CN112971199A - Electronic cigarette tobacco tar helpful for relieving fatigue - Google Patents
Electronic cigarette tobacco tar helpful for relieving fatigue Download PDFInfo
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- CN112971199A CN112971199A CN202110191685.2A CN202110191685A CN112971199A CN 112971199 A CN112971199 A CN 112971199A CN 202110191685 A CN202110191685 A CN 202110191685A CN 112971199 A CN112971199 A CN 112971199A
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- tobacco tar
- relieving fatigue
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
Abstract
The application discloses electronic cigarette tobacco tar helpful for relieving fatigue. The electronic cigarette tobacco tar for relieving fatigue comprises the following raw materials in parts by weight: 10-90 parts of propylene glycol, 10-90 parts of glycerol, 0.5-3 parts of vitamin B3, 0.5-3 parts of vitamin B15, 1-3.5 parts of taurine, 1-3.5 parts of tyrosine and 0.5-1.5 parts of synergist. The electronic cigarette tobacco tar beneficial to relieving fatigue has the advantages of sufficient smoking amount, good satisfaction, rich and rich fragrance, moderate strength and mild and comfortable mouthfeel, improves the human metabolic rate and the organism immunity, and is beneficial to removing free radicals or chelating metal ions by histidine and tyrosine, so that the effect of relieving fatigue is achieved; even effectively reduces the boiling point of the electronic cigarette tobacco tar blend evaporation, further reduces the generation and the emission of aldehyde substances in the smoke, greatly reduces the harm of the electronic cigarette to human bodies, has higher safety performance, and is healthier compared with the traditional tobacco tar.
Description
Technical Field
The application relates to the field of electronic cigarettes, in particular to electronic cigarette tobacco tar helpful for relieving fatigue.
Background
The electronic cigarette controls the smoke output quantity and the working state through a high-tech silicon chip and an airflow inductor, so that the tobacco tar is atomized, the solution of essence, glycerol and propylene glycol contained in the tobacco tar is atomized into particles, the particles are absorbed through the lung, the simulated smoke is discharged at the same time, the simulated smoke does not contain tar and other harmful ingredients in the cigarette, no second-hand smoke is generated, and the simulated smoke cannot be diffused or entwined in a closed space. Electronic cigarettes, as a form of new tobacco products, on the one hand provide consumption habits and satisfaction similar to traditional cigarettes, and on the other hand the hazard index of electronic cigarettes is greatly reduced compared to traditional cigarettes. Therefore, the electronic cigarette has a huge market prospect.
However, as the pace of life of people gets faster and faster, fatigue has become one of the important causes affecting human health, a series of physiochemical changes occur in the organism, including immunity reduction, memory disorder, low working efficiency and the like, and fatigue has become an important factor threatening human physical and mental health.
For the electronic cigarette presenting huge market prospect, the electronic cigarette beneficial to relieving fatigue is developed, and the electronic cigarette has great significance for improving the safety, the working efficiency and the body health function of a user.
Disclosure of Invention
In order to alleviate user's fatigue, the present application provides an electronic cigarette tobacco tar that helps alleviate fatigue.
First aspect, the application provides a help alleviating tired electron cigarette tobacco tar adopts following technical scheme:
the electronic cigarette tobacco tar for relieving fatigue comprises the following raw materials in parts by weight: 10-90 parts of propylene glycol, 10-90 parts of glycerol, 0.5-3 parts of vitamin B3, 0.5-3 parts of vitamin B15, 1-3.5 parts of taurine, 1-3.5 parts of tyrosine and 0.5-1.5 parts of synergist.
Preferably, the synergist is one or more of vitamin A and vitamin E.
Preferably, the electronic cigarette liquid also comprises trehalose for improving the stability of each raw material of the electronic cigarette liquid.
Preferably, the trehalose is used in an amount of 1 to 2.5 parts by weight.
Preferably, the e-liquid further comprises n-propyl benzoate for lowering the boiling point of the e-liquid blend.
Preferably, the n-propyl benzoate is used in an amount of 35 to 50 parts by weight.
Preferably, the mass ratio of the n-propyl benzoate to the glycerol is (40-50): (10-20).
