CN104839883A - Electronic cigarette liquid with characteristics of tobaccos for tobacco pipes - Google Patents
Electronic cigarette liquid with characteristics of tobaccos for tobacco pipes Download PDFInfo
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- CN104839883A CN104839883A CN201510286771.6A CN201510286771A CN104839883A CN 104839883 A CN104839883 A CN 104839883A CN 201510286771 A CN201510286771 A CN 201510286771A CN 104839883 A CN104839883 A CN 104839883A
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- tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- A24F47/002—
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses electronic cigarette liquid with characteristics of tobaccos for tobacco pipes. The electronic cigarette liquid is characterized by being made of, by weight, 5-40% of tobacco extracts, 5%-20% of tobacco essences, 0.5%-2.0% of nicotine, 5%-10% of deionized water, 10%-20% of glycerin and the rest of propylene glycol. The tobacco extracts are extracted from raw tobaccos, and light components are taken after molecular distillation. In order to highlight tobacco characteristics including high fragrance, high penetration, high satisfaction and the like, the raw tobaccos are taken as raw materials of the tobacco extracts; in order to reduce content of high-boiling-point substances in the extracts, the tobacco extracts are separated by means of molecular distillation and are light components after molecular distillation, the light components make fragrance and taste of the electronic cigarettes to be closer to those of traditional cigarettes, deposition of nonvolatile substances on heating wires of the electronic cigarettes is avoided, and service lives of the heating wires of the electronic cigarettes are prolonged while taste of electronic cigarette products is improved.
Description
Technical field
The invention belongs to tobacco juice for electronic smoke technical field, be specifically related to a kind of tobacco juice for electronic smoke with pipe tobacco style and features.
Background technology
Along with coming into effect of " Framework Convention on Tobacco Control ", smoking ban scope in public place, countries in the world progressively expands, and domestic and international tobacco consumption environment just profound change occurs.Electronic cigarette, because it is not containing the harmful components such as tar, CO, does not produce the features such as second-hand-cigarette, receives increasing concern.Tobacco juice for electronic smoke, primarily of propane diols, glycerine and nicotine composition, being aided with various essence to improve taste, having the various tastes such as coffee, peppermint, strawberry.In addition, have also appeared the tobacco juice for electronic smoke of several functions type in recent years, as tooth health (CN 201010254808.4), health-care throat-moistening type (CN 201010576200.3), slim functional form (CN 201010254798.4), medicinal health type (CN 200910104921.1), caries prevention type (CN 200910105219.7) etc. are good in whitening.But electronic cigarette product tobacco aroma is in the market more weak, the use of a large amount of essence and flavoring agent, make electronic cigarette in fragrance, mouthfeel etc., differ comparatively large with traditional cigarette, consumer is difficult to accept, and even has nauseating sensation.These shortcomings or deficiency constrain the development of electronic cigarette, thus, how to improve the quality of tobacco juice for electronic smoke, make it can meet the psychological need of consumer, can reach again certain psychic gratification sense, have important function to the development of electronic cigarette.
In recent years, abroad on market, the consumer group of pipe tobacco increases gradually, and pipe tobacco specializes in use the tobacco product that smokes of tobacco pipe, has sheet or strip or the various shape such as thread.Pipe tobacco gives off a strong fragrance when sucking, and by force, a people aspirates houseful lasting, not only can meet the psychological need of consumer, and strong fragrance makes people be in a cheerful frame of mind, thus rather well received for penetration power and diffusivity.High fragrance high satisfaction that pipe tobacco possesses just electronic cigarette needs improvement badly, although the taste of electronic cigarette has a lot at present, not yet has the tobacco juice for electronic smoke of pipe tobacco style and features.
Summary of the invention
The shortcomings such as the cigarette perfume (or spice) that the object of the invention is to exist for tobacco juice for electronic smoke is not dense, mouthfeel is poor, provide a kind of tobacco juice for electronic smoke with pipe tobacco style and features.Described tobacco juice has the feature of similar pipe tobacco, namely cigarette aromatic strongly fragrant, penetration power is strong, diffusivity good, satisfaction is strong, can meet the Physiological and psychological requirements of consumer.
For achieving the above object, the present invention adopts following technical scheme:
Have a tobacco juice for electronic smoke for pipe tobacco style and features, become by the mixed raw material of following percetage by weight: tobacco extract 5-40%, flavouring essence for tobacco 5%-20%, nicotine 0.5%-2.0%, deionized water 5%-10%, glycerine 10%-20%, surplus is propane diols; Described tobacco extract is with hair cigarette for raw material extracts, and this extract is by getting its light component after molecular clock process.
