CN101744360B - Antrodia camphorata extract and cigarette containing antrodia camphorata extract - Google Patents
Antrodia camphorata extract and cigarette containing antrodia camphorata extract Download PDFInfo
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- CN101744360B CN101744360B CN2010100426966A CN201010042696A CN101744360B CN 101744360 B CN101744360 B CN 101744360B CN 2010100426966 A CN2010100426966 A CN 2010100426966A CN 201010042696 A CN201010042696 A CN 201010042696A CN 101744360 B CN101744360 B CN 101744360B
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- cinnamomum kanahirai
- kanahirai hay
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Abstract
The present invention discloses an antrodia camphorata extract and a cigarette containing antrodia camphorata extract. The present invention aims to realize the techniques of increasing fragrance, keeping moisture and reducing harmful ingredients in cigarettes. The antrodia camphorata extract is prepared with the following method: hot water of which the mass is 3 to 10 times of that of antrodia camphorata coarse powder is added to antrodia camphorata dried and crushed, the antrodia camphorata coarse powder is digested at a temperature of 80 DEG C to 95 DEG C, filtrate filtered is concentrated at a temperature of 60 DEG C under the reduced pressure of 0.05 MPa for 2 hours, and the antrodia camphorata extract is obtained. The cigarette containing antrodia camphorata extract is made by adding antrodia camphorata extract of which the mass accounts for 0.001 to 10% of that of tobacco shreds to the tobacco shreds. Compared with the prior art, the plant extract containing antrodia camphorata active ingredients in the tobacco shreds has excellent solubility. The active ingredients can enter human bodies with the main smoke flow during the smoking and be absorbed by the human bodies through blood circulation. Consequently, the extract performs the functions for resisting tumours, viruses, ageing, etc. Cigarette smoke is pure and free of mixed gas. The quality of the cigarette can be improved, and the harm of the smoke to human bodies is accordingly reduced.
Description
Technical field
The present invention relates to a kind of fungal extract and contain the cigarette of this fungal extract, particularly a kind of Cinnamomum kanahirai hay mushroom extract and contain the cigarette of this Cinnamomum kanahirai hay mushroom extract.
Background technology
According to a research report of the World Health Organization, the whole world has 1,000,000 people every year at least because smoking and dead prematurely.China also pays much attention to the harmful work of falling of cigarette, and since 2005, State Tobacco Monopoly Bureau has organized cigarette harmfulness index system and two great special research work of cigarette flavouring humectation, has obtained certain achievement.At present the Chinese style cigarette has been obtained certain achievement in the research of falling aspect evil, the flavouring humectation, but the research aspect also has no small gap aspect evil, the flavouring humectation falling with internationally famous brand, remains further to be utilized the research and development new product.
Summary of the invention
The purpose of this invention is to provide a kind of Cinnamomum kanahirai hay mushroom extract and contain the cigarette of Cinnamomum kanahirai hay mushroom extract, the technical problem that solve is the flavouring humectation, reduces the harmful components in the cigarette.
The present invention adopts following technical scheme: a kind of Cinnamomum kanahirai hay mushroom extract, and adopt following method to prepare: one, with the Cinnamomum kanahirai hay mushroom, 40-70 ℃ of oven dry is crushed to 10-100 purpose meal; Two, get the Cinnamomum kanahirai hay mushroom meal that crushes, divide to add Cinnamomum kanahirai hay mushroom meal quality 3-10 hot water doubly for 3 times respectively, maintain the temperature at lixiviate in 80-95 ℃, each lixiviate 5 hours merges 3 times water extract; Three, filter, filtrate filtered reduced pressure concentrated 2 hours under 0.05Mpa, 60 ℃ of conditions, received cream, obtained Cinnamomum kanahirai hay mushroom extract.
Cinnamomum kanahirai hay mushroom of the present invention is adopted the Cinnamomum kanahirai hay mushroom of Taiyi national treasure Antrodia camphorata Co., Ltd.
The present invention removes impurity with the Cinnamomum kanahirai hay mushroom, cleans the back oven dry.
After the Cinnamomum kanahirai hay mushroom oven dry of the present invention, moisture is controlled to be 8-12%.