Preferably, the mass ratio of the propylene glycol to the glycerol is (70-90): (10-20).
In a second aspect, the application provides a preparation method of electronic cigarette tobacco tar helpful for relieving fatigue, which adopts the following technical scheme:
a preparation method of electronic cigarette tobacco tar helpful for relieving fatigue comprises the following steps: the electronic cigarette tobacco tar can be obtained by uniformly mixing the raw materials according to the parts by weight, wherein the mixing temperature is 20-60 ℃.
In summary, the present application has the following beneficial effects:
1. according to the application, the vitamin B3, the vitamin B15, the synergist, the taurine and the tyrosine are added into the glycerol and the propylene glycol, so that the prepared electronic cigarette tobacco tar is sufficient in smoking amount, good in satisfaction, rich and rich in fragrance, moderate in strength, mild and comfortable in taste, and capable of improving the human body metabolic rate and the organism immunity, and is beneficial to the removal of free radicals or chelated metal ions by histidine and tyrosine, so that the effect of relieving fatigue is achieved;
2. in the application, preferably, after the vitamin B3, the vitamin B15, the synergist, the taurine and the tyrosine are added into the glycerol and the propylene glycol, the trehalose is further added, the trehalose forms a unique protective film on the surface of each raw material, and the ultraviolet absorption capacity of the tyrosine is combined to effectively protect each raw material from being inactivated without degeneration, so that each raw material can stably and jointly play a role in resisting fatigue,
3. in the application, n-propyl benzoate is preferably additionally added into glycerol and propylene glycol, so that the evaporation boiling point of the electronic cigarette tobacco tar blend is effectively reduced, the generation and emission of aldehyde substances in smoke are reduced, the harm of the electronic cigarette to human bodies is greatly reduced, and the electronic cigarette has higher safety performance and is healthier compared with the traditional tobacco tar; the reduction of the boiling point of the electronic cigarette tobacco tar blend evaporation can also reduce the possibility that the tobacco cotton is burnt by the heating wire in the atomizer, which affects the taste of the electronic cigarette tobacco tar.
Detailed Description
Examples
Example 1
The electronic cigarette tobacco tar for relieving fatigue is prepared from the following raw materials in parts by weight: 90 parts of propylene glycol, 10 parts of glycerol, 2 parts of vitamin B3, 1.5 parts of vitamin B15, 2.5 parts of taurine and 2 parts of tyrosine.
The preparation process of the electronic cigarette tobacco tar of the embodiment is as follows: respectively adding the raw materials into a clean reaction kettle, and stirring to obtain the electronic cigarette tobacco tar, wherein the stirring temperature is 20-60 ℃.
Examples 2 to 3
Examples 2-3 differ from example 1 in the amount of starting material used, see table 1 for details.
Example 4
Example 4 differs from example 1 in that the e-cigarette liquid also includes 1.5 parts of a synergist (by weight); wherein the synergist is vitamin E.
Example 5
Example 5 differs from example 1 in that the e-cigarette liquid also includes 1 part of a synergist (by weight); wherein the synergist is vitamin A.
Example 6
Example 6 differs from example 1 in that the e-liquid further comprises 0.5 parts of a synergist (by weight); wherein the synergist is vitamin A and vitamin E.
Example 7
Example 7 differs from example 1 in that the e-cigarette liquid also includes 1.5 parts trehalose (by weight parts).
Examples 8 to 9
Examples 8-9 differ from example 7 in the amount of trehalose used, see in particular tables 1 and 2.
Example 10
Example 10 differs from example 1 in that the e-cigarette liquid also includes 50 parts n-propyl benzoate (parts by weight).
Examples 11 to 12
Examples 11-12 differ from example 10 in the amount of n-propyl benzoate used, see in particular table 2.
Example 13
The electronic cigarette tobacco tar for relieving fatigue is prepared from the following raw materials in parts by weight: 90 parts of propylene glycol, 10 parts of glycerol, 2 parts of vitamin B3, 1.5 parts of vitamin B15, 2.5 parts of taurine, 2 parts of tyrosine, 1.5 parts of a synergist, 1.5 parts of trehalose, 2.5 parts of mannitol and 50 parts of n-propyl benzoate; wherein the synergist is vitamin E.
