CN104126874A - Electronic cigarette atomized liquid and preparation method thereof - Google Patents
Electronic cigarette atomized liquid and preparation method thereof Download PDFInfo
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- CN104126874A CN104126874A CN201410331945.1A CN201410331945A CN104126874A CN 104126874 A CN104126874 A CN 104126874A CN 201410331945 A CN201410331945 A CN 201410331945A CN 104126874 A CN104126874 A CN 104126874A
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Abstract
The invention relates to electronic cigarette atomized liquid and a preparation method thereof. The preparation method comprises the following steps of (1) feeding aromatic Chinese herbal medicines into an extraction container, adding water into the extraction container, and performing distillation and extraction to obtain Chinese herbal medicine extract liquor; (2) adding solvent into the Chinese herbal medicine extract liquor and performing digestion and extraction on the Chinese herbal medicine extract liquor; (3) mixing Chinese herbal medicine essential oil with coffee bean extractive; (4) complementing the balance for preparing the electronic cigarette atomized liquid with propylene glycol or glycerinum to obtain the electronic cigarette atomized liquid. The electronic cigarette atomized liquid prepared by the method is mellow in aroma and diverse in flavor, and is similar to cigarettes in taste, long-lasting effect of fragrance of natural aroma constituents is achieved, and harm to human bodies caused by ingredients of nicotine and tar in traditional tobaccos can be reduced.
Description
Technical field
The present invention relates to a kind of atomized liquid and preparation method thereof, be specifically related to a kind of electronic cigarette atomizing liquid and preparation method thereof.
Background technology
Electronic cigarette liquid (or claim electronic cigarette atomizing liquid) is popular cigarette substitute products at present, about prescription being dispensed, the preparation process of electronic cigarette liquid, with and reduce in aspects such as health, had many documents and patent report.
Because increasing smoker starts to accept to use electronic cigarette to replace cigarette, also just more and more obvious for the some shortcomings of the atomized liquid of these electronic cigarettes.Consumer generally reflects, electronic cigarette is compared with cigarette, although perceptual image cigarettes such as form, feel, smog, but at the aspect such as fragrance, taste, larger with the perceptual difference distance of product cigarette, the product being especially deployed into various essence and flavoring agents, they are difficult to accept or be accustomed to its fragrance and taste.In addition, the at present fragrance component of electronic cigarette difficult long-term reservation,, best can only deposit about half a year, and " smoke " is just very light or almost do not had, and this is also the problem that consumer is generally reflected.These deficiencies, larger on the quality impact of electronic cigarette, also restricting the universal and popular of electronic cigarette simultaneously.
Summary of the invention
For overcoming above-mentioned existing electronic cigarette atomizing liquid fragrance and taste bad will, the short deficiency of fragrance remaining time, the object of the present invention is to provide that a kind of not only fragrance is mellow, multiple tastes, mouthfeel and cigarette approaches, natural aromatic composition fragrance remaining time is long, the preparation method that also can reduce traditional Nicotine in Tobacco and the tar ingredients electronic cigarette atomizing liquid to harm.
Corresponding therewith, the present invention also provides the electronic cigarette atomizing liquid that adopts described method to prepare.
For achieving the above object, the technical scheme that the present invention takes is: a kind of preparation method of electronic cigarette atomizing liquid, said method comprising the steps of:
(1) take the ratio of 0.05～0.2kg Chinese herbal medicine according to pre-prepared every liter of electronic cigarette atomizing liquid, Chinese herbal medicine is dropped in extraction vessel; Add the ratio of 4～8 ml waters according to every gram of Chinese herbal medicine, water is added in extraction vessel, soak Chinese herbal medicine 40～90 minutes; Heating extraction vessel to 120～130 DEG C, distillation extraction 3～8 hours, makes plant liquid extract;
(2) plant liquid extract of step (1) gained is dropped in separator, add solvent, be uniformly mixed; Heated separator to 45～65 DEG C, insulation lixiviate extraction, after 40～120 minutes, is filtered the solution of lixiviate extraction gained, makes Chinese herbal medicine volatile oil; Wherein, described solvent comprises propane diols and glycerine, and the percent by volume of solvent and pre-prepared electronic cigarette atomizing liquid is 80～95%;
(3) step (2) gained Chinese herbal medicine volatile oil is joined in mixer, take the ratio of 0.01～0.2kg coffee bean extract according to pre-prepared every liter of electronic cigarette atomizing liquid, add coffee bean extract, be uniformly mixed 30～50 minutes;
(4) supply pre-prepared electronic cigarette atomizing liquid surplus with propane diols or glycerine, be uniformly mixed, obtain electronic cigarette atomizing liquid.
