CN111920079A - Electronic atomization inhalant and preparation method thereof - Google Patents

Electronic atomization inhalant and preparation method thereof Download PDF

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Publication number
CN111920079A
CN111920079A CN202011047670.0A CN202011047670A CN111920079A CN 111920079 A CN111920079 A CN 111920079A CN 202011047670 A CN202011047670 A CN 202011047670A CN 111920079 A CN111920079 A CN 111920079A
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China
Prior art keywords
essential oil
parts
solvent
acid ester
fatty acid
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Pending
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CN202011047670.0A
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Chinese (zh)
Inventor
陆春明
欧振洲
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Jiugencao Biotechnology Guangzhou Co ltd
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Jiugencao Biotechnology Guangzhou Co ltd
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Priority to CN202011047670.0A priority Critical patent/CN111920079A/en
Publication of CN111920079A publication Critical patent/CN111920079A/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances

Abstract

The invention discloses an electronic atomization inhalant and a preparation method thereof, which are characterized by comprising, by volume, 10-30 parts of plant essential oil and 70-90 parts of solvent, wherein the plant essential oil is selected from one or more of peppermint, frankincense, dried orange peel, lemon, tea tree, clove, folium artemisiae argyi, rose and lavender essential oil, and the solvent is glycerol, water and emulsifier. According to the invention, the food-grade emulsifier is added into the solvent, so that the problem of mutual solubility of the plant essential oil and the glycerin aqueous solution is solved, the glycerin concentration is reduced under the condition of not reducing the smoke quantity, and the feeling of sweetness and dryness after smoking is reduced. According to the invention, the plant essential oil proportion is prepared to obtain good aroma experience and smoking experience, discomfort caused by smoking is relieved, and the plant essential oil can be used as a substitute of tobacco or electronic cigarette.

