CN109276656A - A kind of processing and storage method of Processed Product of Rhizoma Gastrodiae - Google Patents
A kind of processing and storage method of Processed Product of Rhizoma Gastrodiae Download PDFInfo
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- CN109276656A CN109276656A CN201811070342.5A CN201811070342A CN109276656A CN 109276656 A CN109276656 A CN 109276656A CN 201811070342 A CN201811070342 A CN 201811070342A CN 109276656 A CN109276656 A CN 109276656A
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- rhizoma gastrodiae
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- 238000003860 storage Methods 0.000 title claims abstract description 35
- 238000000034 method Methods 0.000 title claims abstract description 32
- 241000756943 Codonopsis Species 0.000 claims abstract description 21
- 239000009636 Huang Qi Substances 0.000 claims abstract description 21
- 240000006079 Schisandra chinensis Species 0.000 claims abstract description 20
- 235000008422 Schisandra chinensis Nutrition 0.000 claims abstract description 20
- 244000197580 Poria cocos Species 0.000 claims abstract description 17
- 235000008599 Poria cocos Nutrition 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 16
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 37
- 239000000047 product Substances 0.000 claims description 35
- 239000000741 silica gel Substances 0.000 claims description 35
- 229910002027 silica gel Inorganic materials 0.000 claims description 35
- 229960001866 silicon dioxide Drugs 0.000 claims description 35
- 239000002274 desiccant Substances 0.000 claims description 28
- 229920001661 Chitosan Polymers 0.000 claims description 25
- 239000007864 aqueous solution Substances 0.000 claims description 20
- 238000001035 drying Methods 0.000 claims description 18
- 239000000706 filtrate Substances 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 238000007710 freezing Methods 0.000 claims description 8
- 230000008014 freezing Effects 0.000 claims description 8
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 7
- 238000005507 spraying Methods 0.000 claims description 6
- 238000009461 vacuum packaging Methods 0.000 claims description 6
- DQMUQFUTDWISTM-UHFFFAOYSA-N O.[O-2].[Fe+2].[Fe+2].[O-2] Chemical compound O.[O-2].[Fe+2].[Fe+2].[O-2] DQMUQFUTDWISTM-UHFFFAOYSA-N 0.000 claims description 2
- 241000305491 Gastrodia elata Species 0.000 claims 1
- 239000007921 spray Substances 0.000 abstract description 17
- 230000000857 drug effect Effects 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 5
- 239000003223 protective agent Substances 0.000 abstract description 5
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract description 4
- 238000005265 energy consumption Methods 0.000 abstract description 4
- 238000003958 fumigation Methods 0.000 abstract description 4
- 229910052717 sulfur Inorganic materials 0.000 abstract description 4
- 239000011593 sulfur Substances 0.000 abstract description 4
- 230000008569 process Effects 0.000 abstract description 3
- 241000411851 herbal medicine Species 0.000 abstract description 2
- 230000001681 protective effect Effects 0.000 abstract description 2
- 241000270295 Serpentes Species 0.000 description 19
- BVJSUAQZOZWCKN-UHFFFAOYSA-N p-hydroxybenzyl alcohol Chemical compound OCC1=CC=C(O)C=C1 BVJSUAQZOZWCKN-UHFFFAOYSA-N 0.000 description 14
- PUQSUZTXKPLAPR-KSSYENDESA-N 4-(beta-D-Glucopyranosyloxy) benzyl alcohol Natural products O([C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1)c1ccc(CO)cc1 PUQSUZTXKPLAPR-KSSYENDESA-N 0.000 description 10
- PUQSUZTXKPLAPR-UJPOAAIJSA-N Gastrodin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC=C(CO)C=C1 PUQSUZTXKPLAPR-UJPOAAIJSA-N 0.000 description 10
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 10
- 229930193974 gastrodin Natural products 0.000 description 10
- PUQSUZTXKPLAPR-NZEXEKPDSA-N helicidol Natural products O([C@H]1[C@H](O)[C@H](O)[C@@H](O)[C@@H](CO)O1)c1ccc(CO)cc1 PUQSUZTXKPLAPR-NZEXEKPDSA-N 0.000 description 10
- 239000000243 solution Substances 0.000 description 10
- 230000006378 damage Effects 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- WVDDGKGOMKODPV-UHFFFAOYSA-N hydroxymethyl benzene Natural products OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 5
- 239000004615 ingredient Substances 0.000 description 5
- 229910052742 iron Inorganic materials 0.000 description 5
- 208000007443 Neurasthenia Diseases 0.000 description 4
- 241001251949 Xanthium sibiricum Species 0.000 description 4
- 206010003549 asthenia Diseases 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 208000024891 symptom Diseases 0.000 description 4
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 206010028980 Neoplasm Diseases 0.000 description 3
- PBCJIPOGFJYBJE-UHFFFAOYSA-N acetonitrile;hydrate Chemical compound O.CC#N PBCJIPOGFJYBJE-UHFFFAOYSA-N 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 238000004108 freeze drying Methods 0.000 description 3
- 230000006870 function Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000011259 mixed solution Substances 0.000 description 3
