CN103564647A - Preparation method of traditional Chinese medicine spices for tobaccos - Google Patents
Preparation method of traditional Chinese medicine spices for tobaccos Download PDFInfo
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Abstract
The invention discloses a preparation method of traditional Chinese medicine spices for tobaccos. The preparation method includes the following steps: 1), taking tangerine peels, scutellaria baicalensis, radix ophiopogonis, rehmannia, jasmine, semen lepidii, perilaseed and liquorice; continuously extracting 2-4 times by using a solvent, combining extracting solutions, concentrating the extracting solutions into a concentrated solution, recycling volatile oil, and combining the concentrated solution with the volatile oil to obtain a main spice agent; 2), taking vanillin, cananga oil, ethyl cinnamate, leaf alcohol, trichloroacetic acid methyl benzene methyl ester, sandalwood oil, ethanol and propylene glycol, and uniformly mixing to obtain a surface spice agent; 3), uniformly mixing the main spice agent with the surface spice agent to obtain the traditional Chinese medicine spices. The traditional Chinese medicine spices prepared by the method have effect of clearing heat and decreasing internal heat and freeing lung and relieving asthma; after the traditional Chinese medicine spices are added into the tobaccos, aroma quantity, aroma quality and harmony of the tobaccos can be richened and improved, and strength, stimulation and offensive odor can be reduced.
Description
Technical field
The present invention relates to tobacco aromatics using technical field, be specifically related to the preparation method of Chinese medicine spices for a kind of cigarette.
Background technology
China is tobacco production and consumption big country, and the annual tobacco consuming accounts for the more than 1/3 of world's total sales volume.Approximately there is the estimation of 300,000,000 thickness Min,Er Ju China Preventive Medicial Science Institute in China, and China also has the passive second-hand-cigarette of sucking of people more than 400,000,000.Tobacco, when meeting people's hobby, has also produced serious infringement to human body.The most directly injury that smoking causes is the spread effect to respiratory system, and often contact can cause cough, throat discomfort etc., and smoking all the year round may cause lung cancer.Harm smoker being produced for reducing cigarette, by producing cigarette with reduced toxicity, reducing cigarette is the development trend of World tobacco industry to the mankind's murder by poisoning.State Tobacco Monopoly Bureau in 2003 have proposed the strategic problem of development Chinese-style cigarette, formulated < < Chinese cigarette development in science and technology outline > >, with reducing tar and reducing harm, improve quality, economize on resources and serve as theme, actively develop the research work of Chinese-style cigarette.Present stage, makes full use of traditional knowledge of TCM, and in conjunction with modern advanced scientific research condition, adds Chinese herbal medicine to become one of effective way reducing cigarette harm in cigarette.This relates generally to two types: the one, in former cigarette, add Chinese herbal medicine or its extract; The 2nd, with Chinese herbal medicine, replace traditional tobacco leaf.But the Chinese-style cigarette much developing, when reaching the harm of reduction cigarette, has also brought such as problems such as the decline of cigarette quality, fragrance weaken.
Summary of the invention
The technical problem to be solved in the present invention is to provide the preparation method of Chinese medicine spices for a kind of cigarette, the effect that the cigarette making has heat-clearing and fire-reducing, freeings lung and relieving asthma with Chinese medicine spices, add perfume quantity, fragrance matter and the harmony that in tobacco product, can enrich and improve tobacco product to, reduce strength, stimulation and assorted gas.