The pre-prepared electronic cigarette atomizing liquid of the present invention amasss the volume (finally preparing the volume of the electronic cigarette atomizing liquid of gained) for the electronic cigarette atomizing liquid of plan preparation; Chinese herbal medicine of the present invention has armaticity, is armaticity Chinese herbal medicine, and Chinese herbal medicine is that Chinese Industrial Standards (CIS) GB 2760-2011 allows the food flavor using; Propane diols or glycerine that solvent of the present invention, honey and being used for is supplied electronic cigarette atomizing liquid surplus are medicinal or edible rank, and water of the present invention can be selected pure water.
The present invention adopts the method that distillation extraction is combined with lixiviate extraction phase to extract Chinese herbal medicine volatile oil, can not only keep to greatest extent natural aromatic composition and nutritional labeling in former Chinese herbal medicine to enter electronic cigarette atomizing liquid, make the fragrance, taste of electronic cigarette atomizing liquid substantially from the natural aromatic of Chinese herbal medicine, can also make to enter natural aromatic composition fragrance remaining time in electronic cigarette atomizing liquid longer.
Make solvent with propane diols and glycerine, under comparatively gentle condition, extract Chinese herbal medicine volatile oil, can avoid under the concentrated condition of complicated procedures of forming and high temperature some volatile or to temperature than more sensitive Chinese herbal medicine fragrance ingredient loss or destroy.In addition, compared with the solvent of the extraction fragrance ingredient conventional with other, propane diols and glycerine have advantages of that viscosity is large, have certain performance of keeping humidity, fragrance ingredient is had to better stick effect.Electronic cigarette atomizing liquid of the present invention is deposited more than 2 years, and fragrance still can well retain.
As the preparation method's of electronic cigarette atomizing liquid of the present invention preferred embodiment, the Chinese herbal medicine in described step (1) comprises at least 3 kinds in Radix Glycyrrhizae, reed rhizome, ginger, myrrh, levisticum, Radix Angelicae Sinensis, the root of Dahurain angelica, nutmeg, Pogostemon cablin, Chinese cassia tree, sweet osmanthus, valerian, styrax, peppermint, Fructus Caryophylli; As the preparation method's of electronic cigarette atomizing liquid of the present invention more preferably embodiment, described Chinese herbal medicine comprises the component of following weight portion: 10 parts, Radix Glycyrrhizae, 10 parts of reed rhizomes, 5 parts, ginger, 5 parts of myrrhs, 5 parts of levisticums, 5 parts of Radix Angelicae Sinensis, 5 parts of the roots of Dahurain angelica, 5 parts of nutmegs, 5 parts of Pogostemon cablin, 5 parts of Chinese cassia trees, 10 parts of sweet osmanthus, 10 parts of valerians, 10 parts of styraxes, 5 parts of peppermints, 5 parts of Fructus Caryophyllis.
In order to reduce the impurity in the electronic cigarette atomizing liquid making, and make Chinese herbal medicine effect of extracting better, said herbal medicine mixes after dropping into before extraction vessel and remove respectively impurity, cleaning, smash to pieces.The present invention can adopt the mode being uniformly mixed that Chinese herbal medicine is mixed.
As the preparation method's of electronic cigarette atomizing liquid of the present invention preferred embodiment, in described step (2), solvent is made up of propane diols, glycerine and honey; As the preparation method's of electronic cigarette atomizing liquid of the present invention more preferably embodiment, described solvent is uniformly mixed 30～50 minutes gained by propane diols, glycerine and honey; Best, in described solvent, the percent by volume of each component is: propane diols 80%, glycerine 15%, honey 5% or propane diols 15%, glycerine 80%, honey 5%.That honey can be augmented is fragrant and sweet, hide assorted taste, reduce penetrating odor and acid; In solvent, add honey, the electronic cigarette atomizing liquid that can make to make has Tianjin and moistens tasty and refreshing smoke.
