CN102793265B - Preparation method of natural tobacco moisture retaining fumet and applications of natural tobacco moisture retaining fumet in cigarette - Google Patents
Preparation method of natural tobacco moisture retaining fumet and applications of natural tobacco moisture retaining fumet in cigarette Download PDFInfo
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- CN102793265B CN102793265B CN201210337408.9A CN201210337408A CN102793265B CN 102793265 B CN102793265 B CN 102793265B CN 201210337408 A CN201210337408 A CN 201210337408A CN 102793265 B CN102793265 B CN 102793265B
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Abstract
A preparation method of a natural tobacco moisture retaining fumet is characterized in that pittosporum tobira is taken as a raw material, is crushed, subjected to solvent extraction, filtered and concentrated to obtain the natural tobacco moisture retaining fumet. The natural tobacco moisture retaining fumet is added into tobacco shreds, so that the moisture content of the tobacco shreds basically can not be changed along with the environment humidity, the flexibility and the processing resistance of the tobacco shreds can be improved, the dry sensation and the irritation of smoke can be alleviated, the fragrance of the smoke is increased, the smoking smell is improved, and the cigarette smoke is endowed with gentle and slight faint scent. The preparation method has the outstanding characteristics that a new usage of the pittosporum tobira, pericarps and seeds is developed by a common method of a frequently-used solvent, and a new natural tobacco moisture retaining fumet is promoted.
Description
Technical field
The present invention relates to tobacco additive agent field, the specifically preparation method of a kind of natural baccy moist-keeping flavouring agent and the application in cigarette thereof, this moist-keeping flavouring agent is together with cigarette feed liquid or add separately in tobacco leaf, can improve the retention ability of tobacco, increases pliability and the resist processing of tobacco, smoker is made not have dry sensation, there is soft flue gas, dispel assorted gas, reduce excitant, improve and inhale taste, improve the effect of flue gas aroma quality.
Background technology
Production of cigarettes is a complicated process, and operation is various, advanced technology, and quality requirement is strict.The fine quality of cigarette mainly comes from the raw tobacco material used in formula, and to the processing and treating method of tobacco leaf in production of cigarettes process, and each manufacturing procedure also plays an important role.Even formula, excellent tobacco leaf preferably, also may deal with improperly because of processing or manufacture in a rough and slipshod way and scrap; Otherwise poor tobacco leaf, through meticulously suitable processing, also can make up the deficiency of its some aspect and produce good product.So scientific and rational processing technology is the guarantee of cigarette quality.In production of cigarettes process, in order to increase pliability and the resist processing of tobacco, in order to improve and improve the smoking quality of cigarette, also reinforced and perfuming process to be carried out to tobacco leaf, offal and pipe tobacco.The additive of cigarette charging is just feed liquid.Except comprising in cigarette feed liquid: except cocoa power and/or its extract, licorice powder and/or its extract, corn syrup, high-fructose corn syrup, sucrose, invert sugar, honey, molasses, dried prune concentrate, fig concentrate and raisins concentrate, also add a certain amount of humectant.The most frequently used application cigarette humectant is the earliest glycerine, propane diols, secondly also has sorbierite, diethylene glycol (DEG) and triethylene glycol etc.Wherein, what humectation ability was the strongest is glycerine and propane diols, and the two usually with the use of.Glycerine and propane diols are polyalcohols because of it, stronger water imbibition and have good cigarette humid keeping performance.But, just because of glycerine, propane diols, there is stronger water imbibition, and make the impact of the moisture content of the cigarette shreds adding glycerine and propane diols usually by ambient humidity very large.Ambient humidity is low, and the moisture content of cigarette shreds is low, and the mildness of cigarette smoke is deteriorated; Ambient humidity is large, and the moisture content of cigarette shreds is high, and cigarette shreds may go mouldy, especially at south China plum rain season.Therefore, in order to find better humectant, tobacco business just starts the developmental research of the moist-keeping agent for tobacco reducing the consumption of glycerine cigarette or alternative glycerine from the eighties in 20th century, so far developed multiple tobacco humectant, such as modified starch, KSAP-T(konjaku glucomannan and acrylic acid a kind of graft copolymer), CPL-NR(natural polysaccharide), lactic acid and lactate, citric acid, malic acid, lactic acid and Fe III, Mn II, Zn II, the complex of Ce III, pomace and orange skin water soluble pectin extract etc.Although the humid keeping performance of these humectants some be better than tobacco humectant propane diols, glycerine and the sorbierite etc. commonly used, but it adds to when burning in pipe tobacco may bring adverse influence to cigarette smoke, for example the water soluble pectin extract etc. of modified starch, KSAP-T, CPL-NR and pomace, orange skin all belongs to natural polysaccharide, add the releasing content of coke tar that not only can increase flue gas in cigarette shreds, but also the excitant of flue gas can be made to increase, inhale taste and be deteriorated; The complex of citric acid, malic acid, lactic acid and Fe III, Mn II, Zn II, Ce III may bring Fe III, Mn II, Zn II, Ce III to cigarette smoke.Therefore, development of new tobacco humectant remains one of heat subject of tobacco business research so far.
