CN114098139B - Electronic atomized liquid with rich and durable mouth feeling and preparation method thereof - Google Patents

Electronic atomized liquid with rich and durable mouth feeling and preparation method thereof Download PDF

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Publication number
CN114098139B
CN114098139B CN202111370588.6A CN202111370588A CN114098139B CN 114098139 B CN114098139 B CN 114098139B CN 202111370588 A CN202111370588 A CN 202111370588A CN 114098139 B CN114098139 B CN 114098139B
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tobacco
oil
plant
perfume
fragrance
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CN114098139A (en
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邹阳
邹军
刘梅森
陈慧
唐忠月
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Shenzhen Zinwi Biotech Co Ltd
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Shenzhen Zinwi Biotech Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/022Refining
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Abstract

The invention relates to the technical field of electronic atomized liquid, in particular to electronic atomized liquid with rich and durable mouth feel and a preparation method thereof. An electronic atomized liquid with rich and durable mouth feel consists of 0.1 to 10 weight percent of tobacco essence and 90 to 99.9 weight percent of solvent, wherein the tobacco essence is prepared from a tobacco fragrance light component and a plant natural spice; the cigarette fragrance light component is prepared by taking waste and inferior tobacco stems and tobacco leaves as raw materials through alkali pretreatment, fermentation, filtration and molecular distillation; the plant natural perfume comprises a plant perfume A, a plant perfume B and a plant perfume C, wherein the plant perfume A has a fruity fragrance note, the plant perfume B has a flowery fragrance note, and the plant perfume C has a costustoot fragrance note. The invention mixes and ages the fermented and separated cigarette fragrance light components and the plant natural perfume, and a large amount of alcohol substances generated by fermentation can react with the components in the plant perfume to generate softer and more mellow fragrance, which is also beneficial to synchronous release of the fragrant components during atomization, and has good overall harmony and rich and lasting smoking taste.

Description

Electronic atomized liquid with rich and durable mouth feeling and preparation method thereof
Technical Field
The invention relates to the technical field of electronic atomized liquid, in particular to electronic atomized liquid with rich and durable mouth feel and a preparation method thereof.
Background
With the enhancement of health consciousness of people, the traditional cigarette is gradually replaced by new products such as an electronic nicotine delivery system, a cigarette which is not burnt by heating and the like because a large amount of toxic substances such as tar, smoke and the like are generated in the heating and burning process. The electronic atomization liquid is atomized to form aerosol by heating, so that the harmfulness of the cigarette is greatly reduced compared with that of the traditional cigarette. Most of the electronic atomization liquid is prepared by adding essence, spice, nicotine or nicotine salt and the like to simulate the taste and the aroma of cigarettes. Although the electronic atomization liquid sold in the market at present has a plurality of varieties and tastes, the source, the composition and the release behavior of the aroma substances of the electronic atomization liquid are different from those of cigarettes, so that the electronic atomization liquid has larger difference from the traditional cigarette smoking sensory effect, and cannot meet the pursuit of consumers on natural feeling and smoking quality particularly in the aspects of smoke characteristics, aroma style, comfort level and the like.
The traditional cigarette has complex aroma components, the tobacco flavor spice prepared by manual blending is difficult to restore the real cigarette aroma, the chemical smell of the product of the synthetic spice is obvious, the aroma structure is simple, the taste is numerous but the discrimination is low, the smoking experience is single, and the phenomenon of uneven aroma release is often generated when the electronic atomization device is heated. The tobacco refined product is also an important fragrant raw material in the preparation of tobacco essence, can strengthen the tobacco fragrance to a certain extent, can make up the deficiency of the tobacco fragrance especially when being used in electronic atomization liquid, and enriches the smoking taste and mouthfeel. In order to obtain higher flavor fidelity, natural tobacco extracts are often added into electronic atomized liquid in the prior art, for example, in patent CN103919274B, a tobacco liquid extraction perfume, an effective part extract of a non-tobacco plant, a synthetic edible perfume and natural nicotine are mixed to prepare the electronic atomized liquid, however, compared with the traditional cigarette, the aromatic components of a single variety of tobacco extracts are still lost, and the problems of poor harmony, unstable fragrance and the like are easily caused by compound perfuming, the release behaviors of the fragrant components from different sources are inconsistent, the synchronous delivery of the plant perfume and the endogenous fragrant components of tobacco is difficult to realize, the phenomenon of fragrance separation or covering may occur in the smoking process, and the smoking experience of consumers is influenced.