Description

Electronic atomization inhalant and preparation method thereof
Technical Field
The invention relates to the field of electronic cigarette oil, in particular to an electronic atomizing agent containing plant essential oil and a preparation method thereof.
Background
The electronic cigarette is a substitute of traditional tobacco, and the principle of the electronic cigarette is that under the action of an electronic atomizer, tobacco tar is atomized to generate smoke similar to the traditional tobacco for a consumer to suck. The components of the electronic cigarette oil comprise glycerin, propylene glycol, nicotine, essence and other additives. With the increasing concern of consumers on the health risks of the electronic cigarettes, new electronic cigarette oil formulations are also continuously developed and updated. For example, patent publication No. CN106617276A discloses an electronic cigarette oil added with Chinese herbal medicine components, which is prepared by mixing Chinese herbal medicines, adding a solvent, pulverizing to obtain base cigarette oil, and adding essence to obtain Chinese herbal medicine electronic cigarette oil; the application publication No. CN106018113A discloses an electronic cigarette tobacco tar with a gum health care effect, which has certain health care effects of gum care, antibiosis, antiphlogosis and halitosis elimination by adding a traditional Chinese medicine extracting solution into a base solution.
The electronic cigarette oil adopts water-soluble glycerin/propylene glycol as a solvent, and essence is added for blending, so that the long-term smoking experience is poor. The plant essential oil is a fat-soluble aromatic substance which is specially extracted from plants and has certain pleasure and health care effects, but the plant essential oil is not dissolved in a glycerin/propylene glycol solvent system and is rarely used for blending the fragrance of the electronic cigarette oil at present.
Disclosure of Invention
The invention aims to provide an electronic atomizing agent for blending fragrance by using plant essential oil, which is characterized in that a food-grade emulsifier is added to enable the plant essential oil and a glycerol aqueous solution to be mutually dissolved, so that the smoking experience of tobacco tar is improved, and meanwhile, the plant essential oil contained in the electronic atomizing agent also has certain health-care and pleasant beneficial effects.
The technical purpose of the invention is realized by the following technical scheme: an electronic atomization inhalant is characterized by comprising 10-30 parts by volume of a vegetable essential oil mixture and 70-90 parts by volume of a solvent; wherein the plant essential oil mixture comprises one or more of peppermint, frankincense, dried orange peel, lemon, tea tree, clove, folium artemisiae argyi, rose and lavender essential oil, the solvent components comprise 60-100 parts of glycerol and 0-40 parts of water by volume, and 1-3% (w/v) of emulsifier is added.
Preferably, the plant essential oil mixture comprises the following components in parts by volume: 3-7 parts of mint essential oil, 1-2 parts of frankincense essential oil, 2-3 parts of dried orange peel essential oil, 2-5 parts of lemon essential oil, 1-2 parts of tea tree essential oil, 0.5-1 part of clove essential oil, 1-1.5 parts of folium artemisiae argyi essential oil and 1-4 parts of rose essential oil.
Preferably, the plant essential oil mixture comprises the following components in parts by volume: 4-7 parts of mint essential oil, 1-2 parts of frankincense essential oil, 2-3 parts of dried orange peel essential oil, 5-10 parts of lemon essential oil, 3-5 parts of tea tree essential oil and 2-3 parts of lavender essential oil.
Preferably, the plant essential oil mixture comprises the following components in parts by volume: 5-9 parts of mint essential oil, 1-2 parts of tea tree essential oil, 3-7 parts of rose essential oil and 1-2 parts of lavender essential oil.
Preferably, the solvent emulsifier is one or more of sucrose fatty acid ester, polyglycerol fatty acid ester, soybean lecithin, diacetyl tartaric acid ester, caprylic capric acid glyceride, sorbitan fatty acid ester and polyoxyethylene sorbitan fatty acid ester.
Preferably, the solvent emulsifier comprises, by mass, 0-1 part of sucrose fatty acid ester, 0-1 part of polyglycerol fatty acid ester, 0-1 part of soybean lecithin, 0-1 part of diacetyl tartaric acid ester, 0-1 part of caprylic/capric acid glyceride, 0-1 part of sorbitan fatty acid ester and 0-1 part of polyoxyethylene sorbitan fatty acid ester.
Another object of the present invention is to provide a method for preparing an electronic aerosol inhalation, which is achieved by the following technical solutions: a method for preparing an electronic aerosol inhalant, comprising the steps of:
(1) weighing each component of the plant essential oil according to the component proportion, uniformly mixing, and standing for 24-96 hours to obtain a plant essential oil mixture;
(2) weighing and weighing each component of the solvent according to the component proportion, stirring and fully dissolving the components, and standing for 24 hours to obtain the solvent;
(3) weighing the plant essential oil mixture and the solvent according to the component proportion, and stirring to fully and uniformly mix the plant essential oil mixture and the solvent.
Compared with the prior art, the invention has the beneficial effects that:
(1) the product contains no tobacco extract or nicotine (salt), has no addiction, and can be used as substitute for conventional tobacco and electronic cigarette;
(2) the plant essential oil is used for replacing essence, so that the smoking experience is improved, the phenomena of dry mouth and throat discomfort are reduced, and the selected plant essential oil has the effects of making people pleasant and being beneficial to health.
