CN104687240B - There is electronic cigarette liquid of Ambra Grisea fragrance and preparation method thereof - Google Patents
There is electronic cigarette liquid of Ambra Grisea fragrance and preparation method thereof Download PDFInfo
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- CN104687240B CN104687240B CN201510027817.2A CN201510027817A CN104687240B CN 104687240 B CN104687240 B CN 104687240B CN 201510027817 A CN201510027817 A CN 201510027817A CN 104687240 B CN104687240 B CN 104687240B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
Abstract
The invention discloses a kind of tobacco juice for electronic smoke with Ambra Grisea fragrance, it is characterized in that, electronic cigarette liquid and preparation method thereof described in every 1 5mL is as follows: be dissolved in the mixed solution of the water of 1 5mL, propylene glycol and glycerol by the Ambra Grisea fragrance solution of the tobacco extract solution of 0.005 0.02mL, the flavouring essence for tobacco solution of 0.001 0.01mL and 0.005 0.05mL, the invention have the benefit that tobacco juice for electronic smoke prepared by the present invention, there is fresh and sweet odor type style and features, and with noble quiet and tastefully laid out Ambra Grisea fragrance, enrich the suction local flavor of electronic cigarette；Tobacco juice for electronic smoke prepared by the present invention, in flavouring essence for tobacco used, choosing of flavor component is added according to the content distribution in cigarette smoke with addition, and its fragrance characteristic, closer to cigarette smoke, can more preferably meet consumer's demand to fragrance.
Description
Technical field
The present invention relates to electronic cigarette technical field, be specifically related to a kind of electronic cigarette liquid with Ambra Grisea fragrance and
Its preparation method.
Background technology
Electronic cigarette is a kind of novel tobacco goods, and it is typically made up of elements such as lithium battery, nebulizer, cigarette bullets,
By nebulizer, nicotine solution being atomized into steam state, consumer meets psychological need by suction.With tradition
Medicated cigarette is compared, and electronic cigarette does not contains the harmful substance such as tar, carbon monoxide, less to smoker's actual bodily harm；
It addition, the aerosol that the nicotine of electronic cigarette is formed through atomization, it is rapidly diluted in atmosphere, reduces week
Enclose people and produce the risk of harm.Electronic cigarette, as the succedaneum of medicated cigarette, obtains market in the world and recognizes
Can, sales volume presents ascendant trend year by year.
Electronic cigarette is through the development of several generations, compared with regular-size cigarette, although shape, feel, smog etc. are felt
As Medicated cigarette, but the tobacco juice being used for these electronic cigarettes remains some shortcomings.Compared with traditional cigarette, electronic cigarette
The smog that liquid produces is bigger with traditional cigarette gap in terms of fragrance, although the tobacco juice for electronic smoke of current report has
Tradition extraction means are used to prepare electronic cigarette tobacco extract from Nicotiana tabacum L., again that it is the most fragrant with cigarette
Essence, deionized water, glycerol, propylene glycol etc. are mixed and made into tobacco juice for electronic smoke, but Nicotiana tabacum L. flavor component and cigarette
It is relatively big that gas flavor component compares content difference, is difficult to be simulated in flue gas by interpolation tobacco extract
Flavor component content distribution, smoker generally feels that the perfume quantity of these electronic cigarettes and aroma quality do not reach its life
Reason demand, leverages the sustainable health development of electronic cigarette.
Summary of the invention
Instant invention overcomes prior art to use the tobacco juice for electronic smoke prepared of traditional approach to exist to make smoker universal
Sensation perfume quantity and aroma quality do not reach its psychological need, leverage the sustainable health development of electronic cigarette
Deficiency, it is provided that one realize electronic cigarette simulation cigarette smoke fresh and sweet odor type style and features, and with noble quality excellent
The tobacco juice for electronic smoke with Ambra Grisea fragrance of refined Ambra Grisea fragrance.
For achieving the above object, the present invention is by the following technical solutions:
A kind of tobacco juice for electronic smoke with Ambra Grisea fragrance, electronic cigarette liquid hold-up described in every 1-5mL is as follows:
The tobacco extract solution of 0.005-0.02mL, the flavouring essence for tobacco solution of 0.001-0.01mL and
The Ambra Grisea fragrance solution of 0.005-0.05mL, the water of 1-5mL, propylene glycol and the mixed solution of glycerol.