A kind of cigarette of containing Cinnamomum kanahirai hay mushroom extract has pipe tobacco, contains the Cinnamomum kanahirai hay mushroom extract that accounts for tobacco quality 0.001-10% in the said pipe tobacco; Said Cinnamomum kanahirai hay mushroom extract adopts following method to prepare: one, with the Cinnamomum kanahirai hay mushroom, 40-70 ℃ of oven dry is crushed to 10-100 purpose meal; Two, get the Cinnamomum kanahirai hay mushroom meal that crushes, divide to add Cinnamomum kanahirai hay mushroom meal quality 3-10 hot water doubly for 3 times respectively, maintain the temperature at lixiviate in 80-95 ℃, each lixiviate 5 hours merges 3 times water extract; Three, filter, filtrate filtered reduced pressure concentrated 2 hours under 0.05Mpa, 60 ℃ of conditions, received cream, obtained Cinnamomum kanahirai hay mushroom extract.
Cinnamomum kanahirai hay mushroom of the present invention is removed impurity, cleans the back oven dry.
After the Cinnamomum kanahirai hay mushroom oven dry of the present invention, moisture is controlled to be 8-12%.
The cigarette of containing Cinnamomum kanahirai hay mushroom extract of the present invention adopts following method to prepare: with Cinnamomum kanahirai hay mushroom extract with 70-90 ℃ of hot water or 75% dissolve with ethanol; Solution quality concentration after the dissolving is 0.1-80%; Account for the ratio of tobacco quality 0.001～10% in Cinnamomum kanahirai hay mushroom extract; Evenly be sprayed on the pipe tobacco, dry naturally, process cigarette by conventional cigarette processing technology again.
Contain the Cinnamomum kanahirai hay mushroom extract that accounts for tobacco quality 0.1% in the pipe tobacco of the present invention.
Contain the Cinnamomum kanahirai hay mushroom extract that accounts for tobacco quality 0.01% in the pipe tobacco of the present invention.
The present invention compared with prior art contains the plant extracts of Cinnamomum kanahirai hay mushroom active component in the pipe tobacco, dissolubility is good; In smoking process, can get into human body with main flume; Be absorbed by the body through blood circulation, thereby bring into play its antitumor, antiviral, anti-ageing effect of waiting for a long time, the pure and mild nothing of the cigarette smoke gas of mixing; Can improve cigarette quality, thereby reduce the harmfulness of flue gas human body.
The specific embodiment
Below in conjunction with embodiment the present invention is done further explain.Cinnamomum kanahirai hay mushroom extract of the present invention, adopt following method to prepare: one,, remove impurity, clean the fresh Cinnamomum kanahirai hay mushroom of Taiwan Taiyi national treasure Antrodia camphorata Co., Ltd, 40-70 ℃ of oven dry, moisture is controlled to be 8-12%, is crushed to 10-100 purpose meal; Two, get the Cinnamomum kanahirai hay mushroom meal that crushes, divide to add Cinnamomum kanahirai hay mushroom meal quality 3-10 hot water doubly for 3 times respectively, maintain the temperature at lixiviate in 80-95 ℃, each lixiviate 5 hours merges 3 times water extract; Three, filter, filtrate filtered reduced pressure concentrated 2 hours under 0.05Mpa, 60 ℃ of conditions, received cream, obtained Cinnamomum kanahirai hay mushroom extract.
With the above-mentioned Cinnamomum kanahirai hay mushroom extract that makes with 70-90 ℃ of hot water or 75% dissolve with ethanol; Solution quality concentration after the dissolving is 0.1-80%; Account for the ratio of tobacco quality 0.001～10% in Cinnamomum kanahirai hay mushroom extract; Evenly be sprayed on the pipe tobacco, dry naturally, process cigarette by conventional cigarette processing technology again.
The cigarette of containing Cinnamomum kanahirai hay mushroom extract of the present invention, during smoking, sweet, the free from extraneous odour of cigarette smoke has the evil effect of falling.Following advantage is arranged: 1, promote cigarette smoke strength, 2, reduce harmful components nitrosamine, crotonaldehyde in the cigarette mainstream flue gas, 3, do not change the original processing technology of cigarette, 4, the flavouring humectation, sweet sense is arranged, reduce the flue gas spread effect, 5 have no side effect.
