normal temperatures is obtained.Wherein described mixed type tobacco molecular distillation light component is formulated after the mixing of flue-cured tobacco molecular distillation light component, Turkish tobaccos molecular distillation light component and Maryland molecular distillation light component, and the natural flavouring essence for tobacco is to be formulated by licorice, beet extract, wolfberry fruit extract, red date extract according to mass percent.The present invention prepares electronic cigarette liquid energy allows you to obtain larger satisfaction again while tar is relatively low, and is perfume quantity foot, mouthfeel coordination, and fragrance, pleasant impression is pure, assigns the fragrance of tobacco feature.
Description
Technical field
The invention belongs to electronic cigarette technical field, the specifically a kind of sub- electronic cigarette liquid of mixed type tobacco molecular distillation light component
And preparation method thereof.
Background technology
What the flue gas that the consumption pattern of cigarette is mainly cigarette combustion generation was carried out, flue gas easily causes smoker to suffer from respectively
Plant respiratory disease, the symptom such as tracheitis, bronchitis, pharyngitis, coughing with a lot of sputum.Hybrid cigarette compares traditional cigarette
You can be allowed to obtain larger satisfaction again while tar is relatively low, hybrid cigarette is with several different types of tobacco leaves
Configuration mixing by a certain percentage, usually with flue-cured tobacco, Turkish tobaccos, Maryland, which together mixes presentation mouthfeel, to be coordinated, and fragrance is remaining
Taste is pure.
Electronic cigarette is into particulate, by pulmonary absorption, together by the solution atomization containing tobacco extract and flavouring essence for tobacco
When spue simulation smoke, electronic cigarette has the outward appearance similar to cigarette and close taste, cigarette can be also suctioned out as cigarette
Taste and sensation, but there is no other harmful components such as tar, suspended particulates in cigarette in electronic cigarette, will not produce two yet
Hand cigarette also will not diffuse or curl up in confined space；And conventional cigarette is, with tobacco leaf or tobacco ignition, to compromise simultaneously
Smoker and the health of non-smoker.Reducing tar and reducing harm is always the emphasis problem of tobacco business, in recent years, with various circles of society pair
Smoking and the pay attention to day by day of healthy relation, Tobacco Control action are risen in many places, and ban on opium-smoking and the opium trade the going out of regulation comprehensively for public arena
Platform, but many cigarette smokers can not give up cigarette again, so in order to reduce harm of smoking, people can be with electronic cigarette come generation
For cigarette.
Although although electronic cigarette can reduce harm of smoking, the discomfort of smoker's throat and lung can not be improved；And
The problem of current electronics smoke product also has one generally, is exactly that electronic cigarette liquid lacks the flavor characteristics of tobacco or tobacco flavor spy
Levy weak, there is relatively large deviation with sucking cigarette in style, on the whole close to style food.
The content of the invention
It is an object of the invention to overcome the shortcomings of existing tobacco juice for electronic smoke, there is provided a kind of mixed type tobacco molecular distillation is light
Group molecule electronic cigarette liquid and preparation method thereof, it by different types of leaf tobacco extract is raw material that the electronic cigarette liquid, which is, improves electricity
Basic smoke, the cigarette perfume of sub- cigarette are rich, fine and smooth sense and satisfaction, while can play cough-relieving refreshing effect again, increase throat
Comfort.
The purpose of the present invention is achieved by following technical proposals：A kind of mixed type tobacco molecular distillation light component electronics
Tobacco juice, it is characterised in that include the component of following percetage by weight：
Said components overall weight percent is 100%；
Wherein, the mixed type tobacco molecular distillation light component is made up of the component of following mass percent：Flue-cured tobacco is carried
Take thing light component 20-45%, spices tobacco extract light component 20-45%, Maryland extract light component 20-45%；
The natural tobacco aromaticss are made up of the component of following mass percent：Licorice 5-35%, beet is carried
Take thing 5-35%, wolfberry fruit extract 5-35%, red date extract 5-35%；Said extracted thing is the commodity directly bought, its
Middle licorice is purchased from Shaanxi Yong Yuan Bioisystech Co., Ltd；Beet extract is purchased from the clear happy limited public affairs of biotechnology in Xi'an
Department；Wolfberry fruit extract is purchased from Guangzhou Huabao Flavor Co., Ltd.；Red date extract is limited purchased from the precious essence and flavoring agent of Guangzhou China
Company；
The thickener is from one or both of sodium alginate, sodium carboxymethylcellulose and network protein acid sodium；
The present invention preferably technical scheme：The stabilizer is guar gum.