For solving the problems of the technologies described above, the present invention by the following technical solutions:
A preparation method for Chinese medicine spices for cigarette, comprises the following steps:
1) prepare type-odor:
Take the type-odor raw material of following weight parts: 10~14 parts of dried orange peels, 10~14 parts of the roots of large-flowered skullcap, 4~8 parts of the tubers of dwarf lilyturf, 4~8 parts of glutinous rehmannia, 22~26 parts of cape jasmines, 10~14 parts of lepidium seeds, 10~14 parts of perillaseeds, 2~6 parts, Radix Glycyrrhizae; Then with the solvent of 8000~12000 weight portions, extract 2~4 times continuously, each 30~90 minutes, merge extract, then be condensed into the concentrate of 280~320 weight portions, and reclaim the volatile oil of 90~110 weight portions, and concentrate and volatile oil are merged, obtain type-odor;
2) preparation table pastil:
Take the table pastil raw material of following weight parts: 0.3~0.6 part of vanillic aldehyde, 0.12~0.17 part of cananga oil, 0.08~0.12 part of ethyl cinnamate, 0.05~0.07 part of leaf-alcohol, 0.08~0.12 part of trichloroacetic acid methylbenzene methyl esters, 0.08~0.12 part of sandalwood oil, 42~47 parts of ethanol, 42~47 parts of propane diols; Table pastil raw material is mixed, obtain table pastil;
3) type-odor and the step 2 that step 1) are made) the table pastil that makes mixes, and obtains described cigarette Chinese medicine spices.
Preferably, the weight portion of described type-odor raw material is: 12 parts of dried orange peels, 12 parts of the roots of large-flowered skullcap, 6 parts of the tubers of dwarf lilyturf, 6 parts of glutinous rehmannia, 24 parts of cape jasmines, 12 parts of lepidium seeds, 12 parts of perillaseeds, 4 parts, Radix Glycyrrhizae.
Preferably, the weight portion of described table pastil raw material is: 0.45 part of vanillic aldehyde, 0.15 part of cananga oil, 0.1 part of ethyl cinnamate, 0.06 part of leaf-alcohol, 0.1 part of trichloroacetic acid methylbenzene methyl esters, 0.1 part of sandalwood oil, 45 parts of ethanol, 45 parts of propane diols.
Described type-odor raw material is to be undertaken by traditional solvent extraction process, and described solvent can be water, ethanolic solution or propylene glycol solution.Preferably, described solvent is water.During with solvent extraction medicinal herb components, conventionally adopt infusion process, percolation, decocting method, reflux extraction etc.The preferred reflux extraction of the present invention.
Each raw material synergy of type-odor of the present invention, the effect of there is heat-clearing and fire-reducing, freeinging lung and relieving asthma, its extract adds in tobacco product, can reduce and stimulate and harm reduction.
Wherein, dried orange peel: warm in nature, taste is pungent, bitter; Enter the spleen channel, stomach warp, lung channel; Regulating qi-flowing for strengthening spleen, in tune, eliminating dampness, reduces phlegm; Cure mainly the abdominal fullness and distention of the taste stagnation of the circulation of vital energy or pain, indigestion, abdominal distension uncomfortable in chest, indigestion and loss of appetite loose stool in wet turbid resistance, the wet cough and asthma of stopping up lung of phlegm.
The root of large-flowered skullcap: cold in nature, bitter; Return lung, courage, spleen, large intestine, small intestinl channel; Heat-clearing and damp-drying drug, purging intense heat and detonicating, hemostasis, antiabortive, hypotensive; For damp-warm syndrome, the heat temperature evil of vomitting uncomfortable in chest, damp and hot ruffian is full, rushes down dysentery, jaundice, and cough with lung heat, high hot polydipsia, blood-head is told nosebleed, carbuncle sore tumefacting virus, fetal irritability.
The tuber of dwarf lilyturf: sweet, the micro-hardship of taste, cold nature; Nourishing Yin and promoting production of body fluid, moistening lung clears away heart-fire; For dryness of the lung dry cough, deficiency of Yin consumptive disease is coughed, larynx numbness pharyngalgia, and Tianjin wound is thirsty, and interior heat is quenched one's thirst, vexed insomnia, the dry constipation of intestines.
Glutinous rehmannia: cool in nature, taste is sweet; Enter the heart, liver, spleen, lung four warps; Clearing heat and promoting fluid, enriching yin, nourishes blood; For fever due to yin deficiency, quench one's thirst, spit blood, bleeding from five sense organs or subcutaneous tissue, metrorrhagia, irregular menstruation, fetal irritability, the moon is hindered constipation.
Cape jasmine: cold in nature, bitter; Enter the heart, liver, lung, stomach warp; Heat-clearing, purging intense heat, cool blood; Control pyreticosis restlessness of asrhenia type and insomnia, jaundice, gonorrhoea, quenches one's thirst, hot eyes, pharyngalgia, spits blood, bleeding from five sense organs or subcutaneous tissue, bloody flux, hematuria, pathopyretic ulcer, sprains and swells and ache.
