Summary of the invention
For solving the shortcoming and defect part of prior art, primary and foremost purpose of the present invention is to provide a kind of atomized liquid containing Radix Angelicae Sinensis composition.This atomized liquid does not add nicotine, and containing the functional component such as Chinese angelica volatile oil, organic acid, allow women ES can while progressively giving up smoking, regulating menstruation and activating blood, blood-enrich, improve the fitness of women.
Another object of the present invention is to the preparation method that the above-mentioned atomized liquid containing Radix Angelicae Sinensis composition is provided.
For achieving the above object, the present invention adopts following technical scheme:
An atomized liquid containing Radix Angelicae Sinensis composition, it comprises the component of following percentage by weight: 55-75% propane diols, 10-20% glycerine, 5-10% Radix Angelicae Sinensis composition and 5-15% distilled water; Described Radix Angelicae Sinensis composition is Chinese angelica volatile oil and eumenol, and above weight percentages of components sum is 100%.
Preferably, the described atomized liquid containing Radix Angelicae Sinensis composition comprises the component of following percentage by weight: 72% propane diols, 15% glycerine, 5% Radix Angelicae Sinensis composition and 8% distilled water.
Preferably, the described atomized liquid containing Radix Angelicae Sinensis composition comprises the component of following percentage by weight: 65% propane diols, 12% glycerine, 8% Radix Angelicae Sinensis composition and 15% distilled water.
Preferably, the described atomized liquid containing Radix Angelicae Sinensis composition comprises the component of following percentage by weight: 63% propane diols, 20% glycerine, 10% Radix Angelicae Sinensis composition and 7% distilled water.
The preparation method of the above-mentioned atomized liquid containing Radix Angelicae Sinensis composition, comprises the following steps:
(1) pulverized by Radix Angelicae Sinensis and cross 80 mesh sieves, adding the water of 12-14 times of Radix Angelicae Sinensis quality, lixiviate twice at the temperature of 40-60 DEG C, each each 1h, obtains volatile oil compositions and extract; Volatile oil compositions obtains Chinese angelica volatile oil through petroleum ether extraction and reduced pressure concentration, and extract obtains eumenol through reduced pressure concentration;
(2) Chinese angelica volatile oil obtained in step (1) and eumenol weight sum are counted the weight of Radix Angelicae Sinensis composition, take all the other component raw material according to the percentage by weight of each component; The eumenol that step (1) is obtained is added distilled water dissolve, obtain By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the Chinese angelica volatile oil that step (1) is obtained again, emulsifying 5-10min under the rotating speed of 3000-4000rpm, obtain the described atomized liquid containing Radix Angelicae Sinensis composition.
Preferably, the emulsifying temperature described in step (2) is 25-30 DEG C.
Compared with prior art, the present invention has the following advantages and beneficial effect:
(1) traditional electronic atomized liquid is the composition that skims the cream off milk from tobacco, is dissolved in the solvent of food-grade, adds a small amount of essence and flavoring agent simultaneously.The Essence of the multiple green plants of extracting, is inhaled in body the unique effects having and remove the cigarette poison rested in human body, remove craving for tobacco.But, still containing carcinogens such as nicotines in atomized liquid, the health of harmful to human.Smoking population has caused the infringement of its lung in long-term smoking process, and immunologic function declines, and the present invention adds medicinal herb components and substitutes tobacco extract in conditional electronic cigarette in electronic atomized liquid, and the effect that both can reach smoking cessation also has health-care efficacy.
(2) Radix Angelicae Sinensis of the present invention adopts relatively mild Hot water extraction to extract, and can ensure Radix Angelicae Sinensis forulic acid, polysaccharide, volatilization wet goods composition all extracts, volatile oil compositions adopts special extraction concentration technique, ensures that active component is not damaged.
Chinese angelica volatile oil composition can not only reduce blood pressure, improve myocardial ischemia, anti-arrhythmia cordis, have and relieving asthma, suppress central nervous system, improve the pharmacological action such as body's immunity and anti-inflammatory and antalgic, also there is aromatic smell, the present invention replaces tobacco elite by adding Chinese angelica volatile oil, obtained atomized liquid is effective especially to women smoker, and having enriches blood invigorates blood circulation, menstruction regulating and pain relieving, the health-care efficacy that relaxes bowel, can make user while quitting tobacco dependency gradually, absorb Radix Angelicae Sinensis medicinal ingredient, improve physiological function, strengthen fitness.
