CN104585883B - A kind of atomized liquid containing Radix Angelicae Sinensis composition and preparation method thereof - Google Patents
A kind of atomized liquid containing Radix Angelicae Sinensis composition and preparation method thereof Download PDFInfo
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- CN104585883B CN104585883B CN201410855364.8A CN201410855364A CN104585883B CN 104585883 B CN104585883 B CN 104585883B CN 201410855364 A CN201410855364 A CN 201410855364A CN 104585883 B CN104585883 B CN 104585883B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F47/00—Smokers' requisites not otherwise provided for
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/232—Angelica
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/10—Dispersions; Emulsions
- A61K9/12—Aerosols; Foams
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Abstract
The invention discloses a kind of atomized liquid containing Radix Angelicae Sinensis composition and preparation method thereof.The atomized liquid includes following components in percentage by weight：55 75% propane diols, 10 20% glycerine, 5 10% Radix Angelicae Sinensis compositions and 5 15% distilled water.The present invention substitutes tobacco elite by adding Chinese angelica volatile oil, obtained atomized liquid is especially effective to women smoker, and with replenishing and activating blood, menstruction regulating and pain relieving, the health-care efficacy to relax bowel, user can be made while gradual quitting tobacco dependency, absorb Radix Angelicae Sinensis medicinal ingredient, improve physiological function, strengthen fitness.
Description
Technical field
The invention belongs to electronic cigarette field, and in particular to a kind of atomized liquid containing Radix Angelicae Sinensis composition and preparation method thereof.
Background technology
As people are more and more deep to the understanding of cigarette harm, smokers are highly desirable to there is cigarette substitute to save
Their health.Wherein, electronic cigarette is as one of cigarette substitute, positive effect of giving up smoking.The electronic cigarette of health is free of tar, nothing
The harmful substances such as carbon monoxide, nitrogen dioxide, arsenic, lead, mercury, the harm of " second-hand-cigarette " to surrounding population can be avoided.By several generations
Development, at present electronic cigarette atomizing liquid taste can realize variation, meet the need that different smokers are selected different taste
Ask.But the main material of still being given up using tobacco extract, nicotine etc. as craving for tobacco of electronics smoke product on the market adds atomized liquid
In formula, can not really meet the needs of consumer health's smoking cessation, can not especially meet the smoker's with some special illnesss
Treatment of smoking cessation demand, the envelop of function of electronics smoke product is limited to.Electronics smoke product market potential is huge, and in the market is electronic atomized
Liquid function is single, especially rare with the tasty product of traditional Chinese medicine ingredients.
Chinese herbal medicine category natural drug, toxic side effect are small.Wherein, Radix Angelicae Sinensis has replenishing and activating blood, menstruction regulating and pain relieving, relaxed bowel
Effect, main pharmacodynamics composition are water miscible forulic acid and fat-soluble Ligustilide, and forulic acid is organic acid composition, Jehol Ligusticum Rhizome
Lactone is phthalide constituents, belongs to higher boiling volatile oil component, available for moisturize laxation, intestines are dry and shit is difficult, qi-blood deficiency, liver depression gas
Stagnant, dizziness of having a headache, can both stimulate the menstrual flow menstruation regulating, and can active pain relieving, be particularly suitable for the illnesss such as irregular menstruation, dysmenorrhoea, deficiency of blood amenorrhoea, quilt
Ancients are referred to as " gynaecology's panacea ".But also it can play smoking cessation and improvement women containing angelica extract without a on the market at present
The electronic atomized liquid product of health status.
The content of the invention
To solve the shortcomings that prior art and weak point, primary and foremost purpose of the invention be to provide it is a kind of containing Radix Angelicae Sinensis into
The atomized liquid divided.The atomized liquid does not add nicotine, containing Chinese angelica volatile oil, organic acid and other functional ingredient, allows women smokers
Can be while progressively giving up smoking, regulating menstruation and activating blood, blood-enrich, improve the fitness of women.
Another object of the present invention is to provide the preparation method of the above-mentioned atomized liquid containing Radix Angelicae Sinensis composition.
For achieving the above object, the present invention adopts the following technical scheme that：
A kind of atomized liquid containing Radix Angelicae Sinensis composition, it includes following components in percentage by weight：55-75% propane diols, 10-
20% glycerine, 5-10% Radix Angelicae Sinensis composition and 5-15% distilled water；The Radix Angelicae Sinensis composition is Chinese angelica volatile oil and eumenol, the above
Weight percentages of components sum is 100%.