Lepidium seed: cold in nature, taste is pungent, bitter; Enter lung, the heart, liver, stomach, urinary bladder channel; Purging the lung of pathogenic fire sending down abnormally ascending, eliminating phlegm and relieving asthma, inducing diuresis for removing edema, lets out by heresy; Cure mainly sputum and stop up the dyspnea and cough with excessive sputum of lung, lung carbuncle, oedema, chest abdomen ponding, difficult urination, chronic cor pulmonale, breathing heavily of heart failure is swollen, scrofula tuberculosis.
Perillaseed: warm in nature, taste is pungent; Return lung channel; Sending down abnormally ascending dissolving phlegm, relievings asthma, ease constipation; For phlegm, stop up the circulation of vital energy in the wrong direction, cough and asthma, the dry constipation of intestines.
Radix Glycyrrhizae: property is flat, and taste is sweet; Return 12 warps; Have removing toxic substances, eliminate the phlegm, pain relieving, spasmolysis be so that the pharmacological action such as anticancer; Invigorate the spleen and benefit qi, relieving cough and moistening lung, emergency removing toxic substances, is in harmonious proportion hundred medicines.
Each raw material of type-odor of the present invention also contains the various fragrant chemical compositions that cause, and various in its extract cause fragrant chemical composition, and each raw material of table pastil coordinates mutually, can enrich and improve perfume quantity, fragrance matter and the harmony of tobacco product.
Wherein, dried orange peel: contain multiple volatile oil, as citrene, australene, γ-terpinene, beta-myrcene, add in tobacco and can improve fragrance matter and perfume quantity.
The root of large-flowered skullcap: main component is scutelloside, is subject to discharge a large amount of fragrance matters after thermal cracking; Scutelloside has good antioxidation, adds in tobacco and can reduce the free-radical contents in cigarette, improves fragrance matter.
The tuber of dwarf lilyturf: its chemical composition be mainly ophiopogonin, the tuber of dwarf lilyturf ketone, methyl ophiopogonone and dihydro ophiopogonone, belong to the herbal that has very much charm.
Glutinous rehmannia: the 5 hydroxymethyl furfural containing is a kind of good spices, cream perfume and the powder that can give tobacco uniqueness are fragrant.
Cape jasmine: contain multiple volatile oil, as benzyl acetate, methyl benzoate, flores aurantii tree alcohol etc., there is pleasant delicate fragrance.
Lepidium seed: contain parahydroxyben-zaldehyde, isovanillic acid, syringic acid etc., can increase the solid sense of tobacco product.
Perillaseed: contain carypohyllene, perillaldehyde, α-carypohyllene, citrene, face amino benzoic Acid agalloch eaglewood ester etc., can increase the rich of flue gas.
Radix Glycyrrhizae: its main component is liquiritin and glycyrrhizic acid, has the effect of the Hui Tian that promotes the production of body fluid.
A kind of cigarette of the present invention has the following advantages by the preparation method of Chinese medicine spices:
1, each taste Chinese medicine of picking of raw material of the present invention, the effect of there is heat-clearing and fire-reducing, freeinging lung and relieving asthma, its extract adds in tobacco product, can in and the harm of nicotine to human body, suitably reduce strength, stimulation and the assorted gas of tobacco product;
2, the selected various Chinese herbal medicines that are rich in aroma component of the present invention are as type-odor raw material, and these aroma components and mutually coordinating as the essence and flavoring agent of table pastil raw material are abundant and improved perfume quantity, fragrance matter and the harmony of tobacco product;
3, preparation method of the present invention is simple and easy to control, and raw material sources are extensive, is suitable for promoting.
The specific embodiment
With embodiment, be described further below, but the present invention is not limited to these embodiment.