Comparative example
Comparative example 1
Comparative example 1 and example 10 differ in that n-propyl benzoate was used in an amount of 70 parts, which was greater than that of examples 10-13, such that the mass ratio of n-propyl benzoate to glycerol was 7: 1.
Comparative example 2
The electronic cigarette tobacco tar for relieving fatigue is prepared from the following raw materials in parts by weight: 90 parts of propylene glycol and 10 parts of glycerol.
TABLE 1 amounts of raw materials used in examples 1-8
TABLE 2 amounts of raw materials used in examples 9 to 13 and comparative examples 1 to 2
Test method
First, evaluation of sensory Effect
1. Design of experiments
The electronic cigarette plumes in examples 1 to 13 and comparative examples 1 to 2 were added to the electronic cigarette device and sensory evaluation was performed, respectively (wherein the electronic cigarette plumes in examples 7 to 9 were electronic cigarette plumes after being left at room temperature for one year).
The sensory effect evaluation method comprises the following steps: setting 5 evaluation indexes including irritation, satisfaction, characteristic style, Chinese herbal medicine fragrance, aroma and smoke quantity, and endowing different scores according to different influence degrees of each evaluation index on the sensory quality of the electronic cigarette tobacco.
The irritation means: the smoke generated by atomizing the smoke oil inhaled into the electronic cigarette can generate uncomfortable feeling on sense organs including oral cavity, throat and nasal cavity;
the satisfaction refers to: the smoke strength, concentration and aroma generated by atomizing the electronic cigarette tobacco tar are comprehensively felt in the oral cavity and the nasal cavity of a sensory organ;
the characteristic style is as follows: the electronic cigarette tobacco tar is different from other similar electronic cigarette tobacco tar in sense of pleasure;
the aroma means: the quality degree of pleasant breath is sensed through smell and taste in the smoking process;
the smoke amount is: the electronic cigarette tobacco tar generates the amount of smoke through atomization.
The sensory quality evaluation indexes and the evaluation value meaning tables of the electronic cigarette tobacco tar are shown in table 3.
TABLE 3 sensory quality evaluation index and evaluation value of electronic cigarette tobacco tar
2. Evaluation method
15 smoke evaluators were set, each person used an electronic cigarette tobacco sensory quality evaluation table, smoking the electronic cigarette tobacco tar prepared in examples 1-13 and comparative examples 1-2 by a dark evaluation scoring method and an overall circular smoking method, and comprehensive evaluation was performed on the sensory quality of the electronic cigarette tobacco tar by a percentage scoring method according to the meaning of the five sensory quality evaluation index scoring values in table 3, and each evaluation index was scored by twenty points.
According to the evaluation indexes and the score values in table 3, the suckers should perform sensory quality evaluation on each evaluation index and record the evaluation results, and the minimum score unit of the score value is 0.5.
3. Statistics of results
The lowest score and the highest score are removed from the sensory quality evaluation results of all smokers, the arithmetic mean of the scores of the remaining effective single evaluation indexes is calculated, finally, the sensory quality evaluation comprehensive score of the electronic cigarette tobacco tar is the sum of the arithmetic mean of the scores of the single indexes, the total score is obtained, and the comparative evaluation results of the electronic cigarette tobacco tar prepared in the examples 1-13 and the comparative examples 1-2 are shown in the table 4.
TABLE 4 comparative evaluation results of E-cigarette tobacco tar obtained in examples 1 to 13 and comparative examples 1 to 2
As can be seen from table 4, the electronic cigarette oils prepared in examples 1 to 3 are characterized by sufficient smoking amount, good satisfaction, rich and rich aroma, moderate strength, and mild and comfortable taste. In examples 4 to 6, a synergist is added, the synergist is one or more of vitamin a and vitamin E, and the synergist plays a role in enhancing the effects of vitamin B3 and vitamin B15, so that vitamin B3 and vitamin B15 can play a better anti-fatigue effect, and the smoking sensory experience of the electronic cigarette liquid is not affected.