The microbial fermentation technology is applied to research and development of tobacco flavors and fragrances, screening of aroma-producing strains, extraction and treatment of tobacco and other plant raw materials are the main research directions in China at present, and some synthetic products based on biological fermentation show good effects in cigarette flavoring. If the endogenous fragrant components of the tobacco and other natural spices are compounded and added into the electronic atomization liquid, the natural feeling can be enhanced, the smoking quality can be improved, but the purification difficulty of the natural spices is high, and the generated smell is not lasting, so that consumers cannot well feel satisfied and pleasant.
Disclosure of Invention
Aiming at the technical problems, the invention provides the natural and healthy electronic atomized liquid with rich and lasting taste, and the aging process integrates strong fruit fragrance, fragrant flower fragrance, wood fragrance and tobacco fragrance, thereby providing unique smoking experience.
The above object of the present invention is achieved by the following technical solutions:
an electronic atomized liquid with rich and durable mouth feel consists of 0.1 to 10 weight percent of tobacco essence and 90 to 99.9 weight percent of solvent, wherein the tobacco essence is prepared from light components of tobacco fragrance and plant natural perfume; the light component of the tobacco fragrance is prepared by taking waste and inferior tobacco stems and tobacco leaves as raw materials and performing alkali pretreatment, fermentation, filtration and molecular distillation.
Natural and rich tobacco fragrance and plant fragrance are difficult to restore through blending of synthetic spices, and the smoking experience is influenced because the fragrance structure is single or the fragrance smell is too heavy. The tobacco essence disclosed by the invention combines the tobacco refined substance and the plant natural perfume, so that the problem of insufficient tobacco fragrance of the electronic atomizer can be well solved, and meanwhile, the natural perfume is only added, so that the tobacco essence is healthier, has stronger natural feeling and richer smoking taste.
The invention uses waste tobacco stems and tobacco leaves as raw materials, adopts a microbial fermentation technology to enrich aroma substances, and then uses molecular distillation to enrich small molecular aroma substances and remove miscellaneous gases or substances with unpleasant odor, so that the aromatic smell of the tobacco can be provided, meanwhile, the light components of the tobacco aroma also contain a small amount of nicotine, so that the invention has better addiction-removing property, can meet the pursuit of consumers on throat feeling and brings better physiological pleasure. Meanwhile, the electronic atomized liquid of the invention can be added with no nicotine or nicotine salt, which is beneficial to relieving the dependence of consumers on nicotine and reducing the harm to human bodies.
The waste and inferior tobacco stems and tobacco leaves are renewable organic resources, lignin components in the waste and inferior tobacco stems and tobacco leaves prevent cellulose from being contacted with cellulase, so that difficulty is caused in secondary utilization, and the lignin in the raw materials can be removed after alkaline pretreatment, so that the accessibility of the enzyme and a substrate is promoted, and full fermentation is facilitated. Meanwhile, alcohol substances such as ethanol and the like generated by fermentation are compounded with the plant natural perfume to generate more fragrant components through esterification, condensation and other reactions, so that the fragrance is richer and fuller.
Preferably, the plant natural perfume of the invention comprises plant perfume A, plant perfume B and plant perfume C, wherein the plant perfume A has fruity scent, the plant perfume B has flowery scent, and the plant perfume C has costustoot scent.