Pittosporum tobira, pittosporum tobira section pittosporum tobira belongs to, formal name used at school
pittosporum tobiraait, English name Seatung, another name daphne odera, mountain winter daphne, mountain alum.Pittosporum tobira is evergreen dungarunga or shrub, reaches as high as 3 m.The most consor branch top of leaf, narrow obovate, long 5 ~ 12 cm, wide 1 ~ 4 cm, Quan Yuan, the blunt circle in top or indent, base portion wedge shape, edge is outer volume often, has handle.Cyme top is raw; Floral white or band yellow green, have refreshing fragrance, long 0.8 ~ 1.5 cm of anthocaulus; Sepal, petal, stamen each 5; Ovary is upper, close raw pubescence.Capsule is subsphaeroidal, has corner angle, reaches 1.5 cm, and time ripe, 3 lobes split, and fruit lobe is wooden, flows out the oil-based liquid of transparent thickness, and give out a kind of simple and elegant delicate fragrance in fruit lobe; Seed cerise, also wraps up one deck oily liquids outside seed, therefore its seed is glossy shinny, and color is red gorgeous.May at florescence, fructescence October.Main component in oriental variegated coralbean leaf volatile oil is viridiflorol (40.09%), hexadecane (15.13%); Main component in tobira volatile oil is green grey dried layer alcohol (60.33%), myristicin (17.40%), ledol (5.69%), also has hendecane, nonane, α-cubebene, α-pepper alkene, α-farnesene, beta-myrcene, verbenene etc. in addition.Sea Oleum Verniciae fordii contains 6 kinds of aliphatic acid, and main fatty acid is palmitic acid (C16: 0) and oleic acid (C18: 1), and its content is respectively palmitic acid 29.66% ~ 34.72%, oleic acid 66.43% ~ 62.54%; All containing phenolic constituent, tannin, sugar, polysaccharide and glucoside, saponin, steroidal, ter penoids in pittosporum tobira seed and pericarp, flavones and the composition such as glucoside, lactone, cumarin and glucoside thereof, amino acid, polypeptide, protein, volatile oil, grease class thereof, all not containing anthraquinone and glucoside thereof, alkaloid, cupreol, fan beans alcohol and oleanolic acid in pittosporum tobira seed, are also detected.And do not detect in pericarp.Pittosporum tobira root, leaf and seed can be used as medicine.Root can dispelling, collateral-activating, blood stasis removing analgesic; Leaf can detoxify, stop blooding; Seed can puckery intestines, controlling nocturnal emission with astringent drugs.Pittosporum tobira has stronger resistance to toxic gases such as sulfur dioxide.But, except these researchs above-mentioned, about the research for application and development of solvent extractable matter in cigarette moist-keeping flavouring of paulownia leaf, flower, seed and pericarp there is no report.
Summary of the invention
Object of the present invention does not have the problem of other purposes for the cigarette shreds moisture content adding glycerine humectant in above-mentioned existing cigarette charging technology with the leaf of the variation issue of ambient humidity and pittosporum tobira, fruit and develops the oriental variegated coralbean leaf of preparation, the extract of fruit just--the agent of a kind of natural baccy moist-keeping flavouring, and to substitute or the existing cigarette humectant glycerine of Some substitute.
The object of the invention is to be achieved through the following technical solutions:
The preparation method of natural baccy moist-keeping flavouring of the present invention agent take pittosporum tobira as raw material, through pulverizing → solvent extraction → filtration → concentrated, obtains the agent of natural baccy moist-keeping flavouring.