- 239000013558 reference substance Substances 0.000 description 3
- 241000238631 Hexapoda Species 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 235000019445 benzyl alcohol Nutrition 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 210000000952 spleen Anatomy 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000012085 test solution Substances 0.000 description 2
- 206010000234 Abortion spontaneous Diseases 0.000 description 1
- 206010000242 Abortion threatened Diseases 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 241000305492 Gastrodia Species 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- 208000025747 Rheumatic disease Diseases 0.000 description 1
- 208000005985 Threatened Abortion Diseases 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 230000003474 anti-emetic effect Effects 0.000 description 1
- 239000002111 antiemetic agent Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000001882 diuretic effect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 230000004064 dysfunction Effects 0.000 description 1
- 201000006549 dyspepsia Diseases 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- -1 hydroxyl Benzyl Chemical group 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 208000015994 miscarriage Diseases 0.000 description 1
- 210000003097 mucus Anatomy 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- YTJSFYQNRXLOIC-UHFFFAOYSA-N octadecylsilane Chemical compound CCCCCCCCCCCCCCCCCC[SiH3] YTJSFYQNRXLOIC-UHFFFAOYSA-N 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000000552 rheumatic effect Effects 0.000 description 1
- 238000007665 sagging Methods 0.000 description 1
- 231100000241 scar Toxicity 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 208000000995 spontaneous abortion Diseases 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 230000004206 stomach function Effects 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 208000011580 syndromic disease Diseases 0.000 description 1
- 238000011003 system suitability test Methods 0.000 description 1
- 238000009777 vacuum freeze-drying Methods 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
- A61K36/8988—Gastrodia
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/06—Fungi, e.g. yeasts
- A61K36/07—Basidiomycota, e.g. Cryptococcus
- A61K36/076—Poria
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/34—Campanulaceae (Bellflower family)
- A61K36/344—Codonopsis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/481—Astragalus (milkvetch)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/57—Magnoliaceae (Magnolia family)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/79—Schisandraceae (Schisandra family)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
- A61K36/815—Lycium (desert-thorn)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
- A61K47/36—Polysaccharides; Derivatives thereof, e.g. gums, starch, alginate, dextrin, hyaluronic acid, chitosan, inulin, agar or pectin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0087—Galenical forms not covered by A61K9/02 - A61K9/7023
- A61K9/0095—Drinks; Beverages; Syrups; Compositions for reconstitution thereof, e.g. powders or tablets to be dispersed in a glass of water; Veterinary drenches
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P25/00—Drugs for disorders of the nervous system
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Mycology (AREA)
- Engineering & Computer Science (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Neurosurgery (AREA)
- Neurology (AREA)
- Biomedical Technology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Pain & Pain Management (AREA)
- Rheumatology (AREA)
- Gastroenterology & Hepatology (AREA)
- Inorganic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to a kind of processing and storage methods of Processed Product of Rhizoma Gastrodiae, belong to Chinese herbal medicine processing and storage field.The following steps are included: (1) weighs raw material, cleans, drains；(2) prepare Schisandra chinensis, fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos extracting solution, filter it is spare；(3) precooling；(4) it is sliced；(5) spray Schisandra chinensis, fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos extracting solution；(6) protective agent is sprayed；(7) microwave vacuum freeze is dry；(8) it packs；(9) it stores.Processed Product of Rhizoma Gastrodiae of the present invention is processed, storage practice is simple, it is environmentally protective, save energy consumption, the Processed Product of Rhizoma Gastrodiae that the method for the present invention processes, without using sulfur fumigation in whole process, the shortcomings that overcoming in the prior art using sulfur fumigation, resulting Processed Product of Rhizoma Gastrodiae drug effect is stronger, and health-care effect is more preferable.
Description
Technical field
The present invention relates to a kind of processing and storage methods of Processed Product of Rhizoma Gastrodiae, belong to Chinese herbal medicine processing and storage field.
