CN108041688A - A kind of electronic cigarette tobacco tar and preparation method - Google Patents
A kind of electronic cigarette tobacco tar and preparation method Download PDFInfo
- Publication number
- CN108041688A CN108041688A CN201810056796.0A CN201810056796A CN108041688A CN 108041688 A CN108041688 A CN 108041688A CN 201810056796 A CN201810056796 A CN 201810056796A CN 108041688 A CN108041688 A CN 108041688A
- Authority
- CN
- China
- Prior art keywords
- tobacco
- electronic cigarette
- leaf
- extract
- extraction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A24F47/002—
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
Abstract
The present invention provides a kind of electronic cigarette tobacco tars, and including non-tobacco extract, flavouring essence for tobacco and organic solvent, non-tobacco extract includes the extract of non-tobacco plant material, and non-tobacco plant material includes folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves.Because the ingredient of folium artemisiae argyi, eggplant leaf, tomato leaf and Alkaloids In Tea is similar with the ingredient of alkaloid in traditional tobacco leaf, and then the taste of folium artemisiae argyi, eggplant leaf, the taste of tomato leaf and tealeaves after atomizer is atomized with traditional tobacco leaf after atomizer is atomized is similar.Therefore, but user can be made to experience the taste identical with conventional cigarette without any tobacco substance using the electronic cigarette tobacco tar that folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves are prepared.Electronic cigarette tobacco tar provided by the invention, fragrance enriches, comfortable taste, satisfaction are good, and without any tobacco extract, not only meets the demand of user, but also will not jeopardize the health of user.
Description
Technical field
The invention belongs to electronic cigarette tobacco tar technical fields, and in particular to a kind of electronic cigarette tobacco tar and preparation method.
Background technology
A kind of form of the electronic cigarette as novel tobacco product, presents huge market prospects, reason essentially consists in
One side electronic cigarette provides the consumption habit and satisfaction similar with traditional flue-cured tobacco, the hazard index ratio of another aspect electronic cigarette
Traditional flue-cured tobacco substantially reduces.The public place management rule that no smoking is put into effect in Chinese more and more cities, it is believed that soon
Electronic cigarette can occupy a tiny space in Chinese market afterwards.
In order to simulate the fragrance of traditional flue-cured tobacco, fragrance and mouthfeel to the full extent, the electronic cigarette in electronic cigarette at present
Tobacco tar most commonly adds tobacco extract, and is mixed according to a certain ratio with flavouring essence for tobacco and organic solvent.But in electricity
Inevitably contain tobacco substance in tobacco extract in sub- cigarette tobacco tar, still can endanger the health of consumer.And
In electronic cigarette tobacco tar field, the electricity of traditional tobacco taste is realized currently without the substance for finding alternative tobacco extract
Sub- cigarette tobacco tar.
The content of the invention
In consideration of it, to solve the above-mentioned problems, the present invention provides a kind of electronic cigarette tobacco tar and preparation method, using non-cigarette
The extract of careless plant simulates the electronic cigarette tobacco tar of traditional tobacco taste, not only meets consumer demand, but also will not endanger
Evil arrives the health of consumer.
First aspect present invention provides a kind of electronic cigarette tobacco tar, including non-tobacco extract, flavouring essence for tobacco and organic molten
Agent, the non-tobacco extract include the extract of non-tobacco plant material, and the non-tobacco plant material includes folium artemisiae argyi, eggplant
Leaf, tomato leaf and tealeaves.
Wherein, count in parts by weight, the non-tobacco plant material includes：10-40 parts of folium artemisiae argyi, 5-25 parts of eggplant leaf,
1-10 parts of 2-25 parts of tomato leaf and tealeaves.
Wherein, the non-tobacco plant material further includes one kind or more in fibert, almond, cocoa bean, carrot and aloe
Kind；Wherein, count in parts by weight, 5-30 parts of fibert, 1-20 parts of almond, 5-30 parts of cocoa bean, 1-10 parts of carrot, aloe
1-10 parts.
Wherein, by mass percentage, including non-tobacco extract 1%-20%, flavouring essence for tobacco 0.1%-2% and organic
Solvent 60%-98%.
Wherein, the flavouring essence for tobacco is included in Ethyl vanillin, ethylmaltol, citronellol, geraniol and damascenone
It is one or more.
Wherein, the organic solvent includes the one or more in ethyl alcohol, propylene glycol and glycerine.
In a kind of electronic cigarette tobacco tar that first aspect present invention provides, because in folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves
The ingredient of alkaloid is similar with the ingredient of alkaloid in traditional tobacco extract, and taste caused by electronic cigarette tobacco tar mainly comes
Come from alkaloid generated taste after atomization.Moreover, also permitted in addition to alkaloid component in traditional tobacco extract
The substance more being hazardous to the human body, and in folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves in addition to alkaloid component, do not have but
There is the substance being hazardous to the human body.The aromatic property of wherein each leaves of plants is as follows：Folium artemisiae argyi has special fragrant and certain
Bitter taste；Eggplant leaf has sugariness, pungent taste, certain penetrating odor and roasting fragrance；Tomato leaf is pungent with certain irritation
Taste and roasting fragrance；Tealeaves has strong roasting fragrance.