Heretofore described flue-cured tobacco extract light component, spices tobacco extract light component, Maryland extract light component
It is using flue-cured tobacco, Turkish tobaccos and Maryland as raw material, after being shredded, according to solid-liquid ratio 1 respectively:10 addition concentration are 50%
Ethanol extracts 2-3h under conditions of temperature is 60-70 DEG C, then filters extract solution, takes filtrate true under the conditions of 50 DEG C respectively
Sky is concentrated into flue-cured tobacco extract, spices tobacco extract and the Maryland extract of the density 1.150~1.170 of relative water, then
The propane diols that its weight is 20% is added to the extract solution obtained after concentration respectively and carry out molecular distillation, obtain the density of relative water
For 1.030~1.040 flue-cured tobacco extract light component, spices tobacco extract light component and Maryland extract light component；Institute
The condition for stating molecular distillation is：Vapo(u)rizing temperature be 50~60 DEG C, material flow be 2~2.5ml/min, knifing rotating speed be 60~
70r/min, vacuum is 15~25Pa.
A kind of preparation method for mixed type tobacco molecular distillation light component electronic cigarette liquid that the present invention is provided, it is characterised in that
Comprise the following steps that：
(1) flue-cured tobacco raw material is taken, 50% ethanol of 10 times of its weight is added after being crushed under the conditions of temperature is 60-70 DEG C
2-3h is extracted, after extract solution is filtered, it is 1.150~1.170 in the density that 50 DEG C of conditions are concentrated into relative water to take filtrate, is obtained
Flue-cured tobacco extract；
(2) the flue-cured tobacco extract prepared in step (1) is taken, the propane diols of flue-cured tobacco extract weight 20% is added, and mixed
It is added to after uniform in molecular distillation instrument and carries out molecular distillation, retain the distillation light component flowed out along chamber walls, detects flue-cured tobacco
Extract light component is 1.030~1.040 with respect to the density of water, that is, obtains the flue-cured tobacco molecular distillation light component；Described the third two
The addition of alcohol is 20% of total mixed liquor weight before molecular distillation, and the condition of molecular distillation is：Vapo(u)rizing temperature is 50~60 DEG C,
Material flow is 2~2.5ml/min, and knifing rotating speed is 60~70r/min, and vacuum is 15~25Pa；
(3) using Turkish tobaccos as raw material, repeat step (1) and step (2) obtain Turkish tobaccos molecular distillation light component；The perfume (or spice)
The density for expecting the relative water of cigarette molecular distillation light component is 1.030~1.040；
(4) using Maryland as raw material, repeat step (1) and step (2) obtain Maryland molecular distillation light component；Institute
The density for stating the relative water of Maryland molecular distillation light component is 1.030~1.040；
(5) component proportion according to mixed type tobacco molecular distillation light component in claim 1 will be prepared in step (3)
The Maryland prepared in the Turkish tobaccos molecular distillation light component and step (5) that are prepared in flue-cured tobacco molecular distillation light component, step (4)
Mixed type tobacco molecular distillation light component is configured to after the mixing of cigarette molecular distillation light component；
(6) raw material is prepared according to the weight percentages of components of following mixed type tobacco molecular distillation light component electronic cigarette liquid：
Mixed type tobacco molecular distillation the light component 45-65%, natural tobacco aromaticss 6-14%, glycerine 5-10% prepared in step (5),
Deionized water 5-15%, thickener 3-6%, stabilizer 0.5-2%, surplus is 1,3-BDO；The natural flavouring essence for tobacco is
It is formulated by licorice, beet extract, wolfberry fruit extract, red date extract according to mass percent；The thickening
Agent is from one or both of sodium alginate, sodium carboxymethylcellulose and network protein acid sodium；The stabilizer uses guar gum.
(7) deionized water is heated to 50~70 DEG C, adds thickener and stabilizer, be sufficiently stirred for, then add mixing
Type tobacco molecular distillation light component is uniformly mixing to obtain mixed liquor；
(8) natural flavouring essence for tobacco, glycerine and 1,3-BDO is added in the mixed liquor prepared in step (7), in normal temperature
Under stir and just obtain the tobacco juice for electronic smoke of the mixed type tobacco molecular distillation light component.