In examples 7 to 9, trehalose is added to form a unique protective film on the surface of each raw material, so that each raw material is effectively protected from inactivation without denaturation, and thus each raw material stably and jointly exerts an anti-fatigue effect, and even sweet and greasy taste of propylene glycol in smoke generated after atomization is improved, thereby improving the richness of the fragrance of the electronic cigarette smoke.
N-propyl benzoate is added in embodiments 10-12, and n-propyl benzoate has the fragrance of nut and fruit, can also improve the abundant degree of fragrance of electron cigarette tobacco tar, and the sweet greasy taste that propylene glycol can have in the smog that produces after atomizing is improved with trehalose combined action, forms good atomization effect, promotes the smoking experience of electron cigarette tobacco tar.
In example 13, compared with examples 1 to 3, the synergist, trehalose and n-propyl benzoate are mixed, so that the smoking experience of the electronic cigarette is not affected, and the sensory experiences of the electronic cigarette tobacco tar on irritation, satisfaction, characteristic style, aroma and smoke amount are comprehensively improved.
From comparative example 1, it can be seen that the content of n-propyl benzoate increases, presenting a tendency to decrease the smoking experience of e-cigarette liquid, so that it is not the better the content of n-propyl benzoate is.
Comparative example 2 as a control test, the smoking experience of e-cigarette liquid is greatly reduced with only propylene glycol and glycerin as the main components of the e-cigarette liquid.
Second, evaluation of harm reduction Effect
The contents of aldehydes (including formaldehyde, acetaldehyde and acrolein) in the smoke generated by the electronic cigarette smoke provided in examples 1, 4, 7, 10-13 and 1-2 were measured by YC/T254-2008 "high performance liquid chromatography for measuring main carbonyl compounds in mainstream smoke of cigarette", and the results are shown in table 5.
TABLE 5 content of aldehydes in smoke generated in E-cigarette smoke
From the results in table 5, it can be seen that the electronic cigarette liquid prepared by the present invention has no formaldehyde detected, and the acetaldehyde and acrolein contents are much lower than those of the electronic cigarette liquid prepared by the conventional propylene glycol and glycerin. The electronic cigarette tobacco tar provided by the invention can effectively reduce the generation of aldehyde substances, has higher safety performance and is healthier compared with the traditional tobacco tar.
Thirdly, aspiration questionnaire survey is carried out on the volunteers
1. Design of experiments
A total of 88 volunteers were observed between 20 and 50 years old who were fatiguing but did not meet the clinical or subclinical diagnosis of diseases associated with modern medicine, of which 56 men, 32 years old on average, 65kg on average, 32 women, 28 years old on average, 46kg on average; three consecutive puffs (one each day, in the morning, in the evening, 8 puffs or more, about 2 seconds per puff) of the electronic cigarette oils prepared by examples 1, 4-7, 10, 13 and 2 and added to the electronic cigarette device [ 11 volunteers (7 male volunteers and 4 female volunteers out of 11 volunteers) were each assigned for each example and comparative example for smoking observation ], and basic information and a relevant questionnaire for self-test of fatigue degree were filled in by the volunteers before and after the experiment, wherein the electronic cigarette oil in example 7 was one year after being left at room temperature. Specific results are shown in table 6.
2. Criteria for effect determination
Obviously effective: the vigor and the face color are all well changed, the working state is obviously improved, and the exercise capacity is obviously enhanced;
the method comprises the following steps: the energy is full, the complexion is improved, the working state is improved, and the exercise capacity is enhanced;
no obvious difference exists before and after use: the fatigue symptoms are not improved.
3. Results of the experiment
TABLE 6 summary of fatigue-relieving effects of volunteers after smoking E-cigarette tobacco tar
Fourthly, the blood lactic acid and SOD of the volunteers are measured
1. Design of experiments
A total of 18 volunteers (males) who smoked (smoked 8 or more puffs, about 2 seconds per puff) the e-liquid tobacco obtained from example 1, example 4, example 7, example 10, example 13 and comparative example 2 and added to the e-liquid device were observed, the 18 volunteers having an average age of 28 years and an average weight of 65 kg. 21 volunteers were randomly divided into 6 groups of 3 persons each. The 6 groups of volunteers were subjected to fitness training of the same subject for 30 minutes in the same time period, and the blood lactate and serum superoxide dismutase (SOD) contents were measured after training, respectively. After completion of training, 6 groups of volunteers were assigned to smoking e-cigarette smoke puffs prepared in example 1, example 4, example 7, example 10, example 13 and comparative example 2 and added to the e-cigarette device, and blood lactate and serum superoxide dismutase (SOD) levels were determined after smoking was completed, respectively. The specific experimental groupings and results are shown in table 7.