As the preparation method's of electronic cigarette atomizing liquid of the present invention preferred embodiment, in described step (2), separator is negative-pressure vacuum separator; Filter in described step (2) in vacuum pressure is the negative-pressure vacuum separator of-0.08～-0.09Mpa and carry out.
As the preparation method's of electronic cigarette atomizing liquid of the present invention preferred embodiment, in described step (3), the preparation method of coffee bean extract is: first coffee bean being pulverized is 30～90 object coffee bean powders, again coffee bean powder is dropped in the boiler of sandwich, add the ratio of 4～8 ml distilled waters according to every gram of coffee bean powder, distilled water is added in coffee bean powder to coffee soaking bean powder 40～90 minutes; Heating boiler to 120～130 DEG C, distillation extraction coffee bean powder 3～8 hours; Be under the condition of-0.08～-0.09MPa at vacuum pressure, filter extract by negative-pressure vacuum separator, reduced pressure concentration filtrate to proportion is 1.2～1.5, and gained medicinal extract is coffee bean extract.The recovery rate of coffee bean extract is 45～70%.
As the preparation method's of electronic cigarette atomizing liquid of the present invention preferred embodiment, the speed stirring in described step (4) is 1400 revs/min, and the time being uniformly mixed is 45 minutes.The present invention can adopt thrust by airscrew device to stir.In described step (4), add propane diols or glycerine to supply after electronic cigarette atomizing liquid surplus, be stirred to electronic cigarette atomizing liquid and mix.
Meanwhile, the present invention also provides a kind of electronic cigarette atomizing liquid that adopts said method to prepare.
Beneficial effect of the present invention is: the present invention adopts the method that distillation extraction is combined with lixiviate extraction phase to extract Chinese herbal medicine volatile oil, can not only keep to greatest extent natural aromatic composition and nutritional labeling in former Chinese herbal medicine to enter electronic cigarette atomizing liquid, make the fragrance, taste of electronic cigarette atomizing liquid substantially from the natural aromatic of Chinese herbal medicine, can also make to enter natural aromatic composition fragrance remaining time in electronic cigarette atomizing liquid longer.Electronic cigarette atomizing liquid fragrance that the method for the invention prepares is mellow, multiple tastes, mouthfeel more approach cigarette taste, natural aromatic composition fragrance remaining time are longer, can be applicable to hyundai electronics smoking set, being realized and being sucked by electrons heat atomization, is the formulated product of imitating cigarette taste.The method of the invention prepares electronic cigarette atomizing liquid and is all obviously better than conditional electronic aerosolization liquid from mouthfeel and fragrance performance, can meet the consumption demand of consumer to conditional electronic cigarette and cigarette, can effectively reduce again nicotine and the harm of tar ingredients to human body in traditional tobacco, but also give a kind of more healthy joyful psychology of consumer from sense organ, more can cater to consumer's taste and pursue.
Detailed description of the invention
For the object, technical solutions and advantages of the present invention are described better, below in conjunction with specific embodiment, the invention will be further described.
In embodiment, the container of use is 304 stainless steels.Prepare in plant liquid extract process, the boiler that the extraction vessel of employing is sandwich, the water of use is pure water; Preparing separator used in Chinese herbal medicine volatile oil process by plant liquid extract is negative-pressure vacuum separator; In the mixed process of Chinese herbal medicine volatile oil and coffee bean extract, using agitator tank as mixer.Certainly, extraction vessel is not limited to the boiler of sandwich, and separator is not limited to negative-pressure vacuum separator, and mixer is not limited to agitator tank, and container all can need to be selected according to experiment.
In embodiment, Chinese herbal medicine is that Chinese Industrial Standards (CIS) GB 2760-2011 allows the food flavor using, and propane diols or glycerine are medicinal or edible rank.
In embodiment, in order to reduce the impurity in the electronic cigarette atomizing liquid making, and make Chinese herbal medicine effect of extracting better, Chinese herbal medicine mixes after dropping into before extraction vessel and remove respectively impurity, cleaning, smash to pieces.