Compared with prior art, the present invention has advantages below：
1st, the flue-cured tobacco extract light component, spices tobacco extract light component and Maryland extract light component propane diols
Content is up to more than 60%, so being used as solvent without addition propane diols in addition；
2nd, compared with conventional hybrid type cigarette, the electronic cigarette liquid energy of mixed type tobacco molecular distillation light component is in tar phase
To it is relatively low while allow you to obtain larger satisfaction again, and be that perfume quantity foot, mouthfeel are coordinated, fragrance, pleasant impression is pure, assigns cigarette
The fragrance of careless feature；
3rd, natural tobacco aromaticss licorice, beet extract, wolfberry fruit extract, jujube are added in tobacco juice for electronic smoke
Extract can play cough-relieving refreshing effect, increase throat comfort, at the same can play it is abundant, coordinate electronic cigarette cigarette perfume, can be with
Meet the smoking demand of smoker.
Embodiment
The invention is further illustrated by the following examples, it will be appreciated that embodiment is not right only to explain the present invention
The restriction of technical solution of the present invention.
Embodiment 1, a kind of mixed type tobacco molecular distillation light component electronic cigarette liquid, is prepared from by following steps：
(1) mixed type tobacco molecular distillation light component is prepared：
A, 10kg flue-cured tobaccos are crushed, add 100kg concentration and extract 2h for 50% ethanol stirring, Extracting temperature is 60 DEG C；
After extract solution is filtered, take out filtrate and acquisition flue-cured tobacco extract is concentrated in vacuo under the conditions of 50 DEG C, flue-cured tobacco extract is with respect to water
Density is 1.150~1.170；
B, the flue-cured tobacco extract progress molecular distillation by gained：The flue-cured tobacco extract 1000g prepared in step a is weighed, plus
Enter 200g propane diols, be added in molecular distillation instrument and distilled after being well mixed：Molecular distillation is determined by Preliminary Experiment
The optimum condition for preparing flue-cured tobacco extract light component is：Vapo(u)rizing temperature is 60 DEG C, and material flow is 2ml/min, and knifing rotating speed is
60r/min, vacuum is 25Pa；Retain the distillation light component flowed out along chamber walls, detection flue-cured tobacco extract light component is relative
The density of water is 1.0380；
C, spices tobacco extract light component and Maryland extract light component preparation detect Turkish tobaccos with step a and b
Extract light component is 1.0385 with respect to the density of water, and Maryland extract light component is 1.0392 with respect to the density of water；
D, by above-mentioned flue-cured tobacco extract light component, spices tobacco extract light component and Maryland extract light component according to
Following mass percent is hybridly prepared into mixed type tobacco molecular distillation light component：Flue-cured tobacco extract light component 20%, Turkish tobaccos
Extract light component 35%, Maryland extract light component 45%；
(2) preparation raw material of natural tobacco aromaticss is prepared according to the material of following mass percent：Licorice 20%,
Beet extract 25%, wolfberry fruit extract 30%, red date extract 25%；Then above-mentioned raw materials are stirred at normal temperatures
Natural tobacco aromaticss；
(3) 5g deionized waters are weighed and are heated to 50 DEG C, 3g sodium alginates, 0.5g guar gums is added, 50g steps are then added
(1) the mixed type tobacco molecular distillation light component prepared in, stirring and dissolving uniformly obtains mixed liquor；
(4) the natural flavouring essence for tobacco prepared in 8g steps (2) is weighed, 5g glycerine and 1,3-BDO 28.5g add step
(3) in the mixed liquor prepared in, stir just obtain the electronics of the mixed type tobacco molecular distillation light component at normal temperatures
Cigarette tobacco juice (1).