For highlighting the features such as pipe tobacco height fragrance, high satisfaction, tobacco material described in the present invention is hair cigarette, and especially with the solarization Huang that Yunnan Mao Yanwei represents, and the solarization that Sichuan Mao Yanwei represents is red; The object of employing molecular clock process is the content in order to reduce high boiling substance in tobacco extract, improves the mouthfeel of electronic cigarette.
In the present invention, the preparation method of tobacco extract specifically comprises the following steps: raw meal is broken to 10 ~ 100 orders by (1); (2) add organic solvent and carry out lixiviate; (3) be separated leaching liquor after filtering, leaching liquor reduced pressure concentration obtains tobacco extract; (4) ethanol back dissolving, freezing dewaxing: the high concentration ethanol (95% ethanol or absolute ethyl alcohol) adding 5 ~ 10 times of quality in gained tobacco extract, after abundant dissolving, this solution is placed in refrigerator (0 ~-20 DEG C) freezing 8 ~ 20 h, after insoluble matter is fully separated out, decompress filter or centrifugation supernatant, supernatant reduced pressure concentration obtains tobacco concentrate; (5) molecular clock: gained concentrate can directly be separated with molecular clock, or carries out molecular clock separation again after adding propane diols dissolving, and the consumption adding propane diols is 1 ~ 3 times of concentrate quality, described molecular clock condition: vacuum 1 ~ 10
-2mbar, vapo(u)rizing temperature 50-100 DEG C, scraper plate rotating speed 150-240 rpm, charging rate 2-5 mL/min, collect light component after molecular clock is separated and namely obtain described tobacco extract.
At least one in described step (2) during extraction in organic solvent benzinum used, ethyl acetate, ether, 95% ethanol, absolute ethyl alcohol etc., feed liquid mass ratio is 1:6 ~ 1:10, and extraction time is 1 ~ 3 h.
Described flavouring essence for tobacco is made up of the material of following percentage by weight: oxidation isophorone 0.1%-3%, natural herb 1%-5%, vanillic aldehyde 0.1%-1%, blueberry extract 1%-10%, guaiacol 0.5%-2%, Megastigmatrienone 3%-5%, cocoa extract 1%-10%, ethanol 1%-15%, surplus are propane diols.
In order to make the application obtain good effect, described nicotine is natural nicotine.
Relative to prior art, the present invention has the following advantages:
(1) for highlighting the style and features of pipe tobacco height fragrance high satisfaction, in the present invention with hair cigarette for raw material, especially Yunnan hair cigarette and Sichuan hair cigarette.Yunnan hair cigarette is cut into willow leaf by light, and because its pipe tobacco is soft, the thin hair cigarette as therefore named in hair of silk, fragrant odour is one of main component of pipe tobacco pipe tobacco.Sichuan hair cigarette adopts paste rice water processing method to ferment further usually, decapacitation is played outside general fermentation (clear water fermentation) usefulness, also has its unique strong point: improve flavor and taste further, smell and have a kind of sour-sweet fragrance, suction fragrance is plentiful, pure, and pleasant impression is pure, comfortable.
(2) tobacco extract that tobacco juice for electronic smoke of the present invention is used, through molecular clock process, can not have volatile-resistant substance to be deposited on the heater strip of electronic cigarette, can improve the life-span of electronic cigarette heater strip and the mouthfeel of electronic cigarette product.
Detailed description of the invention
Below in conjunction with embodiment the present invention will be further explained explanation.
embodiment 1
Have a tobacco juice for electronic smoke for pipe tobacco style and features, obtained by the mixed raw material of following percentage by weight: tobacco extract 5%, flavouring essence for tobacco 20%, nicotine 0.5%, deionized water 5%, glycerine 20%, surplus is propane diols.
Described flavouring essence for tobacco is made up of the material of following percentage by weight: oxidation isophorone 0.1%, natural herb 1%, vanillic aldehyde 0.5%, blueberry extract 5%, guaiacol 0.5%, Megastigmatrienone 3%, cocoa extract 5%, ethanol 5%, surplus are propane diols.