Background technique
Rhizoma Gastrodiae is in irregular lumps or strip and block, surface yellowish-brown or micro-strip brown.There is fine and closely woven vertical wrinkle, entirely
Body has strumae, the plate-like bud scar that the prominent apex of tumor has dark brown sagging more.Main root lower end is slightly thick, tumor dash forward it is larger, upwards it is tapered
Tumor is prominent smaller, and often there is one section of bavin matter stem foot on top.Apparent root trace or fibrous root residual are arranged at lower part.Matter is hard, is not easily broken, section
Yellow-white has the small oil drop being dispersed in, and center crack, and conduit group radiates arrangement, and forming layer is cyclic annular.Gas is fragrant special, sweet in flavor micro-
Toil, slightly mucus.With a big neat, surface yellowish-brown, section yellow-white, the solid person of matter is preferred.With tonifying middle-Jiao and Qi, it is good for
Spleen stomach function regulating, eliminate dampness and have diuretic effect, antiemetic rush down, hidroschesis, miscarriage prevention function.The major functions: the middle deficiency of vital energy is weak, and indigestion caused by dysfunction of the spleen, water
Swelling is full, vomiting dysentery, threatened abortion, the diseases such as physically weak spontaneous perspiration.
The quality and drug effect of Rhizoma Gastrodiae and the processing and storage method of Rhizoma Gastrodiae have obvious relation, due to containing large quantity of moisture in Rhizoma Gastrodiae
And polysaccharide, it is not easy dry and stores, thus at source in process, it generallys use drying or dries, and common sulfur fumigation
With reach drying, bleaching, sterilization and anticorrosion, improve appearance, it is easily stored the purpose of.When drying or drying too due to drying temperature
Height, exposure in air, will lead to active constituent, effective component is largely lost for a long time.It will cause Rhizoma Gastrodiaes to have for sulfur fumigation
Constituent reduction is imitated, the residual of poisonous and harmful substance but will be caused, is affected the treatment and safety.
Freeze Drying Technique is much studied and is reported in the application of the dry processing of Rhizoma Gastrodiae at present, it with dry, hot wind
Seasoning production Rhizoma Gastrodiae compare, not only phenols, vitamin and heat-sensitive ingredients etc. are not damaged, and Gastrodin, to hydroxyl
Benzyl alcohol and other flavor substances also lose the color that can seldom keep fresh goods Rhizoma Gastrodiae to the maximum extent, nutritional ingredient, outer
Sight and active material.However, simple vacuum freeze drying Rhizoma Gastrodiae, energy consumption is big, and the production cycle is long, constrains freeze-drying
The industrialized production of technology.Freeze-drying time could be saved when in some methods by being cut into very thin thickness, but yield just declines,
Specific energy consumption is increased by.Therefore how to enhance the drug effect of Rhizoma Gastrodiae, reduce Gastrodin, p-Hydroxybenzylalcohol isoreactivity component damages and
The problem of destruction of appearance is those skilled in the art's urgent need to resolve.
Summary of the invention
The technical scheme to solve the above technical problems is that
The processing and storage method of Processed Product of Rhizoma Gastrodiae of the present invention, comprising the following steps:
(1) weigh following raw material: 150-180 parts of Rhizoma Gastrodiae, 2-3 parts of Schisandra chinensis, 3-5 parts of fructus lycii, 1-3 parts of Radix Astragali,
3-5 parts of Radix Codonopsis, 2-3 parts of Poria cocos, above-mentioned raw materials are cleaned, are drained；
(2) Schisandra chinensis described in step (1), fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos is broken, it adds water to cook, filters, obtain filtrate
It is spare；
(3) by the Rhizoma Gastrodiae precooling of step (1)；
(4) Rhizoma Gastrodiae for obtaining step (3) is sliced；
(5) step (2) resulting filtrate is uniformly sprayed into the Rhizoma Gastrodiae slice surface obtained in step (4)；
(6) chitosan aqueous solution is uniformly sprayed into the Rhizoma Gastrodiae slice surface obtained in step (5) in spraying form；
(7) microwave vacuum freeze is dry: by the Rhizoma Gastrodiae slice that step (6) obtains be put into microwave vacuum freezing dryer into
Row drying；
(8) it packs: the Rhizoma Gastrodiae slice vacuum packaging that step (7) is obtained, and it is put into silica-gel desiccant.
(9) it stores: the Rhizoma Gastrodiae slice that step (8) obtains is placed in storeroom storage.