Embodiment 2, a kind of mixed type tobacco molecular distillation light component electronic cigarette liquid, is prepared from by following steps：
(1) mixed type tobacco molecular distillation light component is prepared：
A, 10kg flue-cured tobaccos are crushed, add 100kg concentration and extract 2.5h for 50% ethanol stirring, Extracting temperature is 70
℃；After extract solution is filtered, take out filtrate and acquisition flue-cured tobacco extract is concentrated in vacuo under the conditions of 50 DEG C, flue-cured tobacco extract is with respect to water
Density be 1.150~1.170；
B, the flue-cured tobacco extract progress molecular distillation by gained：The flue-cured tobacco extract 1000g prepared in step a is weighed, plus
Enter 200g propane diols, be well mixed, be added in molecular distillation instrument and distilled：Molecular distillation system is determined by Preliminary Experiment
The optimum condition of standby flue-cured tobacco extract light component is：Vapo(u)rizing temperature is 50 DEG C, and material flow is 2.5ml/min, and knifing rotating speed is
70r/min, vacuum is 20Pa；Retain the distillation light component flowed out along chamber walls, detection flue-cured tobacco extract light component is relative
The density of water is 1.0395；
C, spices tobacco extract light component and Maryland extract light component preparation detect Turkish tobaccos with step a and b
Extract light component is 1.0389 with respect to the density of water, and Maryland extract light component is 1.0385 with respect to the density of water；
D, by above-mentioned flue-cured tobacco extract light component, spices tobacco extract light component and Maryland extract light component according to
Following mass percent is hybridly prepared into mixed type tobacco molecular distillation light component：Flue-cured tobacco extract light component 30%, Turkish tobaccos
Extract light component 35%, Maryland extract light component 35%；
(2) preparation raw material of natural tobacco aromaticss is prepared according to the material of following mass percent：Licorice 25%,
Beet extract 25%, wolfberry fruit extract 20%, red date extract 30%；Then above-mentioned raw materials are stirred at normal temperatures
Natural tobacco aromaticss；
(3) weigh deionized water 6g and be heated to 50 DEG C, add sodium carboxymethylcellulose 4g, guar gum 0.8g, then add
The mixed type tobacco molecular distillation light component prepared in 55g steps (1), stirring and dissolving uniformly obtains mixed liquor；
(4) weigh the natural flavouring essence for tobacco 10g, glycerine 7g and 1,3-BDO 17.2g prepared in step (2) and add step
(3) in the mixed liquor prepared in, stir just obtain the electronics of the mixed type tobacco molecular distillation light component at normal temperatures
Cigarette tobacco juice (2).
Embodiment 3, a kind of mixed type tobacco molecular distillation light component electronic cigarette liquid, is prepared from by following steps：
(1) mixed type tobacco molecular distillation light component is prepared：
A, 10kg flue-cured tobaccos are crushed, add 100kg concentration and extract 3h for 50% ethanol stirring, Extracting temperature is 65 DEG C；
After extract solution is filtered, take out filtrate and acquisition flue-cured tobacco extract is concentrated in vacuo under the conditions of 50 DEG C, flue-cured tobacco extract is with respect to water
Density is 1.150~1.170；
B, the flue-cured tobacco extract progress molecular distillation by gained：The flue-cured tobacco extract 1000g prepared in step a is weighed, plus
Enter 200g propane diols, be well mixed, be added in molecular distillation instrument and distilled：Molecular distillation system is determined by Preliminary Experiment
The optimum condition of standby flue-cured tobacco extract light component is：Vapo(u)rizing temperature is 57 DEG C, and material flow is 2ml/min, and knifing rotating speed is
60r/min, vacuum is 15Pa；Retain the distillation light component flowed out along chamber walls, detection flue-cured tobacco extract light component is relative
The density of water is 1.0395；
C, spices tobacco extract light component and Maryland extract light component preparation detect Turkish tobaccos with step a and b
Extract light component is 1.0396 with respect to the density of water, and Maryland extract light component is 1.0394 with respect to the density of water；
D, by above-mentioned flue-cured tobacco extract light component, spices tobacco extract light component and Maryland extract light component according to
Following mass percent is hybridly prepared into mixed type tobacco molecular distillation light component：Flue-cured tobacco extract light component 28%, Turkish tobaccos
Extract light component 42%, Maryland extract light component 30%；
(2) preparation raw material of natural tobacco aromaticss is prepared according to the material of following mass percent：Licorice 27%,
Beet extract 24%, wolfberry fruit extract 26%, red date extract 23%；Then above-mentioned raw materials are stirred at normal temperatures
Natural tobacco aromaticss；
(3) weigh deionized water 7g and be heated to 50 DEG C, add sodium alginate 2, network protein acid sodium 3g, guar gum 1g, then
The mixed type tobacco molecular distillation light component prepared in 57g steps (1) is added, stirring and dissolving uniformly obtains mixed liquor；
D, weigh natural flavouring essence for tobacco 12g, glycerine 8g and 1,3-BDO 10g and add in the mixed liquor prepared in step c,
Stir at normal temperatures and just obtain the tobacco juice for electronic smoke (3) of the mixed type tobacco molecular distillation light component.