According to YC/T184-2004 tobacco and tobacco product; The peculiar N-nitrosamine of tobacco is measured; Press the mensuration of main carbonyls in the YC/T254-2008 cigarette mainstream flue gas; The cigarette of containing Cinnamomum kanahirai hay mushroom extract of the present invention is compared with the blank cigarette, measured, measure result such as table 1 by Zhengzhou tobacco research institute.The cigarette of containing Cinnamomum kanahirai hay mushroom extract of the present invention is reduced tobacco-specific nitrosamine, crotonaldehyde in the flue gas; Reduction scope 10-20%, Guangdong provincial cigarette teacher of the smokeing panel test flue gas delicate fragrance when specification requirement is smoked panel test according to GB5606.4-2005 cigarette sense organ, full, pure and mild sweet, free from extraneous odour, assorted gas.The animal toxicity test demonstration has no side effect, and can reduce respiratory tract injury.
Embodiment 1, gets the bright Cinnamomum kanahirai hay mushroom of Taiwan Taiyi national treasure Antrodia camphorata Co., Ltd, removes impurity, cleans; 60 ℃ of oven dry, moisture is controlled to be 8%, and is crushed to the 10-100 order, divides the hot water that adds 10 times of Cinnamomum kanahirai hay mushroom meal quality for 3 times respectively; Keep 80-95 ℃ of following lixiviate of temperature, each 5 hours, merge 3 times water extract, filter; Filtrating, decompression concentrates under 0.05Mpa, 60 ℃, 2 hours conditions, obtains Cinnamomum kanahirai hay mushroom extract.With 70-90 ℃ of hot water dissolving, mass concentration is 20% with Cinnamomum kanahirai hay mushroom extract, is that 0.1% ratio of tobacco quality evenly is sprayed onto on the pipe tobacco in Cinnamomum kanahirai hay mushroom extract consumption, dries naturally, processes cigarette by conventional cigarette process again.When Guangdong provincial cigarette teacher of the smokeing panel test, cigarette smoke was pure and mild, sweet, the free from extraneous odour gas of mixing.Flue gas detects tobacco-specific nitrosamine, the crotonaldehyde that reduces in the flue gas, reduces scope 10-20%, shows the evil effect of falling.
Embodiment 2, get the bright Cinnamomum kanahirai hay mushroom of Taiwan Taiyi national treasure Antrodia camphorata Co., Ltd, remove impurity, clean; 50 ℃ of oven dry, moisture is controlled to be 12%, and is crushed to the 10-100 order, divides the hot water that adds 10 times of Cinnamomum kanahirai hay mushroom meal quality for 3 times respectively; Keep 80-95 ℃ of following lixiviate of temperature, each 5 hours, merge 3 times water extract, filter; Filtrating, decompression concentrates under 0.05Mpa, 60 ℃, 2 hours conditions, obtains Cinnamomum kanahirai hay mushroom extract.Cinnamomum kanahirai hay mushroom extract is used 75% dissolve with ethanol, and mass concentration is 20%, is that 0.01% ratio of tobacco quality evenly is sprayed onto on the pipe tobacco in Cinnamomum kanahirai hay mushroom extract consumption, dries naturally, processes cigarette by conventional cigarette process again.When Guangdong provincial cigarette teacher of the smokeing panel test, cigarette smoke was pure and mild, sweet, the free from extraneous odour gas of mixing; Flue gas detects tobacco-specific nitrosamine, the crotonaldehyde that reduces in the flue gas, reduces scope 10-20%, shows the evil effect of falling.
About the consumption of Cinnamomum kanahirai hay mushroom extract,, all can reach certain effect at the 0.001-10% of tobacco quality.
