CN104544555A - Electronic cigarette smoke solution with blood sugar decreasing function - Google Patents
Electronic cigarette smoke solution with blood sugar decreasing function Download PDFInfo
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- CN104544555A CN104544555A CN201410849793.4A CN201410849793A CN104544555A CN 104544555 A CN104544555 A CN 104544555A CN 201410849793 A CN201410849793 A CN 201410849793A CN 104544555 A CN104544555 A CN 104544555A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
Abstract
The invention relates to an electronic cigarette smoke solution with the blood sugar decreasing function. The electronic cigarette smoke solution is prepared from the following components in parts by mass: 50 to 80 parts of propylene glycol, 5 to 30 parts of glycerinum, 2 to 5 parts of edible alcohol, 1 to 30 parts of tobacco extract, 0.5 to 15 parts of tobacco flavor, and 0.5 to 10 parts of Chinese herbal medicine extract with the appetite improving and digestion prompting functions. According to the electronic cigarette smoke solution, the Chinese herbal medicine extract with the appetite improving and digestion prompting functions are mixed with the tobacco extract, so that the fragrance of the electronic cigarette smoke solution is rich, coordinated and increases the sense of satisfaction; the disadvantage of insufficient fragrance and taste of the electronic cigarette smoke solution is reduced to some extent; in addition, the electronic cigarette smoke solution has the effect of decreasing the blood sugar.
Description
Technical field
The present invention relates to a kind of tobacco juice for electronic smoke with function of blood sugar reduction, belong to electronic cigarette technical field.
Background technology
Traditional cigarette is generally provide nicotine and relevant aroma components by the mode of cigarette of burning to consumer.Because the reasons such as Pintsch process and flue gas migration cause containing a large amount of harmful components in main flume in sucking process, fraction is wherein had to have carcinogenic danger as condensed-nuclei aromatics is proved.Also produce a large amount of flue gas smog in the process of smoking property of cigarette, not only cause environmental pollution, also bring the harm of second-hand-cigarette simultaneously to non-smoker.Along with the progressively enforcement of the international Framework Convention on Tobacco Control and the enhancing gradually of health of people consciousness, traditional cigarette selling market is subject to powerful impact.Electronic cigarette takes atomizing type to generate smog sensation, does not produce tar and CO, produces second-hand-cigarette harm hardly simultaneously, is regarded as non-harmful smoking cessation product or substitute of tobacco, receives showing great attention to and extensively studying of domestic and international each large tobacco enterprise.The selling market of current electronic cigarette is mainly in the U.S., and Europe, Asia then possess good growth trends, and particularly the market of China Electronics's cigarette is also in the cultivation and exploitation stage.The electronic cigarette product taste developed at present is partial to blended type cigarette, compares the taste custom meeting foreign consumers, and Chinese Consumer's preference flue-cured tobacco, taste is comparatively strong, and the mouthfeel of electronic cigarette is difficult to reach requirement.It is the key opening Chinese market that improvement electronic cigarette formula of liquid makes it to meet Chinese Consumer's custom.
Electronic cigarette, as a kind of form in novel tobacco goods, presents great market prospect, and reason is mainly to provide the consumption habit similar with traditional cigarette and satisfaction on the one hand, and the hazard index of electronic cigarette reduces greatly than traditional cigarette on the other hand.Electronic cigarette formula of liquid is the key highlighting electronic cigarette advantage.In order to simulate the fragrance of traditional cigarette, fragrance and mouthfeel to the full extent, solution the most general at present adds tobacco extract in tobacco juice.Tobacco juice for electronic smoke is mixed to get according to a certain ratio by the essential oil of tobaccos and Alevaire, flavouring essence for tobacco that extract acquisition.The less harmful of electronic cigarette is that what to make to suck human body by incombustible mode is atomized liquid and non-burning pyrolysis product.Many Chinese herbal medicine compositions not only have certain characteristic flavor compounds, also have certain health-care effect simultaneously, have even and alleviate some disease effect.Tobacco extract is combined with Chinese herbal medicine extract, not only compensate for the shortcoming of tobacco juice for electronic smoke flavor component deficiency to a certain extent, be different from external tobacco juice for electronic smoke simultaneously, the tobacco juice for electronic smoke of Chinese style characteristic can be built, meet consumer's custom, certain health-care effect is provided simultaneously.