2. Measurement method
Measuring blood lactic acid with YSI 1500 SPORT LACTATE ANALYZER by enzyme electrode method; serum superoxide dismutase (SOD) is measured by xanthine oxidase method with 721 type spectrophotometer.
3. Results of the experiment
TABLE 7 comparison of blood lactic acid content and SOD content before and after aspiration of volunteers
It can be seen from tables 4-7 that the electronic cigarette tobacco tar prepared in examples 1-3 has the specific characteristics of sufficient smoking amount, good satisfaction, rich and rich fragrance, moderate strength, and mild and comfortable taste during smoking. For modern people with stress, frequent mental stress and restlessness, vitamin B3 has good effect on maintaining the health of nervous system and normal operation of brain function of vitamin B3; the vitamin B15 can improve oxygen metabolism rate of human tissue, bring oxygen to various parts of the whole body, improve nutrition of various organs, enhance functions of various organs of the human body, and improve some sub-health symptoms of modern people; taurine can regulate the metabolism of the organism and promote the enhancement of the immunity of the organism; the tyrosine is beneficial to removing free radicals or chelating metal ions by histidine and tyrosine, and the vitamin B3, the vitamin B15, the taurine and the tyrosine play a synergistic effect together, thereby playing a role in relieving fatigue.
Lactic acid is a product obtained by catabolism of endogenous substances in the body during exercise, and a large amount of acidic substances are accumulated, so that muscles and joints are sore and fatigued. The free radicals of the body are increased due to movement, and the excessive free radicals can lead to the inactivation of some important metabolic enzymes due to cross-linking polymerization, thereby causing a series of pathological changes, leading to the reduction of the working capacity of the human body and the generation of fatigue feeling.
In the examples 4-6, the synergist is added, the synergist is one or more of vitamin a and vitamin E, the synergist has an enhancing effect on the effects of vitamin B3 and vitamin B15, and is helpful for accelerating the removal rate of blood lactic acid in vivo, effectively promoting the increase of body SOD, enhancing the ability of the body to resist free radicals, improving the function of the body in resisting oxidation and defense, promoting fatigue recovery, and reducing the damage of peroxidation to the body, so that the vitamin B3 and the vitamin B15 can play a better anti-fatigue effect, and are beneficial for prolonging exercise endurance, improving exercise capacity, and simultaneously, the sensory experience of smoking electronic cigarette oil is not influenced.
In examples 7 to 9, trehalose is added, and can form a unique protective film on the surface of each raw material, so that each raw material is effectively protected from inactivation without denaturation, and thus each raw material can stably and jointly play a role in resisting fatigue, and the fragrance of trehalose even improves the sweet and greasy taste of propylene glycol in smoke generated after atomization, thereby improving the richness of the fragrance of electronic cigarette smoke; the absorption capacity of tyrosine to ultraviolet rays is combined, the decomposition of the ultraviolet rays to each raw material is reduced, the stability of the vitamin B3, the vitamin B15 and the synergist is further improved, and the raw materials stably and jointly play a role in resisting fatigue.
Glycerin and propylene glycol are used as common raw materials of electronic cigarette smoke oil, wherein the boiling point of the glycerin is as high as 291 ℃, the boiling point of the propylene glycol is 188.2 ℃, and the evaporability of the glycerin is far lower than that of the propylene glycol, so that the high temperature is required for evaporating the glycerin to form smoke, and the glycerin and the propylene glycol are easily evaporated on a high-temperature atomizer and are decomposed into harmful aldehyde substances such as formaldehyde, acetaldehyde and acrolein, which are harmful to human bodies.