The Cinnamomum kanahirai hay mushroom is to be grown in the mountain area, Taiwan, distinctive national treasure level child care class seeds between 450～2000 meters of height above sea level---the rotten heartwood inwall (treehole) of Cinnamomum kanahirai hay tree Cinnamomum kanehirai Hay trunk, or the surface of the dark humidity of the Cinnamomum kanahirai hay timber of withered lodging.The Cinnamomum kanahirai hay mushroom mainly is distributed in ground such as peach garden, Miaoshu, southern throwing, Tai Dong and Kaohsiung in Taiwan at present.The Cinnamomum kanahirai hay mushroom has many physiologically active compositions; Like polysaccharide, three obedient compounds, adenosine (adenosine), protein (containing immune protein), vitamin (like Vit.B, niacin, etembonate liquor-saturated (ergosterol)), trace element (like calcium, phosphorus, germanium), amino acid etc., physiological active functions includes: antitumor, increase immunocompetence, antiviral, antiallergy, anti-hypertension, hypoglycemic, solid liquor-saturated, the antibacterium of courage, protection liver etc. fall.
The pharmacological action of Cinnamomum kanahirai hay mushroom has: 1, anti-cancer, anticancer: β-D-glucan (callose) has anticancer effect in the Cinnamomum kanahirai hay mushroom polysaccharides, adds its a large amount of triterpene compound compositions, can increase anticancer effect.It can suppress liver cancer cell growth the experiment confirm of the big research institute of platform.2, hypotensive: as to be mainly derivative and some triterpene compound of Lanostane class, can to suppress (ACE) and reach hypotensive purpose.3, hypoglycemic: hypoglycemic composition is mainly the Polysaccharides compound.4, reducing blood lipid: reduce the effect of cholesterol and blood fat.5, protect the liver: the detoxication of Cinnamomum kanahirai hay mushroom tool, can reduce SGPT, promote liver cell regeneration.Has GPT value the acute hepatopathy mouse blood of reduction from Cinnamomum kanahirai hay massee fruiting bodies type of isolating triterpenes Compound β.The triterpenes extraction quantity of Cinnamomum kanahirai hay mushroom is up to 30% extraction quantity that surpasses glossy ganoderma 3% far away.Cinnamomum kanahirai hay mushroom bitter taste is more much better than than glossy ganoderma.The many oxidized forms class triterpene and the steroid content that show the camphor tree sesame are very abundant.Experiment confirm Cinnamomum kanahirai hay mushroom has the effect that reduces SGPT and SGOT index, the snperoxiaized ability of liver fat that promotes the liver antioxidative enzyme and suppress hepatic tissue is arranged, and reach the liver protecting effect.6, immunity: the Cinnamomum kanahirai hay mushroom can promote macrophage and lysosomal activity, also can suppress the synthetic of lymphocyte DNA.
Table 1 contains the cigarette and the blank cigarette mensuration result of Cinnamomum kanahirai hay mushroom extract
Claims (7)
1. Cinnamomum kanahirai hay mushroom extract, adopt following method to prepare: one, with the Cinnamomum kanahirai hay mushroom, remove impurity, clean the 40-70 ℃ of oven dry in back, moisture is controlled to be 8-12%, is crushed to 10-100 purpose meal; Two, get the Cinnamomum kanahirai hay mushroom meal that crushes, divide to add Cinnamomum kanahirai hay mushroom meal quality 3-10 hot water doubly for 3 times respectively, maintain the temperature at lixiviate in 80-95 ℃, each lixiviate 5 hours merges 3 times water extract; Three, filter, filtrate filtered reduced pressure concentrated 2 hours under 0.05Mpa, 60 ℃ of conditions, received cream, obtained Cinnamomum kanahirai hay mushroom extract.
2. a cigarette of containing Cinnamomum kanahirai hay mushroom extract has pipe tobacco, it is characterized in that: contain the Cinnamomum kanahirai hay mushroom extract that accounts for tobacco quality 0.001-10% in the said pipe tobacco; Said Cinnamomum kanahirai hay mushroom extract adopts following method to prepare: one, with the Cinnamomum kanahirai hay mushroom, and 40-70 ℃ of oven dry, moisture is controlled to be 8-12%, is crushed to 10-100 purpose meal; Two, get the Cinnamomum kanahirai hay mushroom meal that crushes, divide to add Cinnamomum kanahirai hay mushroom meal quality 3-10 hot water doubly for 3 times respectively, maintain the temperature at lixiviate in 80-95 ℃, each lixiviate 5 hours merges 3 times water extract; Three, filter, filtrate filtered reduced pressure concentrated 2 hours under 0.05Mpa, 60 ℃ of conditions, received cream, obtained Cinnamomum kanahirai hay mushroom extract.