The present invention has the Chinese herbal medicine extract of effect of lowering blood sugar by preparation, afterwards it is mixed with tobacco extract, be aided with and use suitable essence spice for cigarette to modify, can prepare that fragrance enriches, comfortable taste, satisfaction are got well and there is the tobacco juice for electronic smoke of certain Hyperglycemic health care function.
Summary of the invention
The object of the present invention is to provide a kind of tobacco juice for electronic smoke with function of blood sugar reduction, improve existing tobacco juice for electronic smoke mouthfeel not good, the shortcomings such as fragrance is not enough, give electronic cigarette certain hypoglycemic health care simultaneously.
The present invention is achieved by the following technical solutions:
A kind of tobacco juice for electronic smoke, comprises following component according to the mass fraction: propane diols 50 ~ 80 parts, glycerine 5 ~ 30 parts, edible alcohol 2 ~ 5 parts, tobacco extract 1 ~ 30 part, flavouring essence for tobacco 0.5 ~ 15 part, has the Chinese herbal medicine extract 0.5 ~ 10 part of effect of lowering blood sugar.
Preferably, described a kind of tobacco juice for electronic smoke, comprises following component according to the mass fraction: propane diols 65 ~ 80 parts, glycerine 10 ~ 25 parts, edible alcohol 2 ~ 4 parts, tobacco extract 10 ~ 20 parts, flavouring essence for tobacco 1 ~ 5 part, has the Chinese herbal medicine extract 1 ~ 5 part of effect of lowering blood sugar.
Optimum, described a kind of tobacco juice for electronic smoke, comprises following component according to the mass fraction: propane diols 70 parts, glycerine 20 parts, edible alcohol 3 parts, tobacco extract 15 parts, flavouring essence for tobacco 3 parts, has the Chinese herbal medicine extract 3 parts of effect of lowering blood sugar.
Described Chinese herbal medicine extract is selected from ginseng, the coptis, golden cypress, gynostemma pentaphylla, the root bark of Chinese wolf-berry, and the one or more combination in the Radix Astragali, highland rhodiola root, chrysanthemum, hairyvein agrimony, corn stigma, the root of kudzu vine, American Ginseng, radix scrophulariae, mulberry leaf, the fleece-flower root, the fruit of Chinese wolfberry, the tuber of dwarf lilyturf, the wind-weed, rhizoma atractylodis, rhizome of chuanxiong, Poria cocos, radix polygonati officinalis, Chinese yam, matrimony vine, cactus, great burdock achene, sealwort is through extracting obtained concentrate.
Most preferred, described Chinese herbal medicine is the combination of the coptis, ginseng, the tuber of dwarf lilyturf, Chinese yam, and in a preferred embodiment, described Chinese herbal medicine is the combination of the coptis 50 parts, ginseng 100 parts, the tuber of dwarf lilyturf 100 parts, Chinese yam 150 parts; Or,
The combination of mulberry leaf, the root of kudzu vine, radix scrophulariae, sealwort, the root bark of Chinese wolf-berry, golden cypress, matrimony vine, the Radix Astragali, rhizoma atractylodis, in a preferred embodiment, described Chinese herbal medicine is the combination of 45 parts, mulberry leaf, the root of kudzu vine 30 parts, radix scrophulariae 30 parts, sealwort 30 parts, the root bark of Chinese wolf-berry 30 parts, golden cypress 36 parts, matrimony vine 24 parts, the Radix Astragali 30 parts, rhizoma atractylodis 24 parts; Or,
The combination of matrimony vine, great burdock achene, radix scrophulariae, the root of kudzu vine, golden cypress, in a preferred embodiment, described Chinese herbal medicine is the combination of matrimony vine 100 parts, great burdock achene 50 parts, radix scrophulariae 50 parts, the root of kudzu vine 50 parts, golden cypress 50 parts; Or,
The combination of hairyvein agrimony, the root of kudzu vine, mulberry leaf, the fleece-flower root, American Ginseng, in a preferred embodiment, described Chinese herbal medicine is the combination of hairyvein agrimony 100 parts, the root of kudzu vine 100 parts, 70 parts, mulberry leaf, the fleece-flower root 35 parts, American Ginseng 20 parts.
Chinese herbal medicine extract described in the present invention can adopt method conventional in prior art to obtain.