Embodiment 1
A kind of embodiment of the preparation method of electronic cigarette atomizing liquid of the present invention, the volume of the pre-prepared electronic cigarette atomizing liquid of the present embodiment is 500 liters, the preparation method of described electronic cigarette atomizing liquid comprises the following steps:
(1) by Radix Glycyrrhizae, Radix Angelicae Sinensis, styrax, ginger, myrrh, levisticum respectively decontamination, clean, smash to pieces after, be uniformly mixed the Chinese herbal medicine that obtains mixing; Wherein, in Chinese herbal medicine, the weight portion of each component is respectively: 20 parts, Radix Glycyrrhizae, 10 parts of Radix Angelicae Sinensis, 20 parts of styraxes, 20 parts, ginger, 10 parts of myrrhs, 20 parts of levisticums;
(2) take the Chinese herbal medicine that 70 kilograms of steps (1) gained mixes, drop in the boiler of sandwich, then add 300 liters of pure water in boiler, soak Chinese herbal medicine 90 minutes; Heating boiler to 120 DEG C, distillation extraction 4 hours, makes plant liquid extract;
(3) ratio that is 80%, 15%, 5% by propane diols, glycerine and honey according to percent by volume is uniformly mixed 30 minutes, makes the solvent mixing; The plant liquid extract of step (2) gained is dropped in negative-pressure vacuum separator, add 430 liters of solvents that mix, be uniformly mixed; Heating negative-pressure vacuum separator to 45 DEG C, insulation lixiviate extraction 80 minutes, at vacuum pressure be-0.09Mpa condition under, filter lixiviate and extract the solution of gained by negative-pressure vacuum separator, make Chinese herbal medicine volatile oil;
(4) prepare coffee bean extract: take 40 kilograms of coffee beans, pulverizing is 30 object coffee bean powders, coffee bean powder is dropped in the boiler of another sandwich, adds 240 liters of distilled water, coffee soaking bean powder 40 minutes; The raw material of heating in boiler, in 120 DEG C of distillation extraction coffee bean powders 5 hours; At vacuum pressure be-condition of 0.085Mpa under, filter extract by negative-pressure vacuum separator, reduced pressure concentration filtrate to proportion is 1.2, gained medicinal extract (24 kilograms) is coffee bean extract;
(5) Chinese herbal medicine volatile oil step (3) being made joins in agitator tank, to the coffee bean extract that adds 15 kilograms of steps (4) to make in agitator tank, is uniformly mixed 35 minutes;
(6) be 500 liters to adding propane diols to cumulative volume in agitator tank, adopt thrust by airscrew device to be uniformly mixed 45 minutes with the speed of 1400 revs/min, make described electronic cigarette atomizing liquid.
Embodiment 2
A kind of embodiment of the preparation method of electronic cigarette atomizing liquid of the present invention, the volume of the pre-prepared electronic cigarette atomizing liquid of the present embodiment is 500 liters, the preparation method of electronic cigarette atomizing liquid comprises the following steps described in the present embodiment:
(1) by reed rhizome, ginger, the root of Dahurain angelica, sweet osmanthus, Pogostemon cablin, Chinese cassia tree respectively decontamination, clean, smash to pieces after, be uniformly mixed the Chinese herbal medicine that obtains mixing; Wherein, in Chinese herbal medicine, the weight portion of each component is respectively: 10 parts of reed rhizomes, 20 parts, ginger, 30 parts of the roots of Dahurain angelica, 20 parts of sweet osmanthus, 10 parts of Pogostemon cablin, 10 parts of Chinese cassia trees;
(2) take the Chinese herbal medicine that 60 kilograms of steps (1) gained mixes, drop in the boiler of sandwich, then add 450 liters of pure water in boiler, soak Chinese herbal medicine 60 minutes; Heating boiler to 120 DEG C, distillation extraction 6 hours, makes plant liquid extract;
(3) ratio that is 80%, 15%, 5% by propane diols, glycerine and honey according to percent by volume is uniformly mixed 30 minutes, makes the solvent mixing; The plant liquid extract of step (2) gained is dropped in negative-pressure vacuum separator, add 440 liters of solvents that mix, be uniformly mixed; Heating negative-pressure vacuum separator to 55 DEG C, insulation lixiviate extraction 60 minutes, at vacuum pressure be-0.08Mpa condition under, filter lixiviate and extract the solution of gained by negative-pressure vacuum separator, make Chinese herbal medicine volatile oil;
(4) prepare coffee bean extract: take 40 kilograms of coffee beans, pulverizing is 90 object coffee bean powders, coffee bean powder is dropped in the boiler of another sandwich, adds 320 liters of distilled water, coffee soaking bean powder 90 minutes; The raw material of heating in boiler, in 130 DEG C of distillation extraction coffee bean powders 6 hours; At vacuum pressure be-condition of 0.085Mpa under, filter extract by negative-pressure vacuum separator, reduced pressure concentration filtrate to proportion is 1.5, gained medicinal extract (25 kilograms) is coffee bean extract;
(5) Chinese herbal medicine volatile oil step (3) being made joins in agitator tank, to the coffee bean extract that adds 20 kilograms of steps (4) to make in agitator tank, is uniformly mixed 35 minutes;
(6) be 500 liters to adding propane diols to cumulative volume in agitator tank, adopt thrust by airscrew device to be uniformly mixed 45 minutes with the speed of 1400 revs/min, make described electronic cigarette atomizing liquid.
