CN104585863A - Electronic cigarette juice - Google Patents
Electronic cigarette juice Download PDFInfo
- Publication number
- CN104585863A CN104585863A CN201510027136.6A CN201510027136A CN104585863A CN 104585863 A CN104585863 A CN 104585863A CN 201510027136 A CN201510027136 A CN 201510027136A CN 104585863 A CN104585863 A CN 104585863A
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- Prior art keywords
- extract
- tobacco
- electronic smoke
- rum
- airing
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses electronic cigarette juice. The electronic cigarette juice is characterized in that the electronic cigarette juice is prepared by uniformly mixing the following components in percentage by mass: 10-30% of aired tobacco extract, 1-3% of rum, 1-10% of tobacco flavor, 1-30% of glycerol, 1-10% of deionized water, and the balance of propylene glycol, wherein the aired tobacco extract is obtained by supercritical CO2 extraction. The electronic cigarette juice has the advantage that the aired tobacco extract obtained by supercritical CO2 extraction has heavy cigar flavor and nicotine flavor, so the electronic cigarette juice prepared by the aired tobacco extract also has heavy cigar flavor, and the physiological requirement on nicotine by consumers is also met.
Description
Technical field
The invention belongs to electronic cigarette technical field, be specifically related to a kind of tobacco juice for electronic smoke.
Background technology
Smoking not only endangers the healthy of smoker, and its second-hand-cigarette produced forms harm to the health of people around.Compared with cigarette, electronic cigarette containing tar, without harmful substances such as carbon monoxide, does not reduce the risk to the healthy injury of smoker; In addition, the nicotine of electronic cigarette, through the aerosol of atomization formation, is diluted rapidly in atmosphere, is also reduced risk people around being produced to harm.Electronic cigarette is as the substitute of cigarette, and obtain market accreditation in the world, sales volume presents ascendant trend year by year.
Current tobacco juice for electronic smoke is mainly that raw material adopts tradition or modern extraction means to prepare electronic cigarette tobacco extract with flue-cured tobacco, and then be mixed and made into tobacco juice for electronic smoke with flavouring essence for tobacco, deionized water, glycerine, propane diols etc., still can not meet the consumer group of preference cigar taste.Also there is not yet in prior art and utilize airing tobacco extract to prepare the report with the tobacco juice for electronic smoke of cigar flavor.
Summary of the invention
The object of the invention is for the deficiency of existing electronic cigarette in the suction such as fragrance, mouthfeel sensation, a kind of airing tobacco extract that utilizes is provided to prepare the tobacco juice for electronic smoke with cigar flavor, described tobacco juice for electronic smoke can enrich the suction local flavor of electronic cigarette, improve the inherent suction quality of electronic cigarette, meets the consumer group of preference cigar flavor.
In order to reach above-mentioned technique effect, the present invention takes following technical scheme:
The invention provides a kind of tobacco juice for electronic smoke, described tobacco juice for electronic smoke comprises the component of following mass percent: airing tobacco extract 10-30%, Rum 1-3%, tobacco aromatics 1-10%, glycerine 1-30%, deionized water 1-10%, and surplus is propane diols.
According to the preferred embodiment of the present invention, the component of described tobacco juice for electronic smoke mass percent is: airing tobacco extract 15-25%, Rum 1-3%, tobacco aromatics 5-10%, glycerine 10-30%, deionized water 5-10%, and surplus is propane diols.
According to the preferred embodiment of the present invention, described tobacco juice for electronic smoke, it is characterized in that: the preparation method of described airing tobacco extract is as follows: after airing cigarette tobacco leaf is pulverized, be placed in supercritical extraction unit to extract, extracting pressure is 15-30Mpa, extraction temperature is 30-50 DEG C, and extraction time is 1-3h, and extraction mode is static extracting.