Further technical scheme is, described tobacco extract solution comprise Huidong County, Sichuan, Huili County,
Puge County, Flos Bombacis Malabarici, Xiangyun, yunnan county red big Nicotiana tabacum L. in one or more.
Further technical scheme is, the concentration of described flavouring essence for tobacco solution is 20%-50%, and solute is that cigarette is used
Essence, solvent is ethanol.
Further technical scheme is, described flavouring essence for tobacco is benzyl alcohol, phenethanol, linalool, Herba Pelargonii Graveolentis
Alcohol, 5 hydroxymethyl furfural, beta-damascenone, β-damascone, alpha, beta-lonone, 2-acetyl furan
In one or more.
Further technical scheme is, described flavouring essence for tobacco is by benzyl alcohol, phenethanol, linalool, Herba Pelargonii Graveolentis
Alcohol, 5 hydroxymethyl furfural, beta-damascenone, β-damascone, alpha, beta-lonone, 2-acetyl furan
Composition, its mass fraction ratio is: 1:(0.5-0.9): (0.2-0.7): (0.1-0.3): (20-70):
(0.05-0.2): (0.05-0.2): (0.1-0.3): (1-3).
Further technical scheme is, the concentration of described Ambra Grisea fragrance solution is 10-30%, and solute is dragon
Saliva essence, solvent is ethanol.
Further technical scheme is, described Ambra Grisea essence is in ambrein and ambrox
Plant or multiple.
Further technical scheme is, described Ambra Grisea essence is made up of ambrein and ambrox,
Its mass fraction ratio is: 1:(0.1-10).
The present invention utilizes GC × GC-ToFMS (two-dimensional gas chromatography time-of-flight mass spectrometry (TOFMS)) measure and there is delicate fragrance
The red big Nicotiana tabacum L. in Huidong County, Sichuan of type style, the red big Nicotiana tabacum L. in Huili County, the red big Nicotiana tabacum L. in Puge County, Flos Bombacis Malabarici are red
Big Nicotiana tabacum L. and Xiangyun, yunnan county red opium cigar flue gas have the material of clear (sweet) fragrant feature content (as
Shown in table 1):
Table 1
According to benzyl alcohol in table 1, phenethanol, linalool, geraniol, 5-methylol-furfural, beta-damascenone, β-
Damascone, alpha, beta-lonone, 2-acetyl furan etc. have the content of the material of clear (sweet) fragrant feature.
By the content of above-mentioned substance in simulation cigarette smoke, thus draw flavouring essence for tobacco be benzyl alcohol, phenethanol,
Linalool, geraniol, 5 hydroxymethyl furfural, beta-damascenone, β-damascone, alpha, beta-lonone,
One or more in 2-acetyl furan, the most described flavouring essence for tobacco can be by benzyl alcohol, phenethanol, virtue
Camphor tree alcohol, geraniol, 5 hydroxymethyl furfural, beta-damascenone, β-damascone, alpha, beta-lonone, 2-
Acetyl furan forms, and its mass fraction ratio is: 1:(0.5-0.9): (0.2-0.7): (0.1-0.3):
(20-70): (0.05-0.2): (0.05-0.2): (0.1-0.3): (1-3), by manually
Allotment flavouring essence for tobacco, due in flavouring essence for tobacco used the composition of fragrance choose with addition be all according to
Content distribution in cigarette smoke is added, and just makes tobacco juice for electronic smoke have simulation cigarette smoke clear (sweet)
Odor type style and features, its fragrance characteristic, closer to cigarette smoke, can better meet consumer to fragrance
Demand.