Described pittosporum tobira is pittosporum tobira leaf or the pittosporum tobira fruit of ripe fresh or baking, and described pittosporum tobira fruit is the pittosporum tobira seed of fruit shell and its parcel.Described baking pittosporum tobira leaf or pittosporum tobira fruit are that ripe fresh pittosporum tobira leaf or pittosporum tobira fruit toast 1 ~ 24 hour at 50 ~ 300 DEG C, toast 3 ~ 5 hours at being preferably 100 ~ 130 DEG C.
Raw meal pulverized powder granularity is 40 ~ 300 orders, is preferably 100 ~ 200 orders.
At solvent extracting process, described solvent be in water, ethanol, propane diols, glycerine, ether, ethyl acetate, acetonitrile, acetone, carrene, chloroform, cyclohexane, supercritical carbon dioxide any one or its mixing, be preferably in water, ethanol, propane diols any one or its mixing.
At solvent extracting process, described extracting mode is left at room temperature immersion, mechanical oscillation, ultrasonic, add hot reflux, heating using microwave, Simultaneous distillation-extraction, surname extraction or supercritical fluid extraction, be preferably left at room temperature soak extraction combine heating reflux extraction.
Described concentration process is that under normal pressure, distillation and concentration or decompression distillation concentrate, and is preferably decompression distillation and concentrates.
Natural baccy moist-keeping flavouring of the present invention agent is added in cigarette shreds, the moisture content of added cigarette shreds can be made substantially not change with ambient humidity, increase the pliability of cigarette shreds, reduce dry sensation and the excitant of flue gas, strengthen the fragrance of flue gas, improve and inhale taste, and give the light delicate fragrance of a kind of gracefulness of cigarette smoke.The consumption of natural baccy moist-keeping flavouring agent is 0.01% ~ 1% of tobacco leaf or tobacco quality, is preferably 0.1% ~ 0.5%, during use use water, ethanol or ethanol and water mixture diluted after spray and be added on tobacco leaf smoked sheet or in pipe tobacco.Described concentration of alcohol is 50% ~ 70%.
Outstanding feature of the present invention is: the novelty teabag developing a kind of oriental variegated coralbean leaf, pericarp and seed by the method that conventional solvent is common, is proposed a kind of new natural baccy moist-keeping flavouring agent.This moist-keeping flavouring agent is together with cigarette feed liquid or add separately in tobacco leaf, the retention ability of tobacco can be improved, increase pliability and the resist processing of tobacco, reduce making of tobacco in process broken, effectively can also stop production of cigarettes, transport, storage, the scattering and disappearing of selling period cigarette shreds moisture simultaneously, smoker is made not have dry sensation, there is soft flue gas, dispel assorted gas, reduce excitant, improve and inhale taste, improve the effect of flue gas aroma quality, and give the light delicate fragrance of a kind of gracefulness of cigarette smoke.
Detailed description of the invention
The present invention is further described below in conjunction with embodiment but does not limit the present invention.
Example 1
Get the fresh oriental variegated coralbean leaf of 50g, be crushed to 100 ~ 200 orders, 50mL water is added in the slurries obtained, stir, flood 1 hour under room temperature, filter, the water of filter residue with amount repeats extraction 2 times under similarity condition, merge No. 3 extracts, under normal pressure, distillation and concentration is to thickness, obtains natural baccy moist-keeping flavouring agent I.
Example 2
Get the fresh pittosporum tobira pericarp of 50g, be crushed to 100 ~ 200 orders, 50 mL 70% ethanol are added in the powder obtained, stir, add hot reflux 0.5 ~ 1 hour, filter, 70% ethanol of filter residue with amount repeats extraction 2 times under similarity condition, merge No. 3 extracts, decompression distillation is concentrated into thickness, obtains natural baccy moist-keeping flavouring agent II.
Example 3
Get the fresh pittosporum tobira seed of 100g, toast 3 hours at 105 DEG C, pulverize, cross 100 ~ 200 mesh sieves, the mixture of 80 mL water, ethanol and 1,2-PD is added, water, ethanol and 1 in the powder obtained, the mass fraction of 2-propane diols is respectively 30%, 65% and 5%, stir, sonic oscillation 1 hour under room temperature, filter, filter residue repeats extraction 2 times with measuring with the water combining ratio, ethanol and 1,2-PD mixture under similarity condition, merges No. 3 extracts, decompression distillation is concentrated into thickness, obtains natural baccy moist-keeping flavouring agent III.