Embodiment 1
Cigarette is prepared as follows with Chinese medicine spices:
1) prepare type-odor:
Take the type-odor raw material of following weight parts: 12 parts of dried orange peels, 12 parts of the roots of large-flowered skullcap, 6 parts of the tubers of dwarf lilyturf, 6 parts of glutinous rehmannia, 24 parts of cape jasmines, 12 parts of lepidium seeds, 12 parts of perillaseeds, 4 parts, Radix Glycyrrhizae; Then with the water of 10000 weight portions, extract 3 times continuously, each 50 minutes, merge extract, be then condensed into the concentrate of 300 weight portions, and reclaim the volatile oil of 100 weight portions, concentrate and volatile oil are merged, obtain type-odor;
2) preparation table pastil:
Take the table pastil raw material of following weight parts: 0.45 part of vanillic aldehyde, 0.15 part of cananga oil, 0.1 part of ethyl cinnamate, 0.06 part of leaf-alcohol, 0.1 part of trichloroacetic acid methylbenzene methyl esters, 0.1 part of sandalwood oil, 45 parts of ethanol, 45 parts of propane diols; Table pastil raw material is mixed, obtain table pastil;
3) type-odor and the step 2 that step 1) are made) the table pastil that makes mixes, and obtains described cigarette Chinese medicine spices.
The cigarette making is added in reconstituted tobacoo according to 0.05% of tobacco product gross weight with Chinese medicine spices, in climatic chamber, balance is 48 hours, then make cigarette, finally by perfumer, adopt the blind method of commenting to carry out sensory evaluating smoking's evaluation, consequently: cigarette fragrance is fine and smooth, thoroughly send out, abundant, have a sweet sense; Fragrance is abundant, coordination, slightly assorted gas; Strength medium (with thin slice); Pleasant impression is comfortable, clean, slightly Hui Tian promotes the production of body fluid.
Embodiment 2
Cigarette is prepared as follows with Chinese medicine spices:
1) prepare type-odor:
Take the type-odor raw material of following weight parts: 10 parts of dried orange peels, 10 parts of the roots of large-flowered skullcap, 4 parts of the tubers of dwarf lilyturf, 4 parts of glutinous rehmannia, 26 parts of cape jasmines, 14 parts of lepidium seeds, 14 parts of perillaseeds, 6 parts, Radix Glycyrrhizae; Then with the water of 12000 weight portions, extract 4 times continuously, each 90 minutes, merge extract, be then condensed into the concentrate of 280 weight portions, and reclaim the volatile oil of 90 weight portions, concentrate and volatile oil are merged, obtain type-odor;
2) preparation table pastil:
Take the table pastil raw material of following weight parts: 0.6 part of vanillic aldehyde, 0.17 part of cananga oil, 0.12 part of ethyl cinnamate, 0.07 part of leaf-alcohol, 0.08 part of trichloroacetic acid methylbenzene methyl esters, 0.08 part of sandalwood oil, 42 parts of ethanol, 42 parts of propane diols; Table pastil raw material is mixed, obtain table pastil;
3) type-odor and the step 2 that step 1) are made) the table pastil that makes mixes, and obtains described cigarette Chinese medicine spices.
The cigarette making is added in reconstituted tobacoo according to 0.05% of tobacco product gross weight with Chinese medicine spices, in climatic chamber, balance is 48 hours, then make cigarette, finally by perfumer, adopt the blind method of commenting to carry out sensory evaluating smoking's evaluation, consequently: cigarette fragrance is fine and smooth, thoroughly send out, abundant, have a sweet sense; Fragrance is abundant, coordination, slightly assorted gas; Strength medium (with thin slice); Pleasant impression is comfortable, clean, slightly Hui Tian promotes the production of body fluid.