Heretofore described Ambra Grisea essence is one or more in ambrein and ambrox, simultaneously
Described Ambra Grisea essence is made up of ambrein and ambrox, and its mass fraction ratio is: 1:(0.1-10),
Ambra Grisea is that one of spice is treasured greatly in the world four, has fragrance soft as the most delicate staple, fixation energy
Power is strong, and fragrance is lasting, and harmony is good.The most representational Ambra Grisea material be ambrox and
Ambrein, ambrox has strong, plentiful Ambra Grisea fragrance, and lasting is the most lasting；Ambrein
Fragrance can be produced after placing in atmosphere, after extreme dilution, have pleasant Ambra Grisea gas.Ambra Grisea material
Under variable concentrations, the Ambra Grisea gas of its performance has certain difference, according to conventional amount used plus feeling evaluation,
Draw at mass fraction ratio as 1:(0.1～10), consumption be the 0.05%～0.4% Ambra Grisea gas shown strong,
Comfortable, so that tobacco juice for electronic smoke has noble graceful Ambra Grisea fragrance, enrich the suction air of electronic cigarette
Taste.
Instant invention overcomes the deficiencies in the prior art, it is provided that a kind of tobacco juice for electronic smoke system with Ambra Grisea fragrance
Preparation Method.
For achieving the above object, the present invention is by the following technical solutions:
By the tobacco extract solution of 0.005-0.02mL, the flavouring essence for tobacco solution of 0.001-0.01mL and
The Ambra Grisea fragrance solution of 0.005-0.05mL is dissolved in the mixed solution of the water of 1-5mL, propylene glycol and glycerol
In.
Further technical scheme is, described tobacco extract solution manufacturing method is as follows:
A, choose in the red big Nicotiana tabacum L. in Huidong County, Sichuan, Huili County, Puge County, Flos Bombacis Malabarici, Xiangyun, yunnan county
One or more, altogether weigh 10-100g, in the baking oven that temperature is 40-50 DEG C dry, use pulverizer
It is ground into offal；
B, by step a offal add 50-200mL dichloromethane, supersound extraction 10-30min, then
Standing 2h, filter out offal, collect organic facies, the concentration adding 50-100mL in organic facies is 5%
Dilute sulfuric acid, is divided into twice addition, collects aqueous phase；
C, the pH value of the aqueous phase in step b is transferred to 8-10, adds the extraction of food stage ethyl acetate, isolate
Organic facies, then organic facies is concentrated to 1-5mL, obtain tobacco extract solution.
Compared with prior art, the invention has the beneficial effects as follows:
(1) tobacco juice for electronic smoke prepared by the present invention, has fresh and sweet odor type style and features, and quiet and tastefully laid out with noble quality
Ambra Grisea fragrance, enrich the suction local flavor of electronic cigarette；
(2) tobacco juice for electronic smoke prepared by the present invention, in flavouring essence for tobacco used, flavor component chooses and adds
Amount is added according to the content distribution in cigarette smoke, and its fragrance characteristic, can be more closer to cigarette smoke
Meet well consumer's demand to fragrance.
Detailed description of the invention
Embodiment 1
Choose each 2g of red big Nicotiana tabacum L. in Huidong County, Sichuan, Huili County, Puge County, Flos Bombacis Malabarici, Xiangyun, yunnan county,
The baking oven that temperature is 40 DEG C is dried, is ground into offal with pulverizer；Offal is added 50mL dichloromethane,
Supersound extraction 10min, then stand 2h, filter out offal, collect organic facies, in organic facies, add 50mL
The dilute sulfuric acid that concentration is 5%, be divided into twice addition, collect aqueous phase；The pH value of aqueous phase is transferred to 8, adds
Food stage ethyl acetate extracts, and isolates organic facies, then organic facies is concentrated to 1mL, obtain tobacco extract
Solution；
According to mass fraction than for 1:0.5:0.2:0.1:20:0.05:0.05:0.1:1 by benzyl alcohol,
Phenethanol, linalool, geraniol, 5 hydroxymethyl furfural, beta-damascenone, β-damascone, β-purple
Rowland ketone, 2-acetyl furan are configured to the solution (ethanol dissolving) that total mass concentration is 20%, and the cigarette of system is used
Fragrance solution；
It is 10% by mass fraction than ambrein and ambrox being configured to total mass concentration for 1:0.1
Solution (ethanol dissolving), prepares Ambra Grisea fragrance solution；
The tobacco extract solution of 0.005mL, the flavouring essence for tobacco solution of 0.001mL and 0.005mL Ambra Grisea is fragrant
It is that 10% water, mass percent are 80% propylene glycol and mass percent is that essence solution is dissolved in 1mL mass percent
In the mixed liquor of 10% glycerol, obtain tobacco juice for electronic smoke.
