CN104664588A - Nebulized liquid containing ginseng and preparing method thereof - Google Patents
Nebulized liquid containing ginseng and preparing method thereof Download PDFInfo
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- CN104664588A CN104664588A CN201410855137.5A CN201410855137A CN104664588A CN 104664588 A CN104664588 A CN 104664588A CN 201410855137 A CN201410855137 A CN 201410855137A CN 104664588 A CN104664588 A CN 104664588A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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Abstract
The invention discloses nebulized liquid containing ginseng and a preparing method thereof. The nebulized liquid comprises, by weight, 55% to 75% of propylene glycol, 10% to 20% of glycerol, 5% to 10% of ginseng and 5% to 15% of distilled water. The nebulized liquid has the advantages that a formula of the nebulized liquid has no tobacco extract and nicotine but the herbal medicinal ginseng; a ratio of the propylene glycol, the glycerol and water is appropriate, mist of the nebulized liquid is thick, and no stimulus is caused to the throat; no flavors and fragrances but essential oil of the ginseng is added, and no second-hand smoke damage is caused; ginsenoside, as main effective ingredient in the ginseng can be nebulized and inhaled to produce thick fragrance and efficacy, thus achieving health functions such as tonifying qi, restoring the pulse to relieve desertion, tonifying the spleen and lung, regenerating bodily fluids to relieve thirst, tranquilizing the mind and promoting the intelligence.
Description
Technical field
The invention belongs to electronic cigarette field, be specifically related to a kind of atomized liquid containing constituent of ginseng and preparation method thereof.
Background technology
Along with the understanding of people to cigarette harm is more and more deep, smokers urgently wish to occur that cigarette substitute is to save their health.Wherein, electronic cigarette as one of cigarette substitute, smoking cessation successful.Healthy electronic cigarette containing tar, without harmful substances such as carbon monoxide, nitrogen dioxide, arsenic, lead, mercury, can not avoid " second-hand-cigarette " to the harm of surrounding population.Through the development of several generations, current electronic cigarette atomizing liquid taste can realize variation, meets the demand that different smoker selects different taste.But electronic cigarette product on the market is mainly still given up material and is added in atomized liquid formula using tobacco extract, nicotine etc. as craving for tobacco, really cannot meet the demand of consumer health's smoking cessation, especially can not meet the treatment of smoking cessation demand of the smoker suffering from some special illness, limit to the envelop of function of electronic cigarette product.Electronic cigarette produce market has a high potential, electronics atomized liquid function singleness on market, especially rare with the product that traditional Chinese medicine ingredients is tasty.
Chinese herbal medicine is the rarity of the Chinese nation, the good reputation that ginseng has since ancient times " kings of hundred grass ", is more described as the superfine product of " enriching yin is mended raw, strengthens the body resistance to consolidate the constitution " by oriental medicine circle.Ginsenoside is the main composition of ginseng, has and reinforces vital energy, and multiple arteries and veins takes off admittedly, reinforces the spleen to benefit the lung, promotes the production of body fluid to quench thirst, the health cares such as intelligence development of calming the nerves.
Summary of the invention
For solving the shortcoming and defect part of prior art, primary and foremost purpose of the present invention is to provide a kind of atomized liquid containing constituent of ginseng.This atomized liquid contains ginsenoside, and nicotine content is zero, allows ES while progressively giving up smoking, can absorb ginsenoside, regulates body immunity, improves the various angiocardiopathy such as diabetes, hypertension.
Another object of the present invention is to the preparation method that the above-mentioned atomized liquid containing constituent of ginseng is provided.
For achieving the above object, the present invention adopts following technical scheme:
An atomized liquid containing constituent of ginseng, comprises the component of following percentage by weight: 55-75% propane diols, 10-20% glycerine, 5-10% constituent of ginseng and 5-15% distilled water; Described constituent of ginseng is ginseng essential oil and Radix Ginseng extractum, and above weight percentages of components sum is 100%.
Preferably, the described atomized liquid containing constituent of ginseng comprises the component of following percentage by weight: 72% propane diols, 15% glycerine, 5% constituent of ginseng and 8% distilled water.
Preferably, the described atomized liquid containing constituent of ginseng comprises the component of following percentage by weight: 65% propane diols, 12% glycerine, 8% constituent of ginseng and 15% distilled water.
Preferably, the described atomized liquid containing constituent of ginseng comprises the component of following percentage by weight: 63% propane diols, 20% glycerine, 10% constituent of ginseng and 7% distilled water.
The preparation method of the above-mentioned atomized liquid containing constituent of ginseng, comprises the following steps:
(1) pulverized by ginseng medicine materical crude slice and cross 80 mesh sieves, add 95% alcohol extract 3 times of 2-3 times of Ginseng Quality, each 2h, Extracting temperature 40-50 DEG C, obtain volatile oil compositions and extract; Volatile oil compositions obtains ginseng essential oil through petroleum ether extraction and reduced pressure concentration, and extract obtains Radix Ginseng extractum through reduced pressure concentration;
(2) ginseng essential oil obtained in step (1) and Radix Ginseng extractum's weight sum are counted the weight of constituent of ginseng, take all the other component raw material according to the percentage by weight of each component; The Radix Ginseng extractum that step (1) is obtained is dissolved with distilled water, obtains By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the ginseng essential oil that step (1) is obtained again, emulsifying 5-10min under the rotating speed of 3000-4000rpm, obtain the described atomized liquid containing constituent of ginseng.
Preferably, the temperature of the described extract reduced pressure concentration of step (1) is 60 DEG C.
Preferably, the emulsifying temperature described in step (2) is 25-30 DEG C.
Compared with prior art, the present invention has the following advantages and beneficial effect:
(1) traditional electronic cigarette atomizing liquid is the composition that skims the cream off milk from tobacco, is dissolved in the solvent of food-grade, adds a small amount of essence and flavoring agent simultaneously.The Essence of the multiple green plants of extracting, is inhaled in body the unique effects having and remove the cigarette poison rested in human body, remove craving for tobacco.But, still containing carcinogens such as nicotines in atomized liquid, the health of harmful to human.
Do not add tobacco extract in atomized liquid of the present invention, not containing nicotine, the substitute is and with the addition of Chinese herbal medicine ginseng medicinal ingredient.The present invention is by selecting the ginseng medicine materical crude slice of high-quality, adopt abstraction technique, from ginseng, extraction and isolation goes out main active as ginsenoside and volatile oil, wherein volatile oil component smell is aromatic, have disperse induce sweat, the effect of resuscitation with aromatics, for replacing obtained by tobacco essence atomized liquid, not only smell is aromatic for it, also has health-care efficacy.
(2) atomized liquid formula of the present invention, the ratio of propane diols, G & W is suitable, atomized liquid smog is dense, to throat nonirritant; Do not add essence and flavoring agent, the substitute is the pure natural fragrance of ginseng essential oil, endanger without second-hand-cigarette; The principle active component of ginseng is ginsenoside, and can produce drug effect while of being sucked to be entered after in body not only strongly fragrant by atomization, reach and reinforce vital energy, multiple arteries and veins takes off admittedly, reinforces the spleen to benefit the lung, promotes the production of body fluid to quench thirst, the health cares such as intelligence development of calming the nerves.
Accompanying drawing explanation
Fig. 1 is the embodiment of the present invention 1 constituent of ginseng extraction process flow chart;
Fig. 2 is the atomized liquid preparation technology flow chart of the embodiment of the present invention 1 containing constituent of ginseng.
Detailed description of the invention
Below in conjunction with embodiment and accompanying drawing, the present invention is described in further detail, but embodiments of the present invention are not limited thereto.
The invention discloses a kind of atomized liquid containing constituent of ginseng, it comprises the component of following percentage by weight: 55-75% propane diols, 10-20% glycerine, 5-10% constituent of ginseng and 5-15% distilled water.The preparation process that should contain the atomized liquid of constituent of ginseng is as follows:
(1) ginseng medicine materical crude slice was pulverized 80 mesh sieves, add 95% alcohol extract 3 times (Extracting temperature 40-50 DEG C) into 2-3 times of Ginseng Quality, each 2h, obtains volatile oil compositions and extract; Volatile oil compositions obtains ginseng essential oil through petroleum ether extraction and reduced pressure concentration, and extract obtains Radix Ginseng extractum through reduced pressure concentration;
(2) ginseng essential oil obtained in step (1) and Radix Ginseng extractum's weight sum are counted the weight of constituent of ginseng, take all the other component raw material according to the percentage by weight of each component; The Radix Ginseng extractum that step (1) is obtained is dissolved with distilled water, obtains By Chinese Medicines; Then add propane diols and glycerine stirs, obtain primary atomization liquid; Add the ginseng essential oil that step (1) is obtained again, emulsifying 5-10min under the rotating speed of 3000-4000rpm, obtain the described atomized liquid containing constituent of ginseng.After the atomized liquid bottling capping obtained, through sterilizing, lamp inspection, finally packaging warehouse-in stores.
The preparation process of above-mentioned atomized liquid is after determining rational formula, is mainly realized by abstraction technique and emulsifying technology.Make electronic atomized liquid have medical value and reach best atomizing effect, suitable extraction of panax ginseng must be selected and prepare good properties and stable atomized liquid, its each composition especially ginseng essential oil and aqueous phase can be uniformly distributed, without effects such as composition delays during atomization.Prepare good properties and stable electronic atomized liquid, need to solve the difficult problem in stirring and emulsifying hybrid technology, design optimal parameter, wherein temperature, emulsification times, mixing speed all play vital effect.
Found by test, after using emulsifying to stir, obtained atomized liquid water-oil phase is uniformly dispersed, and can keep stable, and two-phase is not easy again to be separated.This system water oil is liquid, at room temperature can reach good emulsifying effectiveness, and higher than this temperature (40-70 DEG C) emulsifying effectiveness without work change, the energy that high temperature consumes is more, from cost-saving angle, emulsifying temperature is set to 25-30 DEG C.
Find in test that the water-oil phase dispersion effect of the obtained atomized liquid of high rotating speed (4000-6000rpm) is good, but the foam produced during emulsify at a high speed is more, the stirring at low speed of 3000rpm can cancellation bubble.Rotating speed too small (1000-2000rpm) shearing force is not enough to make the two-phase of atomized liquid to complete dispersion even, fine and smoothly.
Emulsification times also can impact the quality of atomized liquid, and because in atomized liquid formula of the present invention, the component content of volatile oil is less, viscosity is lower, can complete dispersion within a short period of time.5-10min, the few oil slick of atomized liquid foam is few, emulsion-stabilizing.Be less than 3min, because the time is too short, do not reach the effect of stable dispersion.
Embodiment 1
A preparation method for atomized liquid containing constituent of ginseng, as illustrated in fig. 1 and 2, comprises the following steps:
(1) ginseng medicine materical crude slice was pulverized 80 mesh sieves, and added 95% ethanol of 2 times of Ginseng Qualities, extract 3 times (Extracting temperature 40 DEG C), each 2h, obtains volatile oil compositions and extract; Volatile oil compositions obtains ginseng essential oil through petroleum ether extraction and reduced pressure concentration, and extract obtains Radix Ginseng extractum through reduced pressure concentration;
(2) ginseng essential oil obtained in step (1) and Radix Ginseng extractum's weight sum are counted the weight of constituent of ginseng, take all the other component raw material according to the percentage by weight of each component; The Radix Ginseng extractum that step (1) is obtained is dissolved with distilled water, obtains By Chinese Medicines; Then add propane diols and glycerine stirs, obtain primary atomization liquid; Add the ginseng essential oil that step (1) is obtained again, with vacuum homogeneous emulsifying machine emulsifying 10min under the rotating speed of 3000rpm, emulsifying temperature is normal temperature (25-30 DEG C), obtains the described atomized liquid containing constituent of ginseng; After the atomized liquid bottling capping obtained, through sterilizing, lamp inspection;
Wherein the above-mentioned atomized liquid containing constituent of ginseng comprises the component of following percentage by weight: 72% propane diols, 15% glycerine, 5% constituent of ginseng and 8% distilled water; Described constituent of ginseng is ginseng essential oil obtained in step (1) and Radix Ginseng extractum.
In this embodiment, constituent of ginseng ratio is less than normal, and smog is dense, is applicable to the crowd that just given up smoking.
Embodiment 2
A preparation method for atomized liquid containing constituent of ginseng, comprises the following steps:
(1) ginseng medicine materical crude slice was pulverized 80 mesh sieves, and added 95% ethanol of 3 times of Ginseng Qualities, extract 3 times, each 2h, obtains volatile oil compositions and extract; Volatile oil compositions obtains ginseng essential oil through petroleum ether extraction and reduced pressure concentration, and extract obtains Radix Ginseng extractum through reduced pressure concentration;
(2) ginseng essential oil obtained in step (1) and Radix Ginseng extractum's weight sum are counted the weight of constituent of ginseng, take all the other component raw material according to the percentage by weight of each component; The Radix Ginseng extractum that step (1) is obtained adds distilled water, obtains By Chinese Medicines; Then add propane diols and glycerine, obtain primary atomization liquid; Add the ginseng essential oil that step (1) is obtained again, with vacuum homogeneous emulsifying machine emulsifying 5min under the rotating speed of 4000rpm, emulsifying temperature is normal temperature (25-30 DEG C), and sterilizing after bottling capping, lamp inspection, obtain the described atomized liquid containing constituent of ginseng;
Wherein the above-mentioned atomized liquid containing constituent of ginseng comprises the component of following percentage by weight: 65% propane diols, 12% glycerine, 8% constituent of ginseng and 15% distilled water; Described constituent of ginseng is ginseng essential oil obtained in step (1) and Radix Ginseng extractum.
In this embodiment, constituent of ginseng ratio is moderate, can play a role in health care.
Embodiment 3
A preparation method for atomized liquid containing constituent of ginseng, comprises the following steps:
(1) ginseng medicine materical crude slice was pulverized 80 mesh sieves, and added 95% ethanol of 2 times of Ginseng Qualities, extract 3 times, each 2h, obtains volatile oil compositions and extract; Volatile oil compositions obtains ginseng essential oil through petroleum ether extraction and reduced pressure concentration, and extract obtains Radix Ginseng extractum through reduced pressure concentration;
(2) ginseng essential oil obtained in step (1) and Radix Ginseng extractum's weight sum are counted the weight of constituent of ginseng, take all the other component raw material according to the percentage by weight of each component; The Radix Ginseng extractum that step (1) is obtained adds distilled water, obtains By Chinese Medicines; Then add propane diols and glycerine, obtain primary atomization liquid; Add the ginseng essential oil that step (1) is obtained again, with vacuum homogeneous emulsifying machine emulsifying 10min under the rotating speed of 3000rpm, emulsifying temperature is normal temperature (25-30 DEG C), and sterilizing after bottling capping, lamp inspection, obtain the described atomized liquid containing constituent of ginseng;
Wherein the above-mentioned atomized liquid containing constituent of ginseng comprises the component of following percentage by weight: 63% propane diols, 20% glycerine, 10% constituent of ginseng and 7% distilled water; Described constituent of ginseng is ginseng essential oil obtained in step (1) and Radix Ginseng extractum.
In this embodiment, ginseng medicinal ingredient ratio is higher, and atomizing effect is good, and health-care effect is obvious.
For verifying the smoking cessation effect of atomized liquid of the present invention and health-care effect, testing after adopting the atomized liquid formula in embodiment 3 to make electronic cigarette, randomly drawing 100 routine smokers, all have food less, burnout, void coughs the ill symptomses such as syndrome characterized by dyspnea.Put into electronic cigarette atomizing inhalator with atomized liquid 5ml of the present invention, suck 10 every day, within 2 months, draw 80ml altogether.Test effect, 87% craving for tobacco significantly declines, and 63% tired and void is coughed syndrome characterized by dyspnea symptom and all made moderate progress, and illustrates that atomized liquid of the present invention has remarkable result to smoking cessation, has health-care effects such as reinforcing vital energy, reinforce the spleen to benefit the lung simultaneously.
Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not restricted to the described embodiments; change, the modification done under other any does not deviate from Spirit Essence of the present invention and principle, substitute, combine, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (7)
1. the atomized liquid containing constituent of ginseng, is characterized in that, comprise the component of following percentage by weight: 55-75% propane diols, 10-20% glycerine, 5-10% constituent of ginseng and 5-15% distilled water; Described constituent of ginseng comprises ginseng essential oil and Radix Ginseng extractum, and above weight percentages of components sum is 100%.
2. the atomized liquid containing constituent of ginseng according to claim 1, it is characterized in that, this atomized liquid comprises the component of following percentage by weight: 72% propane diols, 15% glycerine, 5% constituent of ginseng and 8% distilled water.
3. the atomized liquid containing constituent of ginseng according to claim 1, it is characterized in that, this atomized liquid comprises the component of following percentage by weight: 65% propane diols, 12% glycerine, 8% constituent of ginseng and 15% distilled water.
4. the atomized liquid containing constituent of ginseng according to claim 1, it is characterized in that, this atomized liquid comprises the component of following percentage by weight: 63% propane diols, 20% glycerine, 10% constituent of ginseng and 7% distilled water.
5. the preparation method of the atomized liquid containing constituent of ginseng described in any one of Claims 1-4, is characterized in that, comprise the following steps:
(1) pulverized by ginseng medicine materical crude slice and cross 80 mesh sieves, add 95% alcohol extract 3 times of 2-3 times of Ginseng Quality, each 2h, Extracting temperature 40-50 DEG C, obtain volatile oil compositions and extract; Volatile oil compositions obtains ginseng essential oil through petroleum ether extraction and reduced pressure concentration, and extract obtains Radix Ginseng extractum through reduced pressure concentration;
(2) ginseng essential oil obtained in step (1) and Radix Ginseng extractum's weight sum are counted the weight of constituent of ginseng, take all the other component raw material according to the percentage by weight of each component; The Radix Ginseng extractum that step (1) is obtained is dissolved with distilled water, obtains By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the ginseng essential oil that step (1) is obtained again, emulsifying 5-10min under the rotating speed of 3000-4000rpm, obtain the described atomized liquid containing constituent of ginseng.
6. preparation method according to claim 5, is characterized in that, the temperature of the described extract reduced pressure concentration of step (1) is 60 DEG C.
7. preparation method according to claim 5, is characterized in that, the emulsifying temperature described in step (2) is 25-30 DEG C.
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| CN201410855137.5A CN104664588B (en) | 2014-12-31 | 2014-12-31 | Nebulized liquid containing ginseng |
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| CN104664588B CN104664588B (en) | 2017-01-11 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105146733A (en) * | 2015-08-13 | 2015-12-16 | 深圳市施美乐科技股份有限公司 | Electronic cigarette atomization liquid with anti-aging function and preparation method thereof |
| CN113384635A (en) * | 2021-07-21 | 2021-09-14 | 福建省隆丰生物科技有限公司 | Mixture for reducing liver injury of organism and preparation method thereof |
| CN113749277A (en) * | 2021-09-11 | 2021-12-07 | 深圳市真味生物科技有限公司 | Atomized liquid with ambergris fragrance and preparation method thereof |
| CN113854623A (en) * | 2021-10-28 | 2021-12-31 | 中科分子生物(广东)股份有限公司 | Herbal low-temperature atomized electronic cigarette tobacco tar free of nicotine salt |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105146733A (en) * | 2015-08-13 | 2015-12-16 | 深圳市施美乐科技股份有限公司 | Electronic cigarette atomization liquid with anti-aging function and preparation method thereof |
| CN113384635A (en) * | 2021-07-21 | 2021-09-14 | 福建省隆丰生物科技有限公司 | Mixture for reducing liver injury of organism and preparation method thereof |
| CN113749277A (en) * | 2021-09-11 | 2021-12-07 | 深圳市真味生物科技有限公司 | Atomized liquid with ambergris fragrance and preparation method thereof |
| CN113749277B (en) * | 2021-09-11 | 2023-09-12 | 深圳市真味生物科技有限公司 | Atomized liquid with ambergris fragrance and preparation method thereof |
| CN113854623A (en) * | 2021-10-28 | 2021-12-31 | 中科分子生物(广东)股份有限公司 | Herbal low-temperature atomized electronic cigarette tobacco tar free of nicotine salt |
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