Preferably, the atomized liquid containing Radix Angelicae Sinensis composition includes following components in percentage by weight：72% propane diols,
15% glycerine, 5% Radix Angelicae Sinensis composition and 8% distilled water.
Preferably, the atomized liquid containing Radix Angelicae Sinensis composition includes following components in percentage by weight：65% propane diols,
12% glycerine, 8% Radix Angelicae Sinensis composition and 15% distilled water.
Preferably, the atomized liquid containing Radix Angelicae Sinensis composition includes following components in percentage by weight：63% propane diols,
20% glycerine, 10% Radix Angelicae Sinensis composition and 7% distilled water.
The preparation method of the above-mentioned atomized liquid containing Radix Angelicae Sinensis composition, comprises the following steps：
(1) Radix Angelicae Sinensis is crushed and crosses 80 mesh sieves, added the water of 12-14 times of Radix Angelicae Sinensis quality, extracted at a temperature of 40-60 DEG C
Twice, each each 1h, obtains volatile oil compositions and extract solution；Volatile oil compositions are through petroleum ether extraction and are concentrated under reduced pressure to give Radix Angelicae Sinensis
Volatile oil, extract solution is through being concentrated under reduced pressure to give eumenol；
(2) obtained Chinese angelica volatile oil and eumenol weight sum in step (1) is calculated as to the weight of Radix Angelicae Sinensis composition, pressed
Remaining component raw material is weighed according to the percentage by weight of each component；Eumenol made from step (1) is added into distilled water dissolving, obtained
To Chinese Medicines；Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid；Add and work as made from step (1)
Return volatile oil, the emulsifying 5-10min under 3000-4000rpm rotating speed, obtain the atomized liquid containing Radix Angelicae Sinensis composition.
Preferably, the emulsifying temperature described in step (2) is 25-30 DEG C.
Compared with prior art, the present invention has advantages below and beneficial effect：
(1) traditional electronic atomized liquid is the composition that skimmed the cream off milk from tobacco, is dissolved in the solvent of food-grade, adds simultaneously
Add a small amount of essence and flavoring agent.The Essence of a variety of green plantss of extraction, it is inhaled into the cigarette for having removing to rest in human body in vivo
Poison, the unique effects for removing craving for tobacco.But still containing the carcinogens such as nicotine, the health of harmful to human in atomized liquid.Smoking
Crowd has resulted in the infringement of its lung during long-term smoking, and immunologic function declines, and the present invention adds in electronic atomized liquid
Medicinal herb componentses are added to substitute the tobacco extract in conditional electronic cigarette, the effect that can both reach smoking cessation also has health-care efficacy.
(2) Radix Angelicae Sinensis of the present invention is extracted using relatively mild Hot water extraction, can guarantee that Radix Angelicae Sinensis forulic acid, polysaccharide, volatile oil
All extracted Deng composition, volatile oil compositions use special extraction concentration technique, ensure that active component is not destroyed.
Chinese angelica volatile oil composition can not only reduce blood pressure, improve myocardial ischemia, anti-arrhythmia cordis, have and relieving asthma, suppress
Central nervous system, the pharmacological action such as body's immunity and anti-inflammatory and antalgic is improved, also passed through with aromatic smell, the present invention
Chinese angelica volatile oil substitution tobacco elite is added, obtained atomized liquid is especially effective to women smoker, and with work of enriching blood
Blood, menstruction regulating and pain relieving, the health-care efficacy to relax bowel, user can be made while gradual quitting tobacco dependency, absorb Radix Angelicae Sinensis it is medicinal into
Point, improve physiological function, strengthen fitness.
Brief description of the drawings
Fig. 1 is the Radix Angelicae Sinensis constituents extraction process chart of the embodiment of the present invention 1；
Fig. 2 is atomized liquid preparation technology flow chart of the embodiment of the present invention 1 containing Radix Angelicae Sinensis composition.
Embodiment
With reference to embodiment and accompanying drawing, the present invention is described in further detail, but embodiments of the present invention are unlimited
In this.
The invention discloses a kind of atomized liquid containing Radix Angelicae Sinensis composition, including following components in percentage by weight：55-75%
Propane diols, 10-20% glycerine, 5-10% Radix Angelicae Sinensis composition and 5-15% distilled water；The Radix Angelicae Sinensis composition include Chinese angelica volatile oil and
Eumenol.The preparation process that this contains the atomized liquid of Radix Angelicae Sinensis composition is as follows：
(1) Radix Angelicae Sinensis be crushed into 80 mesh sieves, adds the water of the amount of 12-14 times of Radix Angelicae Sinensis quality, extraction twice, each 1h, obtains
To volatile oil compositions and extract solution；Volatile oil compositions extract and are concentrated under reduced pressure to give Chinese angelica volatile oil through oily ether, and extract solution is through subtracting
Pressure is concentrated to give eumenol；
(2) obtained Chinese angelica volatile oil and eumenol weight sum in step (1) is calculated as to the weight of Radix Angelicae Sinensis composition, pressed
Remaining component raw material is weighed according to the percentage by weight of each component；Eumenol made from step (1) is dissolved with distilled water, obtained
Chinese Medicines；Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid；Add Radix Angelicae Sinensis made from step (1)
Volatile oil, emulsifying 5-10min under 3000-4000rpm rotating speed, obtain the atomized liquid containing Radix Angelicae Sinensis composition.