Take 1mL tobacco juice for electronic smoke to add in nebulizer, smoke panel test through the specialty personnel that smoke panel test, there is fresh and sweet odor type style
Feature, and with Ambra Grisea fragrance.
Embodiment 2
Choose each 10g of red big Nicotiana tabacum L. in Huidong County, Sichuan, Huili County, Puge County, Flos Bombacis Malabarici, Xiangyun, yunnan county,
The baking oven that temperature is 42 DEG C is dried, is ground into offal with pulverizer；Offal is added 100mL dichloromethane,
Supersound extraction 20min, then stand 2h, filter out offal, collect organic facies, in organic facies, add 70mL's
Concentration is the dilute sulfuric acid of 5%, is divided into twice addition, collects aqueous phase；The pH value of aqueous phase is transferred to 9, adds food
Level ethyl acetate extracts, and isolates organic facies, then organic facies is concentrated to 2mL, obtain tobacco extract solution；
According to mass fraction than for 1:0.6:0.5:0.2:40:0.1:0.1:0.2:2 by benzyl alcohol,
Phenethanol, linalool, geraniol, 5 hydroxymethyl furfural, beta-damascenone, β-damascone, β-purple
Rowland ketone, 2-acetyl furan are configured to the solution (ethanol dissolving) that total mass concentration is 40%, prepare cigarette and use
Fragrance solution；
Than for 1:1, ambrein and ambroxide it is configured to the solution that total mass concentration is 20% by mass fraction
(ethanol dissolving), prepares Ambra Grisea fragrance solution；
The tobacco extract solution of 0.01mL, the flavouring essence for tobacco solution of 0.005mL and 0.008mL Ambra Grisea is fragrant
It is that 15% water, mass percent are 70% propylene glycol and mass percent is that essence solution is dissolved in 3mL mass percent
In the mixed liquor of 15% glycerol, obtain tobacco juice for electronic smoke；
Take 1mL tobacco juice for electronic smoke to add in nebulizer, smoke panel test through the specialty personnel that smoke panel test, there is fresh and sweet odor type style
Feature, and with Ambra Grisea fragrance.
Embodiment 3
Choose each 20g of red big Nicotiana tabacum L. in Huidong County, Sichuan, Huili County, Puge County, Flos Bombacis Malabarici, Xiangyun, yunnan county,
The baking oven that temperature is 45 DEG C is dried, is ground into offal with pulverizer；Offal is added 150mL dichloromethane,
Supersound extraction 25min, then stand 2h, filter out offal, collect organic facies, in organic facies, add 80mL's
Concentration is the dilute sulfuric acid of 5%, is divided into twice addition, collects aqueous phase；The pH value of aqueous phase is transferred to 10, adds food
Grade ethyl acetate extracts, and isolates organic facies, then organic facies is concentrated to 5mL, obtain tobacco extract molten
Liquid；
According to mass fraction than for 1:0.9:0.7:0.3:70:0.2:0.3 by benzyl alcohol, phenethanol,
Linalool, geraniol, 5 hydroxymethyl furfural, β-damascone, alpha, beta-lonone are configured to gross mass
Concentration is the solution (ethanol dissolving) of 50%, prepares flavouring essence for tobacco solution；
By mass fraction than for 1:10 ambrein and ambroxide be configured to total mass concentration be 30% molten
Liquid (ethanol dissolving), prepares Ambra Grisea fragrance solution；
By the tobacco extract solution of 0.005mL, the flavouring essence for tobacco solution of 0.01mL and 0.01mL Ambra Grisea essence
It is that 20% water, mass percent are 60% propylene glycol and mass percent is that solution is dissolved in 5mL mass percent
In the mixed liquor of 20% glycerol, obtain tobacco juice for electronic smoke；
Take 1mL tobacco juice for electronic smoke to add in nebulizer, smoke panel test through the specialty personnel that smoke panel test, there is fresh and sweet odor type style
Feature, and with Ambra Grisea fragrance.