Preferably, the plant spice A is one or more of hawthorn tincture, dark plum tincture, grapefruit oil, bergamot oil, lemon extract, tangerine oil, sweet orange essential oil, sour orange essential oil, bitter orange essential oil, sweet orange peel extract, fragrant orange peel oil, high-power natural apple spice, plum extract and pineapple extract.
Preferably, the plant spice B is one or more of clove bud oil, marigold essential oil, chrysanthemum morifolium ramat flower oil, chamomile essential oil, white orchid essential oil, rose essential oil, iris resin, acacia oil, jasmine essential oil, daidai flower oil, gardenia essential oil, tree orchid essential oil, sweet osmanthus essential oil and lavender essential oil.
More preferably, the plant spice C is one or more of patchouli oil, costus oil, bay essential oil, spikenard oil, wintergreen essential oil, cedar essential oil, sandalwood oil, storax oil, balsam fir oil and cajeput oil.
The invention adds three types of plant spices with different fragrance notes simultaneously, has complementary effect, and has synergistic aroma enhancement and rich taste. The aromatic component of the plant spice A is mostly a micromolecular compound with stronger volatility, the plant spice A has strong characteristic fruity fragrance, the atomized plant spice A is instantly full of nasal cavities and oral cavities, the aromatic component and the light component of the cigarette fragrance are simultaneously released to bring stronger throat hitting feeling and physiological pleasure, the fragrance duration is shorter, the fragrant substance of the plant spice B is softer, the dwell time after atomization is slightly longer, the plant spice A is a main characteristic fragrant substance, is fragrant and delicate, and can easily generate pleasant comfort when sliding through the throat, the plant spice C is mostly a component with higher boiling point and smaller volatility, the fragrance can penetrate all the time after atomization, the residual fragrance can still be sensed in the nasal cavities after the former two fragrance charms disappear, and the plant spice A is fresh and elegant.
The proportions of the plant spice A, the plant spice B and the plant spice C are not limited, and can be determined according to the fragrance of actual essential oil.
The invention also provides a preparation method of the electronic atomized liquid with rich and durable mouth feel, which comprises the following steps:
s1, carrying out alkaline pretreatment on waste and inferior tobacco stems and tobacco leaves, mixing the waste and inferior tobacco stems and the tobacco leaves with water and aroma-producing yeast for fermentation, filtering to obtain a tobacco aroma fermentation liquor, and carrying out molecular distillation separation to obtain a tobacco aroma light component of a T distillation section;
s2, mixing the light components of the tobacco fragrance with the plant natural perfume, putting the mixture into a closed container for aging, cooling and centrifuging the mixed solution, and separating the supernatant to obtain the tobacco essence;
and S3, mixing the tobacco essence in the S2 with a solvent to prepare the electronic atomized liquid.
Different types of natural flavors, while having rich and natural aroma structures, are often not long lasting or can not be delivered in synchrony with tobacco endogenous aroma components and are poorly coordinated with each other, and aroma separation may occur. The plant spices of the three types of aroma are mixed with the light components of the tobacco aroma obtained through fermentation and separation for aging, the natural tobacco aroma substances and molecules in the plant spices continuously collide and react in the process to generate new and more stable aromatic substances, particularly a large amount of alcohols generated by the fermentation of the tobacco can be condensed with the acutely fragrant aldehyde-ketone compounds in the plant spices to generate compounds with softer aroma, and meanwhile, the plant spice C can also be directly used as an aroma fixing agent, so that the aroma of the essence is more mellow, mellow and well-done, the durability is better, and the aroma quality is integrally improved. The aged tobacco flavor can synchronously release all aroma components, has good cooperativity, and can smell fresh fragrance and costustoot in sequence after the initial tobacco fragrance and fruit fragrance are diluted, thereby having layering sense and natural connection and bringing comfortable and pleasant sensory experience.
Preferably, the manner of alkali pretreatment in step S1 is: adding waste tobacco stems and tobacco leaves into an alkali solution, uniformly stirring, heating for 2-5 hours, filtering, and washing with pure water to be neutral.
Preferably, the temperature T = 70-100 ℃ of the distillation section in step S1.