Above-mentioned preparation process is it is determined that after rational formula, is mainly realized by abstraction technique and emulsifying technology.Will
Make electronic atomized liquid that there is medical value and reach optimal atomizing effect, suitable Radix Angelicae Sinensis extraction process and preparation must be selected
Go out good properties and stable atomized liquid, its each composition especially Chinese angelica volatile oil can be uniformly distributed with aqueous phase, during atomization without into
Divide delay and other effects.Good properties and stable electronic atomized liquid are prepared, it is necessary to solve in stirring and emulsifying hybrid technology
Problem, designs optimal parameter, and wherein temperature, emulsification times, mixing speed all serves vital.
It is found by experiment that, obtained atomized liquid water-oil phase is uniformly dispersed after being stirred using emulsifying, and can keep
Stable, two-phase is not easy to separate again.The system water oil is liquid, can reach good emulsifying effectiveness at room temperature, high
In this temperature (40-70 DEG C) emulsifying effectiveness without change is write, the energy of high temperature consumption is more, will emulsification temperature from cost-effective angle
Degree is arranged to 25-30 DEG C.
Find that the water-oil phase dispersion effect of the obtained atomized liquid of high rotating speed (4000-6000rpm) is good in experiment, but at a high speed
Foam is more caused by emulsification, and 3000rpm stirring at low speed can eliminate bubble.Too small (1000-2000rpm) shearing force of rotating speed is not
It is enough to make the two-phase of atomized liquid uniformly, fine and smoothly to complete to disperse.
Emulsification times will also result in influence to the quality of atomized liquid, due to the present invention atomization formula of liquid in volatile oil into
Point content is less, and viscosity is relatively low, can complete to disperse within a short period of time.5-10min, the few oil slick of atomized liquid foam is few, and emulsion is steady
It is fixed.Less than 3min, because the time is too short, the not up to effect of stable dispersion.
Embodiment 1
A kind of preparation method of the atomized liquid containing Radix Angelicae Sinensis composition, as illustrated in fig. 1 and 2, comprises the following steps：
(1) 100g Radix Angelicae Sinensis be crushed into 80 mesh sieves, adds the water of the amount of 12 times of Radix Angelicae Sinensis quality, 55 DEG C extract twice, every time
1h, obtain volatile oil compositions and extract solution；Volatile oil compositions extract and are concentrated under reduced pressure to give Chinese angelica volatile oil, extract solution through oily ether
Through being concentrated under reduced pressure to give eumenol；
(2) obtained Chinese angelica volatile oil and eumenol weight sum in step (1) is calculated as to the weight of Radix Angelicae Sinensis composition, pressed
Remaining component raw material is weighed according to the percentage by weight of each component；Eumenol made from step (1) is dissolved with distilled water, obtained
Chinese Medicines；Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid；Add Radix Angelicae Sinensis made from step (1)
Volatile oil, with vacuum homogeneous emulsifying machine, the emulsifying 5min under 3000rpm rotating speed, emulsifying temperature is normal temperature (25-30
DEG C), sterilizing, lamp inspection after bottling capping, obtain the atomized liquid containing Radix Angelicae Sinensis composition；
The wherein above-mentioned atomized liquid containing Radix Angelicae Sinensis composition includes following components in percentage by weight：72% propane diols, 15%
Glycerine, 5% Radix Angelicae Sinensis composition and 8% distilled water；The Radix Angelicae Sinensis composition is obtained Chinese angelica volatile oil and Radix Angelicae Sinensis leaching in step (1)
Cream.
Radix Angelicae Sinensis component ratio is less than normal in this embodiment, and smog is dense, is adapted to just smoking cessation crowd.