Detailed Description
Example 1: weighing 3 ml of mint essential oil, 1 ml of frankincense essential oil, 1 ml of dried orange peel essential oil, 2 ml of lemon essential oil, 1 ml of tea tree essential oil, 0.5 ml of clove essential oil, 0.5 ml of folium artemisiae argyi essential oil and 1 ml of rose essential oil, uniformly mixing, and standing for 24 hours to obtain a plant essential oil mixture; weighing 60 ml of glycerol and 40 ml of water, uniformly mixing, adding 1 g of sucrose fatty acid ester and 1 g of polyglycerol fatty acid ester, and fully mixing and dissolving to obtain a solvent; weighing 10 ml of plant essential oil mixture, adding 90 ml of solvent, and uniformly stirring until the liquid is not layered to obtain the electronic atomization inhalant.
Example 2: weighing 7 ml of mint essential oil, 2 ml of frankincense essential oil, 3 ml of dried orange peel essential oil, 5 ml of lemon essential oil, 2 ml of tea tree essential oil, 1 ml of clove essential oil, 1 ml of argy wormwood leaf essential oil and 4 ml of rose essential oil, uniformly mixing, and standing for 96 hours to obtain a plant essential oil mixture; weighing 100 ml of glycerol, adding 1 g of soybean lecithin, and fully mixing and dissolving to obtain a solvent; weighing 25 ml of plant essential oil mixture, adding 75 ml of solvent, and uniformly stirring until the liquid is not layered to obtain the electronic atomization inhalant.
Example 3: weighing 7 ml of mint essential oil, 2 ml of frankincense essential oil, 3 ml of dried orange peel essential oil, 10 ml of lemon essential oil, 5 ml of tea tree essential oil and 3 ml of lavender essential oil, uniformly mixing, and standing for 48 hours to obtain a plant essential oil mixture; weighing 70 ml of glycerol and 30 ml of water, uniformly mixing, adding 0.5 g of sorbitan fatty acid ester and 0.5 g of diacetyl tartaric acid glyceride, and fully mixing and dissolving to obtain a solvent; weighing 30 ml of the plant essential oil mixture, adding 70 ml of the solvent, and uniformly stirring until the liquid is not layered to obtain the electronic atomization inhalant.
Example 4: weighing 4 ml of mint essential oil, 1 ml of frankincense essential oil, 2 ml of dried orange peel essential oil, 5 ml of lemon essential oil, 3 ml of tea tree essential oil and 2 ml of lavender essential oil, uniformly mixing, and standing for 72 hours to obtain a plant essential oil mixture; weighing 80 ml of glycerol and 20 ml of water, uniformly mixing, adding 1 g of sucrose fatty acid ester and 1 g of soybean lecithin, and fully and uniformly mixing and dissolving to obtain a solvent; weighing 17 ml of plant essential oil mixture, adding 83 ml of solvent, and uniformly stirring until the liquid is not layered to obtain the electronic atomization inhalant.
Example 5: weighing 5 ml of mint essential oil, 1 ml of tea tree essential oil, 3 ml of rose essential oil and 1 ml of lavender essential oil, uniformly mixing, and standing for 24 hours to obtain a plant essential oil mixture; weighing 90 ml of glycerol and 10 ml of water, uniformly mixing, adding 1 g of sucrose fatty acid ester and 1 g of caprylic/capric glyceride, and fully and uniformly mixing and dissolving to obtain a solvent; weighing 10 ml of plant essential oil mixture, adding 90 ml of solvent, and uniformly stirring until the liquid is not layered to obtain the electronic atomization inhalant.
Example 6: weighing 9 ml of mint essential oil, 2 ml of tea tree essential oil, 7 ml of rose essential oil and 2 ml of lavender essential oil, uniformly mixing, and standing for 96 hours to obtain a plant essential oil mixture; weighing 90 ml of glycerol and 10 ml of water, uniformly mixing, adding 1 g of polyoxyethylene sorbitan fatty acid ester, and fully mixing and dissolving to obtain a solvent; weighing 20 ml of the plant essential oil mixture, adding 80 ml of the solvent, and uniformly stirring until the liquid is not layered to obtain the electronic atomization inhalant.
Comparative example 1: an electronic atomizing inhalant is prepared according to the mixture ratio of the components in the example 1, but corresponding essence sold in the market is used for replacing plant essential oil, and the addition ratio suggested by the essence is specifically as follows: measuring 100 ml of glycerol, adding 1 g of sucrose fatty acid ester and 1 g of polyglycerol fatty acid ester, fully and uniformly mixing and dissolving to obtain a solvent, measuring 0.5 ml of mint essence, 0.1 ml of frankincense essence, 0.1 ml of dried orange peel essence, 0.2 ml of lemon essence, 0.1 ml of clove essence, 0.1 ml of wormwood essence and 0.2 ml of rose essence, adding 100 ml of solvent, and uniformly stirring to obtain the comparative electronic atomization inhalant.
Comparative example 2: an electronic atomizing inhalant is prepared according to the mixture ratio of the components in the example 3, but corresponding essence sold in the market is used for replacing plant essential oil, and the addition ratio suggested by the essence is specifically as follows: measuring 100 ml of glycerol, adding 0.5 g of sorbitan fatty acid ester and 0.5 g of diacetyl tartaric acid glyceride, fully and uniformly mixing and dissolving to obtain a solvent, measuring 0.5 ml of mint essence, 0.1 ml of frankincense essence, 0.1 ml of dried orange peel essence, 0.2 ml of lemon essence and 0.1 ml of lavender essence, adding 100 ml of the solvent, and uniformly stirring to obtain the comparative electronic atomization inhalant.