Preferably, the mixing ratio of the tobacco flavor light components and the plant natural spice in the step S2 is 100: (1-10) (w/w).
Preferably, the aging time in step S2 is 15 to 45 days, and the cooling temperature is 0 to 5 ℃.
Compared with the prior art, the invention has the following beneficial effects:
(1) According to the invention, the fermented and separated light components of the cigarette fragrance and the plant natural perfume are mixed and aged, and a large amount of alcohol substances generated by fermentation can react with the components in the plant perfume to generate softer, round and lasting fragrance, so that the fragrant components can be synchronously released during atomization, the smoking taste is enriched, and the natural feeling is enhanced;
(2) The tobacco fermentation product is used as one of the raw materials of the tobacco essence, so that not only can rich tobacco fragrance components be provided, but also nicotine can be directly provided, the pursuit of consumers on throat feeling is met, and better physiological pleasure feeling is brought;
(3) The three types of plant spices with different fragrance notes are added simultaneously, the three types of plant spices complement each other and increase fragrance synergistically, and after aging, the strong fruit fragrance, the fragrant flower fragrance, the woody fragrance and the tobacco fragrance are integrated, so that the taste is natural, rich and lasting;
(4) The method takes waste and inferior tobacco stems and tobacco leaves as raw materials, adopts a microbial fermentation technology to enrich aroma substances, is green and environment-friendly in production mode and less in pollution, can directly take nicotine contained in a fermentation product as a raw material of electronic atomized liquid, promotes enzymolysis through alkaline pretreatment, and improves the utilization rate of the raw material and the production efficiency of alcohol substances;
(5) The formula of the electronic atomized liquid only adopts natural raw materials, does not add synthetic spice or synthetic nicotine, has higher flavor fidelity and reduction degree, and can reduce the harm to human bodies.
Detailed Description
The technical solution of the present invention is further described and illustrated by the following specific examples. The raw materials used in the examples of the present invention are those commonly used in the art, and the methods used in the examples are those conventional in the art, unless otherwise specified. It should be understood that the specific embodiments described herein are merely to aid in the understanding of the invention and are not intended to limit the invention specifically.
Example 1:
(1) Weighing 100g of crushed waste and inferior tobacco stems and tobacco leaves, adding 500mL of NaOH solution with the mass fraction of 4%, starting stirring, heating to 75 ℃, preserving heat for 3h, filtering to obtain a tobacco filter cake, and washing the tobacco filter cake to be neutral by pure water for later use;
(2) Weighing 0.2g of aroma-producing active dry yeast, putting the dry yeast into 20 times of 2.5% sucrose water, and activating for 10 hours at 33-35 ℃; smashing the tobacco filter cake in the step (1), putting the smashed tobacco filter cake into a fermentor, adding 500mL of purified water, stirring to completely immerse the tobacco filter cake, adding the activated aroma-producing yeast, setting the temperature to be kept at 25 ℃, fermenting for 15 days, and extruding and filtering to obtain 488g of tobacco aroma fermentation liquor;
(3) Performing molecular distillation on the cigarette flavor fermentation liquor, setting the distillation temperature T =70 ℃, the feeding temperature 60 ℃ and the rotating speed 280r/min, adjusting the blanking flow in real time to prevent bumping, and collecting 251g of cigarette flavor light components in a distillation section with the temperature T =70 ℃ for later use;
(4) Weighing 200g of the cigarette light components, 1g of lemon oil, 2g of clove bud oil and 1g of patchouli oil, adding the materials into a stainless steel reaction kettle, placing the reaction kettle in a constant temperature chamber at 15 ℃, aging for 20 days, immersing the sealed reaction kettle into 0 ℃ frozen water for 4 hours, taking supernate and centrifuging at high speed to obtain 184g of tobacco essence, and dissolving the tobacco essence into basic atomized tobacco oil according to the addition amount of 1% (w/w) to obtain the electronic atomized liquid A.