3. the cigarette of containing Cinnamomum kanahirai hay mushroom extract according to claim 2 is characterized in that: said Cinnamomum kanahirai hay mushroom is removed impurity, cleans the back oven dry.
4. the cigarette of containing Cinnamomum kanahirai hay mushroom extract according to claim 3 is characterized in that: after the said Cinnamomum kanahirai hay mushroom oven dry, moisture is controlled to be 8-12%.
5. the cigarette of containing Cinnamomum kanahirai hay mushroom extract according to claim 4; It is characterized in that: the said cigarette of containing Cinnamomum kanahirai hay mushroom extract adopts following method to prepare: with Cinnamomum kanahirai hay mushroom extract with 70-90 ℃ of hot water or 75% dissolve with ethanol; Solution quality concentration after the dissolving is 0.1-80%, accounts for the ratio of tobacco quality 0.001～10% in Cinnamomum kanahirai hay mushroom extract, evenly is sprayed on the pipe tobacco; Naturally dry, process cigarette by conventional cigarette processing technology again.
6. the cigarette of containing Cinnamomum kanahirai hay mushroom extract according to claim 5 is characterized in that: contain the Cinnamomum kanahirai hay mushroom extract that accounts for tobacco quality 0.1% in the said pipe tobacco.
7. the cigarette of containing Cinnamomum kanahirai hay mushroom extract according to claim 6 is characterized in that: contain the Cinnamomum kanahirai hay mushroom extract that accounts for tobacco quality 0.01% in the said pipe tobacco.
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| CN101744360B true CN101744360B (en) | 2012-05-23 |
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| CN102687852B (en) * | 2012-05-09 | 2014-01-01 | 广东神农烟科技术有限公司 | Method for extracting lactarius hatsudake tanaka extract and cigarettes containing lactarius hatsudake tanaka extract |
| CN105661629B (en) * | 2016-01-15 | 2018-03-23 | 深圳市仁泰生物科技有限公司 | Antrodia cigarette and preparation method thereof |
| CN108329999A (en) * | 2018-02-09 | 2018-07-27 | 平潭迈康生物科技有限公司 | A kind of extracting method of Antrodia camphorata essential oil and its application in teenager's health care |
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| CN1176748A (en) * | 1997-05-17 | 1998-03-25 | 严良荣 | Process for extracting polysaccharide and polyphenol mixed crystal from fresh crude and old tea leaves |
| CN1316494A (en) * | 2000-04-06 | 2001-10-10 | 张高 | Process for extracting antioxidizing agent and perfume from rosemary |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1176748A (en) * | 1997-05-17 | 1998-03-25 | 严良荣 | Process for extracting polysaccharide and polyphenol mixed crystal from fresh crude and old tea leaves |
| CN1316494A (en) * | 2000-04-06 | 2001-10-10 | 张高 | Process for extracting antioxidizing agent and perfume from rosemary |
| CN1907149A (en) * | 2006-07-31 | 2007-02-07 | 福建省安溪县铁观音文化传播有限公司 | Method for manufacturing tealamina for cigarette |
Non-Patent Citations (1)
| Title |
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| 刘华等.樟芝菌丝体的不同提取方法及其抗肿瘤活性的研究.《分离与提取》.2008,第34卷(第12期),第172-174页. * |
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Owner name: SHENZHEN DABAIHUI TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: SHENNONG YANKE TECHNOLOGY CO., LTD., GUANGDONG Effective date: 20130627 |
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Effective date of registration: 20130627 Address after: 518102 Guangdong province Shenzhen city road salt Yantian District grand Parkway high tech Industrial Park A building 11 floor Patentee after: Shenzhen Dabaihui Technology Co., Ltd. Address before: No. 2002 grand Parkway high tech Industrial Park in Deep Salt Road in Shenzhen city of Guangdong Province in 518102 Yantian District 4 Building Patentee before: Shennong Yanke Technology Co., Ltd., Guangdong |