Detailed description of the invention
Below in conjunction with embodiment and accompanying drawing, the present invention is described in further detail, but embodiments of the present invention are not limited thereto.
The invention discloses a kind of atomized liquid containing Radix Angelicae Sinensis composition, comprise the component of following percentage by weight: 55-75% propane diols, 10-20% glycerine, 5-10% Radix Angelicae Sinensis composition and 5-15% distilled water; Described Radix Angelicae Sinensis composition comprises Chinese angelica volatile oil and eumenol.The preparation process that should contain the atomized liquid of Radix Angelicae Sinensis composition is as follows:
(1) Radix Angelicae Sinensis is pulverized 80 mesh sieves, added the water of the amount of 12-14 times of Radix Angelicae Sinensis quality, lixiviate twice, each 1h, obtain volatile oil compositions and extract; Volatile oil compositions obtains Chinese angelica volatile oil through oily ether extraction and reduced pressure concentration, and extract obtains eumenol through reduced pressure concentration;
(2) Chinese angelica volatile oil obtained in step (1) and eumenol weight sum are counted the weight of Radix Angelicae Sinensis composition, take all the other component raw material according to the percentage by weight of each component; The eumenol distilled water that step (1) is obtained dissolves, and obtains By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the Chinese angelica volatile oil that step (1) is obtained again, emulsifying 5-10min under the rotating speed of 3000-4000rpm, obtain the described atomized liquid containing Radix Angelicae Sinensis composition.
Above-mentioned preparation process is after determining rational formula, is mainly realized by abstraction technique and emulsifying technology.Make electronic atomized liquid have medical value and reach best atomizing effect, suitable Radix Angelicae Sinensis extraction process must be selected and prepare good properties and stable atomized liquid, its each composition especially Chinese angelica volatile oil and aqueous phase can be uniformly distributed, without effects such as composition delays during atomization.Prepare good properties and stable electronic atomized liquid, need to solve the difficult problem in stirring and emulsifying hybrid technology, design optimal parameter, wherein temperature, emulsification times, mixing speed all play vital effect.
Found by test, after using emulsifying to stir, obtained atomized liquid water-oil phase is uniformly dispersed, and can keep stable, and two-phase is not easy again to be separated.This system water oil is liquid, at room temperature can reach good emulsifying effectiveness, and higher than this temperature (40-70 DEG C) emulsifying effectiveness without work change, the energy that high temperature consumes is more, from cost-saving angle, emulsifying temperature is set to 25-30 DEG C.
Find in test that the water-oil phase dispersion effect of the obtained atomized liquid of high rotating speed (4000-6000rpm) is good, but the foam produced during emulsify at a high speed is more, the stirring at low speed of 3000rpm can cancellation bubble.Rotating speed too small (1000-2000rpm) shearing force is not enough to make the two-phase of atomized liquid to complete dispersion even, fine and smoothly.
Emulsification times also can impact the quality of atomized liquid, and because in atomized liquid formula of the present invention, the component content of volatile oil is less, viscosity is lower, can complete dispersion within a short period of time.5-10min, the few oil slick of atomized liquid foam is few, emulsion-stabilizing.Be less than 3min, because the time is too short, do not reach the effect of stable dispersion.
Embodiment 1
A preparation method for atomized liquid containing Radix Angelicae Sinensis composition, as illustrated in fig. 1 and 2, comprises the following steps:
(1) 100g Radix Angelicae Sinensis was pulverized 80 mesh sieves, and added the water of the amount of 12 times of Radix Angelicae Sinensis quality, 55 DEG C of lixiviates twice, each 1h, obtains volatile oil compositions and extract; Volatile oil compositions obtains Chinese angelica volatile oil through oily ether extraction and reduced pressure concentration, and extract obtains eumenol through reduced pressure concentration;
(2) Chinese angelica volatile oil obtained in step (1) and eumenol weight sum are counted the weight of Radix Angelicae Sinensis composition, take all the other component raw material according to the percentage by weight of each component; The eumenol distilled water that step (1) is obtained dissolves, and obtains By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the Chinese angelica volatile oil that step (1) is obtained again, with vacuum homogeneous emulsifying machine, emulsifying 5min under the rotating speed of 3000rpm, emulsifying temperature is normal temperature (25-30 DEG C), sterilizing after bottling capping, lamp inspection, obtain the described atomized liquid containing Radix Angelicae Sinensis composition;
Wherein the above-mentioned atomized liquid containing Radix Angelicae Sinensis composition comprises the component of following percentage by weight: 72% propane diols, 15% glycerine, 5% Radix Angelicae Sinensis composition and 8% distilled water; Described Radix Angelicae Sinensis composition is Chinese angelica volatile oil obtained in step (1) and eumenol.