Example 2:
(1) Weighing 100g of crushed waste and inferior tobacco stems and tobacco leaves, adding 500mL of NaOH solution with the mass fraction of 4%, starting stirring, heating to 75 ℃, preserving heat for 3h, filtering to obtain a tobacco filter cake, and washing the tobacco filter cake to be neutral by pure water for later use;
(2) Weighing 0.2g of aroma-producing active dry yeast, putting the dry yeast into 25 times of 2.5% sucrose water, and activating for 10 hours at 33-35 ℃; smashing the tobacco filter cake obtained in the step (1), putting the smashed tobacco filter cake into a fermenter, adding 500mL of purified water, stirring to completely immerse the smashed tobacco filter cake, adding the activated aroma-producing yeast, setting the temperature to be 28 ℃, fermenting for 15 days, and performing extrusion filtration to obtain 492g of tobacco aroma fermentation liquor;
(3) Performing molecular distillation on the tobacco aroma fermentation liquor, setting the distillation temperature T =80 ℃, the feeding temperature 70 ℃ and the rotating speed 280r/min, adjusting the blanking flow in real time, preventing bumping, and collecting 297g of tobacco aroma light components in a distillation section with the temperature T =80 ℃ for later use;
(4) Weighing 200g of the cigarette fragrance light component, 1g of orange oil, 1g of chamomile essential oil and 2g of costus oil, adding the materials into a stainless steel reaction kettle, placing the reaction kettle in a constant temperature chamber at 15 ℃, aging for 30 days, then soaking the sealed reaction kettle into freezing water at 0 ℃ for 4 hours, taking supernate and centrifuging at high speed to obtain 187g of cigarette essence, and dissolving the cigarette essence in basic atomized tobacco oil according to the addition amount of 1% (w/w) to obtain the electronic atomized liquid B.
Example 3:
(1) Weighing 100g of crushed waste and inferior tobacco stems and tobacco leaves, adding 500mL of NaOH solution with the mass fraction of 4%, starting stirring, heating to 75 ℃, preserving heat for 3h, filtering to obtain a tobacco filter cake, and washing the tobacco filter cake to be neutral by pure water for later use;
(2) Weighing 0.2g of aroma-producing active dry yeast, putting the dry yeast into 25 times of 2.5% sucrose water, and activating for 10 hours at 33-35 ℃; smashing the tobacco filter cake in the step (1), putting the smashed tobacco filter cake into a fermenter, adding 500mL of purified water, stirring to completely immerse the smashed tobacco filter cake, adding the activated aroma-producing yeast, setting the temperature to be kept at 25 ℃, fermenting for 20 days, and extruding and filtering to obtain 479g of tobacco aroma fermentation liquor;
(3) Performing molecular distillation on the cigarette aroma fermentation liquor, setting the distillation temperature T =90 ℃, the feeding temperature 80 ℃ and the rotating speed 280r/min, adjusting the blanking flow in real time to prevent bumping, and collecting 354g of cigarette aroma light components in a distillation section with the temperature T =90 ℃ for later use;
(4) Weighing 200g of the cigarette fragrance light component, 2g of plum extract, 2g of sweet osmanthus essential oil and 2g of sandalwood oil, adding the materials into a stainless steel reaction kettle, placing the reaction kettle in a constant temperature room at 15 ℃, aging for 35 days, immersing the sealed reaction kettle into 0 ℃ chilled water for 4 hours, taking supernate, centrifuging at high speed to obtain 191g of cigarette essence, and dissolving the cigarette essence into basic atomized tobacco oil according to the addition of 1% (w/w) to obtain the electronic atomized liquid C.