Preferably, the extracting method of described Chinese herbal medicine extract is: get Chinese herbal medicine raw material, crushed after being dried powdered, hot reflux is added after solvent soaking, then be separated and remove filter residue, and the liquid of acquisition is carried out centrifugal treating, afterwards by the supernatant membrane filtration of centrifugal acquisition, finally by the filtrate reduced in volume of membrane filtration and get final product.
Preferably, the powder size after described pulverizing is 40 ~ 100 orders, is more preferably 40 ~ 60 orders.
Preferably, described solvent is the aqueous solution of ethanol, and percentage by volume is 40% ~ 80%.
Preferably, during immersion, the mass ratio of described Chinese herbal medicine powder and described solvent is 1:(2 ~ 5), shake up, sealing, soaks 8 ~ 12 hours; Preferred, the mass ratio of described Chinese herbal medicine powder and described solvent is 1:(2.5 ~ 3.5).
Preferably, the time adding hot reflux described in is 1 ~ 5 hour; Be more preferably 2.5 ~ 3.5 hours.
Preferably, described centrifugal rotating speed is 2500 ~ 4000r/min, centrifugal 10 ~ 30min; More preferably at 4000r/min, centrifugal 20min.
Preferably, the specification of the filter sizes of described membrane filtration is 0.45 μm.
Preferably, described simmer down to is under 50 ~ 90 DEG C of conditions, and decompression is revolved and desolventized to obtain Chinese herbal medicine extract; More preferably concentrated at 60 ~ 80 DEG C.
Described tobacco extract is selected from the tobacco leaf of flue-cured tobacco, air-curing of tobacco leaves and suncured tabacco or pipe tobacco through extracting obtained extract; Described air-curing of tobacco leaves comprises burley tobaccos, Maryland; Described suncured tabacco comprises Turkish tobaccos, Dark sun-cured, Sun cured tobacco and Nicotiniana rustica.
Preferably, described tobacco extract is mass ratio is 1:(0.9-1.1) flue-cured tobacco and the tobacco leaf of burley tobaccos or pipe tobacco through extracting obtained concentrate.
Tobacco extract described in the present invention can adopt method conventional in prior art to obtain.
Preferably, the extracting method of described tobacco extract, for: get tobacco leaf or pipe tobacco, crushed after being dried powdered, be placed in solvent and carry out ultrasonic extraction, through sedimentation, filtration and reduced pressure concentration i.e. obtained described tobacco extract.
Preferably, the grinding particle size of described tobacco leaf or pipe tobacco is 40 ~ 100 orders, is more preferably 40 ~ 60 orders.
Preferably, described ultrasonic extraction process, the mass ratio of tobacco leaf or pipe tobacco powder and solvent is 1:(2 ~ 5); Be more preferably 1:(2.5 ~ 3.5).
Preferably, described solvent is deionized water or ethanol.
Preferably, the temperature of described ultrasonic extraction is 30 ~ 60 DEG C, is more preferably 40 ~ 60 DEG C.
Preferably, the time of described ultrasonic extraction is 2 ~ 5 hours, is more preferably 3.5 ~ 4.5 hours.
Preferably, under 50 ~ 90 DEG C of conditions, decompression is revolved and is desolventized to obtain tobacco extract, and more excellent is 60 ~ 80 DEG C.
The present invention does not have special restriction to the kind of described tobacco essence and source, adopts flavouring essence for tobacco well known to those skilled in the art.
Preferably; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3,5,5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine and 2; 3,5-trimethylpyrazine.
Preferably, described flavouring essence for tobacco is the component being selected from following weight percent: 1 ~ 10% Ethyl vanillin, 1 ~ 10% benzyl acetate, 1 ~ 8% furfural, 4 ~ 20% dorinones, 2 ~ 15% β-damascone, 10 ~ 30% Megastigmatrienones, 2 ~ 15% dihydroactinidiolides, 1 ~ 8% dimethyl succinate, 1 ~ 5%2, 6, 6-trimethyl-2-cyclohexene-1, 4-diketone, 1 ~ 5%2-hydroxyl-3, 5, 5-trimethyl-2-cyclonene, 3 ~ 15% geranyl acetones, 5 ~ 30% alpha, beta-lonones, 3 ~ 15% phenmethylols, 2 ~ 7% palmitic acids, 1 ~ 4% isovaleric acid, 1 ~ 4%2-methylvaleric acid, 1 ~ 3% indoles, 1 ~ 3% pyridine, 1 ~ 5%3-acetylpyridine and 1 ~ 5%2, 3, multiple combination in 5-trimethylpyrazine, and to meet summation be 100wt%.