By the flue-cured tobacco extract obtained in above-described embodiment 1 and flue-cured tobacco extract light component, spices tobacco extract and spices
Tobacco extract light component, Maryland extract and Maryland extract light component enter to pass through GC-MS analysis, identify respectively
26 and 27,32 and 31,29 and 30 kind of volatile ingredient and tar percentage contents, it the results are shown in Table one.
Table 1 is flue-cured tobacco extract and flue-cured tobacco extract light component, spices tobacco extract and spices tobacco extract light component, horse
In blue tobacco extract and Maryland extract light component main volatile chemical composition and the contrast of tar percentage contents
It can show that flue-cured tobacco extract, spices tobacco extract, Maryland extract are handled through molecular distillation by table one
The fragrance matter of tobacco itself can be enriched with, tar percentage contents are reduced.
The flue-cured tobacco extract light component obtained in above-described embodiment 1, spices tobacco extract light component, Maryland are extracted
Thing light component detects percentage contents of the propane diols in extract light component by GB/T-23813-2009, the results are shown in Table
Two.
The flue-cured tobacco extract light component of table 2, spices tobacco extract light component, the main propane diols phase of Maryland extract light component
To percentage composition
It can be drawn by table two and be used as solvent without adding propane diols again in the above-described embodiments
The electronic cigarette tobacco tar that each component ratio of comparative example 1,2 and 3 is made is added to identical with identical addition
In disposable electric cigarette, and contrast sensory evaluation is carried out with traditional cigarette, the standard of smokeing panel test uses GB5606.4-2005, sense organ matter
Amount evaluation result is shown in Table 3,
Table 3：Tobacco juice for electronic smoke 1,2 and 3 contrasts smoking result with blended type cigarette sense organ
| Sample | Gloss | Fragrance | Coordinate | Miscellaneous gas | Stimulate | Pleasant impression | It is total |
| Blended type cigarette | 0 | 24.5 | 4.5 | 8.4 | 17.0 | 21.0 | 75.4 |
| Tobacco juice for electronic smoke 1 | 0 | 24.3 | 4.3 | 8.0 | 16.2 | 20.5 | 73.3 |
| Tobacco juice for electronic smoke 2 | 0 | 24.4 | 4.3 | 8.1 | 16.1 | 20.6 | 73.5 |
| Tobacco juice for electronic smoke 3 | 0 | 24.0 | 4.4 | 8.3 | 16.0 | 20.4 | 73.3 |
Drawn by table 3, the tobacco juice for electronic smoke obtained by the application is approached with traditional cigarette on sensory evaluating smoking.
The tobacco juice for electronic smoke of mixed type tobacco molecular distillation light component obtained by this patent and conventional hybrid type are fragrant in summary
Cigarette is compared, and you can be allowed to obtain larger satisfaction again while tar is relatively low, and be perfume quantity foot, mouthfeel coordination, sweet smell
Virtue, pleasant impression is pure, assigns the fragrance of tobacco feature；Natural tobacco aromaticss licorice, beet are added in tobacco juice for electronic smoke
Extract, wolfberry fruit extract, red date extract can play cough-relieving refreshing effect, increase throat comfort, while can play rich
Rich, coordination electronic cigarette cigarette perfume, can meet the smoking demand of smoker, have wide application prospect in tobacco juice for electronic smoke market.