Example 4:
(1) Weighing 100g of crushed waste and inferior tobacco stems and tobacco leaves, adding 500mL of NaOH solution with the mass fraction of 4%, starting stirring, heating to 75 ℃, preserving heat for 3h, filtering to obtain a tobacco filter cake, and washing the tobacco filter cake to be neutral by pure water for later use;
(2) Weighing 0.2g of aroma-producing active dry yeast, putting the dry yeast into 25 times of 2.5% sucrose water, and activating for 10 hours at 33-35 ℃; smashing the tobacco filter cake obtained in the step (1), putting the smashed tobacco filter cake into a fermenter, adding 500mL of purified water, stirring to completely immerse the smashed tobacco filter cake, adding the activated aroma-producing yeast, setting the temperature to be kept at 25 ℃, fermenting for 20 days, and performing extrusion filtration to obtain 476g of tobacco aroma fermentation liquor;
(3) Performing molecular distillation on the tobacco aroma fermentation liquor, setting the distillation temperature T =100 ℃, the feeding temperature 90 ℃ and the rotating speed 250r/min, adjusting the blanking flow in real time to prevent bumping, and collecting 367g of the tobacco aroma light component of the distillation section with the temperature T =100 ℃ for later use;
(4) Weighing 200g of the cigarette fragrance light component, 3g of pineapple extract, 2g of tree orchid oil and 2g of nardostachys oil, adding the materials into a stainless steel reaction kettle, placing the reaction kettle in a 15 ℃ thermostatic chamber, aging for 40 days, immersing the closed reaction kettle into 0 ℃ frozen water for 4 hours, taking supernatant, centrifuging at high speed to obtain 190g of cigarette essence, and dissolving the cigarette essence in basic atomized tobacco oil according to the addition of 1% (w/w) to obtain the electronic atomized liquid D.
Example 5:
(1) Weighing 100g of crushed waste and inferior tobacco stems and tobacco leaves, adding 500mL of NaOH solution with the mass fraction of 4%, starting stirring, heating to 75 ℃, preserving heat for 3h, filtering to obtain a tobacco filter cake, and washing the tobacco filter cake to be neutral by pure water for later use;
(2) Weighing 0.2g of aroma-producing active dry yeast, putting the dry yeast into 25 times of 2.5% sucrose water, and activating for 10 hours at 33-35 ℃; smashing the tobacco filter cake obtained in the step (1), putting the smashed tobacco filter cake into a fermenter, adding 500mL of purified water, stirring to completely immerse the smashed tobacco filter cake, adding the activated aroma-producing yeast, setting the temperature to be kept at 25 ℃, fermenting for 23 days, and performing extrusion filtration to obtain 463g of tobacco aroma fermentation liquor;
(3) Performing molecular distillation on the cigarette aroma fermentation liquor, setting the distillation temperature T =100 ℃, the feeding temperature 90 ℃ and the rotating speed 250r/min, adjusting the blanking flow in real time to prevent bumping, and collecting 370g of cigarette aroma light components in the distillation section with the temperature T =100 ℃ for later use;
(4) Weighing 200g of the cigarette fragrance light component, 5g of pericarpium citri reticulatae oil, 3g of gardenia essential oil and 2g of storax oil, adding the materials into a stainless steel reaction kettle, placing the reaction kettle in a 15 ℃ thermostatic chamber, aging for 45 days, immersing the sealed reaction kettle into 0 ℃ chilled water for 4 hours, taking supernatant, centrifuging at high speed to obtain 195g of cigarette essence, and dissolving the cigarette essence in basic atomized tobacco oil according to the addition of 1% (w/w) to obtain the electronic atomized liquid E.
Comparative example 1
(1) Weighing 100g of crushed waste and inferior tobacco stems and tobacco leaves, adding 500mL of NaOH solution with the mass fraction of 4%, starting stirring, heating to 75 ℃, preserving heat for 3h, filtering to obtain a tobacco filter cake, and washing the tobacco filter cake to be neutral by pure water for later use;
(2) Weighing 0.2g of aroma-producing active dry yeast, putting the dry yeast into 20 times of 2.5% sucrose water, and activating for 10 hours at 33-35 ℃; smashing the tobacco filter cake in the step (1), putting the smashed tobacco filter cake into a fermenter, adding 500mL of purified water, stirring to completely immerse the smashed tobacco filter cake, adding the activated aroma-producing yeast, setting the temperature to be kept at 25 ℃, fermenting for 15 days, and extruding and filtering to obtain 475g of tobacco aroma fermentation liquor; taking 50g of fermentation liquor, 0.25g of mixed lemon oil, 0.5g of clove bud oil and 0.25g of patchouli oil to obtain mixed essence, and dissolving the mixed essence into the basic atomized tobacco oil according to the addition amount of 1% (w/w) to obtain the electronic atomized liquid F.