Preferably, described flavouring essence for tobacco is following several formula (percentage by weight):
Formula one: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Said components is mixed in vortex oscillator.
Formula two: 15% dorinones, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol; Said components is mixed in vortex oscillator.
Formula three: 15% dorinones, 30% Megastigmatrienone, 5%2,3,5-trimethylpyrazines, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 12% phenmethylol.
Formula four: 30% Megastigmatrienones, 5% benzyl acetate, 6% furfural, 8% Ethyl vanillin, 7% palmitic acid, 3%2,3,5-trimethylpyrazines, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 15% phenmethylol.
Formula five: 15% dorinones, 30% Megastigmatrienone, 5%2,3,5-trimethylpyrazines, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% alpha, beta-lonone, 12% phenmethylol.
Preferably, described glycerine and propane diols are food grade product.
The preparation of electronic cigarette liquid of the present invention, for mixing described each composition mix and blend and get final product.
The Chinese herbal medicine extract with effect of lowering blood sugar provided by the present invention, is mixed to get tobacco juice for electronic smoke with tobacco extract, flavouring essence for tobacco, propane diols, glycerine etc.Compared with prior art, the present invention has following beneficial effect:
(1) the present invention mixes with tobacco extract by choosing the Chinese herbal medicine extract specifically with effect of lowering blood sugar, and by using specific flavouring essence for tobacco formula, makes tobacco juice for electronic smoke fragrance abundanter; In addition, adding of described Chinese herbal medicine extract does not only affect only containing the sensory evaluation of the tobacco juice of tobacco extract, and make its fragrance more coordinate on the contrary, satisfaction is good, improves the shortcoming of tobacco juice for electronic smoke fragrance and taste deficiency to a great extent.
(2) tobacco juice for electronic smoke of the present invention generates smog sensation owing to taking atomizing type, does not produce tar and CO, does not produce second-hand-cigarette harm simultaneously.
(3) the present invention is by adding containing the Chinese herbal medicine extract with effect of lowering blood sugar, has hypoglycemic effect.
Detailed description of the invention
Below by way of specific instantiation, technical scheme of the present invention is described.Should be understood that one or more method steps that the present invention mentions do not repel and before and after described combination step, also to there is additive method step or can also insert additive method step between these steps clearly mentioned; Should also be understood that these embodiments are only not used in for illustration of the present invention to limit the scope of the invention.And, except as otherwise noted, the numbering of various method steps is only the convenient tool differentiating various method steps, but not be ordering or the enforceable scope of restriction the present invention of restriction various method steps, the change of its relativeness or adjustment, when changing technology contents without essence, when being also considered as the enforceable category of the present invention.
Embodiment 1:
The preparation of tobacco extract: get cured tobacco leaf sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 100 orders.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, afterwards standing sedimentation 4h, sand core funnel filters to get filtrate, and 70 ± 10 DEG C of vacuum rotary steams are concentrated into 3mL, obtain tobacco extract.
The preparation of Chinese herbal medicine extract: take coptis 50g, ginseng 100g, the tuber of dwarf lilyturf 100g, Chinese yam 150g, through pulverizer grind be 40 ~ 100 order powder after mix, add 80% ethanol/water mixed solvent, controlling feed liquid weight ratio is 1:3, shake up, sealing, soaks 12 hours.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract is in the centrifugal 20min of 4000r/min, and supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 12mL, obtains Chinese herbal medicine extract.
Flavouring essence for tobacco (percentage by weight): 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
There is the tobacco juice for electronic smoke preparation of function of blood sugar reduction, following components in mass portion number meter batching: tobacco extract 25 parts, flavouring essence for tobacco 3 parts, there is effect of lowering blood sugar Chinese herbal medicine extract 8 parts, glycerine 20 parts, edible alcohol 2 parts, propane diols 80 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Embodiment 2:
The preparation of tobacco extract: get burley tobaccos tobacco sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 100 orders.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h, standing sedimentation 4h afterwards under 50 ± 5 DEG C of conditions, sand core funnel filters to get filtrate, and 70 ± 10 DEG C of vacuum rotary steams are concentrated into 3mL, obtain tobacco extract.