Embodiment 4
Choose each 20g of red big Nicotiana tabacum L. in Huidong County, Sichuan, Huili County, Puge County, Flos Bombacis Malabarici, Xiangyun, yunnan county,
The baking oven that temperature is 47 DEG C is dried, is ground into offal with pulverizer；Offal is added 150mL dichloromethane,
Supersound extraction 30min, then stand 2h, filter out offal, collect organic facies, in organic facies, add 100mL
The dilute sulfuric acid that concentration is 5%, be divided into twice addition, collect aqueous phase；The pH value of aqueous phase is transferred to 10, adds
Food stage ethyl acetate extracts, and isolates organic facies, then organic facies is concentrated to 5mL, obtain tobacco extract
Solution；
According to mass fraction than for 1:0.9:0.7:0.3:70:0.2:0.2:0.3:3 by benzyl alcohol,
Phenethanol, linalool, geraniol, 5 hydroxymethyl furfural, beta-damascenone, β-damascone, β-purple
Rowland ketone, 2-acetyl furan are configured to the solution (ethanol dissolving) that total mass concentration is 50%, prepare cigarette and use
Fragrance solution；
By mass fraction than for 1:10 ambrein and ambroxide be configured to total mass concentration be 30% molten
Liquid (ethanol dissolving), prepares Ambra Grisea fragrance solution；
By the tobacco extract solution of 0.005mL, the flavouring essence for tobacco solution of 0.01mL and 0.03mL Ambra Grisea essence
It is that 15% water, mass percent are 70% propylene glycol and mass percent is that solution is dissolved in 5mL mass percent
In the mixed liquor of 15% glycerol, obtain tobacco juice for electronic smoke；
Take 1mL tobacco juice for electronic smoke to add in nebulizer, smoke panel test through the specialty personnel that smoke panel test, there is fresh and sweet odor type style
Feature, and with Ambra Grisea fragrance.
Embodiment 5
Choose each 2g of red big Nicotiana tabacum L. in Huidong County, Sichuan, Huili County, Puge County, Flos Bombacis Malabarici, Xiangyun, yunnan county,
The baking oven that temperature is 50 DEG C is dried, is ground into offal with pulverizer；Offal is added 200mL dichloromethane,
Supersound extraction 30min, then stand 2h, filter out offal, collect organic facies, in organic facies, add 90mL's
Concentration is the dilute sulfuric acid of 5%, is divided into twice addition, collects aqueous phase；The pH value of aqueous phase is transferred to 9, adds food
Level ethyl acetate extracts, and isolates organic facies, then organic facies is concentrated to 1mL, obtain tobacco extract solution；
According to mass fraction than for 1:0.5:0.2:0.1:20:0.05:0.05:0.1:1 by benzyl alcohol,
Phenethanol, linalool, geraniol, 5 hydroxymethyl furfural, beta-damascenone, β-damascone, β-purple
Rowland ketone, 2-acetyl furan are configured to the solution (ethanol dissolving) that total mass concentration is 20%, prepare cigarette and use
Fragrance solution；
Ambrox is configured to the solution (ethanol dissolving) that mass concentration is 10%, prepares Ambra Grisea essence
Solution；
The tobacco extract solution of 0.005mL, the flavouring essence for tobacco solution of 0.001mL and 0.005mL Ambra Grisea is fragrant
It is that 10% water, mass percent are 80% propylene glycol and mass percent is that essence solution is dissolved in 1mL mass percent
In the mixed liquor of 10% glycerol, obtain tobacco juice for electronic smoke；
Take 1mL tobacco juice for electronic smoke to add in nebulizer, smoke panel test through the specialty personnel that smoke panel test, there is fresh and sweet odor type wind
Lattice feature, and with Ambra Grisea fragrance.