Application comparison example
Get natural baccy moist-keeping flavouring agent I, II, III, glycerine, propane diols, sorbierite and each 10g of modified starch, respectively with the dilution of 90g 50% ethanol, dilution is halved, and is sprayed on equably respectively on 0.5,1kg flue-cured tobacco pipe tobacco.Contrast adds the same amount flue-cured tobacco pipe tobacco of 50g 50% ethanol for spraying.Spray add natural baccy moist-keeping flavouring agent I, II, III, glycerine, propane diols and sorbierite pipe tobacco with contrast pipe tobacco in temperature (22 ± 1) DEG C with relative humidity (60 ± 2) % environment in regulate 48 hours, its equilibrium moisture content of employing oven method measuring.The method is divided into 3 steps: (1) surveys vessel culture dish constant weight.The culture dish writing number is put into same baking oven, dries 2 hours at 100 DEG C, take out, put into silica gel drier and be cooled to room temperature, weigh immediately
m 0, repeat, until the culture dish constant mass claimed; (2) balance mass is measured.Get 10g tobacco sample, be spread out in surface plate equably, respectively at temperature 22 DEG C, balance 48 hours in relative humidity (RH) 40%, 80% environment, rapidly by the culture dish of pipe tobacco impouring constant weight, add a cover and weigh immediately
m b; (3) balance shredded tobacco baking quality is measured.Balance pipe tobacco after weighing is put into same baking oven, opens the lid of culture dish, dry 2 hours at 100 DEG C, cover the lid of culture dish, take out, put into silica gel drier rapidly, be cooled to room temperature, weigh immediately
m dry.Calculate pipe tobacco equilibrium moisture content according to the following formula:
Pipe tobacco equilibrium moisture content=[(
m b-
m 0)-(
m dry-
m 0)]/(
m b-
m 0) × 100%
=[(
m b-
m dry)/(
m b-
m 0)] × 100%
The equilibrium moisture content testing result of tobacco sample is as table 1.Found out by table 1, the impact of equilibrium moisture content all by equilibrium humidity of contrast, interpolation glycerine, propane diols, sorbierite and modified starch tobacco sample is comparatively large, and equilibrium humidity is little, and pipe tobacco equilibrium moisture content is low, and equilibrium humidity is large, and pipe tobacco equilibrium moisture content is high.In contrast, it is less by the impact of equilibrium humidity to add the equilibrium moisture content of 3 kinds of moist-keeping flavouring agent tobacco sample prepared by the present invention, and diminishes along with the increase influence degree of addition.May be because, natural baccy moist-keeping flavouring agent I prepared by the present invention, II, III all containing a certain amount of plant wax, these plant waxs define one deck cere on pipe tobacco surface, and this cere is hydrophobic, and it can stop the moisture loss in pipe tobacco, the aqueous vapor in environment can be stoped again to enter in pipe tobacco, therefore it have good humid keeping performance.In addition, natural baccy moist-keeping flavouring agent I, II prepared by the present invention, III compares, and the humectation effect of No. II is best, III number it, No. I is slightly poor.May be less containing plant wax in the raw materials oriental variegated coralbean leaf of No. I, and these plant waxs be insoluble to the cause of its Extraction solvent water; Although the raw materials pittosporum tobira seed surface of No. III is coated with a large amount of plant waxs and grease, baking room may partly be destroyed, therefore its humectation proterties is slightly poor.Have a large amount of plant waxs and grease in the raw materials pittosporum tobira fruit shell of No. II, and be not destroyed during extracting, therefore its humectation effect is best.