Prepared by Chinese herbal medicine extract: take mulberry leaf 45g, root of kudzu vine 30g, radix scrophulariae 30g, sealwort 30g, root bark of Chinese wolf-berry 30g, golden cypress 36g, matrimony vine 24g, Radix Astragali 30g, rhizoma atractylodis 24g, through pulverizer grind be 40 ~ 100 order powder after mix, add 80% ethanol/water mixed solvent, controlling feed liquid weight ratio is 1:3, shakes up, sealing, soaks 12h.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract is in the centrifugal 20min of 4000r/min, and supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 8mL, obtains Chinese herbal medicine extract.
Flavouring essence for tobacco (percentage by weight): 15% dorinone, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
Preparation has the tobacco juice for electronic smoke of function of blood sugar reduction, following components in mass portion number meter batching: tobacco extract 20 parts, flavouring essence for tobacco 5 parts, there is effect of lowering blood sugar Chinese herbal medicine extract 4 parts, glycerine 10 parts, edible alcohol 3 parts, propane diols 65 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Embodiment 3:
Prepared by tobacco extract: get Sun cured tobacco tobacco sample, extract, extracting method is with embodiment 1.
Chinese herbal medicine extract prepare: take matrimony vine 100g great burdock achene 50g, radix scrophulariae 50g, root of kudzu vine 50g, golden cypress 50g, through pulverizer grind be 40 ~ 100 order powder after mix, add 80% ethanol/water mixed solvent, controlling feed liquid weight ratio is 1:3, shake up, sealing, soak 10h.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract is in the centrifugal 20min of 4000r/min, and supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 9mL, obtains Chinese herbal medicine extract.
Flavouring essence for tobacco (percentage by weight): 15% dorinone, 30% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 12% phenmethylol.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
Preparation has the tobacco juice for electronic smoke of function of blood sugar reduction, following components in mass portion number meter batching: tobacco extract 5 parts, flavouring essence for tobacco 8 parts, there is effect of lowering blood sugar Chinese herbal medicine extract 5 parts, glycerine 25 parts, edible alcohol 4 parts, propane diols 60 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Embodiment 4:
Prepared by tobacco extract: get flue-cured tobacco and the mixing of burley tobaccos tobacco leaf that mass ratio is 1:1, then extract obtained tobacco extract according to the mode of embodiment 1.
Prepared by Chinese herbal medicine extract: claim hairyvein agrimony 100g, root of kudzu vine 100g, mulberry leaf 70g, fleece-flower root 35g, American Ginseng 20g, by the extracting method of embodiment 1, obtains Chinese herbal medicine extract.
Flavouring essence for tobacco (percentage by weight): 30% Megastigmatrienone, 5% benzyl acetate, 6% furfural, 8% Ethyl vanillin, 7% palmitic acid, 3%2,3,5-trimethylpyrazine, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 15% phenmethylol.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
Preparation has the tobacco juice for electronic smoke of function of blood sugar reduction, following components in mass portion number is counted: tobacco extract 15 parts, flavouring essence for tobacco 3 parts, there is effect of lowering blood sugar Chinese herbal medicine extract 3 parts, glycerine 20 parts, edible alcohol 3 parts, propane diols 70 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Embodiment 5:
Prepared by tobacco extract: the pipe tobacco mixing of getting flue-cured tobacco that mass ratio is 1:1 and burley tobaccos, then extracts obtained tobacco extract according to the mode of embodiment 1.
Prepared by Chinese herbal medicine extract: get hairyvein agrimony 100g, root of kudzu vine 100g, mulberry leaf 70g, fleece-flower root 35g, American Ginseng 20g, by the extracting method of embodiment 1, obtains Chinese herbal medicine extract.