Embodiment 3
Cigarette is prepared as follows with Chinese medicine spices:
1) prepare type-odor:
Take the type-odor raw material of following weight parts: 14 parts of dried orange peels, 14 parts of the roots of large-flowered skullcap, 8 parts of the tubers of dwarf lilyturf, 8 parts of glutinous rehmannia, 24 parts of cape jasmines, 12 parts of lepidium seeds, 12 parts of perillaseeds, 4 parts, Radix Glycyrrhizae; Then with 95% ethanolic solution of 8000 weight portions, extract 2 times continuously, each 30 minutes, merge extract, be then condensed into the concentrate of 300 weight portions, and reclaim the volatile oil of 100 weight portions, concentrate and volatile oil are merged, obtain type-odor;
2) preparation table pastil:
Take the table pastil raw material of following weight parts: 0.3 part of vanillic aldehyde, 0.12 part of cananga oil, 0.08 part of ethyl cinnamate, 0.05 part of leaf-alcohol, 0.08 part of trichloroacetic acid methylbenzene methyl esters, 0.1 part of sandalwood oil, 45 parts of ethanol, 45 parts of propane diols; Table pastil raw material is mixed, obtain table pastil;
3) type-odor and the step 2 that step 1) are made) the table pastil that makes mixes, and obtains described cigarette Chinese medicine spices.
The cigarette making is added in reconstituted tobacoo according to 0.05% of tobacco product gross weight with Chinese medicine spices, in climatic chamber, balance is 48 hours, then make cigarette, finally by perfumer, adopt the blind method of commenting to carry out sensory evaluating smoking's evaluation, consequently: cigarette fragrance is fine and smooth, thoroughly send out, abundant, have a sweet sense; Fragrance is abundant, coordination, slightly assorted gas; Strength medium (with thin slice); Pleasant impression is comfortable, clean, slightly Hui Tian promotes the production of body fluid.
Embodiment 4
Cigarette is prepared as follows with Chinese medicine spices:
1) prepare type-odor:
Take the type-odor raw material of following weight parts: 12 parts of dried orange peels, 12 parts of the roots of large-flowered skullcap, 6 parts of the tubers of dwarf lilyturf, 6 parts of glutinous rehmannia, 22 parts of cape jasmines, 10 parts of lepidium seeds, 10 parts of perillaseeds, 2 parts, Radix Glycyrrhizae; Then with the propylene glycol solution of 10000 weight portions, extract 3 times continuously, each 60 minutes, merge extract, be then condensed into the concentrate of 320 weight portions, and reclaim the volatile oil of 110 weight portions, concentrate and volatile oil are merged, obtain type-odor;
2) preparation table pastil:
Take the table pastil raw material of following weight parts: 0.6 part of vanillic aldehyde, 0.17 part of cananga oil, 0.12 part of ethyl cinnamate, 0.07 part of leaf-alcohol, 0.1 part of trichloroacetic acid methylbenzene methyl esters, 0.1 part of sandalwood oil, 45 parts of ethanol, 45 parts of propane diols; Table pastil raw material is mixed, obtain table pastil;
3) type-odor and the step 2 that step 1) are made) the table pastil that makes mixes, and obtains described cigarette Chinese medicine spices.
The cigarette making is added in reconstituted tobacoo according to 0.05% of tobacco product gross weight with Chinese medicine spices, in climatic chamber, balance is 48 hours, then make cigarette, finally by perfumer, adopt the blind method of commenting to carry out sensory evaluating smoking's evaluation, consequently: cigarette fragrance is fine and smooth, thoroughly send out, abundant, have a sweet sense; Fragrance is abundant, coordination, slightly assorted gas; Strength medium (with thin slice); Pleasant impression is comfortable, clean, slightly Hui Tian promotes the production of body fluid.
Claims (4)
1. a preparation method for Chinese medicine spices for cigarette, is characterized in that: comprise the following steps:
1) prepare type-odor:
Take the type-odor raw material of following weight parts: 10~14 parts of dried orange peels, 10~14 parts of the roots of large-flowered skullcap, 4~8 parts of the tubers of dwarf lilyturf, 4~8 parts of glutinous rehmannia, 22~26 parts of cape jasmines, 10~14 parts of lepidium seeds, 10~14 parts of perillaseeds, 2~6 parts, Radix Glycyrrhizae; Then with the solvent of 8000~12000 weight portions, extract 2~4 times continuously, each 30~90 minutes, merge extract, then be condensed into the concentrate of 280~320 weight portions, and reclaim the volatile oil of 90~110 weight portions, and concentrate and volatile oil are merged, obtain type-odor;
2) preparation table pastil:
Take the table pastil raw material of following weight parts: 0.3~0.6 part of vanillic aldehyde, 0.12~0.17 part of cananga oil, 0.08~0.12 part of ethyl cinnamate, 0.05~0.07 part of leaf-alcohol, 0.08~0.12 part of trichloroacetic acid methylbenzene methyl esters, 0.08~0.12 part of sandalwood oil, 42~47 parts of ethanol, 42~47 parts of propane diols; Table pastil raw material is mixed, obtain table pastil;
3) type-odor and the step 2 that step 1) are made) the table pastil that makes mixes, and obtains described cigarette Chinese medicine spices.