Therefore, the non-tobacco extract being made of folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves is after atomizer is atomized, Chinese mugwort
Leaf, eggplant leaf, tomato leaf and the alkaloid in tealeaves can generate the taste after similar traditional tobacco extract atomization.And lead to
The synergistic effect crossed between folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves many kinds of substance can make tobacco flavor more abundant, strong, make
User experiences and with fragrance as the electronic cigarette oils of traditional tobacco extract allotment.
And folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves extract in without the substance being hazardous to the human body, it is therefore non-
Tobacco extract will not generate the substance being hazardous to the human body after atomizer is atomized.Therefore, it ensure that traditional tobacco mouth
While taste, the health of user will not be endangered.And flavouring essence for tobacco makes electronics tobacco tar not only can make the taste of electronic cigarette tobacco tar more
Close to the taste of conventional cigarette, it can also use family and good flue gas effect generated when burning and sucking.Therefore it is provided by the invention
Electronic cigarette tobacco tar, fragrance enriches, comfortable taste, satisfaction are good, and is free of any tobacco extract, not only meets the need of user
It asks, and the health of user will not be jeopardized.
Second aspect of the present invention provides a kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
The non-tobacco plant material is prepared into target size by negated tobacco plant material, then will be described non-tobacco
40-80 mesh is ground to after plant material is toasted；
The non-tobacco plant material after grinding is added in Extraction solvent impregnated successively, ultrasonic extraction and mistake
Filter, obtains extracting solution, obtains non-tobacco extract after the extracting solution is concentrated, the Extraction solvent is including carbon number
C2-C5Alcohols solvent, C3-C7Lipid solvent and C3-C7Ketone solvent in one or more and the mixed solutions of water；
The non-tobacco extract and flavouring essence for tobacco and organic solvent are mixed and stirred for uniformly, obtaining electronic cigarette tobacco tar.
Wherein, the Extraction solvent includes the mixed solution of second alcohol and water, and the ethyl alcohol accounts for the body of the mixed solution
Product percentage is 60%-95%.
Wherein, in the baking process, the temperature of baking is 100-250 DEG C, and the time of baking is 0.5-3h, described
In process of lapping, the rotating speed of grinding is 1500-3000r/min, milling time 10-15min.
Wherein, the extraction operation and the concentration operation are carried out using ultrasonic wave extraction concentration technology, in the extraction
In the process, the temperature of extraction is 40-70 DEG C, and the time of extraction is 20-40min, and in the concentration process, the temperature of concentration is
40-70 DEG C, the time of concentration is 10-30min.
The preparation method for a kind of electronic cigarette tobacco tar that second aspect of the present invention provides, by the way that non-tobacco plant material is dried
Roasting, grinding, immersion, extraction, filtering and concentration, can obtain non-tobacco extract.Again by non-tobacco extract and flavouring essence for tobacco and
Organic solvent by simply mix can obtain fragrance enrich, comfortable taste, satisfaction it is good, and without any tobacco extract
Object not only meets the demand of user, but also will not jeopardize the electronic cigarette tobacco tar of the health of user.Therefore the present invention
Preparation method is simple, at low cost, is suitble to large-scale production, has very strong practicability.
Description of the drawings
It to describe the technical solutions in the embodiments of the present invention more clearly, below will be to required in the embodiment of the present invention
The attached drawing used illustrates.
Fig. 1 is the process flow chart of the preparation method of electronic cigarette tobacco tar in the present embodiment.
Specific embodiment
It is the preferred embodiment of the present invention below, it is noted that for those skilled in the art,
Various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also considered as this hair
Bright protection domain.
A kind of electronic cigarette tobacco tar provided in an embodiment of the present invention, including non-tobacco extract, flavouring essence for tobacco and organic solvent,
The non-tobacco extract includes the extract of non-tobacco plant material, the non-tobacco plant material include folium artemisiae argyi, eggplant leaf,
Tomato leaf and tealeaves.
It is raw in folium artemisiae argyi, eggplant leaf, tomato leaf and the ingredient of Alkaloids In Tea and tradition tobacco leaf in non-tobacco extract
The ingredient of alkaloids is similar, and folium artemisiae argyi, eggplant leaf, the taste of tomato leaf and tealeaves after atomizer is atomized are passed through with traditional tobacco leaf
Taste after atomizer atomization is similar.Such as：
Folium artemisiae argyi：In addition to containing main component volatile oil, also containing tannin, flavones, alcohol, polysaccharide, trace element and other
Organic principle etc., the bitter taste for having special fragrant certain.
Eggplant leaf：Containing protein, carbohydrate, vitamin and various metals, there is sugariness and pungent taste, certain thorn
Swash property, bake fragrance.
Tomato leaf：Containing organic base, tomatidine and vitamin A, vitamin B, vitamin C and calcium, magnesium, potassium, sodium, phosphorus, iron
Minerals are waited, volatile ingredient is mostly nitrogenous compound and ester type compound, has the pungent taste of intense irritation, bakes fragrance.
Tealeaves：Protein, amino acid, caffeine, polyatomic phenol, carbohydrate, lipid, ore deposit are mainly included in ingredient
Substance, phytochrome, vitamin, volatile ingredient, organic acid have strong roasting fragrance.
Because alkaloid in folium artemisiae argyi, eggplant leaf, tomato leaf and the ingredient of Alkaloids In Tea and traditional tobacco extract
Ingredient it is similar, and taste caused by electronic cigarette tobacco tar is mainly derived from alkaloid generated taste after atomization.Moreover,
In traditional tobacco extract in addition to alkaloid component, there are many more the substance being hazardous to the human body, and in folium artemisiae argyi, eggplant
In leaf, tomato leaf and tealeaves in addition to alkaloid component, the substance that is not hazardous to the human body but.