Comparative example 2
Taking 50G of the cigarette fragrance light component obtained in the step (3) in the example 2, 0.25G of mixed orange oil, 0.25G of chamomile essential oil and 0.5G of costus root oil to obtain mixed essence, and dissolving the mixed essence in the basic atomized tobacco oil according to the addition amount of 1% (w/w) to obtain the electronic atomized liquid G.
Comparative example 3
Taking 50g of the cigarette aroma light component obtained in the step (3) of the example 3 and 0.5g of the mixed plum extract to obtain mixed essence, and dissolving the mixed essence into the basic atomized tobacco oil according to the addition amount of 1% (w/w) to obtain the electronic atomized liquid H.
Comparative example 4
50g of the cigarette fragrance light component obtained in the step (3) in the example 4 and 0.5g of mixed tree orchid oil are taken to obtain mixed essence, and the mixed essence is dissolved in the basic atomized tobacco oil according to the addition amount of 1% (w/w) to obtain the electronic atomized liquid I.
Comparative example 5
50g of the cigarette flavor light component obtained in the step (3) in the example 5 is taken and 0.5g of storax oil is mixed to obtain mixed essence, and the mixed essence is dissolved in the basic atomized tobacco oil according to the addition amount of 1% (w/w) to obtain the electronic atomized liquid J.
Comparative example 6
Taking 50g of the cigarette fragrance light component obtained in the step (3) in the example 5, mixing 0.5g of gardenia essential oil and 0.5g of storax oil, adding the mixture into a stainless steel reaction kettle, placing the reaction kettle in a constant temperature chamber at 15 ℃, aging for 45 days, then soaking the closed reaction kettle into 0 ℃ frozen water for 4 hours, taking the supernatant, centrifuging at high speed to obtain 45g of cigarette essence, and dissolving the cigarette essence into the basic atomized cigarette oil according to the addition of 1% (w/w) to obtain the electronic atomized liquid K.
Sensory product absorption is carried out on the electronic atomized liquids A, B, C, D, E, F, G, H, I, J and K of examples 1-5 and comparative examples 1-6, and the product absorption results are shown in the following table.
TABLE 1 composite fragrance product sorption results of examples 1-5 and comparative examples 1-6
Figure BDA0003362292040000081
The tobacco essence prepared in the examples 1-5 has good comfort and novel and pleasant flavor through the result absorption of sensory products, and through the aging effect of the endogenous flavor and the flower-fruit-wood composite flavor for the tobacco, the flavor is full and rich, is full and not deficient, and simultaneously, each flavor can be harmonious and consistent, the tobacco flavor, the flower flavor and the fruit flavor have high identification degree without obvious segmentation, and the tobacco flavor and the elecampane are pure and long. Comparative example 1 also had the advantages of novel taste, tobacco aroma, floral aroma, and harmonious, abundant, and long-lasting aucklandia root.
The above embodiments are not exhaustive of the range of parameters of the claimed technical solutions of the present invention and the new technical solutions formed by equivalent replacement of single or multiple technical features in the technical solutions of the embodiments are also within the scope of the claimed technical solutions of the present invention, and if no specific description is given for all the parameters involved in the technical solutions of the present invention, there is no unique combination of the parameters with each other that is not replaceable.
The specific embodiments described herein are merely illustrative of the spirit of the invention and do not limit the scope of the invention. The technical solutions similar or similar to the present invention can be obtained by those skilled in the art through equivalent replacement or equivalent transformation, and all fall within the protection scope of the present invention.