Embodiment 2
A kind of preparation method of the atomized liquid containing Radix Angelicae Sinensis composition, comprises the following steps：
(1) Radix Angelicae Sinensis be crushed into 80 mesh sieves, adds the water of the amount of 14 times of Radix Angelicae Sinensis quality, 50 DEG C of extractions twice, each 1h, obtain
To volatile oil compositions and extract solution；Volatile oil compositions extract and are concentrated under reduced pressure to give Chinese angelica volatile oil through oily ether, and extract solution is through subtracting
Pressure is concentrated to give eumenol；
(2) obtained Chinese angelica volatile oil and eumenol weight sum in step (1) is calculated as to the weight of Radix Angelicae Sinensis composition, pressed
Remaining component raw material is weighed according to the percentage by weight of each component；Eumenol made from step (1) is added into distilled water dissolving, obtained
To Chinese Medicines；Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid；Add and work as made from step (1)
Return volatile oil, with vacuum homogeneous emulsifying machine, the emulsifying 5min under 4000rpm rotating speed, emulsifying temperature is normal temperature (25-30
DEG C), sterilizing, lamp inspection after bottling capping, obtain the atomized liquid containing Radix Angelicae Sinensis composition；
The wherein above-mentioned atomized liquid containing Radix Angelicae Sinensis composition, including following components in percentage by weight：65% propane diols, 12%
Glycerine, 8% Radix Angelicae Sinensis composition and 15% distilled water；The Radix Angelicae Sinensis composition is obtained Chinese angelica volatile oil and Radix Angelicae Sinensis leaching in step (1)
Cream.
Radix Angelicae Sinensis component ratio is moderate in this embodiment, can play a role in health care.
Embodiment 3
A kind of preparation method of the atomized liquid containing Radix Angelicae Sinensis composition, comprises the following steps：
(1) Radix Angelicae Sinensis be crushed into 80 mesh sieves, adds the water of the amount of 14 times of Radix Angelicae Sinensis quality, 55 DEG C of extractions twice, each 1h, obtain
To volatile oil compositions and extract solution；Volatile oil compositions extract and are concentrated under reduced pressure to give Chinese angelica volatile oil through oily ether, and extract solution is through subtracting
Pressure is concentrated to give eumenol；
(2) obtained Chinese angelica volatile oil and eumenol weight sum in step (1) is calculated as to the weight of Radix Angelicae Sinensis composition, pressed
Remaining component raw material is weighed according to the percentage by weight of each component；Eumenol made from step (1) is added into distilled water dissolving, obtained
To Chinese Medicines；Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid；Add and work as made from step (1)
Return volatile oil, with vacuum homogeneous emulsifying machine, the emulsifying 10min under 3000rpm rotating speed, emulsifying temperature is normal temperature (25-30
DEG C), sterilizing, lamp inspection after bottling capping, obtain the atomized liquid containing Radix Angelicae Sinensis composition；
The wherein above-mentioned atomized liquid containing Radix Angelicae Sinensis composition, including following components in percentage by weight：63% propane diols, 20%
Glycerine, 10% Radix Angelicae Sinensis composition and 7% distilled water；The Radix Angelicae Sinensis composition is obtained Chinese angelica volatile oil and Radix Angelicae Sinensis leaching in step (1)
Cream.
Radix Angelicae Sinensis medicinal ingredient ratio is higher in this embodiment, and health-care effect is obvious and smog is dense.
To verify the smoking cessation effect and health-care effect of atomized liquid of the present invention, it is made of the atomization formula of liquid in embodiment 3
Tested after electronic cigarette, 100 female smokers, there are the ill symptomses such as sallow complexion, anaemia, the deficiency of vital energy, irregular menstruation.Will
5ml atomized liquids are put into electronic cigarette atomizing inhalator, suck daily 10 times, draw 80ml altogether within 2 months.Test effect, 89% craving for tobacco
It is remarkably decreased, 52% insufficiency of vital energy and blood, the symptom of sallow complexion make moderate progress, and illustrate that atomized liquid of the present invention has notable effect to smoking cessation
Fruit, while the anaemia deficiency of vital energy of women is had some improvement.
Above-described embodiment is the preferable embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any Spirit Essences without departing from the present invention with made under principle change, modification, replacement, combine, simplification,
Equivalent substitute mode is should be, is included within protection scope of the present invention.