Therefore, the non-tobacco extract being made of folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves is after atomizer is atomized, Chinese mugwort
Leaf, eggplant leaf, tomato leaf and the alkaloid in tealeaves can generate the taste after similar traditional tobacco extract atomization.And lead to
The synergistic effect crossed between folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves many kinds of substance can make tobacco flavor more abundant, strong, make
User experiences and with fragrance as the electronic cigarette oils of traditional tobacco extract allotment.
And folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves extract in without the substance being hazardous to the human body, it is therefore non-
Tobacco extract will not generate the substance being hazardous to the human body after atomizer is atomized.Therefore, it ensure that traditional tobacco mouth
While taste, the health of user will not be endangered.And flavouring essence for tobacco makes electronics tobacco tar not only can make the taste of electronic cigarette tobacco tar more
Close to the taste of conventional cigarette, it can also use family and good flue gas effect generated when burning and sucking.Therefore it is provided by the invention
Electronic cigarette tobacco tar, fragrance enriches, comfortable taste, satisfaction are good, and is free of any tobacco extract, not only meets the need of user
It asks, and the health of user will not be jeopardized.
It in embodiment of the present invention, counts in parts by weight, the non-tobacco plant material includes：10-40 parts of folium artemisiae argyi, eggplant
1-10 parts of 5-25 parts of cotyledon, 2-25 parts of tomato leaf and tealeaves.Folium artemisiae argyi, eggplant leaf, tomato leaf and the tealeaves of the present invention needs
It can just be made to play maximum effect in a specific range, make the closest traditional tobacco leaf of taste of non-tobacco plant material
Taste.
In embodiment of the present invention, the non-tobacco plant material further includes fibert, almond, cocoa bean, carrot and aloe
In one or more.The present invention except indispensable folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves, can also include fibert,
One or more in almond, cocoa bean, carrot and aloe.Their ingredient and taste is as follows：
Fibert：Fibert is rich in grease (being mostly unrighted acid), protein, carbohydrate, vitamin (vitamin
E), minerals, sugared fiber, the β-special compositions such as Gu sterol and antioxidant carbolic acid, the fibert toasted is with strong aromatic
Taste.
Almond：Protein, fat, sugar, micro amarogentin have certain fragrant and sweet taste and semen armeniacae amarae taste.
Cocoa bean：There are nerve centers excitatory substance and the pellets such as carbohydrate, fat, protein, vitamin B caffeine
Rather, there is dense cocoa aroma.
Carrot：Rich in carbohydrate, fat, volatile oil, carrotene, vitamin A, vitamin B1, vitamin B2, anthocyanidin,
The nutritional ingredients such as calcium, iron have strong carrot sweet.
Aloe：To contain anthraquinone and its glycosides, naphthalenone, resin, organic acid, there is slight bitter and unique aloe book on Chinese herbal medicine fragrance.
The fragrance and tobacco that ingredient in fibert, almond, cocoa bean, carrot and aloe generates after atomizer is atomized carry
Take the fragrance that the substance in object in addition to alkaloid component generates after atomizer is atomized similar.Therefore, folium artemisiae argyi, eggplant leaf,
The perfume (or spice) generated after the roasting fragrance and fibert, almond, cocoa bean, carrot and the aloe atomization that are generated after tomato leaf and tealeaves atomization
After taste is mutually mixed, the taste of electronic cigarette tobacco tar can be made to be closer to the taste of traditional tobacco leaf, greatly improve user
Experience sense.And raw material is simple, and it is of low cost.
Wherein, count in parts by weight, 5-30 parts of fibert, 1-20 parts of almond, 5-30 parts of cocoa bean, 1-10 parts of carrot
With 1-10 parts of aloe.Fibert, almond, cocoa bean, carrot and the aloe of the present invention cooperates in above-mentioned scope, can make
The perfume (or spice) that substance in the fragrance and tobacco extract that are generated after atomization in addition to alkaloid component generates after atomizer is atomized
Taste is closest.
Preferably, non-tobacco plant material includes：10-40 parts of folium artemisiae argyi, 5-25 parts of eggplant leaf, 2-25 parts of tomato leaf
With 1-10 parts of tealeaves, 5-30 parts of fibert, 1-20 parts of almond, 5-30 parts of cocoa bean, 1-10 parts of carrot and aloe 1-10
Part.Within the above range, the roasting fragrance and fibert, almond, cocoa generated after folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves atomization
After the fragrance generated after beans, carrot and aloe atomization is mutually mixed, the taste that electronic cigarette tobacco tar can be made generated after being atomized is most
Close to the fragrance of traditional tobacco.
In embodiment of the present invention, by mass percentage, including non-tobacco extract 1%-20%, flavouring essence for tobacco
0.1%-2% and organic solvent 60%-98%.
In embodiment of the present invention, the flavouring essence for tobacco includes Ethyl vanillin, ethylmaltol, citronellol, geraniol
With the one or more in damascenone, the organic solvent includes the one or more in ethyl alcohol, propylene glycol and glycerine.Cigarette is used
Essence is to specialize in each tobacco articles flavoring flavoring to use, and tobacco product is made to generate a kind of cigarette of good flue gas effect when burning and sucking
The additive of straw-made articles, thus it is particularly significant to the proportioning of flavouring essence for tobacco in electronics tobacco tar.Organic solvent can make non-tobacco
Extract and flavouring essence for tobacco spread more evenly across, and electronic cigarette tobacco tar is made more easily to burn.