In this embodiment, Radix Angelicae Sinensis component ratio is less than normal, and smog is dense, is applicable to the crowd that just given up smoking.
Embodiment 2
A preparation method for atomized liquid containing Radix Angelicae Sinensis composition, comprises the following steps:
(1) Radix Angelicae Sinensis was pulverized 80 mesh sieves, and added the water of the amount of 14 times of Radix Angelicae Sinensis quality, 50 DEG C of lixiviates twice, each 1h, obtains volatile oil compositions and extract; Volatile oil compositions obtains Chinese angelica volatile oil through oily ether extraction and reduced pressure concentration, and extract obtains eumenol through reduced pressure concentration;
(2) Chinese angelica volatile oil obtained in step (1) and eumenol weight sum are counted the weight of Radix Angelicae Sinensis composition, take all the other component raw material according to the percentage by weight of each component; The eumenol that step (1) is obtained is added distilled water dissolve, obtain By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the Chinese angelica volatile oil that step (1) is obtained again, with vacuum homogeneous emulsifying machine, emulsifying 5min under the rotating speed of 4000rpm, emulsifying temperature is normal temperature (25-30 DEG C), sterilizing after bottling capping, lamp inspection, obtain the described atomized liquid containing Radix Angelicae Sinensis composition;
Wherein the above-mentioned atomized liquid containing Radix Angelicae Sinensis composition, comprises the component of following percentage by weight: 65% propane diols, 12% glycerine, 8% Radix Angelicae Sinensis composition and 15% distilled water; Described Radix Angelicae Sinensis composition is Chinese angelica volatile oil obtained in step (1) and eumenol.
In this embodiment, Radix Angelicae Sinensis component ratio is moderate, can play a role in health care.
Embodiment 3
A preparation method for atomized liquid containing Radix Angelicae Sinensis composition, comprises the following steps:
(1) Radix Angelicae Sinensis was pulverized 80 mesh sieves, and added the water of the amount of 14 times of Radix Angelicae Sinensis quality, 55 DEG C of lixiviates twice, each 1h, obtains volatile oil compositions and extract; Volatile oil compositions obtains Chinese angelica volatile oil through oily ether extraction and reduced pressure concentration, and extract obtains eumenol through reduced pressure concentration;
(2) Chinese angelica volatile oil obtained in step (1) and eumenol weight sum are counted the weight of Radix Angelicae Sinensis composition, take all the other component raw material according to the percentage by weight of each component; The eumenol that step (1) is obtained is added distilled water dissolve, obtain By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the Chinese angelica volatile oil that step (1) is obtained again, with vacuum homogeneous emulsifying machine, emulsifying 10min under the rotating speed of 3000rpm, emulsifying temperature is normal temperature (25-30 DEG C), sterilizing after bottling capping, lamp inspection, obtain the described atomized liquid containing Radix Angelicae Sinensis composition;
Wherein the above-mentioned atomized liquid containing Radix Angelicae Sinensis composition, comprises the component of following percentage by weight: 63% propane diols, 20% glycerine, 10% Radix Angelicae Sinensis composition and 7% distilled water; Described Radix Angelicae Sinensis composition is Chinese angelica volatile oil obtained in step (1) and eumenol.
In this embodiment, Radix Angelicae Sinensis medicinal ingredient ratio is higher, and health-care effect is obvious and smog is dense.
For verifying smoking cessation effect and the health-care effect of atomized liquid of the present invention, test after adopting the atomized liquid formula in embodiment 3 to make electronic cigarette, 100 routine female smokers, all have the ill symptomses such as sallow complexion, anaemia, the deficiency of vital energy, irregular menstruation.5ml atomized liquid is put into electronic cigarette atomizing inhalator, sucks 10 every day, within 2 months, draw 80ml altogether.Test effect, 89% craving for tobacco significantly declines, and the symptom of 52% insufficiency of vital energy and blood, sallow complexion all makes moderate progress, and illustrates that atomized liquid of the present invention has remarkable result to smoking cessation, has some improvement to the anaemia deficiency of vital energy of women simultaneously.
Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not restricted to the described embodiments; change, the modification done under other any does not deviate from Spirit Essence of the present invention and principle, substitute, combine, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.