2. the preparation method of Chinese medicine spices for cigarette according to claim 1, is characterized in that: the weight portion of described type-odor raw material is: 12 parts of dried orange peels, 12 parts of the roots of large-flowered skullcap, 6 parts of the tubers of dwarf lilyturf, 6 parts of glutinous rehmannia, 24 parts of cape jasmines, 12 parts of lepidium seeds, 12 parts of perillaseeds, 4 parts, Radix Glycyrrhizae.
3. the preparation method of Chinese medicine spices for cigarette according to claim 1, is characterized in that: the weight portion of described table pastil raw material is: 0.45 part of vanillic aldehyde, 0.15 part of cananga oil, 0.1 part of ethyl cinnamate, 0.06 part of leaf-alcohol, 0.1 part of trichloroacetic acid methylbenzene methyl esters, 0.1 part of sandalwood oil, 45 parts of ethanol, 45 parts of propane diols.
4. the preparation method of Chinese medicine spices for cigarette according to claim 1, is characterized in that: described solvent is water, ethanolic solution or propylene glycol solution.
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CN104664589A (en) * | 2014-12-31 | 2015-06-03 | 广东金成生物科技工程有限公司 | Nebulized liquid containing Korean ginseng and preparing method thereof |
CN104664586A (en) * | 2014-12-31 | 2015-06-03 | 广东金成生物科技工程有限公司 | Nebulized liquid containing Astragalus root and preparing method thereof |
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CN104664588A (en) * | 2014-12-31 | 2015-06-03 | 广东金成生物科技工程有限公司 | Nebulized liquid containing ginseng and preparing method thereof |
CN104664587A (en) * | 2014-12-31 | 2015-06-03 | 广东金成生物科技工程有限公司 | Nebulized liquid containing American ginseng and preparing method thereof |
CN104664589A (en) * | 2014-12-31 | 2015-06-03 | 广东金成生物科技工程有限公司 | Nebulized liquid containing Korean ginseng and preparing method thereof |
CN104664586A (en) * | 2014-12-31 | 2015-06-03 | 广东金成生物科技工程有限公司 | Nebulized liquid containing Astragalus root and preparing method thereof |
CN104664589B (en) * | 2014-12-31 | 2016-09-21 | 广东金成生物科技工程有限公司 | A kind of atomized liquid containing Korean Ginseng composition and preparation method thereof |
CN104664586B (en) * | 2014-12-31 | 2016-11-30 | 广东金成生物科技工程有限公司 | A kind of atomized liquid containing astragalus root components and preparation method thereof |
CN104585883B (en) * | 2014-12-31 | 2018-01-16 | 广东金成生物科技工程有限公司 | A kind of atomized liquid containing Radix Angelicae Sinensis composition and preparation method thereof |
CN106281685A (en) * | 2016-08-30 | 2017-01-04 | 湖北中烟工业有限责任公司 | A kind of Cortex Cinnamomi odor type cigar flavouring essence for tobacco and its preparation method and application |
CN110655985A (en) * | 2019-08-23 | 2020-01-07 | 广东中烟工业有限责任公司 | Spices with Chinese flue-cured tobacco characteristic aroma and heating non-combustible cigarette prepared from spices |
CN115058291A (en) * | 2022-06-08 | 2022-09-16 | 吉林烟草工业有限责任公司 | Composite plant volatile oil, preparation method thereof and tobacco product |
CN115058291B (en) * | 2022-06-08 | 2024-07-12 | 吉林烟草工业有限责任公司 | Composite plant volatile oil, preparation method thereof and tobacco product |
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Application publication date: 20140212 |