the equilibrium moisture content of the tobacco sample balanced under table 12 kinds of humidity
Humectant addition/% equilibrium moisture content/%
Under RH40% under RH80%
Contrast (water) 0.5 7.26 22.85
1.0 7.26 22.85
Propane diols 0.5 7.59 23.60
1.0 7.78 24.46
Sorbierite 0.5 7.35 23.42
1.0 7.97 24.67
Glycerine 0.5 7.34 23.18
1.0 7.88 24.46
Modified starch 0.5 7.54 24.26
1.0 7.83 24.62
Moist-keeping flavouring agent I 0.5 9.96 15.85
1.0 10.73 14.56
Moist-keeping flavouring agent II 0.5 10.24 14.97
1.0 12.35 13.87
Moist-keeping flavouring agent III 0.5 10.06 15.25
1.0 11.69 14.23
Claims (7)
1. the application of pittosporum tobira natural baccy moist-keeping flavouring agent in cigarette, it is characterized in that: the agent of natural baccy moist-keeping flavouring is added in cigarette shreds, the moisture of cigarette shreds can be kept, increase the pliability of cigarette shreds, reduce dry sensation and the excitant of flue gas, strengthen the fragrance of flue gas, improve and inhale taste, and give the light delicate fragrance of a kind of gracefulness of cigarette smoke; The agent of described pittosporum tobira natural baccy moist-keeping flavouring is prepared from by the following method: pittosporum tobira raw material, through pulverizing → solvent extraction → filtration → concentrated, obtains the agent of natural baccy moist-keeping flavouring;
Described pittosporum tobira is pittosporum tobira leaf or the pittosporum tobira fruit of ripe fresh or baking, described pittosporum tobira fruit is the pittosporum tobira seed of fruit shell and shell parcel, and described baking pittosporum tobira leaf or pittosporum tobira fruit are that ripe fresh pittosporum tobira leaf or pittosporum tobira fruit toast 1 ~ 24 hour at 50 ~ 300 DEG C.
2. the application of pittosporum tobira natural baccy moist-keeping flavouring agent according to claim 1 in cigarette, is characterized in that: raw meal pulverized powder granularity is 40 ~ 300 orders.
3. the application of pittosporum tobira natural baccy moist-keeping flavouring agent according to claim 1 in cigarette, it is characterized in that: at solvent extracting process, described solvent be in water, ethanol, propane diols, glycerine, ether, ethyl acetate, acetonitrile, acetone, carrene, chloroform, cyclohexane, supercritical carbon dioxide any one or its mixing.
4. the application of pittosporum tobira natural baccy moist-keeping flavouring agent according to claim 1 in cigarette, it is characterized in that: at solvent extracting process, described extracting mode be left at room temperature immersion, mechanical oscillation, ultrasonic, add hot reflux, heating using microwave, Simultaneous distillation-extraction, surname extraction or supercritical fluid extraction.
5. the application of pittosporum tobira natural baccy moist-keeping flavouring agent according to claim 1 in cigarette, is characterized in that: described concentration process is that under normal pressure, distillation and concentration or decompression distillation concentrate.
6. the application of pittosporum tobira natural baccy moist-keeping flavouring agent according to claim 1 in cigarette, it is characterized in that: the consumption of natural baccy moist-keeping flavouring agent is 0.01% ~ 1% of tobacco leaf or tobacco quality, during use use water, ethanol or ethanol and water mixture diluted after spray and be added on tobacco leaf smoked sheet or in pipe tobacco.
7. the application of pittosporum tobira natural baccy moist-keeping flavouring agent according to claim 6 in cigarette, is characterized in that: described concentration of alcohol is 50% ~ 70%.
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| CN106174686B (en) * | 2016-07-15 | 2018-06-01 | 福建中烟工业有限责任公司 | A kind of preparation method of long column winter daphne extract |
| CN106977359A (en) * | 2017-05-03 | 2017-07-25 | 淮海工学院 | A kind of preparation method and purposes of pittosporum tobira fruit extract |
| CN107361398A (en) * | 2017-06-26 | 2017-11-21 | 河南中烟工业有限责任公司 | A kind of tea extraction in May and preparation method thereof and the application in cigarette |
| WO2019210607A1 (en) * | 2018-08-17 | 2019-11-07 | 邦泰生物工程(深圳)有限公司 | Stable nicotinamide riboside composition and preparation method therefor |
| CN109280580A (en) * | 2018-09-13 | 2019-01-29 | 云南中烟工业有限责任公司 | A kind of tealeaves baking Studies of The Aromatic Substances and the preparation method and application thereof |
| WO2024209528A1 (en) * | 2023-04-04 | 2024-10-10 | 日本たばこ産業株式会社 | Tobacco extract and method for producing same, tobacco material, tobacco rod, flavor inhaler, and smokeless tobacco |
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