Referring to Fig. 1, a kind of preparation method of electronic cigarette tobacco tar provided in an embodiment of the present invention, comprises the following steps：
Step 1：The non-tobacco plant material is prepared into target size by negated tobacco plant material, then by described in
40-80 mesh is ground to after non-tobacco plant material is toasted；
Step 2：The non-tobacco plant material after grinding is added in Extraction solvent impregnated successively, ultrasound carries
It takes and filters, obtain extracting solution, non-tobacco extract is obtained after the extracting solution is concentrated, the Extraction solvent includes carbon atom
Number is C2-C5Alcohols solvent, C3-C7Lipid solvent and C3-C7Ketone solvent in one or more and the mixed solutions of water；
Step 3：The non-tobacco extract and flavouring essence for tobacco and organic solvent are mixed and stirred for uniformly, obtaining electronic cigarette
Tobacco tar.
A kind of preparation method of electronic cigarette tobacco tar provided in an embodiment of the present invention, by by non-tobacco plant material through dry
Roasting, grinding, immersion, extraction, filtering and concentration, can obtain non-tobacco extract.Again by non-tobacco extract and flavouring essence for tobacco and
Organic solvent by simply mix can obtain fragrance enrich, comfortable taste, satisfaction it is good, and without any tobacco extract
Object not only meets the demand of user, but also will not jeopardize the electronic cigarette tobacco tar of the health of user.The preparation of the present invention
Method is simple, at low cost, is suitble to large-scale production, has very strong practicability.
In embodiment of the present invention, when non-tobacco plant material is in folium artemisiae argyi, eggplant leaf, tomato leaf, aloe and tealeaves
One or more when, after removing petiole, non-tobacco plant material is cut into the fragment of 1-5mm using cutting-out method；If not cigarette
Careless plant material is also containing fibert, almond, cocoa bean or carrot, it is necessary to smash into fibert, almond, cocoa bean or carrot to pieces 1-
The fragment of 5mm has been done spare.
It, can be by the one or more in folium artemisiae argyi, eggplant leaf, tomato leaf and tealeaves during grinding in embodiment of the present invention
Separate with the one or more in fibert, almond, cocoa bean, carrot and aloe and be ground successively, then each takes what he needs want contain
Amount mixes.
In embodiment of the present invention, the Extraction solvent includes the mixed solution of second alcohol and water, and the ethyl alcohol account for it is described
The percent by volume of mixed solution is 60%-95%.Preferably, the percent by volume that the ethyl alcohol accounts for the mixed solution is
60%-80%.
In embodiment of the present invention, the non-tobacco plant material is 1 with the Extraction solvent mass ratio:5-10.
It in embodiment of the present invention, is toasted using glad DHG-9140A types baking machine, in the baking process, is dried
Roasting temperature is 100-250 DEG C, and the time of baking is 0.5-3h.It is ground using winning into BLS-0.75E grinders, described
In process of lapping, the rotating speed of grinding is 1500-3000r/min, milling time 10-15min.
In embodiment of the present invention, the extraction operation is carried out using ultrasonic wave extraction concentration technology and the concentration is grasped
Make.Preferably, using space inkstone T-TN-C10 type ultrasonic wave extraction thickeners.In the extraction process, the temperature of extraction is 40-
70 DEG C, time of extraction is 20-40min, and in the concentration process, the temperature of concentration is 40-70 DEG C, and the time of concentration is
10-30min。
Multiple embodiments are classified into below the present invention is further detailed.
Embodiment 1
A kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
Step 1：The fragment that folium artemisiae argyi, eggplant leaf, tomato leaf, tealeaves and aloe remove petiole respectively and are cut into 1mm is put
200 DEG C of 1 hours of baking in dryer grind 10min with the rotating speed of 2000r/min with grinder respectively after cooling, and receive
It is spare in clean beaker for 40 mesh powders to collect grain size.Fibert, carrot, almond and cocoa bean are pounded 1mm's respectively again
Fragment is put in 200 DEG C of 2 hours of baking in dryer, is ground respectively with grinder with the rotating speed of 2000r/min after cooling
10min, and collection cut size is spare in clean beaker for 40-80 mesh powders.
Step 2：Weigh respectively Argy Wormwood Leaf 40g, eggplant leaf powder 25g, tomato leaf powder 25g, tea-leaf power 10g,
Fibert powder 30g, almond powder 20g, cocoa bean powder 30g, carrot powder 5g, the mixture of Alose 5g, then use
Extraction solvents of the 200ml containing 80% ethyl alcohol cleans No. 3 beakers, then inserts mixture in beaker, by solid-liquid ratio 1：10 ratio
Example adds in the Extraction solvent that 1900ml contains 80% ethyl alcohol, and stirs 2min using glass bar.After impregnating 2h, soak is moved into super
In sound wave extraction thickener, in extraction process, ultrasonic frequency is 20KHz, and the temperature of extraction is 60 DEG C, and the time of extraction is
30min.Through extracting solution is obtained by filtration after extraction, then extracting solution concentrated.In concentration process, the temperature of concentration is 60
DEG C, the time of concentration is 20min, obtains the non-tobacco extract of brown.