Comparative example 3: electronic aerosol inhalant is prepared according to the mixture ratio of the components in the example 5, but corresponding essence sold in the market is used for replacing plant essential oil, and the addition ratio suggested by the essence is used, specifically: measuring 90 ml of glycerol and 10 ml of water, adding 1 g of sucrose fatty acid ester and 1 g of caprylic/capric glyceride, and fully mixing and dissolving to obtain a solvent; measuring 0.5 ml of mint essence, 0.1 ml of rose essence and 0.1 ml of lavender essence, adding 100 ml of solvent, stirring and mixing uniformly to obtain the comparative electronic atomization inhalant.
The electronic cigarette liquids in the above examples and comparative examples were added to electronic cigarette devices for sensory evaluation, respectively.
The sensory effect evaluation method comprises the following steps:
(1) setting 6 evaluation indexes including irritation, satisfaction, dryness, characteristic style, aroma quality and aroma quantity, and endowing different scores according to different influence degrees of the evaluation indexes on the sensory quality of the electronic cigarette liquid;
the irritation is that: the smoke generated by atomizing the inhaled electronic cigarette liquid generates uncomfortable feelings on sense organs including oral cavity, throat and nasal cavity;
the satisfaction refers to: the smoke strength, concentration and aroma of the electronic cigarette liquid generated by atomization are comprehensively felt on sense organs;
the dry sensation is: the smoke generated by atomizing the electronic cigarette smoke liquid passes through the suction inlet cavity and influences the dryness degree of the mouth cavity after being exhaled;
the characteristic style is as follows: the electronic cigarette liquid is different from other electronic cigarette liquids of the same type in sense of pleasure;
the aroma substances are as follows: the quality degree of pleasant breath is sensed through smell and taste in the smoking process;
the amount of fragrance is as follows: the amount of pleasant breath was measured by oral and nasal cavities during the smoke panel.
(2) 15 smoke evaluators are arranged, each electronic cigarette smoke liquid sensory quality evaluation table adopts a dark evaluation scoring mode and an integral circulation smoking method to smoke the electronic cigarette smoke liquid, each item is divided into 9 points and 54 points according to the meaning of 6 sensory quality evaluation index scoring values in the table 1, each item is divided into scoring units by 1, and the meaning of each scoring value is described in the table 1.
TABLE 1 meaning table of evaluation value of sensory quality evaluation index of electronic cigarette liquid
Score value Irritation property Satisfaction feeling Feeling of dryness Characteristic style Quality of fragrance Amount of fragrance
9 Is free of Is very good Is very light Is very pleasant Is very good Is quite sufficient
8 Look like to have Good taste Light and lightweight Pleasure of Good taste Sufficient (sufficient)
7 Is a little bit Is preferably used Is lighter Is relatively pleasant Is preferably used Is more sufficient
6 Is slightly provided with Is a bit better Good and light Is slightly pleasant Is a bit better Slightly sufficient
5 Is provided with In general In In general In general In general
4 Is slightly larger than Is slightly poor Is a little heavier Is slightly unpleasant Is slightly poor Is slightly provided with
3 Is larger Is poor Heavy weight Is relatively unpleasant Is poor Is a little bit
2 Big (a) Difference (D) Heavy load Is not pleased Difference (D) Look like to have
1 Is very big Is very poor Is very heavy Very unpleasant Is very poor Is free of
(3) And (4) counting results: and (4) enabling the smoking evaluation results of all the suckers to be effective, calculating the arithmetic mean of the single smoking evaluation results of all the suckers, reserving the results to a decimal number, adding the arithmetic mean of all the single items to obtain a total score, and reserving the results to a decimal number.
The electronic cigarette liquid prepared in examples 1 to 6 and the electronic cigarette liquid prepared in comparative examples 1 to 3 were added to an electronic cigarette for sensory quality evaluation. The specific evaluation results are shown in table 2, and the scores of the evaluation indexes in table 2 are the arithmetic average scores of the effective scores of 15 smokers.
Table 2 evaluation results of sensory effect of tobacco juice of electronic cigarette
Evaluation index Irritation property Satisfaction feeling Feeling of dryness Characteristic style Quality of fragrance Amount of fragrance General review
Example 1 8.9 7.9 8.3 7.5 8.2 7.2 48
Example 2 8.6 8.3 6.2 8.3 8.2 8.4 48
Example 3 8.7 8.5 7.7 7.5 8.4 8.4 49.2
Example 4 8.7 8.5 7.2 7.2 8.3 8.1 48
Example 5 8.8 8.1 6.5 8.1 7.9 7.3 46.7
Example 6 8.6 7.9 6.3 7.6 7.5 8.2 46.1
Comparative example 1 7.5 7.2 4.7 6.7 4.3 7.9 38.3
Comparative example 2 7.3 7.1 4.7 6.5 4.2 7.9 37.7
Comparative example 3 7.2 7.2 4.6 6.5 4.4 7.7 37.6
As can be seen from table 2, the tobacco tar of the present invention has a higher total score and the greatest advantage of better aroma quality compared to the three comparative examples, because the aroma of the plant essential oil is richer and more mellow than that of the essence, the experience is better, and secondly the dryness and irritation are lighter, the characteristic profile is better and the satisfaction of the smokers is stronger.
The foregoing is directed to preferred embodiments of the present invention, other and further embodiments of the invention may be devised without departing from the basic scope thereof, and the scope thereof is determined by the claims that follow. However, any simple modification, equivalent change and modification of the above embodiments according to the technical essence of the present invention are within the protection scope of the technical solution of the present invention.