Electronic cigarette sensory quality assessment method:
According to Sensory Quality of Cigarette judgment criteria GB5606.4-2005, in conjunction with electronic cigarette organoleptic features, according to not
6 evaluation indexes and score value are set with weight, are shown in Table 2
Table 2
The tobacco juice for electronic smoke of embodiment 1-embodiment 5 carries out sensory evaluation, and evaluation and analysis result is commented according to each expert
Analysis result tries to achieve arithmetic equal value, and result retains a position effective digital, and statistical result is shown in Table 3
| Sample | Gratification | Fragrance | Harmony | Miscellaneous QI | Zest | Pleasant impression |
| Embodiment 1 | 24.5 | 22.5 | 4.0 | 9.0 | 18.0 | 14.5 |
| Embodiment 2 | 24.0 | 22.5 | 4.5 | 8.0 | 17.5 | 14.0 |
| Embodiment 3 | 23.0 | 23.0 | 4.5 | 8.0 | 16.5 | 13.0 |
| Embodiment 4 | 24.5 | 22.0 | 4.0 | 8.5 | 18.5 | 13.5 |
| Embodiment 5 | 23.5 | 22.0 | 4.0 | 9.0 | 18.5 | 13.5 |
Table 3
The essence of the present invention is described in detail by above detailed description of the invention, but can not be to the guarantor of the present invention
The scope of protecting limits, it should be apparent that, under the enlightenment of the present invention, the art those of ordinary skill
Many improvement and modification can also be carried out, it should be noted that these improve and modify all to fall the present invention's
Within claims.
Claims (6)
- null1. a tobacco juice for electronic smoke with Ambra Grisea fragrance，It is characterized in that，Electronic cigarette liquid hold-up described in every 1-5mL is as follows: the tobacco extract solution of 0.005-0.02mL、The flavouring essence for tobacco solution of 0.001-0.01mL and the Ambra Grisea fragrance solution of 0.005-0.05mL、The water of 1-5mL、Propylene glycol and the mixed solution of glycerol，The concentration of described flavouring essence for tobacco solution is 20%-50%，Solute is flavouring essence for tobacco，Solvent is ethanol，Described flavouring essence for tobacco is by benzyl alcohol、Phenethanol、Linalool、Geraniol、5 hydroxymethyl furfural、Beta-damascenone、β-damascone、Alpha, beta-lonone、2-acetyl furan forms，Its mass fraction ratio is: 1:(0.5-0.9): (0.2-0.7): (0.1-0.3): (20-70): (0.05-0.2): (0.05-0.2): (0.1-0.3): (1-3).
- Tobacco juice for electronic smoke the most according to claim 1, it is characterised in that the raw material of described tobacco extract solution is selected from one or more in the red big Nicotiana tabacum L. in Huidong County, Sichuan, Huili County, Puge County, Flos Bombacis Malabarici, Xiangyun, yunnan county.
- Tobacco juice for electronic smoke the most according to claim 1, it is characterised in that the concentration of described Ambra Grisea fragrance solution is 10-30%, solute is Ambra Grisea essence, and solvent is ethanol.
- Tobacco juice for electronic smoke the most according to claim 3, it is characterised in that described Ambra Grisea essence is one or more in ambrein and ambrox.
- Tobacco juice for electronic smoke the most according to claim 3, it is characterised in that described Ambra Grisea essence is made up of ambrein and ambrox, its mass fraction ratio is: 1:(0.1-10).
- 6. an electronic cigarette liquid and preparation method thereof with Ambra Grisea fragrance, it is characterized in that, by the tobacco extract solution of 0.005-0.02mL, the flavouring essence for tobacco solution of 0.001-0.01mL and the Ambra Grisea fragrance solution of 0.005-0.05mL are dissolved in the water of 1-5mL, in the mixed solution of propylene glycol and glycerol, described tobacco extract solution manufacturing method is as follows: a, choose Huidong County, Sichuan, Huili County, Puge County, Flos Bombacis Malabarici, one or more in the red big Nicotiana tabacum L. in Xiangyun, yunnan county, altogether weigh 10-100g, the baking oven that temperature is 40-50 DEG C is dried, it is ground into offal with pulverizer；B, the offal in step a is added the dichloromethane of 50-200mL, supersound extraction 10-30min, then stand 2h, filter out offal, collect organic facies, in organic facies, add the dilute sulfuric acid that concentration is 5% of 50-100mL, be divided into twice addition, collect aqueous phase；C, the pH value of the aqueous phase in step b is transferred to 8-10, adds the extraction of food stage ethyl acetate, isolate organic facies, then organic facies is concentrated to 1-5mL, obtain tobacco extract solution.