Claims (3)
1. a kind of mixed type tobacco molecular distillation light component electronic cigarette liquid, it is characterised in that include the group of following percetage by weight
Point：
Mixed type tobacco molecular distillation light component 45-65%
Natural tobacco aromaticss 6-14%
Glycerine 5-10%
Deionized water 5-15%
Thickener 3-6%
Stabilizer 0.5-2%
1,3 butylene glycol surplus
Said components overall weight percent is 100%；
Wherein, the mixed type tobacco molecular distillation light component is made up of the component of following mass percent：Flue-cured tobacco extract
Light component 20-45%, spices tobacco extract light component 20-45%, Maryland extract light component 20-45%；
The flue-cured tobacco extract light component, spices tobacco extract light component, Maryland extract light component be respectively with flue-cured tobacco,
Turkish tobaccos and Maryland are raw material, after being shredded, according to solid-liquid ratio 1:10 add the ethanol that concentration are 50% is in temperature
2-3h is extracted under conditions of 60-70 DEG C, then extract solution is filtered, takes filtrate to be concentrated in vacuo to respectively under the conditions of 50 DEG C relatively
Flue-cured tobacco extract, spices tobacco extract and the Maryland extract of the density 1.150 ~ 1.170 of water, then respectively to after concentration
To extract in add the propane diols of its weight 20% and carry out molecular distillation, it is 1.030 ~ 1.040 to obtain the density of relative water
Flue-cured tobacco extract light component, spices tobacco extract light component and Maryland extract light component；The condition of the molecular distillation
For：Vapo(u)rizing temperature is 50~60 DEG C, and material flow is 2~2.5ml/min, and knifing rotating speed is 60~70r/min, and vacuum is 15
~25Pa;
The natural tobacco aromaticss are made up of the component of following mass percent：Licorice 5-35%, beet extract 5-
35%, wolfberry fruit extract 5-35%, red date extract 5-35%；
The thickener is from one or both of sodium alginate, sodium carboxymethylcellulose and network protein acid sodium.
2. a kind of mixed type tobacco molecular distillation light component electronic cigarette liquid according to claim 1, it is characterised in that：It is described
Stabilizer is guar gum.
3. a kind of preparation method of the mixed type tobacco molecular distillation light component electronic cigarette liquid described in claim 1, its feature
It is to comprise the following steps that：
（1）Flue-cured tobacco raw material is taken, 50% ethanol that 10 times of its weight is added after being crushed is extracted under the conditions of temperature is 60-70 DEG C
2-3h, after extract solution is filtered, it is 1.150 ~ 1.170 in the density that 50 DEG C of conditions are concentrated into relative water to take filtrate, obtains flue-cured tobacco
Extract；
（2）Take step（1）The flue-cured tobacco extract of middle preparation, adds the propane diols of flue-cured tobacco extract weight 20%, and it is well mixed after
It is added in molecular distillation instrument and carries out molecular distillation, retain the distillation light component flowed out along chamber walls, detects flue-cured tobacco extract
Light component is 1.030 ~ 1.040 with respect to the density of water, that is, obtains the flue-cured tobacco extract light component；The condition of molecular distillation is：
Vapo(u)rizing temperature be 50~60 DEG C, material flow be 2~2.5ml/min, knifing rotating speed be 60~70r/min, vacuum be 15~
25Pa；
（3）Using Turkish tobaccos as raw material, repeat step（1）And step（2）Obtain spices tobacco extract light component；The Turkish tobaccos are carried
The density for taking the relative water of thing light component is 1.030 ~ 1.040；
（4）Using Maryland as raw material, repeat step（1）And step（2）Obtain Maryland extract light component；The Mali
The density of the relative water of blue tobacco extract light component is 1.030 ~ 1.040；
（5）Mixed type tobacco molecular distillation light component is made in the material mixing of the component of following mass percent：Step（2）In
The flue-cured tobacco extract light component 20-45% of preparation, step（3）The spices tobacco extract light component 20-45% of middle preparation, step（4）
The Maryland extract light component 20-45% of middle preparation；
（6）Prepare raw material according to the weight percentages of components of following mixed type tobacco molecular distillation light component electronic cigarette liquid：Step
（5）Mixed type tobacco molecular distillation the light component 45-65%, natural tobacco aromaticss 6-14%, glycerine 5-10%, deionization of middle preparation
Water 5-15%, thickener 3-6%, stabilizer 0.5-2%, surplus is 1,3-BDO；The natural tobacco aromaticss are extracted by radix glycyrrhizae
Thing, beet extract, wolfberry fruit extract, red date extract are formulated according to mass percent；The thickener selects marine alga
One or both of sour sodium, sodium carboxymethylcellulose and network protein acid sodium；
（7）Deionized water is heated to 50~70 DEG C, thickener and stabilizer is added, is sufficiently stirred for, mixed type cigarette is then added
Careless molecular distillation light component is uniformly mixing to obtain mixed liquor；
（8）Natural tobacco aromaticss, glycerine and 1,3 butylene glycol are added into step（7）In the mixed liquor of middle preparation, stir at normal temperatures
Mix and uniformly just obtain the mixed type tobacco molecular distillation light component electronic cigarette liquid.
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