Claims (9)

1. The electronic atomizing inhalant is characterized by comprising 10-30 parts by volume of a vegetable essential oil mixture and 70-90 parts by volume of a solvent.
2. The electronic aerosol inhalant as claimed in claim 1, wherein the plant essential oil mixture comprises one or more of essential oils selected from peppermint, mastic, dried orange peel, lemon, tea tree, clove, mugwort, rose, and lavender.
3. The electronic aerosol inhalant as claimed in claim 1, wherein the plant essential oil mixture comprises the following components in parts by volume: 3-7 parts of mint essential oil, 1-2 parts of frankincense essential oil, 1-3 parts of dried orange peel essential oil, 2-5 parts of lemon essential oil, 1-2 parts of tea tree essential oil, 0.5-1 part of clove essential oil, 0.5-1 part of folium artemisiae argyi essential oil and 1-4 parts of rose essential oil.
4. The electronic aerosol inhalant as claimed in claim 1, wherein the plant essential oil mixture comprises the following components in parts by volume: 4-7 parts of mint essential oil, 1-2 parts of frankincense essential oil, 2-3 parts of dried orange peel essential oil, 5-10 parts of lemon essential oil, 3-5 parts of tea tree essential oil and 2-3 parts of lavender essential oil.
5. The electronic aerosol inhalant as claimed in claim 1, wherein the plant essential oil mixture comprises the following components in parts by volume: 5-9 parts of mint essential oil, 1-2 parts of tea tree essential oil, 3-7 parts of rose essential oil and 1-2 parts of lavender essential oil.
6. The electronic atomizing inhalant as claimed in claim 1, wherein the solvent component comprises 60-100 parts by volume of vegetable-derived glycerin, 0-40 parts by volume of water, and 1-3% (w/v) of emulsifier.
7. An electronic aerosol inhalation according to claim 1, wherein the solvent emulsifier is one or more selected from sucrose fatty acid ester, polyglycerol fatty acid ester, soybean lecithin, diacetyl tartaric acid ester, caprylic/capric acid glyceride, sorbitan fatty acid ester, and polyoxyethylene sorbitan fatty acid ester.
8. The electronic atomizing inhalant as claimed in claim 1, wherein the solvent emulsifier comprises, by mass, 0-1 part of sucrose fatty acid ester, 0-1 part of polyglycerol fatty acid ester, 0-1 part of soybean lecithin, 0-1 part of diacetyl tartaric acid ester, 0-1 part of caprylic/capric acid ester, 0-1 part of sorbitan fatty acid ester, and 0-1 part of polyoxyethylene sorbitan fatty acid ester.
9. A method of preparing an electronically atomised inhaler according to any of claims 1 to 8, comprising the steps of:
(1) weighing each component of the plant essential oil according to the component proportion, uniformly mixing, and standing for 24-96 hours to obtain a plant essential oil mixture;
(2) weighing each component of the solvent according to the component proportion, stirring and fully dissolving the components, and standing for 24 hours to obtain the solvent;
(3) weighing the plant essential oil mixture and the solvent according to the component proportion, and stirring to fully and uniformly mix the plant essential oil mixture and the solvent.
CN202011047670.0A 2020-09-29 2020-09-29 Electronic atomization inhalant and preparation method thereof Pending CN111920079A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114085711A (en) * 2021-11-22 2022-02-25 深圳市真味生物科技有限公司 Plant essence for electronic atomized liquid and preparation method thereof
CN114304715A (en) * 2022-01-25 2022-04-12 湖南云荟生物科技有限公司 Chinese olive betel nut atomized liquid for sucking betel nut products and preparation method thereof
CN115141680A (en) * 2022-07-04 2022-10-04 深圳梵活生命科学股份有限公司 Grapefruit essence composition special for electronic atomized liquid and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114085711A (en) * 2021-11-22 2022-02-25 深圳市真味生物科技有限公司 Plant essence for electronic atomized liquid and preparation method thereof
CN114085711B (en) * 2021-11-22 2024-03-29 深圳市真味生物科技有限公司 Plant essence for electronic atomized liquid and preparation method thereof
CN114304715A (en) * 2022-01-25 2022-04-12 湖南云荟生物科技有限公司 Chinese olive betel nut atomized liquid for sucking betel nut products and preparation method thereof
CN115141680A (en) * 2022-07-04 2022-10-04 深圳梵活生命科学股份有限公司 Grapefruit essence composition special for electronic atomized liquid and preparation method thereof

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