Embodiment 3
A kind of embodiment of the preparation method of electronic cigarette atomizing liquid of the present invention, the volume of the pre-prepared electronic cigarette atomizing liquid of the present embodiment is 500 liters, the preparation method of electronic cigarette atomizing liquid comprises the following steps described in the present embodiment:
(1) by myrrh, levisticum, nutmeg, valerian, Fructus Caryophylli respectively decontamination, clean, smash to pieces after, be uniformly mixed the Chinese herbal medicine that obtains mixing; Wherein, in Chinese herbal medicine, the weight portion of each component is respectively: 30 parts of myrrhs, 20 parts of levisticums, 20 parts of nutmegs, 10 parts of valerians, 20 parts of Fructus Caryophyllis;
(2) take the Chinese herbal medicine that 50 kilograms of steps (1) gained mixes, drop in the boiler of sandwich, then add 350 liters of pure water in boiler, soak Chinese herbal medicine 40 minutes; Heating boiler to 130 DEG C, distillation extraction 3 hours, makes plant liquid extract;
(3) ratio that is 80%, 15%, 5% by propane diols, glycerine and honey according to percent by volume is uniformly mixed 50 minutes, makes the solvent mixing; The plant liquid extract of step (2) gained is dropped in negative-pressure vacuum separator, add 450 liters of solvents that mix, be uniformly mixed; Heating negative-pressure vacuum separator to 65 DEG C, insulation lixiviate extraction 120 minutes, at vacuum pressure be-0.08Mpa condition under, filter lixiviate and extract the solution of gained by negative-pressure vacuum separator, make Chinese herbal medicine volatile oil;
(4) prepare coffee bean extract: take 200 kilograms of coffee beans, pulverizing is 50 object coffee bean powders, coffee bean powder is dropped in the boiler of another sandwich, adds 1600 liters of distilled water, coffee soaking bean powder 80 minutes; The raw material of heating in boiler, in 120 DEG C of distillation extraction coffee bean powders 8 hours; At vacuum pressure be-condition of 0.09Mpa under, filter extract by negative-pressure vacuum separator, reduced pressure concentration filtrate to proportion is 1.3, gained medicinal extract (120 kg) is coffee bean extract;
(5) Chinese herbal medicine volatile oil step (3) being made joins in agitator tank, to the coffee bean extract that adds 100 kilograms of steps (4) to make in agitator tank, is uniformly mixed 50 minutes;
(6) be 500 liters to adding propane diols to cumulative volume in agitator tank, adopt thrust by airscrew device to be uniformly mixed 45 minutes with the speed of 1400 revs/min, make described electronic cigarette atomizing liquid.