Step 3：Respectively by non-tobacco extract 38g, Ethyl vanillin 0.3g, ethylmaltol 0.25g, citronellol
0.2g, geraniol 0.2g, damascenone 0.3g, propylene glycol 22g, glycerine 140g are added in beaker, and 10min is stirred with glass bar
It can obtain electronic cigarette tobacco tar.
Embodiment 2
A kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
Step 1：The fragment that folium artemisiae argyi, eggplant leaf, tomato leaf, tealeaves and aloe remove petiole respectively and are cut into 5mm is put
100 DEG C of 3 hours of baking in dryer grind 10min with the rotating speed of 2000r/min with grinder respectively after cooling, and receive
It is spare in clean beaker for 80 mesh powders to collect grain size.Fibert, carrot, almond and cocoa bean are pounded 5mm's respectively again
Fragment is put in 100 DEG C of 3 hours of baking in dryer, is ground respectively with grinder with the rotating speed of 2000r/min after cooling
10min, and collection cut size is spare in clean beaker for 80 mesh powders.
Step 2：Argy Wormwood Leaf 40g, eggplant leaf powder 10g, tomato leaf powder 20g, tea-leaf power 5g, hazel are weighed respectively
Sub- powder 30g, almond powder 15g, cocoa bean powder 30g, carrot powder 5g, the mixture of Alose 5g, then use 200ml
Extraction solvent containing 60% ethyl alcohol cleans No. 3 beakers, then inserts mixture in beaker, by solid-liquid ratio 1：5 ratio adds in
800ml contains the Extraction solvent of 60% ethyl alcohol, and stirs 2min using glass bar.After impregnating 2h, soak immigration ultrasonic wave is carried
It takes in thickener, in extraction process, ultrasonic frequency is 15KHz, and the temperature of extraction is 40 DEG C, and the time of extraction is 40min.
Through extracting solution is obtained by filtration after extraction, then extracting solution concentrated.In concentration process, the temperature of concentration is 40 DEG C, concentration
Time for 30min, obtain the non-tobacco extract of brown.
Step 3：Respectively by non-tobacco extract 32g, Ethyl vanillin 0.3g, ethylmaltol 0.25g, citronellol
0.2g, geraniol 0.2g, damascenone 0.25g, propylene glycol 38g, glycerine 130g are added in beaker, are stirred with glass bar
10min can obtain electronic cigarette tobacco tar.
Embodiment 3
A kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
Step 1：The fragment that folium artemisiae argyi, eggplant leaf, tomato leaf, tealeaves and aloe remove petiole respectively and are cut into 5mm is put
250 DEG C of 0.5 hours of baking in dryer, cooling use grinder to grind 10min with the rotating speed of 3000r/min after distinguishing, and
Collection cut size is spare in clean beaker for 60 mesh powders.Fibert, carrot, almond and cocoa bean are pounded 5mm respectively again
Fragment be put in dryer 250 DEG C of 0.5 hours of baking, ground respectively with grinder with the rotating speed of 3000r/min after cooling
10min, and collection cut size is spare in clean beaker for 60 mesh powders.
Step 2：Argy Wormwood Leaf 20g, eggplant leaf powder 25g, tomato leaf powder 25g, tea-leaf power 5g, hazel are weighed respectively
Sub- powder 30g, almond powder 15g, cocoa bean powder 10g, carrot powder 5g, Alose 5g, then contain 60% second with 200ml
The Extraction solvent of alcohol cleans No. 3 beakers, then inserts mixture in beaker, by solid-liquid ratio 1：10 ratio adds in 1400ml and contains
The Extraction solvent of 60% ethyl alcohol, and 2min is stirred using glass bar.After impregnating 2h, soak is moved into ultrasonic wave extraction thickener
In, in extraction process, ultrasonic frequency is 15KHz, and the temperature of extraction is 40 DEG C, and the time of extraction is 40min.It is passed through after extraction
Extracting solution is obtained by filtration, then extracting solution is concentrated.In concentration process, the temperature of concentration is 40 DEG C, and the time of concentration is
30min obtains the non-tobacco extract of brown.
Step 3：Respectively by non-tobacco extract 28g, Ethyl vanillin 0.3g, ethylmaltol 0.25g, citronellol
0.2g, geraniol 0.2g, damascenone 0.35g, propylene glycol 42g, glycerine 120g are added in beaker, are stirred with glass bar
10min can obtain electronic cigarette tobacco tar.
Embodiment 4
A kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
Step 1：The fragment that folium artemisiae argyi, eggplant leaf, tomato leaf, tealeaves and aloe remove petiole respectively and are cut into 5mm is put
250 DEG C of 0.5 hours of baking in dryer, cooling use grinder to grind 10min with the rotating speed of 3000r/min after distinguishing, and
Collection cut size is spare in clean beaker for 60 mesh powders.Fibert, carrot, almond and cocoa bean are pounded 5mm respectively again
Fragment be put in dryer 250 DEG C of 0.5 hours of baking, ground respectively with grinder with the rotating speed of 3000r/min after cooling
10min, and collection cut size is spare in clean beaker for 60 mesh powders.