Tobacco extract is obtained by following methods: Sichuan hair cigarette tobacco leaf powder is broken to 10 orders by (1); (2) add the ethyl acetate of 6 times of quality, circumfluence distillation 1 h, extract 2 times; (3) after extraction terminates, leach leaching liquor with 400 order filter clothes, leaching liquor is evaporated to without till ethyl acetate after merging, and obtains tobacco extract; (4) in this medicinal extract, add 95% ethanol of 10 times of quality, abundant dissolving is placed on (-10 DEG C) in refrigerator freezing 12 h, now insoluble matter is separated out, suction filtration or centrifugation supernatant (4000 rpm, 15 min), supernatant is evaporated to without alcohol taste, obtains tobacco concentrate; (5) molecular clock: take above-mentioned concentrate, be separated by molecular clock, its condition is vacuum 0.5mbar, vapo(u)rizing temperature 60 DEG C, scraper plate rotating speed 200 rpm, charging rate 4 mL/min, collects light component and is described tobacco extract.
embodiment 2
Have a tobacco juice for electronic smoke for pipe tobacco style and features, obtained by the mixed raw material of following percentage by weight: tobacco extract 30%, flavouring essence for tobacco 5%, nicotine 1.0%, deionized water 8%, glycerine 10%, surplus is propane diols.
Described flavouring essence for tobacco is made up of the material of following percentage by weight: oxidation isophorone 3%, natural herb 3%, vanillic aldehyde 0.1%, blueberry extract 1%, guaiacol 1.2%, Megastigmatrienone 4.2%, cocoa extract 1%, ethanol 15%, surplus are propane diols.
Tobacco extract is obtained by following methods: Yunnan hair cigarette tobacco leaf powder is broken to 50 orders by (1); (2) add 95% ethanol of 8 times of quality, circumfluence distillation 3 h, extract 2 times; (3) after extraction terminates, leach leaching liquor with 400 order filter clothes, after leaching liquor merges, reduced pressure concentration obtains tobacco extract; (4) in this medicinal extract, add 95% ethanol of 5 times of quality, after fully dissolving, be placed in freezing 8 h of refrigerator (-20 DEG C).After insoluble matter is separated out, suction filtration or centrifugation supernatant (4000 rpm, 20 min), supernatant is evaporated to without alcohol taste, obtains tobacco concentrate; (5) molecular clock: take above-mentioned concentrate, is added the propane diols of concentrate 3 times amount, is separated after mixing by molecular clock, and its condition is vacuum 10
-2mbar, vapo(u)rizing temperature 50 DEG C, scraper plate rotating speed 150 rpm, charging rate 2.5 mL/min, collect light component and be described tobacco extract.
embodiment 3
Have a tobacco juice for electronic smoke for pipe tobacco style and features, obtained by the mixed raw material of following percentage by weight: tobacco extract 40%, flavouring essence for tobacco 15%, nicotine 2.0%, deionized water 10%, glycerine 15%, surplus is propane diols.
Described flavouring essence for tobacco is made up of the material of following percentage by weight: oxidation isophorone 1.5%, natural herb 5%, vanillic aldehyde 1%, blueberry extract 10%, guaiacol 2%, Megastigmatrienone 5%, cocoa extract 10%, ethanol 1%, surplus are propane diols.
Tobacco extract is obtained by following methods: hair cigarette tobacco leaf powder is broken to 100 orders by (1); (2) add the benzinum of 10 times of quality, circumfluence distillation 2 h, extract 2 times; (3) after extraction terminates, leach leaching liquor with 400 order filter clothes, be evaporated to without till benzinum after twice leaching liquor merges, obtain tobacco extract; (4) in tobacco extract, add the absolute ethyl alcohol of 8 times of quality, fully dissolve and be placed on (-5 DEG C) in refrigerator freezing 20 h, after insoluble matter is separated out, suction filtration or centrifugation (4000 rpm, 30 min), supernatant is evaporated to without alcohol taste, obtains tobacco concentrate; (5) molecular clock: take above-mentioned concentrate, be separated by molecular clock, its condition is vacuum 1mbar, vapo(u)rizing temperature 100 DEG C, scraper plate rotating speed 240 rpm, charging rate 5 mL/min, collects light component and is described tobacco extract.
Claims (6)
1. one kind has the tobacco juice for electronic smoke of pipe tobacco style and features, it is characterized in that: become by the mixed raw material of following percetage by weight: tobacco extract 5-40%, flavouring essence for tobacco 5%-20%, nicotine 0.5%-2.0%, deionized water 5%-10%, glycerine 10%-20%, surplus is propane diols; Described tobacco extract is with hair cigarette for raw material extracts, and this extract is by getting its light component after molecular clock process.
2. the tobacco juice for electronic smoke with pipe tobacco style and features according to claim 1, is characterized in that: described hair tobacco bale draws together the solarization Huang represented with Yunnan Mao Yanwei, or red with the solarization of Sichuan Mao Yanwei representative.
3. the tobacco juice for electronic smoke with pipe tobacco style and features according to claim 1, is characterized in that: the preparation method of tobacco extract specifically comprises the following steps: hair cigarette raw meal is broken to 10 ~ 100 orders by (1); (2) add organic solvent and carry out lixiviate; (3) be separated leaching liquor after filtering, leaching liquor reduced pressure concentration obtains tobacco extract; (4) ethanol back dissolving, freezing dewaxing: the high concentration ethanol adding 5 ~ 10 times of quality in gained tobacco extract, after abundant dissolving, this solution is placed in refrigerator (0 ~-20 DEG C) freezing 8 ~ 20 h, after insoluble matter is fully separated out, decompress filter or centrifugation supernatant, supernatant reduced pressure concentration obtains tobacco concentrate; (5) molecular clock: gained concentrate can directly be separated with molecular clock, or carries out molecular clock separation again after adding propane diols dissolving, and the consumption adding propane diols is 1 ~ 3 times of concentrate quality, described molecular clock condition: vacuum 1 ~ 10
-2mbar, vapo(u)rizing temperature 50-100 DEG C, scraper plate rotating speed 150-240 rpm, charging rate 2-5 mL/min, collect light component after molecular clock is separated and namely obtain described tobacco extract.
4. the tobacco juice for electronic smoke with pipe tobacco style and features according to claim 3, is characterized in that: the high concentration ethanol described in step (4) is 95% ethanol or absolute ethyl alcohol.
5. the tobacco juice for electronic smoke with pipe tobacco style and features according to claim 3, it is characterized in that: the organic solvent described in described step (2) is at least one in benzinum, ethyl acetate, ether, 95% ethanol, absolute ethyl alcohol, feed liquid mass ratio is 1:6 ~ 1:10, and extraction time is 1 ~ 3 h.
6. the tobacco juice for electronic smoke with pipe tobacco style and features according to claim 1, is characterized in that:
Described flavouring essence for tobacco is made up of the material of following percentage by weight: oxidation isophorone 0.1%-3%, natural herb 1%-5%, vanillic aldehyde 0.1%-1%, blueberry extract 1%-10%, guaiacol 0.5%-2%, Megastigmatrienone 3%-5%, cocoa extract 1%-10%, ethanol 1%-15%, surplus are propane diols.
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| CN201510286771.6A CN104839883B (en) | 2015-05-31 | 2015-05-31 | A kind of tobacco juice for electronic smoke with pipe tobacco style and features |
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| CN201510286771.6A CN104839883B (en) | 2015-05-31 | 2015-05-31 | A kind of tobacco juice for electronic smoke with pipe tobacco style and features |
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| CN104839883A true CN104839883A (en) | 2015-08-19 |
| CN104839883B CN104839883B (en) | 2016-05-04 |
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Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105105321A (en) * | 2015-10-14 | 2015-12-02 | 中国烟草总公司郑州烟草研究院 | Electronic cigarette tobacco extract without sweet greasy taste and electronic liquid |
| CN105341998A (en) * | 2015-12-17 | 2016-02-24 | 立场电子科技发展（上海）有限公司 | Method for preparing electronic cigarette liquid through microwave-assisted extraction |
| CN105361237A (en) * | 2015-12-02 | 2016-03-02 | 江苏中烟工业有限责任公司 | Electronic cigarette tobacco juice with cholesterol reducing function and preparation method thereof |
| CN105533793A (en) * | 2016-02-24 | 2016-05-04 | 江西中烟工业有限责任公司 | Preparation method for tobacco extract of dark sun-cured tobacco |
| CN105639718A (en) * | 2016-02-29 | 2016-06-08 | 湖北中烟工业有限责任公司 | Preparation method and application of tobacco extract easy to atomize at low temperature |
| CN105661625A (en) * | 2016-02-29 | 2016-06-15 | 湖北中烟工业有限责任公司 | Preparation method and application of tobacco extract for novel cigarettes |
| CN105754722A (en) * | 2016-03-14 | 2016-07-13 | 湖北中烟工业有限责任公司 | Preparation method and application of tobacco-aroma matters for tobacco sheets |
| CN105852189A (en) * | 2016-05-31 | 2016-08-17 | 湖北中烟工业有限责任公司 | Method for preparing tobacco extract by utilizing waste and inferior tobacco leaves |
| CN106307606A (en) * | 2016-11-22 | 2017-01-11 | 中国烟草总公司郑州烟草研究院 | Method for preparing high-fragrance tobacco extract |
| CN106333384A (en) * | 2016-11-01 | 2017-01-18 | 湖北中烟工业有限责任公司 | Mixed type tobacco molecular distillation light component electronic tobacco liquid and preparation method thereof |
| CN106723303A (en) * | 2016-12-26 | 2017-05-31 | 颐中（青岛）实业有限公司 | A kind of method that wet pulverizing prepares tobacco flavor electronics tobacco tar |
| CN106954887A (en) * | 2016-10-13 | 2017-07-18 | 武汉黄鹤楼香精香料有限公司 | A kind of preparation method of cigarette pineapple extract |
| CN106954883A (en) * | 2016-10-13 | 2017-07-18 | 武汉黄鹤楼香精香料有限公司 | A kind of cigarette preparation method of tuberose flower extract |
| CN106954886A (en) * | 2016-10-13 | 2017-07-18 | 武汉黄鹤楼香精香料有限公司 | A kind of preparation method of cigarette apple extract |
| CN107319637A (en) * | 2016-04-28 | 2017-11-07 | 湖南中烟工业有限责任公司 | A kind of extracting method of the electronic cigarette basic smoke raw material of tobacco source |
| CN109090699A (en) * | 2018-08-28 | 2018-12-28 | 河北中烟工业有限责任公司 | A kind of preparation method heating the tobacco product that do not burn |
| CN109998153A (en) * | 2019-03-22 | 2019-07-12 | 河南中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke prepared using microbial fermentation tobacco leaf |
| CN110338452A (en) * | 2019-06-06 | 2019-10-18 | 钟加川 | A kind of smokeless electronic cigarette tobacco tar |
| CN111000284A (en) * | 2019-12-25 | 2020-04-14 | 贵州中烟工业有限责任公司 | Method for extracting aroma substances in Yunyan tobacco extract, spice and cigarette |
| CN115067539A (en) * | 2022-05-27 | 2022-09-20 | 海南摩尔兄弟科技有限公司 | Aerosol generating substrate, tobacco extract and preparation method thereof |
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| CN106333384B (en) * | 2016-11-01 | 2017-11-07 | 湖北中烟工业有限责任公司 | A kind of mixed type tobacco molecular distillation light component electronic cigarette liquid and preparation method thereof |
| CN106307606A (en) * | 2016-11-22 | 2017-01-11 | 中国烟草总公司郑州烟草研究院 | Method for preparing high-fragrance tobacco extract |
| CN106307606B (en) * | 2016-11-22 | 2018-02-23 | 中国烟草总公司郑州烟草研究院 | A kind of preparation method of high fragrance tobacco extract |
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| CN106723303A (en) * | 2016-12-26 | 2017-05-31 | 颐中（青岛）实业有限公司 | A kind of method that wet pulverizing prepares tobacco flavor electronics tobacco tar |
| CN109090699A (en) * | 2018-08-28 | 2018-12-28 | 河北中烟工业有限责任公司 | A kind of preparation method heating the tobacco product that do not burn |
| CN109998153A (en) * | 2019-03-22 | 2019-07-12 | 河南中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke prepared using microbial fermentation tobacco leaf |
| CN110338452A (en) * | 2019-06-06 | 2019-10-18 | 钟加川 | A kind of smokeless electronic cigarette tobacco tar |
| CN111000284A (en) * | 2019-12-25 | 2020-04-14 | 贵州中烟工业有限责任公司 | Method for extracting aroma substances in Yunyan tobacco extract, spice and cigarette |
| CN111000284B (en) * | 2019-12-25 | 2022-02-01 | 贵州中烟工业有限责任公司 | Method for extracting aroma substances in Yunyan tobacco extract, spice and cigarette |
| CN115067539A (en) * | 2022-05-27 | 2022-09-20 | 海南摩尔兄弟科技有限公司 | Aerosol generating substrate, tobacco extract and preparation method thereof |
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