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| CN105154229B (en) * | 2015-07-16 | 2018-08-14 | 四川中烟工业有限责任公司 | Latent aroma compounds and its preparation method and application with fragrant and sweet rhythm and baking note |
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| CN110819454B (en) * | 2019-11-14 | 2022-07-12 | 湖北中烟工业有限责任公司 | Essence with sweet taste for cigarette not burning during heating |
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Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0338831A2 (en) * | 1988-04-21 | 1989-10-25 | R.J. Reynolds Tobacco Company | Process for providing tobacco extracts |
| CN102559388A (en) * | 2012-02-27 | 2012-07-11 | 浙江中烟工业有限责任公司 | Essential oil of tobaccos as well as preparation method and application thereof to cigarettes |
| CN103040092A (en) * | 2013-01-15 | 2013-04-17 | 济南鼻烟研究所 | Ambergris scent type snuff |
| CN103070472A (en) * | 2013-01-25 | 2013-05-01 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid capable of effectively improving sensory quality of electronic cigarette |
| CN103393214A (en) * | 2013-07-31 | 2013-11-20 | 浙江中烟工业有限责任公司 | Aromatic tobacco ethyl alcohol and propylene glycol mixed solution extract and preparation method and application of aromatic tobacco ethyl alcohol and propylene glycol mixed solution extract |
| CN103436361A (en) * | 2013-08-05 | 2013-12-11 | 湖南中烟工业有限责任公司 | Intelligent fragrance blending and simulating method of cigarette flavor |
| CN103584276A (en) * | 2013-11-13 | 2014-02-19 | 川渝中烟工业有限责任公司 | Ambergris cigarette and ambergris spices |
| CN104041935A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese-style flue-cured tobacco fragrance cigarette juice for electronic cigarette |
| CN104151140A (en) * | 2014-07-11 | 2014-11-19 | 武汉工程大学 | Method for comprehensively extracting multiple effective components from tobacco leaves |
-
2015
- 2015-01-20 CN CN201510027817.2A patent/CN104687240B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0338831A2 (en) * | 1988-04-21 | 1989-10-25 | R.J. Reynolds Tobacco Company | Process for providing tobacco extracts |
| CN102559388A (en) * | 2012-02-27 | 2012-07-11 | 浙江中烟工业有限责任公司 | Essential oil of tobaccos as well as preparation method and application thereof to cigarettes |
| CN103040092A (en) * | 2013-01-15 | 2013-04-17 | 济南鼻烟研究所 | Ambergris scent type snuff |
| CN103070472A (en) * | 2013-01-25 | 2013-05-01 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid capable of effectively improving sensory quality of electronic cigarette |
| CN103393214A (en) * | 2013-07-31 | 2013-11-20 | 浙江中烟工业有限责任公司 | Aromatic tobacco ethyl alcohol and propylene glycol mixed solution extract and preparation method and application of aromatic tobacco ethyl alcohol and propylene glycol mixed solution extract |
| CN103436361A (en) * | 2013-08-05 | 2013-12-11 | 湖南中烟工业有限责任公司 | Intelligent fragrance blending and simulating method of cigarette flavor |
| CN103584276A (en) * | 2013-11-13 | 2014-02-19 | 川渝中烟工业有限责任公司 | Ambergris cigarette and ambergris spices |
| CN104041935A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese-style flue-cured tobacco fragrance cigarette juice for electronic cigarette |
| CN104151140A (en) * | 2014-07-11 | 2014-11-19 | 武汉工程大学 | Method for comprehensively extracting multiple effective components from tobacco leaves |
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Effective date of registration: 20161205 Address after: 610000, Sichuan, Chengdu, Longquanyi economic and Technological Development Zone, Jackie Chan Road, Longquan, No. 2, paragraph Patentee after: CHINA TOBACCO SICHUAN INDUSTRIAL CO., LTD. Patentee after: CHONGQING CHINA TOBACCO INDUSTRIAL CO., LTD. Address before: 610000 Jackie Chan Road, Chengdu economic and Technological Development Zone, Longquanyi District, Sichuan, China, No. 2, No. Patentee before: China Tobacco Chuanyu Industrial Co., Ltd. |