Embodiment 4
A kind of embodiment of the preparation method of electronic cigarette atomizing liquid of the present invention, the volume of the pre-prepared electronic cigarette atomizing liquid of the present embodiment is 500 liters, the preparation method of electronic cigarette atomizing liquid comprises the following steps described in the present embodiment:
(1) by Radix Glycyrrhizae, reed rhizome, ginger, myrrh, levisticum, Radix Angelicae Sinensis, the root of Dahurain angelica, nutmeg, Pogostemon cablin, Chinese cassia tree, sweet osmanthus, valerian, styrax, peppermint, Fructus Caryophylli respectively decontamination, clean, smash to pieces after, be uniformly mixed the Chinese herbal medicine that obtains mixing; Wherein, in Chinese herbal medicine, the weight portion of each component is: 10 parts, Radix Glycyrrhizae, 10 parts of reed rhizomes, 5 parts, ginger, 5 parts of myrrhs, 5 parts of levisticums, 5 parts of Radix Angelicae Sinensis, 5 parts of the roots of Dahurain angelica, 5 parts of nutmegs, 5 parts of Pogostemon cablin, 5 parts of Chinese cassia trees, 10 parts of sweet osmanthus, 10 parts of valerians, 10 parts of styraxes, 5 parts of peppermints, 5 parts of Fructus Caryophyllis;
(2) take the Chinese herbal medicine that 100 kilograms of steps (1) gained mixes, drop in the boiler of sandwich, then add 400 liters of pure water in boiler, soak Chinese herbal medicine 90 minutes; Heating boiler to 125 DEG C, distillation extraction 8 hours, makes plant liquid extract;
(3) ratio that is 15%, 80%, 5% by propane diols, glycerine and honey according to percent by volume is uniformly mixed 40 minutes, makes the solvent mixing; The plant liquid extract of step (2) gained is dropped in negative-pressure vacuum separator, add 400 liters of solvents that mix, be uniformly mixed; Heating negative-pressure vacuum separator to 45 DEG C, insulation lixiviate extraction 90 minutes, at vacuum pressure be-0.085Mpa condition under, filter lixiviate and extract the solution of gained by negative-pressure vacuum separator, make Chinese herbal medicine volatile oil;
(4) prepare coffee bean extract: take 30 kilograms of coffee beans, pulverizing is 60 object coffee bean powders, coffee bean powder is dropped in the boiler of another sandwich, adds 200 liters of distilled water, coffee soaking bean powder 65 minutes; The raw material of heating in boiler, in 125 DEG C of distillation extraction coffee bean powders 3 hours; At vacuum pressure be-condition of 0.08Mpa under, filter extract by negative-pressure vacuum separator, reduced pressure concentration filtrate to proportion is 1.5, gained medicinal extract (13.5 kilograms) is coffee bean extract;
(5) Chinese herbal medicine volatile oil step (3) being made joins in agitator tank, to the coffee bean extract that adds 5 kilograms of steps (4) to make in agitator tank, is uniformly mixed 40 minutes;
(6) be 500 liters to adding propane diols to cumulative volume in agitator tank, adopt thrust by airscrew device to be uniformly mixed 45 minutes with the speed of 1400 revs/min, make described electronic cigarette atomizing liquid.
Embodiment 5
A kind of embodiment of the preparation method of electronic cigarette atomizing liquid of the present invention, the volume of the pre-prepared electronic cigarette atomizing liquid of the present embodiment is 500 liters, the preparation method of electronic cigarette atomizing liquid comprises the following steps described in the present embodiment:
(1) by ginger, styrax, valerian respectively decontamination, clean, smash to pieces after, be uniformly mixed the Chinese herbal medicine that obtains mixing; Wherein, in Chinese herbal medicine, the weight portion of each component is respectively: 30 parts, ginger, 30 parts of styraxes, 40 parts of valerians;
(2) take the Chinese herbal medicine that 25 kilograms of steps (1) gained mixes, drop in the boiler of sandwich, then add 200 liters of pure water in boiler, soak Chinese herbal medicine 90 minutes; Heating boiler to 120 DEG C, distillation extraction 4 hours, makes plant liquid extract;
(3) ratio that is 15%, 80%, 5% by propane diols, glycerine and honey according to percent by volume is uniformly mixed 40 minutes, makes the solvent mixing; The plant liquid extract of step (2) gained is dropped in negative-pressure vacuum separator, add 475 liters of solvents that mix, be uniformly mixed; Heating negative-pressure vacuum separator to 65 DEG C, insulation lixiviate extraction 40 minutes, at vacuum pressure be-0.09Mpa condition under, filter lixiviate and extract the solution of gained by negative-pressure vacuum separator, make Chinese herbal medicine volatile oil;
(4) prepare coffee bean extract: take 100 kilograms of coffee beans, pulverizing is 75 object coffee bean powders, coffee bean powder is dropped in the boiler of another sandwich, adds 400 liters of distilled water, coffee soaking bean powder 50 minutes; The raw material of heating in boiler, in 130 DEG C of distillation extraction coffee bean powders 5 hours; At vacuum pressure be-condition of 0.09Mpa under, filter extract by negative-pressure vacuum separator, reduced pressure concentration filtrate to proportion is 1.4, gained medicinal extract (70 kilograms) is coffee bean extract;
(5) Chinese herbal medicine volatile oil step (3) being made joins in agitator tank, to the coffee bean extract that adds 50 kilograms of steps (4) to make in agitator tank, is uniformly mixed 30 minutes;
(6) be 500 liters to adding propane diols to cumulative volume in agitator tank, adopt thrust by airscrew device to be uniformly mixed 45 minutes with the speed of 1400 revs/min, make described electronic cigarette atomizing liquid.