Step 2：Weigh respectively Argy Wormwood Leaf 10g, eggplant leaf powder 25g, tomato leaf powder 25g, tea-leaf power 10g,
Fibert powder 20g, almond powder 25g, cocoa bean powder 30g, carrot powder 5g, Alose 10g, then contain 60% with 200ml
The Extraction solvent of ethyl alcohol cleans No. 3 beakers, then inserts mixture in beaker, by solid-liquid ratio 1：8 ratio adds in 1280ml
Extraction solvent containing 60% ethyl alcohol, and 2min is stirred using glass bar.After impregnating 2h, soak is moved into ultrasonic wave extraction concentration
In machine, in extraction process, ultrasonic frequency is 15KHz, and the temperature of extraction is 40 DEG C, and the time of extraction is 40min.After extraction
It is filtered to obtain extracting solution, then extracting solution is concentrated.In concentration process, the temperature of concentration is 40 DEG C, the time of concentration
For 30min, the non-tobacco extract of brown is obtained.
Step 3：Respectively by non-tobacco extract 32g, Ethyl vanillin 0.35g, ethylmaltol 0.25g, citronellol
0.2g, geraniol 0.2g, damascenone 0.3g, propylene glycol 38g, glycerine 110g are added in beaker, and 10min is stirred with glass bar
It can obtain electronic cigarette tobacco tar.
Embodiment 5
A kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
Step 1：The fragment that folium artemisiae argyi, eggplant leaf, tomato leaf, tealeaves and aloe remove petiole respectively and are cut into 5mm is put
250 DEG C of 0.5 hours of baking in dryer, cooling use grinder to grind 10min with the rotating speed of 3000r/min after distinguishing, and
Collection cut size is spare in clean beaker for 60 mesh powders.Fibert, carrot, almond and cocoa bean are pounded 5mm respectively again
Fragment be put in dryer 250 DEG C of 0.5 hours of baking, ground respectively with grinder with the rotating speed of 3000r/min after cooling
10min, and collection cut size is spare in clean beaker for 60 mesh powders.
Step 2：Argy Wormwood Leaf 40g, eggplant leaf powder 25g, tomato leaf powder 25g, tea-leaf power 5g, hazel are weighed respectively
Sub- powder 30g, almond powder 10g, cocoa bean powder 10g, carrot powder 5g, Alose 5g, then contain 60% second with 200ml
The Extraction solvent of alcohol cleans No. 3 beakers, then inserts mixture in beaker, by solid-liquid ratio 1：10 ratio adds in 1550ml and contains
The Extraction solvent of 60% ethyl alcohol, and 2min is stirred using glass bar.After impregnating 2h, soak is moved into ultrasonic wave extraction thickener
In, in extraction process, ultrasonic frequency is 15KHz, and the temperature of extraction is 40 DEG C, and the time of extraction is 40min.It is passed through after extraction
Extracting solution is obtained by filtration, then extracting solution is concentrated.In concentration process, the temperature of concentration is 40 DEG C, and the time of concentration is
30min obtains the non-tobacco extract of brown.
Step 3：Respectively by non-tobacco extract 31g, Ethyl vanillin 0.25g, ethylmaltol 0.25g, citronellol
0.2g, geraniol 0.2g, damascenone 0.35g, propylene glycol 69g, glycerine 100g are added in beaker, are stirred with glass bar
10min can obtain electronic cigarette tobacco tar.
Effect example
Electronic cigarette tobacco tar in above-described embodiment is added in electronic cigarette device and carries out sensory effects evaluation respectively.
Sensory effects evaluation method comprises the following steps：
There is provided 5 evaluation indexes, including similarity, mouthfeel, feature style, lasting degree and smoke amount, and according to items
Evaluation index assigns different score values to the Different Effects degree of electronic cigarette tobacco tar aesthetic quality.
The similarity refers to：A tobacco tar with traditional tobacco taste such as permanent letter tobacco is taken to be used with examples detailed above tobacco tar
There is degree with what a electronic cigarette smoke panel test two kinds of different type tobacco tar of comparison；
The mouthfeel refers to：Flue gas strength, concentration and the note that electronic cigarette tobacco tar is generated through atomization on sense organ to producing
Raw comprehensive impression；
The feature style refers to：A kind of electronic cigarette tobacco tar is different from the sense of other homogeneous e cigarette tobacco tar in pleasant feeling
Official's Main Differences show；
The lasting degree refers to：Fragrance stays in the deep or light of oral cavity after discharge smog during smokeing panel test；
The smoke amount refers to：Discharge smog is more or few during smokeing panel test.
The member of smoking of 36 people is set, wherein 18 people are the smoker of 2-10, in addition 18 people are non-smoker, everyone a electronics
Cigarette tobacco tar sensory quality assessment table using the marking mode secretly commented, cycles method of smokeing panel test using whole, electronic cigarette tobacco tar is taken out
It inhales, according to the meaning of 5 sensory quality assessment index score values in table 1, using 50 points of points of point systems processed to electronic cigarette tobacco tar
Aesthetic quality carry out comprehensive grading, every evaluation index by ten system score.
1 electronic cigarette tobacco tar sensory quality assessment index of table and score value meaning table
Evaluation method：Evaluation index and score value in table 1, member of smoking should carry out aesthetic quality to each evaluation index
Evaluation, and its evaluation result is recorded, the minimum score unit of score value is 0.5.