According to the preferred embodiment of the present invention, described airing cigarette be selected from ShenFang,SiChuan hair cigarette, Tongxiang, Zhejiang suncured tabacco, new capital, Sichuan willow cigarette, Wuming, Guangxi suncured tabacco, Guangfeng, Jiangxi suncured tabacco, Hunan Huaihua's suncured tabacco, Fujian saxian's suncured tabacco, An Huisong county suncured tabacco, Nanhsiung, Kwangtung burley tobaccos, Sichuan burley tobaccos one or more.
According to the preferred embodiment of the present invention, the extractant of described supercritical extract is CO
2.
According to the preferred embodiment of the present invention, described Rum be selected from silver-colored Rum, golden Rum, Myers dark Rum one or more.
According to the preferred embodiment of the present invention, described tobacco aromatics is selected from one or more in apple extract, smoked plum extractive, licorice extract, grape extract, red date extract, Fructus Rosae Normalis extract, Fructus Monordicae extract, tendril-leaved fritillary bulb extract, snow pear extract, chrysanthemum extract, dried orange peel extracts.
The present invention is further illustrated below.
A kind of tobacco juice for electronic smoke, described tobacco juice for electronic smoke comprises the component of following mass percent: airing tobacco extract 10-30%, Rum 1-3%, tobacco aromatics 1-10%, glycerine 1-30%, deionized water 1-10%, and surplus is propane diols.
According to the preferred embodiment of the present invention, the component of described tobacco juice for electronic smoke mass percent is: airing tobacco extract 15-25%, Rum 1-3%, tobacco aromatics 5-10%, glycerine 10-30%, deionized water 5-10%, and surplus is propane diols.
In the present invention, by the component mixing by mass percentage of each raw material, after within 1 hour, mixing with 40r/min mechanical agitation, described tobacco juice for electronic smoke is obtained.
According to the preferred embodiment of the present invention, the preparation method of described airing tobacco extract is: after being pulverized by airing cigarette tobacco leaf, be placed in supercritical extraction unit and extract, extracting pressure is 15-30Mpa, extraction temperature is 30-50 DEG C, and extraction time is 1-3h, and extraction mode is static extracting.
In the present invention, at first airing cigarette being placed in 40 DEG C, baking oven, dry 2h, then obtain 40-60 object offal by mechanical crushing airing cigarette sieving, the offal of gained is placed in the extraction equipment that model is HA221-50-02, be 15-30Mpa in extracting pressure, extraction temperature is 30-50 DEG C, uses CO
2as extractant, adopt the mode of static extracting to extract 1-3h, obtain described airing tobacco extract.
According to the preferred embodiment of the present invention, described airing cigarette be selected from ShenFang,SiChuan hair cigarette, Tongxiang, Zhejiang suncured tabacco, new capital, Sichuan willow cigarette, Wuming, Guangxi suncured tabacco, Guangfeng, Jiangxi suncured tabacco, Hunan Huaihua's suncured tabacco, Fujian saxian's suncured tabacco, An Huisong county suncured tabacco, Nanhsiung, Kwangtung burley tobaccos, Sichuan burley tobaccos one or more.
According to the preferred embodiment of the present invention, the extractant of described supercritical extract is CO
2.
According to the preferred embodiment of the present invention, described Rum be selected from silver-colored Rum, golden Rum, Myers dark Rum one or more.
In the present invention, the described Rum place of production is Cuba or Puerto Rico.
According to the preferred embodiment of the present invention, described tobacco aromatics is selected from one or more in apple extract, smoked plum extractive, licorice extract, grape extract, red date extract, Fructus Rosae Normalis extract, Fructus Monordicae extract, tendril-leaved fritillary bulb extract, snow pear extract, chrysanthemum extract, dried orange peel extracts.
In the present invention, described tobacco aromatics is bought to Shenzhen BoDun spice Co., Ltd.
In the present invention, supercritical CO is adopted
2airing tobacco extract prepared by extraction mode has cigar flavor and nicotine taste, and making with this airing tobacco extract is that tobacco juice for electronic smoke prepared by raw material also has cigar flavor and nicotine taste.
The present invention compared with prior art, has following beneficial effect:
Tobacco juice for electronic smoke of the present invention has strong cigar flavor, can meet the consumer group of preference cigar flavor.