Above in each embodiment, the volume of the plant liquid extract making in described step (2) and distillation time, Chinese herbal medicine containing essential oil number relevant, plant liquid extract accounts for the long-pending few part of pre-prepared electronic cigarette atomizing liquid.
Electronic cigarette atomizing liquid fragrance that the method for the invention makes is mellow, multiple tastes, mouthfeel more approach cigarette taste, natural aromatic composition fragrance remaining time are longer.Product of the present invention is according to the Chinese herbal medicine difference of selecting, and taste can be different, mainly contains Radix Glycyrrhizae taste, coffee taste, cloves taste, herbal taste, sweet osmanthus taste, the tastes such as peppermint taste; Product of the present invention is deposited more than 2 years, still remains with fragrance.
Last institute should be noted that; above embodiment is only in order to illustrate technical scheme of the present invention but not limiting the scope of the invention; although the present invention is explained in detail with reference to preferred embodiment; those of ordinary skill in the art is to be understood that; can modify or be equal to replacement technical scheme of the present invention, and not depart from essence and the scope of technical solution of the present invention.
Claims (10)
1. a preparation method for electronic cigarette atomizing liquid, is characterized in that: the preparation method of described electronic cigarette atomizing liquid comprises the following steps:
(1) take the ratio of 0.05～0.2kg Chinese herbal medicine according to pre-prepared every liter of electronic cigarette atomizing liquid, Chinese herbal medicine is dropped in extraction vessel; Add the ratio of 4～8 ml waters according to every gram of Chinese herbal medicine, water is added in extraction vessel, soak Chinese herbal medicine 40～90 minutes; Heating extraction vessel to 120～130 DEG C, distillation extraction 3～8 hours, makes plant liquid extract;
(2) plant liquid extract of step (1) gained is dropped in separator, add solvent, be uniformly mixed; Heated separator to 45～65 DEG C, insulation lixiviate extraction, after 40～120 minutes, is filtered the solution of lixiviate extraction gained, makes Chinese herbal medicine volatile oil; Wherein, described solvent comprises propane diols and glycerine, and the percent by volume of solvent and pre-prepared electronic cigarette atomizing liquid is 80～95%;
(3) step (2) gained Chinese herbal medicine volatile oil is joined in mixer, take the ratio of 0.01～0.2kg coffee bean extract according to pre-prepared every liter of electronic cigarette atomizing liquid, add coffee bean extract, be uniformly mixed 30～50 minutes;
(4) supply pre-prepared electronic cigarette atomizing liquid surplus with propane diols or glycerine, be uniformly mixed, obtain electronic cigarette atomizing liquid.
2. the preparation method of electronic cigarette atomizing liquid as claimed in claim 1, is characterized in that: the Chinese herbal medicine in described step (1) comprises at least 3 kinds in Radix Glycyrrhizae, reed rhizome, ginger, myrrh, levisticum, Radix Angelicae Sinensis, the root of Dahurain angelica, nutmeg, Pogostemon cablin, Chinese cassia tree, sweet osmanthus, valerian, styrax, peppermint, Fructus Caryophylli.
3. the preparation method of electronic cigarette atomizing liquid as claimed in claim 2, is characterized in that: described Chinese herbal medicine comprises the component of following weight portion: 10 parts, Radix Glycyrrhizae, 10 parts of reed rhizomes, 5 parts, ginger, 5 parts of myrrhs, 5 parts of levisticums, 5 parts of Radix Angelicae Sinensis, 5 parts of the roots of Dahurain angelica, 5 parts of nutmegs, 5 parts of Pogostemon cablin, 5 parts of Chinese cassia trees, 10 parts of sweet osmanthus, 10 parts of valerians, 10 parts of styraxes, 5 parts of peppermints, 5 parts of Fructus Caryophyllis.