As a result count：Remove one minimum point and a best result in the sensory quality assessment result of all members of smoking, count
The arithmetic mean of instantaneous value of remaining effective single item evaluation index scoring is calculated, retains a virtual value, last electronic cigarette after decimal point
The sensory quality assessment comprehensive grading of oil is the sum of arithmetic mean of instantaneous value for calculating each single index scoring, obtains total score, as a result protects
Two-decimal is stayed, above-described embodiment comparative evaluation the results are shown in Table 2 and table 3
2 smoker's electronic cigarette tobacco tar sensory effects evaluation result of table
| Evaluation index | Similarity | Mouthfeel | Feature style | Lasting | Smoke amount | Total score |
| Embodiment 1 | 8.1 | 8.5 | 8.9 | 7.8 | 9.3 | 42.6 |
| Embodiment 2 | 7.6 | 8.2 | 8.5 | 7.6 | 9.1 | 41.0 |
| Embodiment 3 | 7.1 | 7.0 | 7.5 | 7.0 | 8.7 | 37.3 |
| Embodiment 4 | 7.6 | 8.1 | 8.2 | 7.4 | 8.5 | 39.8 |
| Embodiment 5 | 7.5 | 8.1 | 8.4 | 7.6 | 8.5 | 40.1 |
3 non-smoker's electronic cigarette tobacco tar sensory effects evaluation result of table
Table 2 and table 3 the result shows that, the electronic cigarette tobacco tar provided by the invention prepared using non-tobacco plant material is in phase
Very high evaluation has been obtained like 5 kinds of degree, mouthfeel, feature style, lasting and smoke amount indexs.It especially presses by embodiment 1
Tobacco tar when matching the non-tobacco extract tobacco tar suction at allotment with tobacco extract allotment has certain similarity, and sends out
Smoke is sufficient, and fragrance enriches strong, and in good taste, unique flavor can most be met the needs of users.And as can be seen from Table 3
Non- smoker has good impression to this tobacco tar.It will be appreciated, however, that the adding proportion of used non-tobacco plant material
Used 5 indexs can be had a huge impact.
The content provided above embodiment of the present invention is described in detail, herein to the principle of the present invention and reality
The mode of applying is set forth and illustrates, described above to be only intended to help the method and its core concept for understanding the present invention；Meanwhile
For those of ordinary skill in the art, thought according to the invention has change in specific embodiments and applications
Become part, in conclusion this specification content should not be construed as limiting the invention.
Claims (10)
1. a kind of electronic cigarette tobacco tar, which is characterized in that including non-tobacco extract, flavouring essence for tobacco and organic solvent, the non-cigarette
Careless extract includes the extract of non-tobacco plant material, and the non-tobacco plant material includes folium artemisiae argyi, eggplant leaf, tomato leaf
And tealeaves.
2. electronic cigarette tobacco tar as described in claim 1, which is characterized in that count in parts by weight, the non-tobacco plant material
Including：1-10 parts of 10-40 parts of folium artemisiae argyi, 5-25 parts of eggplant leaf, 2-25 parts of tomato leaf and tealeaves.
3. electronic cigarette tobacco tar as claimed in claim 1 or 2, which is characterized in that the non-tobacco plant material further include fibert,
One or more in almond, cocoa bean, carrot and aloe；Wherein, count in parts by weight, 5-30 parts of fibert, almond 1-20
Part, 5-30 parts of cocoa bean, 1-10 parts of carrot, 1-10 parts of aloe.
4. electronic cigarette tobacco tar as described in claim 1, which is characterized in that by mass percentage, including non-tobacco extract
1%-20%, flavouring essence for tobacco 0.1%-2% and organic solvent 60%-98%.
5. electronic cigarette tobacco tar as claimed in claim 4, which is characterized in that the flavouring essence for tobacco includes Ethyl vanillin, ethyl
One or more in maltol, citronellol, geraniol and damascenone.
6. electronic cigarette tobacco tar as claimed in claim 4, which is characterized in that the organic solvent includes ethyl alcohol, propylene glycol and third
One or more in triol.
7. a kind of preparation method of electronic cigarette tobacco tar, which is characterized in that comprise the following steps：
The non-tobacco plant material is prepared into target size by negated tobacco plant material, then by the non-tobacco plant
40-80 mesh is ground to after raw material is toasted；
The non-tobacco plant material after grinding is added in Extraction solvent impregnated successively, ultrasonic extraction and filtering,
Extracting solution is obtained, non-tobacco extract is obtained after the extracting solution is concentrated, it is C that the Extraction solvent, which includes carbon number,2-C5
Alcohols solvent, C3-C7Lipid solvent and C3-C7Ketone solvent in one or more and the mixed solutions of water；
The non-tobacco extract and flavouring essence for tobacco and organic solvent are mixed and stirred for uniformly, obtaining electronic cigarette tobacco tar.
8. preparation method as claimed in claim 7, which is characterized in that the mixing that the Extraction solvent includes second alcohol and water is molten
Liquid, and the ethyl alcohol accounts for the percent by volume of the mixed solution as 60%-95%.
9. preparation method as claimed in claim 7, which is characterized in that in the baking process, the temperature of baking is 100-
250 DEG C, time of baking is 0.5-3h, and in the process of lapping, the rotating speed of grinding is 1500-3000r/min, milling time
For 10-15min.