Tobacco juice for electronic smoke of the present invention is with airing tobacco extract for main component, and the flavor component not only containing cigar flavor in extract, also containing a certain amount of nicotine, can meet the psychological need of consumer to nicotine.
Detailed description of the invention
Below in conjunction with embodiments of the invention, the invention will be further elaborated.
Embodiment 1
A kind of preparation method of airing tobacco extract: by the hair cigarette 1.5kg of ShenFang,SiChuan, suncured tabacco 0.5kg, An Huisong county, Wuming, Guangxi suncured tabacco 0.5kg, Sichuan burley tobaccos 0.5kg are dried, pulverized, sieving obtains offal, offal is placed in HA221-50-02 type supercritical extraction unit to extract, extracting pressure is 20Mpa, extraction temperature is 40 DEG C, and extractant is CO
2, the static extracting time is 2.5h, obtains brown paste and is airing tobacco extract.
A kind of tobacco juice for electronic smoke, comprise the component of following mass percent: airing tobacco extract 25%, deionized water 10%, silver-colored Rum 1%, smoked plum extractive 2%, licorice 2%, chrysanthemum extract 1%, glycerine 20%, surplus is propane diols.Each raw material is proportionally mixed, and under normal temperature 40r/min mechanical agitation 1h, each component is fully mixed.
Embodiment 2
A kind of preparation method of airing tobacco extract: Guangfeng, Jiangxi suncured tabacco 0.5kg, Fujian saxian suncured tabacco 0.5kg, Sichuan burley tobaccos 1.5kg, Nanhsiung, Kwangtung burley tobaccos 0.5kg are dried, pulverizes, sieving obtains offal, offal is placed in HA221-50-02 type supercritical extraction unit to extract, extracting pressure is 20Mpa, extraction temperature is 40 DEG C, and extractant is CO
2, the static extracting time is 2.5h, obtains brown paste and is airing tobacco extract.
A kind of tobacco juice for electronic smoke, comprises the component of following quality proportioning: airing tobacco extract 25%, deionized water 10%, golden Rum 1%, smoked plum extractive 4%, apple extract 3%, red date extract 2%, Fructus Rosae Normalis extract 1%, glycerine 20%, surplus is propane diols.Each raw material is proportionally mixed, and under normal temperature 40r/min mechanical agitation 1h, each component is fully mixed.
Embodiment 3
A kind of preparation method of airing tobacco extract: by new capital willow cigarette 0.5kg, Tongxiang, Zhejiang suncured tabacco 1kg, Wuming, Guangxi suncured tabacco 0.5kg, Hunan Huaihua suncured tabacco 0.5kg, Sichuan burley tobaccos 0.5kg are dried, pulverized, sieving obtains offal, offal is placed in HA221-50-02 type supercritical extraction unit to extract, extracting pressure is 20Mpa, extraction temperature is 45 DEG C, and extractant is CO
2, the static extracting time is 2.5h, obtains brown paste and is airing tobacco extract.
A kind of tobacco juice for electronic smoke, comprises the component of following quality proportioning: airing tobacco extract 20%, deionized water 10%, Myers dark Rum 2%, grape extract 2%, licorice 1%, apple extract 1%, Fructus Monordicae extract 1%, glycerine 25%, surplus is propane diols.Each raw material is proportionally mixed, and under normal temperature 40r/min mechanical agitation 1h, each component is fully mixed.
Embodiment 4
A kind of preparation method of airing tobacco extract: the hair cigarette 1.5kg of ShenFang,SiChuan, Tongxiang, Zhejiang suncured tabacco 1.5kg are dried, pulverizes, sieving obtains offal, offal is placed in HA221-50-02 type supercritical extraction unit to extract, extracting pressure is 25Mpa, extraction temperature is 40 DEG C, and extractant is CO
2, the static extracting time is 2.0h, obtains brown paste and is airing tobacco extract.
A kind of tobacco juice for electronic smoke, comprise the component of following quality proportioning: airing tobacco extract 25%, water 10%, silver-colored Rum 3%, tendril-leaved fritillary bulb extract 3%, snow pear extract 3%, licorice 1%, dried orange peel extracts 1%, glycerine 20%, surplus is propane diols.Each raw material is proportionally mixed, and under normal temperature 40r/min mechanical agitation 1h, each component is fully mixed.
Embodiment 5
Electronic cigarette sensory quality assessment method:
According to Sensory Quality of Cigarette judgment criteria GB5606.4-2005, in conjunction with electronic cigarette organoleptic features, according to different weight, 6 evaluation indexes and score value are set, in table 1.
Table 1: electronic cigarette sensory quality assessment method
Tobacco juice for electronic smoke described in embodiment 1 to embodiment 4 is carried out aesthetic quality's evaluation and analysis, and evaluation and analysis result is evaluated and analysed result according to each expert and is tried to achieve arithmetic equal value, and result retains a position effective digital, and statistics is in table 2.
Table 2: embodiment 1 to embodiment 4 sensory quality assessment
| Sample | Satisfaction | Fragrance | Harmony | Assorted gas | Excitant | Pleasant impression |
| Embodiment 1 | 24.0 | 22.5 | 4.0 | 8.5 | 18.0 | 13.5 |
| Embodiment 2 | 24.5 | 22.5 | 4.5 | 8.0 | 17.5 | 14.0 |
| Embodiment 3 | 23.5 | 23.0 | 4.5 | 9.0 | 18.5 | 14.0 |
| Embodiment 4 | 24.5 | 22.0 | 4.0 | 9.0 | 19.0 | 14.5 |
Although with reference to explanatory embodiment of the present invention, invention has been described here, above-described embodiment is only the present invention's preferably embodiment, embodiments of the present invention are not restricted to the described embodiments, should be appreciated that, those skilled in the art can design a lot of other amendment and embodiment, these amendments and embodiment will drop within spirit disclosed in the present application and spirit.
Claims (7)
1. a tobacco juice for electronic smoke, is characterized in that: described tobacco juice for electronic smoke comprises the component of following mass percent: airing tobacco extract 10-30%, Rum 1-3%, tobacco aromatics 1-10%, glycerine 1-30%, deionized water 1-10%, and surplus is propane diols.
2. tobacco juice for electronic smoke according to claim 1, is characterized in that: the component of described tobacco juice for electronic smoke mass percent is: airing tobacco extract 15-25%, Rum 1-3%, tobacco aromatics 5-10%, glycerine 10-30%, deionized water 5-10%, surplus is propane diols.
3. tobacco juice for electronic smoke according to claim 1, it is characterized in that: the preparation method of described airing tobacco extract is as follows: after airing cigarette tobacco leaf is pulverized, be placed in supercritical extraction unit to extract, extracting pressure is 15-30Mpa, extraction temperature is 30-50 DEG C, extraction time is 1-3h, and extraction mode is static extracting.
4. tobacco juice for electronic smoke according to claim 3, is characterized in that: described airing cigarette be selected from ShenFang,SiChuan hair cigarette, Tongxiang, Zhejiang suncured tabacco, new capital, Sichuan willow cigarette, Wuming, Guangxi suncured tabacco, Guangfeng, Jiangxi suncured tabacco, Hunan Huaihua's suncured tabacco, Fujian saxian's suncured tabacco, An Huisong county suncured tabacco, Nanhsiung, Kwangtung burley tobaccos, Sichuan burley tobaccos one or more.
5. tobacco juice for electronic smoke according to claim 3, is characterized in that: described supercritical extract extractant used is CO
2.
6. tobacco juice for electronic smoke according to claim 1, is characterized in that: described Rum be selected from silver-colored Rum, golden Rum, Myers dark Rum one or more.
7. tobacco juice for electronic smoke according to claim 1, is characterized in that: described tobacco aromatics is selected from one or more in apple extract, smoked plum extractive, licorice extract, grape extract, red date extract, Fructus Rosae Normalis extract, Fructus Monordicae extract, tendril-leaved fritillary bulb extract, snow pear extract, chrysanthemum extract, dried orange peel extracts.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510027136.6A CN104585863B (en) | 2015-01-20 | 2015-01-20 | A kind of tobacco juice for electronic smoke |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510027136.6A CN104585863B (en) | 2015-01-20 | 2015-01-20 | A kind of tobacco juice for electronic smoke |
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| CN104585863A true CN104585863A (en) | 2015-05-06 |
| CN104585863B CN104585863B (en) | 2016-08-24 |
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Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104839883A (en) * | 2015-05-31 | 2015-08-19 | 中国烟草总公司郑州烟草研究院 | Electronic cigarette liquid with characteristics of tobaccos for tobacco pipes |
| CN104983064A (en) * | 2015-06-05 | 2015-10-21 | 浙江中烟工业有限责任公司 | Electronic cigarette liquid and preparation method thereof |
| CN104983054A (en) * | 2015-06-04 | 2015-10-21 | 湖北中烟工业有限责任公司 | Preparation method and application of extract to improving cigarette sour and sweet note |
| CN105011351A (en) * | 2015-07-23 | 2015-11-04 | 川渝中烟工业有限责任公司 | Electronic cigarette liquid with tartary buckwheat fragrance |
| CN105132176A (en) * | 2015-09-28 | 2015-12-09 | 中国烟草总公司郑州烟草研究院 | Preparation method of Mao cigarette extract and application of Mao cigarette extract to cigarette filter stick |
| CN105341998A (en) * | 2015-12-17 | 2016-02-24 | 立场电子科技发展（上海）有限公司 | Method for preparing electronic cigarette liquid through microwave-assisted extraction |
| CN106118886A (en) * | 2016-07-29 | 2016-11-16 | 湖北中烟工业有限责任公司 | A kind of cigarette Fructus Rosae Normalis spice and preparation method thereof |
| CN106108102A (en) * | 2016-08-23 | 2016-11-16 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of red pitaya wine odor type electronic cigarette tobacco tar |
| CN106136298A (en) * | 2016-08-23 | 2016-11-23 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of litchi spirit odor type electronic cigarette tobacco tar |
| CN106136299A (en) * | 2016-08-23 | 2016-11-23 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of Morus alba L. odor type electronic cigarette tobacco tar |
| CN106307601A (en) * | 2016-08-23 | 2017-01-11 | 广西壮族自治区农业科学院农产品加工研究所 | Longan wine scent type electronic cigarette liquid |
| CN106418660A (en) * | 2015-08-13 | 2017-02-22 | 上海烟草集团有限责任公司 | Preparation method for tobacco liquid of electronic cigarette and application of same |
| CN107319626A (en) * | 2017-07-07 | 2017-11-07 | 河南中烟工业有限责任公司 | A kind of tobacco aromaticss and preparation method thereof and the application in cigarette |
| CN108107154A (en) * | 2017-08-14 | 2018-06-01 | 广西中烟工业有限责任公司 | A kind of sensory quality assessment method suitable for electronic cigarette |
| CN110558603A (en) * | 2019-09-12 | 2019-12-13 | 深圳雾芯科技有限公司 | Flavor composition and electronic cigarette liquid containing same |
| WO2020258386A1 (en) * | 2019-06-27 | 2020-12-30 | 广东中烟工业有限责任公司 | Slow-release flavorant and application thereof in chinese-flavor tobacco product |
| CN114766710A (en) * | 2022-03-29 | 2022-07-22 | 河南中烟工业有限责任公司 | Cigar-flavored electronic cigarette oil |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104839883A (en) * | 2015-05-31 | 2015-08-19 | 中国烟草总公司郑州烟草研究院 | Electronic cigarette liquid with characteristics of tobaccos for tobacco pipes |
| CN104983054A (en) * | 2015-06-04 | 2015-10-21 | 湖北中烟工业有限责任公司 | Preparation method and application of extract to improving cigarette sour and sweet note |
| CN104983064A (en) * | 2015-06-05 | 2015-10-21 | 浙江中烟工业有限责任公司 | Electronic cigarette liquid and preparation method thereof |
| CN105011351A (en) * | 2015-07-23 | 2015-11-04 | 川渝中烟工业有限责任公司 | Electronic cigarette liquid with tartary buckwheat fragrance |
| CN106418660B (en) * | 2015-08-13 | 2020-03-24 | 上海烟草集团有限责任公司 | Preparation method and application of electronic cigarette liquid |
| CN106418660A (en) * | 2015-08-13 | 2017-02-22 | 上海烟草集团有限责任公司 | Preparation method for tobacco liquid of electronic cigarette and application of same |
| CN105132176A (en) * | 2015-09-28 | 2015-12-09 | 中国烟草总公司郑州烟草研究院 | Preparation method of Mao cigarette extract and application of Mao cigarette extract to cigarette filter stick |
| CN105341998A (en) * | 2015-12-17 | 2016-02-24 | 立场电子科技发展（上海）有限公司 | Method for preparing electronic cigarette liquid through microwave-assisted extraction |
| CN105341998B (en) * | 2015-12-17 | 2017-03-29 | 立场电子科技发展（上海）有限公司 | A kind of method that utilization microwave auxiliary extraction prepares electronic cigarette liquid |
| CN106118886A (en) * | 2016-07-29 | 2016-11-16 | 湖北中烟工业有限责任公司 | A kind of cigarette Fructus Rosae Normalis spice and preparation method thereof |
| CN106307601A (en) * | 2016-08-23 | 2017-01-11 | 广西壮族自治区农业科学院农产品加工研究所 | Longan wine scent type electronic cigarette liquid |
| CN106136299A (en) * | 2016-08-23 | 2016-11-23 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of Morus alba L. odor type electronic cigarette tobacco tar |
| CN106136298A (en) * | 2016-08-23 | 2016-11-23 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of litchi spirit odor type electronic cigarette tobacco tar |
| CN106108102A (en) * | 2016-08-23 | 2016-11-16 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of red pitaya wine odor type electronic cigarette tobacco tar |
| CN107319626A (en) * | 2017-07-07 | 2017-11-07 | 河南中烟工业有限责任公司 | A kind of tobacco aromaticss and preparation method thereof and the application in cigarette |
| CN108107154A (en) * | 2017-08-14 | 2018-06-01 | 广西中烟工业有限责任公司 | A kind of sensory quality assessment method suitable for electronic cigarette |
| WO2020258386A1 (en) * | 2019-06-27 | 2020-12-30 | 广东中烟工业有限责任公司 | Slow-release flavorant and application thereof in chinese-flavor tobacco product |
| US12022856B2 (en) | 2019-06-27 | 2024-07-02 | China Tobacco Guangdong Industrial Co., Ltd. | Slow-release fragrance and application thereof in a tobacco product with Chinese-style flavor |
| CN110558603A (en) * | 2019-09-12 | 2019-12-13 | 深圳雾芯科技有限公司 | Flavor composition and electronic cigarette liquid containing same |
| WO2021046924A1 (en) * | 2019-09-12 | 2021-03-18 | 深圳雾芯科技有限公司 | Flavor composition and e-liquid comprising flavor composition |
| CN114766710A (en) * | 2022-03-29 | 2022-07-22 | 河南中烟工业有限责任公司 | Cigar-flavored electronic cigarette oil |
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Effective date of registration: 20161228 Address after: 610000, Sichuan, Chengdu, Longquanyi economic and Technological Development Zone, Jackie Chan Road, Longquan, No. 2, paragraph Patentee after: CHINA TOBACCO SICHUAN INDUSTRIAL CO., LTD. Patentee after: CHONGQING CHINA TOBACCO INDUSTRIAL CO., LTD. Address before: 610000 Jackie Chan Road, Chengdu economic and Technological Development Zone, Longquanyi District, Sichuan, China, No. 2, No. Patentee before: China Tobacco Chuanyu Industry Co., Ltd. |