4. the preparation method of electronic cigarette atomizing liquid as claimed in claim 1, is characterized in that: in described step (2), solvent is made up of propane diols, glycerine and honey.
5. the preparation method of electronic cigarette atomizing liquid as claimed in claim 4, is characterized in that: described solvent is uniformly mixed 30～50 minutes gained by propane diols, glycerine and honey.
6. the preparation method of the electronic cigarette atomizing liquid as described in claim 4 or 5, is characterized in that: in described solvent, the percent by volume of each component is: propane diols 80%, glycerine 15%, honey 5% or propane diols 15%, glycerine 80%, honey 5%.
7. the preparation method of electronic cigarette atomizing liquid as claimed in claim 1, is characterized in that: in described step (2), separator is negative-pressure vacuum separator; Filter in described step (2) in vacuum pressure is the negative-pressure vacuum separator of-0.08～-0.09Mpa and carry out.
8. the preparation method of electronic cigarette atomizing liquid as claimed in claim 1, it is characterized in that: in described step (3), the preparation method of coffee bean extract is: first coffee bean being pulverized is 30～90 object coffee bean powders, again coffee bean powder is dropped in the boiler of sandwich, add the ratio of 4～8 ml distilled waters according to every gram of coffee bean powder, distilled water is added in coffee bean powder to coffee soaking bean powder 40～90 minutes; Heating boiler to 120～130 DEG C, distillation extraction coffee bean powder 3～8 hours; Be under the condition of-0.08～-0.09MPa at vacuum pressure, filter extract by negative-pressure vacuum separator, reduced pressure concentration filtrate to proportion is 1.2～1.5, and gained medicinal extract is coffee bean extract.
9. the preparation method of electronic cigarette atomizing liquid as claimed in claim 1, is characterized in that: the speed stirring in described step (4) is 1400 revs/min, and the time being uniformly mixed is 45 minutes.
10. one kind adopts the electronic cigarette atomizing liquid that method prepares as claimed in claim 1.
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| CN104770865A (en) * | 2015-03-03 | 2015-07-15 | 华健 | Aromatic plant electronic atomization liquid and preparation method thereof |
| CN105154232A (en) * | 2015-09-15 | 2015-12-16 | 江苏锦宇环境工程有限公司 | Preparation method of tobacco flavor for refreshment |
| WO2015192834A3 (en) * | 2014-06-18 | 2016-04-14 | Klaus Hagen | Method for producing a consumable provided for evaporation |
| CN109588761A (en) * | 2019-01-18 | 2019-04-09 | 薪火高科(深圳)有限公司 | It is a kind of to have effects that relieving cough and reducing sputum tobacco juice for electronic smoke |
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|---|---|---|---|---|
| WO2015192834A3 (en) * | 2014-06-18 | 2016-04-14 | Klaus Hagen | Method for producing a consumable provided for evaporation |
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| CN104585883B (en) * | 2014-12-31 | 2018-01-16 | 广东金成生物科技工程有限公司 | A kind of atomized liquid containing Radix Angelicae Sinensis composition and preparation method thereof |
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| CN105154232A (en) * | 2015-09-15 | 2015-12-16 | 江苏锦宇环境工程有限公司 | Preparation method of tobacco flavor for refreshment |
| CN109588761A (en) * | 2019-01-18 | 2019-04-09 | 薪火高科(深圳)有限公司 | It is a kind of to have effects that relieving cough and reducing sputum tobacco juice for electronic smoke |
| CN110353300A (en) * | 2019-04-16 | 2019-10-22 | 深圳雾芯科技有限公司 | Resin face cream separation composite and preparation method thereof for aerosol device |
| CN113633014A (en) * | 2021-08-04 | 2021-11-12 | 深圳市真味生物科技有限公司 | Coffee-flavored refreshing electronic atomized liquid and preparation method thereof |
| CN113693265A (en) * | 2021-08-31 | 2021-11-26 | 深圳市真味生物科技有限公司 | Nut coffee electronic atomized liquid and preparation method thereof |
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