10. preparation method as claimed in claim 7, which is characterized in that carried using described in the progress of ultrasonic wave extraction concentration technology
Extract operation and the concentration operation, in the extraction process, the temperature of extraction is 40-70 DEG C, and the time of extraction is 20-
40min, in the concentration process, the temperature of concentration is 40-70 DEG C, and the time of concentration is 10-30min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810056796.0A CN108041688B (en) | 2018-01-19 | 2018-01-19 | Electronic cigarette tobacco tar and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810056796.0A CN108041688B (en) | 2018-01-19 | 2018-01-19 | Electronic cigarette tobacco tar and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108041688A true CN108041688A (en) | 2018-05-18 |
| CN108041688B CN108041688B (en) | 2020-10-27 |
Family
ID=62127568
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810056796.0A Active CN108041688B (en) | 2018-01-19 | 2018-01-19 | Electronic cigarette tobacco tar and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108041688B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109549246A (en) * | 2019-01-18 | 2019-04-02 | 薪火高科(深圳)有限公司 | A kind of tobacco juice for electronic smoke and preparation method thereof of adjustable function of human body |
| CN112931920A (en) * | 2019-11-26 | 2021-06-11 | 广东省金叶科技开发有限公司 | Non-tobacco heating non-combustion sheet and preparation method thereof |
| CN113545509A (en) * | 2021-08-12 | 2021-10-26 | 深圳波顿香料有限公司 | Strengthening agent for electronic cigarette oil |
| CN113854620A (en) * | 2021-09-02 | 2021-12-31 | 深圳市艾普生物科技有限公司 | Electronic cigarette liquid additive and preparation method and application thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1360857A (en) * | 2002-01-08 | 2002-07-31 | 张秀莲 | Liquid cigarette preparing process based on burning and scenting technique |
| CN101731742A (en) * | 2008-11-10 | 2010-06-16 | 湖北中烟工业有限责任公司 | Method for catalyzing and adjusting Maillard reaction to produce tobacco flavor |
| CN106912982A (en) * | 2017-01-20 | 2017-07-04 | 深圳瀚星翔科技有限公司 | A kind of electronic cigarette tobacco tar and preparation method thereof |
-
2018
- 2018-01-19 CN CN201810056796.0A patent/CN108041688B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1360857A (en) * | 2002-01-08 | 2002-07-31 | 张秀莲 | Liquid cigarette preparing process based on burning and scenting technique |
| CN101731742A (en) * | 2008-11-10 | 2010-06-16 | 湖北中烟工业有限责任公司 | Method for catalyzing and adjusting Maillard reaction to produce tobacco flavor |
| CN106912982A (en) * | 2017-01-20 | 2017-07-04 | 深圳瀚星翔科技有限公司 | A kind of electronic cigarette tobacco tar and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109549246A (en) * | 2019-01-18 | 2019-04-02 | 薪火高科(深圳)有限公司 | A kind of tobacco juice for electronic smoke and preparation method thereof of adjustable function of human body |
| CN112931920A (en) * | 2019-11-26 | 2021-06-11 | 广东省金叶科技开发有限公司 | Non-tobacco heating non-combustion sheet and preparation method thereof |
| CN113545509A (en) * | 2021-08-12 | 2021-10-26 | 深圳波顿香料有限公司 | Strengthening agent for electronic cigarette oil |
| CN113854620A (en) * | 2021-09-02 | 2021-12-31 | 深圳市艾普生物科技有限公司 | Electronic cigarette liquid additive and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108041688B (en) | 2020-10-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104770863B (en) | Electronic cigarette liquid with herbal tea flavor and application thereof | |
| CN103989245B (en) | The Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke of the sweet soapy feeling in a kind of effective reduction oral cavity | |
| CN108041688A (en) | A kind of electronic cigarette tobacco tar and preparation method | |
| CN104489911A (en) | Tobacco juice of electronic cigarette | |
| CN103054180B (en) | Aromatized composite particle filter stick and production method thereof | |
| CN104544545A (en) | Electronic cigarette smoke solution with blood pressure decreasing function | |
| CN104489908A (en) | Tobacco juice of electronic cigarette | |
| CN104544555A (en) | Electronic cigarette smoke solution with blood sugar decreasing function | |
| CN103070473A (en) | Electronic cigarette tobacco juice prepared from faint scent tobacco leaves | |
| CN104544552A (en) | Electronic cigarette smoke solution prepared through oolong leaf extract | |
| CN104544549A (en) | Electronic cigarette smoke solution prepared through green tea leaf extract | |
| CN102090712B (en) | Method for preparing coarse extract of peanut shell total flavones and application thereof in cigarettes | |
| CN104082853B (en) | A kind of electronic cigarette liquid containing tomato extract and preparation method thereof | |
| CN110205200B (en) | Myrtle-flavored essence and myrtle-flavored electronic cigarette liquid and preparation method thereof | |
| CN103054186A (en) | Chinese medicinal composite particle filter stick and preparation method thereof | |
| CN104544554A (en) | Electronic cigarette smoke solution with blood fat decreasing function | |
| CN104544543A (en) | Electronic cigarette smoke solution prepared through black tea leaf extract | |
| CN104489913A (en) | E-cigarette nicotine liquid with functions of heat clearing and fire removing | |
| CN109852476A (en) | A kind of essence for the smoking article that do not burn suitable for low temperature, preparation method and application | |
| CN104544546A (en) | Electronic cigarette smoke solution with appetite improving and digestion prompting functions | |
| CN104489903A (en) | E-cigarette nicotine liquid with function of tranquilizing by nourishing the heart | |
| CN104544544A (en) | Electronic cigarette smoke solution prepared through white tea leaf extract | |
| CN111920079A (en) | Electronic atomization inhalant and preparation method thereof | |
| CN105077570A (en) | Tobacco extract pyrolysis product and application thereof in novel tobacco product | |
| CN103054187B (en) | Spice composite particle filter stick and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |