CN105146733A - Electronic cigarette atomization liquid with anti-aging function and preparation method thereof - Google Patents
Electronic cigarette atomization liquid with anti-aging function and preparation method thereof Download PDFInfo
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- CN105146733A CN105146733A CN201510495389.6A CN201510495389A CN105146733A CN 105146733 A CN105146733 A CN 105146733A CN 201510495389 A CN201510495389 A CN 201510495389A CN 105146733 A CN105146733 A CN 105146733A
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Abstract
The invention provides electronic cigarette atomization liquid with an anti-aging function and a preparation method thereof. The electronic cigarette atomization liquid is mainly prepared from the following components according to weight ratio: 0.05-2.5 parts of natural nicotine, 3-20 parts of tobacco absolute oil, 1-10 parts of a tobacco extract, 0.5-2 parts of a ginseng extract, 0.4-2 parts of a green tea extract, 0.8-6 parts of distilled water, 26-50 parts of USP-grade glycerin and the balance of food-grade propylene glycol. By adopting the electronic cigarette atomization liquid, harms of nicotine to human bodies are reduced, moreover, the physical health is facilitated, and the anti-aging efficacy is realized.
Description
Technical field
The present invention relates to the technical field of electronic cigarette, particularly a kind of electronic cigarette atomizing liquid with senile-resistant efficacy and preparation method thereof.
Background technology
Cigarette is as a kind of preference, be subject to liking of many people, but the tar in cigarette, carbon monoxide (CO) health to human body is harmful, especially containing several 10 kinds of compositions in tar is carcinogens, at present progressively forbid smoking cigarettes (cigarette) being defined in public place with home government abroad, but for a smoker having smoking history, requirement is accomplished no longer to have cigarette smoking, it is a very difficult thing, so commercially there is the substitute of much cigarette, as: lozenge for stopping smoking, electronic cigarette, found that electronic cigarette was the most common in recent years, this electronic cigarette is atomized by cigarette bullet, and then generation smog, but the function singleness of existing tobacco juice for electronic smoke, just as simple substitute of tobacco, the effect of taking good care of that keeps healthy further cannot be played to human body.
Summary of the invention
The object of the invention is to propose a kind of electronic cigarette atomizing liquid with senile-resistant efficacy and preparation method thereof, craving for tobacco can be met and be conducive to again healthy, there is senile-resistant efficacy.
For achieving the above object, the present invention proposes a kind of electronic cigarette atomizing liquid with senile-resistant efficacy, it is formulated by weight primarily of following composition:
Natural nicotine 0.05 ~ 2.5, pure tobacco oil 3 ~ 20, tobacco extract 1 ~ 10, ginseng extract 0.5 ~ 2, green-tea extract 0.4 ~ 2, distilled water 0.8 ~ 6, USP level (USP standard) glycerine 26 ~ 50, surplus are food grade propylene glycol.
Further, have in the electronic cigarette atomizing liquid of senile-resistant efficacy above-mentioned, purity >=99% of natural nicotine.
Further, have in the electronic cigarette atomizing liquid of senile-resistant efficacy above-mentioned, described in have each composition of electronic cigarette atomizing liquid of senile-resistant efficacy weight ratio be preferably:
Natural nicotine 2.5, pure tobacco oil 20, tobacco extract 10, ginseng extract 2, green-tea extract 2, distilled water 6, USP level glycerine 50, surplus are food grade propylene glycol.
Further, have in the electronic cigarette atomizing liquid of senile-resistant efficacy above-mentioned, described in have each composition of electronic cigarette atomizing liquid of senile-resistant efficacy weight ratio be preferably:
Natural nicotine 2, pure tobacco oil 10, tobacco extract 6, ginseng extract 1, green-tea extract 1.5, distilled water 5, USP level glycerine 30, surplus are food grade propylene glycol.
Further, have in the electronic cigarette atomizing liquid of senile-resistant efficacy above-mentioned, the composition of described green-tea extract comprises: epigallocatechin, gallate, Tea Polyphenols, L-thiamine, theaflavin, tea polysaccharide and Tea Saponin.
Further, have in the electronic cigarette atomizing liquid of senile-resistant efficacy above-mentioned, the composition of described ginseng extract comprises: multiple Saponins, cupreol, flavonoids Kaempferol, trifolin, panasenoside and cyanidenon glycoside.
Further, have in the electronic cigarette atomizing liquid of senile-resistant efficacy above-mentioned, described multiple Saponins is several in Rb1, Rb2, Rd, Rc, Re, Ro, Re, Rf, Rg1, Rg2, Rg3, Rh1, Rh2.
Separately, the present invention also provides the above-mentioned preparation method with the electronic cigarette atomizing liquid of senile-resistant efficacy, comprises the following steps:
A () will weigh pure tobacco oil, tobacco extract, ginseng extract and green-tea extract by formula rate and add in deionized water, be heated to 50 DEG C ~ 65 DEG C and fully stirring is dissolved completely;
B solution in step (a) is added load weighted food grade propylene glycol by (), fully stir, then is heated to 50 DEG C ~ 70 DEG C;
C () adds natural nicotine, glycerine after the solution in step (b) is cooled to 15 ~ 30 DEG C, stir;
D () cools after the filled with solution in step (c) at-5 DEG C ~ 0 DEG C temperature, have the electronic cigarette atomizing liquid of senile-resistant efficacy described in namely obtaining.
Further, in the preparation method of the above-mentioned electronic cigarette atomizing liquid with senile-resistant efficacy, described green-tea extract is made up of following extracting method:
With commercially available 7 grades of green tea for raw material, after grinding, get 10g, add ethanol 100ml, 70 ~ 80 degree of water-bath 30min that mass fraction is 20%, extract 3 times altogether, merge extract;
In extract, add 2gZnCl2 again and make precipitating reagent, add NaHCO3 and the pH of solution is adjusted to 6.4 ~ 8.0, leave standstill 60min, centrifugal or filtration, discards water layer;
The precipitation that centrifugal or filtration obtain is added the sulfuric acid dissolution that mass fraction is 40%, adds extraction into ethyl acetate water layer 3 times, combined ethyl acetate, and add anhydrous sodium sulfate drying, filter, pressure reducing and steaming ethyl acetate, obtains described green-tea extract.
Further, in the preparation method of the above-mentioned electronic cigarette atomizing liquid with senile-resistant efficacy, described ginseng extract is made up of following extracting method:
With dry gen-seng haulms for raw material, through pulverizing, tinning, with the water of 10 times amount for solvent divides extraction of seething with excitement for three times, each 2 hours, extract plate-frame filtering, merged extract;
Merging extract is adsorbed through macroporous resin column, washes with water assorted, and by alcohol-water wash-out general ginsenoside, merge eluent, reclaim ethanol extremely without alcohol;
Continue concentration and evaporation water to proportion d=1.15, spraying dry, obtained described ginseng extract after pulverizing 100 mesh sieves.
What the present invention had the electronic cigarette atomizing liquid employing of senile-resistant efficacy is the material compositions such as tobacco extract, ginseng extract, green-tea extract, thus reduces the content of nicotine in electronic atomized liquid, is conducive to healthy simultaneously, has senile-resistant efficacy.
Wherein, ginseng has postponement cell ageing, extends the function of cell survival.Use flower of Panax ginseng raising honeybee, can obviously life-extending about 10 ~ 15 days.Ginseng all has obvious facilitation to the synthesis of liver cell RNA, and its effect and dose proportional.Experiment finds, ginseng can make active proliferation, metabolic function strengthens, DNA replication dna rate increases.
The main component of ginseng adjustment aging course and prevention early ageing is panaxoside, its Main Function is the low physiological system of stimulatory function, make its biochemical reactions be tending towards normal, and stop the vicious circle because a variety of causes causes, to reach object of promoting longevity.The antioxidation of ginseng is one of important step of ginseng anti-aging effects.The lipid peroxidation of the tissue such as Animal Liver, brain, lung that panaxoside, stem and leaf of Radix Ginseng saponin and panaxan can suppress many factors to bring out, eliminates radical anion.Ginseng general glycoside, panoxadiol can eliminate the Superoxide anion free radical that dimethyl sulfoxide (DMSO) produces under aerobic conditions in vitro, and the effect of ginseng general glycoside is better than panoxadiol.Panaxoside significantly can suppress the lipid peroxidation in mouse brain and liver tissues, improves superoxide dismutase content and catalase activity in red blood cell, and has significant inhibitory action to lipofuscin generation in rat cerebral cortex and liver.Gen-seng haulms, reed head saponin centering, senile rat all have obviously suppression LH and serum lipid overoxidation effect.And effect same is obtained in Aged Mice experiment.
Panaxoside can significantly improve deficiency of yang animal cAMP level, reduces cGMP level, and cAMP/cGMP ratio rises, and effectively can increase the quantity of Kupffer Cell in deficiency of yang Animal Liver.Stem and leaf of Radix Ginseng saponin is then improved the effect of neuroendocrine integration function.Stem and leaf of Radix Ginseng saponin is also improved the effect of rats with deficiency of kidney-Yang Prolactin, and this result support aging is a kind of viewpoint of physiological kidney-yang deficiency state.
The composition Tea Polyphenols of green-tea extract is also WEIDUOFEN, is the general name of Polyphenols of Tea, comprises flavanol compound, anthocyanin class, flavonoids, flavonols and phenolic acid class etc.Wherein important with flavanol compound material (catechin).Tea Polyphenols is tanned or tea tannin also known as tea, and being one of Main Ingredients and Appearance forming Tea color fragrance, is also one of Main Ingredients and Appearance having health care in tealeaves.
Effect of Tea Polyphenols has:
1, there is the effect of very strong elimination harmful free radicals;
2, anti-aging effects;
3, radiation resistance;
4, to the inhibitory action of cancer cell;
5, antibacterial, bactericidal action;
6, to the inhibitory action of AIDS virus;
7, lung's nicotine can be cleaned to smoker is beneficial.
Tea Polyphenols has very strong antioxidation, its oxidation resistance be Prof. Du Yucang antioxidant BHT, BHA 4-6 doubly, be the 6-7 of VE doubly, doubly, and consumption is few for the 5-10 of VC: 0.01-0.03% can work, and without the potential toxic and side effect of synthetic.
To sum up, the present invention's electronic cigarette atomizing liquid with senile-resistant efficacy and preparation method thereof is by adopting the material compositions such as tobacco extract, ginseng extract, green-tea extract, decrease nicotine to harm, be conducive to healthy simultaneously, there is senile-resistant efficacy.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described:
Embodiment 1
Take each component materials that preparation the present invention has the electronic cigarette atomizing liquid of senile-resistant efficacy by weight, described each composition raw material is by weight: natural nicotine (purity >=99%) 2.5, pure tobacco oil 20, tobacco extract 10, ginseng extract 2, green-tea extract 2, distilled water 6, USP level glycerine 50, surplus are food grade propylene glycol; During preparation,
A () will weigh pure tobacco oil, tobacco extract, ginseng extract and green-tea extract by formula rate and add in deionized water, be heated to 65 DEG C and fully stirring is dissolved completely;
B solution in step (a) is added load weighted food grade propylene glycol by (), fully stir, then is heated to 70 DEG C;
C () adds natural nicotine, glycerine after the solution in step (b) is cooled to 30 DEG C, stir;
D () cools after the filled with solution in step (c) at 0 DEG C of temperature, have the electronic cigarette atomizing liquid of senile-resistant efficacy described in namely obtaining.
Embodiment 2
Take each component materials that preparation the present invention has the electronic cigarette atomizing liquid of senile-resistant efficacy by weight, described each composition raw material is by weight: natural nicotine (purity >=99%) 2, pure tobacco oil 10, tobacco extract 6, ginseng extract 1, green-tea extract 1.5, distilled water 5, USP level glycerine 30, surplus are food grade propylene glycol; During preparation,
A () will weigh pure tobacco oil, tobacco extract, ginseng extract and green-tea extract by formula rate and add in deionized water, be heated to 55 DEG C and fully stirring is dissolved completely;
B solution in step (a) is added load weighted food grade propylene glycol by (), fully stir, then is heated to 60 DEG C;
C () adds natural nicotine, glycerine after the solution in step (b) is cooled to 25 DEG C, stir;
D () cools after the filled with solution in step (c) at-2 DEG C of temperature, have the electronic cigarette atomizing liquid of senile-resistant efficacy described in namely obtaining.
Embodiment 3
Take each component materials that preparation the present invention has the electronic cigarette atomizing liquid of senile-resistant efficacy by weight, described each composition raw material is by weight:
Natural nicotine (purity >=99%) 0.05, pure tobacco oil 3, tobacco extract 1, ginseng extract 0.5, green-tea extract 0.4, distilled water 0.8, USP level glycerine 26, surplus are food grade propylene glycol; During preparation,
A () will weigh pure tobacco oil, tobacco extract, ginseng extract and green-tea extract by formula rate and add in deionized water, be heated to 50 DEG C of abundant stirrings and dissolve completely;
B solution in step (a) is added load weighted food grade propylene glycol by (), fully stir, then is heated to 50 DEG C;
C () adds natural nicotine, glycerine after the solution in step (b) is cooled to 15, stir;
D () cools after the filled with solution in step (c) at-5 DEG C of temperature, have the electronic cigarette atomizing liquid of senile-resistant efficacy described in namely obtaining.
Here description of the invention and application is illustrative, not wants by scope restriction of the present invention in the above-described embodiments.Distortion and the change of embodiment disclosed are here possible, are known for the replacement of embodiment those those of ordinary skill in the art and the various parts of equivalence.Those skilled in the art are noted that when not departing from spirit of the present invention or substantive characteristics, the present invention can in other forms, structure, layout, ratio, and to realize with other assembly, material and parts.When not departing from the scope of the invention and spirit, can other distortion be carried out here to disclosed embodiment and change.
Claims (10)
1. have an electronic cigarette atomizing liquid for senile-resistant efficacy, it is characterized in that, it is formulated by weight primarily of following composition:
Natural nicotine 0.05 ~ 2.5, pure tobacco oil 3 ~ 20, tobacco extract 1 ~ 10, ginseng extract 0.5 ~ 2, green-tea extract 0.4 ~ 2, distilled water 0.8 ~ 6, USP level glycerine 26 ~ 50, surplus are food grade propylene glycol.
2. the electronic cigarette atomizing liquid with senile-resistant efficacy according to claim 1, is characterized in that, purity >=99% of described natural nicotine.
3. the electronic cigarette atomizing liquid with senile-resistant efficacy according to claim 1, is characterized in that, described in have each composition of electronic cigarette atomizing liquid of senile-resistant efficacy weight ratio be preferably:
Natural nicotine 2.5, pure tobacco oil 20, tobacco extract 10, ginseng extract 2, green-tea extract 2, distilled water 6, USP level glycerine 50, surplus are food grade propylene glycol.
4. the electronic cigarette atomizing liquid with senile-resistant efficacy according to claim 1, is characterized in that, described in have each composition of electronic cigarette atomizing liquid of senile-resistant efficacy weight ratio be preferably:
Natural nicotine 2, pure tobacco oil 10, tobacco extract 6, ginseng extract 1, green-tea extract 1.5, distilled water 5, USP level glycerine 30, surplus are food grade propylene glycol.
5. the electronic cigarette atomizing liquid with senile-resistant efficacy according to claim 1, it is characterized in that, the composition of described green-tea extract comprises: epigallocatechin, gallate, Tea Polyphenols, L-thiamine, theaflavin, tea polysaccharide and Tea Saponin.
6. the electronic cigarette atomizing liquid with senile-resistant efficacy according to claim 1, it is characterized in that, the composition of described ginseng extract comprises: multiple Saponins, cupreol, flavonoids Kaempferol, trifolin, panasenoside and cyanidenon glycoside.
7. the electronic cigarette atomizing liquid with senile-resistant efficacy according to claim 6, is characterized in that, described multiple Saponins is several in Rb1, Rb2, Rd, Rc, Re, Ro, Re, Rf, Rg1, Rg2, Rg3, Rh1, Rh2.
8. the preparation method with the electronic cigarette atomizing liquid of senile-resistant efficacy as described in any one of claim 1-7, is characterized in that, said method comprising the steps of:
A () will weigh pure tobacco oil, tobacco extract, ginseng extract and green-tea extract by formula rate and add in deionized water, be heated to 50 DEG C ~ 65 DEG C and fully stirring is dissolved completely;
B solution in step (a) is added load weighted food grade propylene glycol by (), fully stir, then is heated to 50 DEG C ~ 70 DEG C;
C () adds natural nicotine, glycerine after the solution in step (b) is cooled to 15 ~ 30 DEG C, stir;
D () cools after the filled with solution in step (c) at-5 DEG C ~ 0 DEG C temperature, have the electronic cigarette atomizing liquid of senile-resistant efficacy described in namely obtaining.
9. the preparation method with the electronic cigarette atomizing liquid of senile-resistant efficacy according to claim 8, it is characterized in that, described green-tea extract is made up of following extracting method:
With commercially available 7 grades of green tea for raw material, after grinding, get 10g, add ethanol 100ml, 70 ~ 80 degree of water-bath 30min that mass fraction is 20%, extract 3 times altogether, merge extract;
In extract, add 2gZnCl2 again and make precipitating reagent, add NaHCO3 and the pH of solution is adjusted to 6.4 ~ 8.0, leave standstill 60min, centrifugal or filtration, discards water layer;
The precipitation that centrifugal or filtration obtain is added the sulfuric acid dissolution that mass fraction is 40%, adds extraction into ethyl acetate water layer 3 times, combined ethyl acetate, and add anhydrous sodium sulfate drying, filter, pressure reducing and steaming ethyl acetate, obtains described green-tea extract.
10. the preparation method with the electronic cigarette atomizing liquid of senile-resistant efficacy according to claim 8, it is characterized in that, described ginseng extract is made up of following extracting method:
With dry gen-seng haulms for raw material, through pulverizing, tinning, with the water of 10 times amount for solvent divides extraction of seething with excitement for three times, each 2 hours, extract plate-frame filtering, merged extract;
Merging extract is adsorbed through macroporous resin column, washes with water assorted, and by alcohol-water wash-out general ginsenoside, merge eluent, reclaim ethanol extremely without alcohol;
Continue concentration and evaporation water to proportion d=1.15, spraying dry, obtained described ginseng extract after pulverizing 100 mesh sieves.
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Cited By (6)
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| CN108142983A (en) * | 2018-02-02 | 2018-06-12 | 新智能生活馆（深圳）有限公司 | A kind of electronic atomized liquid composition and its application |
| CN108420121A (en) * | 2018-05-29 | 2018-08-21 | 云南养瑞科技集团有限公司 | It is a kind of to have effects that improve tobacco juice for electronic smoke of sleep and preparation method thereof |
| CN109275956A (en) * | 2018-09-20 | 2019-01-29 | 云南中烟工业有限责任公司 | A kind of additives of filter tip and preparation method thereof based on the cool taste component of the eastern purple perilla of purification |
| CN113854623A (en) * | 2021-10-28 | 2021-12-31 | 中科分子生物(广东)股份有限公司 | Herbal low-temperature atomized electronic cigarette tobacco tar free of nicotine salt |
| CN113854624A (en) * | 2021-11-05 | 2021-12-31 | 上海纳米技术及应用国家工程研究中心有限公司 | Electronic cigarette liquid containing triterpenoid saponin and preparation method thereof |
| CN115005487A (en) * | 2022-06-22 | 2022-09-06 | 深圳海克尔时代科技有限公司 | Electronic cigarette atomized liquid assisting in smoking control and quitting and preparation method thereof |
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Application publication date: 20151216 |