In the embodiments 10 to 12, n-propyl benzoate is added, and the n-propyl benzoate can form an azeotropic system with glycerol, so that the boiling point of evaporation of the tobacco tar blend of the electronic cigarette can be effectively reduced, generation and emission of aldehyde substances in smoke are reduced, and harm of the electronic cigarette to a human body is greatly reduced; simultaneously, n-propyl benzoate has the fragrance of nut and fruit, can also improve the abundant degree of fragrance of electron cigarette tobacco tar, and improve the sweet greasy taste that propylene glycol can have in the smog that the atomizing back produced with the trehalose combined action, form good atomization effect, promote the suction of electron cigarette tobacco tar and experience.
In example 13, compared with examples 1 to 3, the synergist, trehalose and n-propyl benzoate are further mixed, so that the smoking experience of the electronic cigarette is not affected, the experiences of the electronic cigarette tobacco tar in various senses such as irritation, satisfaction, characteristic style, aroma and smoke quantity are comprehensively improved, the removal rate of blood lactic acid in a body is even further increased, and the increase of SOD in the body is further promoted, so that the anti-fatigue effect of the electronic cigarette tobacco tar is further enhanced.
The higher the content of n-propyl benzoate, the better the azeotropic system formed by n-propyl benzoate, and further lower the boiling point of evaporation of the E-liquid tobacco blend, thereby further reducing the generation and emission of aldehydes in the smoke, but as can be seen from comparative example 1, the content of n-propyl benzoate is increased, and although the generation and emission of aldehydes can be further reduced, the smoking experience of E-liquid tobacco shows a tendency to decrease, so the higher the content of n-propyl benzoate is, the better the content is.
Comparative example 2 is a control test, and in the case where only propylene glycol and glycerin are used as the main components of the electronic cigarette liquid, the smoking experience of the electronic cigarette liquid is greatly reduced, and meanwhile, the effect of relieving fatigue is also expressed to be poor, and the fatigue of the body cannot be well relieved.
In conclusion, the electronic cigarette tobacco tar provided by the invention not only improves the smoking experience of the electronic cigarette tobacco tar, but also can promote the recovery of fatigue.
The above embodiments are preferred embodiments of the present application, and the protection scope of the present application is not limited by the above embodiments, so: all equivalent changes made according to the structure, shape and principle of the present application shall be covered by the protection scope of the present application.
Claims (9)
1. The utility model provides an electron cigarette tobacco tar that helps alleviating fatigue which characterized in that: the electronic cigarette tobacco tar is prepared from the following raw materials in parts by weight: 10-90 parts of propylene glycol, 10-90 parts of glycerol, 0.5-3 parts of vitamin B3, 0.5-3 parts of vitamin B15, 1-3.5 parts of taurine, 1-3.5 parts of tyrosine and 0.5-1.5 parts of synergist.
2. The e-cigarette liquid helpful for relieving fatigue of claim 1, wherein: the synergist is one or more of vitamin A and vitamin E.
3. The e-cigarette liquid helpful for relieving fatigue of claim 1, wherein: the electronic cigarette tobacco tar also comprises trehalose for improving the stability of each raw material of the electronic cigarette tobacco tar.
4. The e-cigarette liquid helpful for relieving fatigue of claim 3, wherein: the dosage of the trehalose is 1-2.5 parts by weight.
5. The e-cigarette liquid helpful for relieving fatigue of claim 1, wherein: the e-cigarette tobacco tar also includes n-propyl benzoate for lowering the boiling point of the e-cigarette tobacco tar blend.
6. The e-cigarette liquid helpful for relieving fatigue of claim 5, wherein: the dosage of the n-propyl benzoate is 35 to 50 parts by weight.
7. The e-cigarette liquid helpful for relieving fatigue of claim 5, wherein: the mass ratio of the n-propyl benzoate to the glycerol is (40-50): (10-20).
8. The e-cigarette liquid helpful for relieving fatigue of claim 5, wherein: the mass ratio of the propylene glycol to the glycerol is (70-90): (10-20).
9. The method of any one of claims 1-8 for preparing an e-cigarette liquid useful for relieving fatigue, comprising the steps of: the electronic cigarette tobacco tar can be obtained by uniformly mixing the raw materials according to the parts by weight, wherein the mixing temperature is 20-60 ℃.
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