Flavouring essence for tobacco (percentage by weight): 15% dorinone, 30% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% alpha, beta-lonone, 12% phenmethylol.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
Preparation has the tobacco juice for electronic smoke of function of blood sugar reduction, following components in mass portion number meter batching: tobacco extract 10 parts, flavouring essence for tobacco 1 part, there is effect of lowering blood sugar Chinese herbal medicine extract 1 part, glycerine 20 parts, edible alcohol 5 parts, propane diols 70 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Comparative example 1 (not containing Chinese herbal medicine extract)
Prepared by tobacco juice for electronic smoke, following components in mass portion number meter batching: tobacco extract 25 parts, flavouring essence for tobacco 3 parts, glycerine 20 parts, edible alcohol 2 parts, and propane diols 80 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke;
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 1;
Comparative example 2 (not containing Chinese herbal medicine extract)
Prepared by tobacco juice for electronic smoke, below each component batching according to the mass fraction: tobacco extract 15 parts, flavouring essence for tobacco 3 parts, glycerine 20 parts, edible alcohol 3 parts, and propane diols 70 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke;
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 4;
Comparative example 3 (not containing flavouring essence for tobacco)
Prepared by tobacco juice for electronic smoke, by following components in mass portion number batching: tobacco extract 15 parts, have effect of lowering blood sugar Chinese herbal medicine extract 3 parts, glycerine 20 parts, edible alcohol 3 parts, propane diols 70 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke;
Tobacco extract composition and extracting method, Chinese herbal medicine extract composition and extracting method thereof are with embodiment 4.
Tobacco juice for electronic smoke liquid in above-described embodiment and comparative example is added in electronic cigarette device and carries out sensory effects evaluation respectively.
Sensory effects evaluation method comprises the following steps:
(1) 9 evaluation indexes are provided with, comprise excitant, satisfaction, concentration, comfort level, feature style, tobacco perfume, aroma quality, perfume quantity and the amount of being fuming, and give different score value according to the Different Effects degree of every evaluation index to tobacco juice for electronic smoke aesthetic quality.
(2) member of smoking of 9 people is set, everyone a tobacco juice for electronic smoke sensory quality assessment table, adopt the marking mode secretly commented, adopt the overall method of smokeing panel test that circulates, tobacco juice for electronic smoke is aspirated, according to the implication of 9 sensory quality assessment index score values in table 1, adopt hundred-mark system point system to carry out comprehensive grading to the aesthetic quality of tobacco juice for electronic smoke, every evaluation index is by five points, ten point system or the scoring of ten the five-grade marking systems.The concrete meaning of the score value of tobacco juice for electronic smoke evaluation index sees the following form 1:
The score value implication table of table 1 tobacco juice for electronic smoke sensory quality assessment index
(3) evaluation method: according to the evaluation index in table 1 and score value, member of smoking tackles each evaluation index and carries out sensory quality assessment, and records its evaluation result, and the minimum score unit of score value is 0.5.
(4) result statistics: remove minimum point and a best result in the sensory quality assessment result of all members of smoking, calculate the arithmetic mean of instantaneous value of remaining effective single item evaluation index scoring, result retains two-decimal, the sensory quality assessment comprehensive grading of last tobacco juice for electronic smoke is the arithmetic mean of instantaneous value sum calculating the scoring of each single index, obtain total score, result retains a decimal.
The tobacco juice for electronic smoke prepared in the tobacco juice for electronic smoke with function of blood sugar reduction prepared in embodiment 1-5 and comparative example 1-3 is added in electronic cigarette and carries out sensory quality assessment.Concrete evaluation result is in table 2, and in table 2, the scoring of every evaluation index is that the arithmetic average that 9 members of smoking effectively mark is divided.
Table 2 tobacco juice for electronic smoke sensory effects evaluation result
Table 2 result shows, the amount of being fuming abundance when tobacco juice for electronic smoke is embodied in suction in above-described embodiment, and fragrance enriches strong, tobacco and faint medicine perfume are coordinated, and strength is moderate, comfortable taste, without obvious irritation and dry sensation, shorten the aesthetic quality's difference with traditional cigarette.But the difference of the Chinese herbal medicine kind used, Tobacco Types, extract adding proportion, essence spice for cigarette adding proportion, can produce Different Effects to investigated 9 indexs; Chinese herbal medicine extract used can provide hypoglycemic action and efficacy simultaneously.
Claims (10)
1. a tobacco juice for electronic smoke, described tobacco juice for electronic smoke according to the mass fraction, comprises following component: propane diols 50 ~ 80 parts, glycerine 5 ~ 30 parts, edible alcohol 2 ~ 5 parts, tobacco extract 1 ~ 30 part, flavouring essence for tobacco 0.5 ~ 15 part, has the Chinese herbal medicine extract 0.5 ~ 10 part of effect of lowering blood sugar.