Claims (5)

1. The electronic atomized liquid with rich and durable mouth feel is characterized by comprising 0.1-10 wt% of tobacco essence and 90-99.9 wt% of solvent, wherein the tobacco essence is prepared from a tobacco fragrance light component and a plant natural perfume; the cigarette fragrance light component is prepared by taking waste and inferior tobacco stems and tobacco leaves as raw materials through alkali pretreatment, fermentation, filtration and molecular distillation;
the plant natural perfume comprises a plant perfume A, a plant perfume B and a plant perfume C, wherein the plant perfume A has a fruity fragrance note, the plant perfume B has a flowery fragrance note, and the plant perfume C has a costustoot fragrance note;
the preparation method of the electronic atomization liquid with rich and durable mouthfeel comprises the following steps:
s1, carrying out alkaline pretreatment on waste and inferior tobacco stems and tobacco leaves, mixing the waste and inferior tobacco stems and the tobacco leaves with water and aroma-producing yeast for fermentation, filtering to obtain a tobacco aroma fermentation liquid, and separating by molecular distillation to obtain a tobacco aroma light component of a distillation section at 70-100 ℃;
s2, mixing the light components of the cigarette fragrance with plant natural perfume according to the ratio of 100: (1-10) (w/w) are mixed, the mixture is placed in a closed container for aging for 15-45 days, then the mixture is cooled and centrifuged, the cooling temperature is 0-5 ℃, and the supernatant is separated to obtain the tobacco essence;
and S3, mixing the tobacco essence in the S2 with a solvent to prepare the electronic atomized liquid.
2. The electronic atomized liquid with abundant and lasting mouthfeel as claimed in claim 1, wherein the plant spice A is one or more of hawthorn tincture, grapefruit oil, bergamot oil, lemon extract, tangerine oil, sweet orange essential oil, lime essential oil, bitter orange essential oil, high-intensity natural apple spice, plum extract and pineapple extract.
3. The electronic atomized liquid with rich and durable mouthfeel according to claim 1, wherein the plant spice B is one or more of clove bud oil, marigold essential oil, chrysanthemum morifolium oil, chamomile essential oil, white orchid essential oil, rose essential oil, iris resin, acacia oil, jasmine essential oil, daidai flower oil, gardenia essential oil, tree orchid oil, sweet osmanthus essential oil and lavender essential oil.
4. The electronic atomized liquid with abundant and lasting mouthfeel according to claim 1, wherein the plant spice C is one or more of patchouli oil, costus oil, bay oil, spikenard oil, wintergreen oil, cedar oil, sandalwood oil, storax oil, balsam fir oil and cajeput oil.
5. The electronic atomized liquid with abundant and durable mouthfeel according to claim 1, wherein the alkaline pretreatment in S1 is as follows: adding waste tobacco stems and tobacco leaves into an alkali solution, uniformly stirring, heating for 2-5 hours, filtering, and washing with pure water to be neutral.
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CN106047481A (en) * 2016-06-03 2016-10-26 湖北中烟工业有限责任公司 Preparation method and application of discarded tobacco leaf fermentation extract
CN106333384B (en) * 2016-11-01 2017-11-07 湖北中烟工业有限责任公司 A kind of mixed type tobacco molecular distillation light component electronic cigarette liquid and preparation method thereof
KR20180068236A (en) * 2016-12-13 2018-06-21 충남대학교산학협력단 Liquid composition for eletronic cigarette and manufacture method thereof
CN109527641B (en) * 2017-09-22 2021-04-27 江西中烟工业有限责任公司 Tobacco extract and preparation method thereof
CN107653066A (en) * 2017-09-28 2018-02-02 河南省新郑金叶香料有限公司 A kind of cigarette radix glycyrrhizae aroma component and its extracting method and application
CN109998153A (en) * 2019-03-22 2019-07-12 河南中烟工业有限责任公司 A kind of tobacco juice for electronic smoke prepared using microbial fermentation tobacco leaf
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