Claims (4)
1. a kind of preparation method of the atomized liquid containing Radix Angelicae Sinensis composition, it is characterised in that comprise the following steps that：
(1) Radix Angelicae Sinensis is crushed and crosses 80 mesh sieves, add the water of 12-14 times of Radix Angelicae Sinensis quality, in 40-60 DEG C of temperature extraction twice, often
Secondary each 1h, obtains volatile oil compositions and extract solution；Volatile oil compositions are through petroleum ether extraction and are concentrated under reduced pressure to give Chinese angelica volatile oil,
Extract solution is through being concentrated under reduced pressure to give eumenol；
(2) obtained Chinese angelica volatile oil and eumenol weight sum in step (1) is calculated as to the weight of Radix Angelicae Sinensis composition, according to each
The percentage by weight of component weighs remaining component raw material；Eumenol made from step (1) is added into distilled water dissolving, in obtaining
Drug solns；Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid；Radix Angelicae Sinensis made from adding step (1) is waved
Hair oil, the emulsifying 5-10min under 25-30 DEG C, 3000-4000rpm rotating speed, obtain the atomization containing Radix Angelicae Sinensis composition
Liquid；The atomized liquid containing Radix Angelicae Sinensis composition consists of the following components in percentage by weight：55-75% propane diols, 10-20% are sweet
Oil, 5-10% Radix Angelicae Sinensis composition and 5-15% distilled water；The Radix Angelicae Sinensis composition is Chinese angelica volatile oil and eumenol, above component weight
It is 100% to measure percentage sum.
2. the preparation method of the atomized liquid according to claim 1 containing Radix Angelicae Sinensis composition, it is characterised in that the atomized liquid by
Following components in percentage by weight forms：72% propane diols, 15% glycerine, 5% Radix Angelicae Sinensis composition and 8% distilled water.
3. the preparation method of the atomized liquid according to claim 1 containing Radix Angelicae Sinensis composition, it is characterised in that the atomized liquid by
Following components in percentage by weight forms：65% propane diols, 12% glycerine, 8% Radix Angelicae Sinensis composition and 15% distilled water.
4. the preparation method of the atomized liquid according to claim 1 containing Radix Angelicae Sinensis composition, it is characterised in that the atomized liquid by
Following components in percentage by weight forms：63% propane diols, 20% glycerine, 10% Radix Angelicae Sinensis composition and 7% distilled water.
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| CN201410855364.8A CN104585883B (en) | 2014-12-31 | 2014-12-31 | A kind of atomized liquid containing Radix Angelicae Sinensis composition and preparation method thereof |
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Families Citing this family (3)
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| CN105341996A (en) * | 2015-10-27 | 2016-02-24 | 深圳瀚星翔科技有限公司 | Electronic cigarette liquid and preparation method thereof |
| CN107467719A (en) * | 2017-08-29 | 2017-12-15 | 贵州普定印象朵贝农业开发有限公司 | A kind of Chinese yew electronic cigarette |
| CN109588761A (en) * | 2019-01-18 | 2019-04-09 | 薪火高科(深圳)有限公司 | It is a kind of to have effects that relieving cough and reducing sputum tobacco juice for electronic smoke |
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|---|---|---|---|---|
| CN1137363A (en) * | 1996-03-26 | 1996-12-11 | 高华选 | Chinese herbal medicine type tobacco liquor and its preparation method |
| CN1994159A (en) * | 2006-12-15 | 2007-07-11 | 姜志荣 | Kidney-strengthening mind-refreshing tobacco liquid for electronic atomized cigarette |
| CN103564647A (en) * | 2012-07-31 | 2014-02-12 | 马瑞 | Preparation method of traditional Chinese medicine spices for tobaccos |
| CN104126874A (en) * | 2014-07-11 | 2014-11-05 | 张伟滨 | Electronic cigarette atomized liquid and preparation method thereof |
-
2014
- 2014-12-31 CN CN201410855364.8A patent/CN104585883B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1137363A (en) * | 1996-03-26 | 1996-12-11 | 高华选 | Chinese herbal medicine type tobacco liquor and its preparation method |
| CN1994159A (en) * | 2006-12-15 | 2007-07-11 | 姜志荣 | Kidney-strengthening mind-refreshing tobacco liquid for electronic atomized cigarette |
| CN103564647A (en) * | 2012-07-31 | 2014-02-12 | 马瑞 | Preparation method of traditional Chinese medicine spices for tobaccos |
| CN104126874A (en) * | 2014-07-11 | 2014-11-05 | 张伟滨 | Electronic cigarette atomized liquid and preparation method thereof |
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Effective date of registration: 20180122 Address after: Shantou Guangdong No. 111 building, 515000 Guangdong Province, Shantou Jinsha Road, building 1 room 1312 Patentee after: Shantou Zhili Technology Co. Ltd. Address before: Zhongshan road two lane 515638 Guangdong Ruan city of Chaozhou province Chaoan District Anbu Maolong No. 23 (two) Patentee before: Guangdong Jin Cheng biotechnology Engineering Co., Ltd |
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Granted publication date: 20180116 Termination date: 20181231 |