2. a kind of tobacco juice for electronic smoke as claimed in claim 1, is characterized in that, described tobacco extract is that the tobacco leaf of flue-cured tobacco, air-curing of tobacco leaves and suncured tabacco or pipe tobacco are through extracting obtained concentrate.
3. a kind of tobacco juice for electronic smoke as claimed in claim 2, is characterized in that, described air-curing of tobacco leaves comprises one or more the combination in burley tobaccos, Maryland; Described suncured tabacco comprises one or more the combination in Turkish tobaccos, Dark sun-cured, Sun cured tobacco and Nicotiniana rustica.
4. a kind of tobacco juice for electronic smoke as described in as arbitrary in claim 2-3, it is characterized in that, the extracting method of described tobacco extract is: get tobacco leaf and/or pipe tobacco, crushed after being dried powdered, be placed in solvent and carry out ultrasonic extraction, through sedimentation and filtration, reduced pressure concentration i.e. obtained described tobacco extract.
5. a kind of tobacco juice for electronic smoke as claimed in claim 4, is characterized in that, described extracting method also to comprise any one of following characteristics or multinomial:
(1) grinding particle size of described tobacco leaf or pipe tobacco is 40 ~ 100 orders;
(2) described ultrasonic extraction process, the mass ratio of tobacco leaf and/or pipe tobacco powder and solvent is 1:(2 ~ 5);
(3) described solvent is deionized water or ethanol;
(4) temperature of described ultrasonic extraction is 30 ~ 60 DEG C;
(5) time of described ultrasonic extraction is 2 ~ 5 hours;
(6) concrete grammar of concentrated i.e. obtained described tobacco extract is: under 50 ~ 90 DEG C of conditions, described filtrate decompression revolved and desolventize to obtain tobacco extract.
6. a kind of tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, described Chinese herbal medicine extract is ginseng, the coptis, golden cypress, gynostemma pentaphylla, the root bark of Chinese wolf-berry, and one or more in the Radix Astragali, highland rhodiola root, chrysanthemum, hairyvein agrimony, corn stigma, the root of kudzu vine, American Ginseng, radix scrophulariae, mulberry leaf, the fleece-flower root, the fruit of Chinese wolfberry, the tuber of dwarf lilyturf, the wind-weed, rhizoma atractylodis, rhizome of chuanxiong, Poria cocos, radix polygonati officinalis, Chinese yam, matrimony vine, cactus, great burdock achene, sealwort are through extracting obtained concentrate.
7. a kind of tobacco juice for electronic smoke as claimed in claim 6, it is characterized in that, the extracting method of described Chinese herbal medicine extract is: get Chinese herbal medicine raw material, crushed after being dried powdered, add hot reflux after solvent soaking, be then separated and remove filter residue, and the liquid of acquisition is carried out centrifugal treating, afterwards the supernatant of centrifugal acquisition is carried out membrane filtration, the filtrate of last membrane filtration concentrates and get final product.
8. a kind of tobacco juice for electronic smoke as claimed in claim 7, is characterized in that, described extracting method also comprises any one or multinomial in following characteristics:
(1) powder size after described pulverizing is 40 ~ 100 orders;
(2) described solvent is the aqueous solution of ethanol, and percent by volume is 40% ~ 80%;
(3), when soaking, the mass ratio of described Chinese herbal medicine powder and described solvent is 1:(2 ~ 5), shake up, sealing, soaks 8 ~ 12 hours;
(4) time adding hot reflux described in is 1 ~ 5 hour;
(5) described centrifugal rotating speed is 2500 ~ 4000r/min, centrifugal 10 ~ 30min;
(6) specification of the filter sizes of described membrane filtration is 0.45 μm;
(7) described simmer down to is under 50 ~ 90 DEG C of conditions, and decompression is revolved and desolventized to obtain Chinese herbal medicine extract.
9. a kind of tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2, 6, 6-trimethyl-2-cyclohexene-1, 4-diketone, 2-hydroxyl-3, 5, 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine and 2, 3, one or more combination in 5-trimethylpyrazine.
10. the preparation method of the tobacco juice for electronic smoke according to the arbitrary claim of claim 1 ~ 9, for directly each component being mixed in setting ratio, to obtain final product.
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Application publication date: 20150429 |