Further, in the step (2), Schisandra chinensis, fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos is crushed to 40-60 mesh, add five
Taste, fructus lycii, Radix Astragali, Radix Codonopsis, 4-5 times of Poria cocos total weight water, decocting temperature is 110-120 DEG C, and decocting time is 20-30 point
Clock.
Further, in the step (3), Rhizoma Gastrodiae is placed in -10 DEG C~-30 DEG C progress pre-freeze 1-2 hours, it is preferable that will
Rhizoma Gastrodiae is placed in -20 DEG C of progress pre-freeze 1.5 hours.
In the step (4), Rhizoma Gastrodiae is cut into the piece of 3-5mm, it is preferable that Rhizoma Gastrodiae is cut into the piece of 4mm.
In the step (6), the concentration of chitosan aqueous solution is 0.005-0.02g/L, and fountain height is every 1000g Rhizoma Gastrodiae
Medicine materical crude slice sprays 0.01-0.05L chitosan aqueous solution, it is preferable that the concentration of chitosan aqueous solution is 0.01g/L, and fountain height is every 1
Kilogram Processed Product of Rhizoma Gastrodiae sprays 0.03L chitosan aqueous solution.
In the step (7), Rhizoma Gastrodiae slice is put into microwave vacuum freezing dryer and is dried, vacuum degree 10-
60Pa, microwave power 50-200W, temperature are -40 DEG C~-45 DEG C, and drying time is 3-6 hours, it is preferable that vacuum degree is
30Pa, microwave power 100W, temperature are -45 DEG C, and drying time is 5 hours.
In the step (8), the dosage of silica-gel desiccant is to be put into silica-gel desiccant 10-50g in every 1L vacuum environment, excellent
Selection of land, the dosage of silica-gel desiccant are to be put into silica-gel desiccant 40g in every 1L vacuum environment.
The silica-gel desiccant has the raw material of following parts by weight to be made: 30-40 parts of silica gel, 8-10 parts of aluminum oxide, and three
Aoxidize 12-14 parts of two iron, it is preferable that silica-gel desiccant has the raw material of following parts by weight to be made: 35 parts of silica gel, aluminum oxide 9
Part, 13 parts of di-iron trioxide.
In the step (9), controlled at 5-10 DEG C in storeroom, relative humidity 5-15%, it is preferable that storeroom
It is interior controlled at 8 DEG C, relative humidity 10%.
The invention has the benefit that after the present invention first passes through spray Schisandra chinensis, fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos decoction
Filtrate, enhances the drug effect of Processed Product of Rhizoma Gastrodiae, then sprays chitosan aqueous solution, on the one hand double action is the ingredient that has additional nutrients, improvement
The mouthfeel of Processed Product of Rhizoma Gastrodiae, color, while having the effect of blocking make slice be not directly contacted with heat source, slowly, be effectively performed it is dry
It is dry, effective component is preferably lockked, makes Processed Product of Rhizoma Gastrodiae be easier to play, discharge its drug effect in application, and be sliced and spray to Rhizoma Gastrodiae
Chitosan aqueous solution is drenched, chitosan has good film forming, fungus growth not only can be effectively prevented, and it is effective to extend Rhizoma Gastrodiae
The ingredients from lossing time extends storage period, plays an important role in the processing and storage method of Processed Product of Rhizoma Gastrodiae of the present invention.It is further right
Precooling temperature and time accurately controls, and reduces the destruction of Gastrodin, p-Hydroxybenzylalcohol isoreactivity component damages and appearance.
Silica-gel desiccant ingredient of the present invention is simple, and drying effect is obvious, reduction drying cost, the processing of invention Processed Product of Rhizoma Gastrodiae,
Storage practice is simple, environmentally protective, saves energy consumption.The fresh Rhizoma Gastrodiae prepared through this method maintains original appearance shape completely
State, Gastrodin, p-Hydroxybenzylalcohol isoreactivity component damages are few, easily crush, long shelf-life, strong operability is easy to spread, through length
The shelf-life of the observation and detection of time, the Processed Product of Rhizoma Gastrodiae that the processing and storage method of Processed Product of Rhizoma Gastrodiae of the present invention obtains can achieve 18
A month, snake, not mouldy, and active constituent content is not reduced.
Specific embodiment
Embodiment below is that the present invention will be described in detail, only presently preferred embodiments of the present invention, not the limitation present invention.
Based on the embodiments of the present invention, obtained by those of ordinary skill in the art without making creative efforts all
Other embodiments shall fall within the protection scope of the present invention.
Embodiment 1
The processing and storage method of Processed Product of Rhizoma Gastrodiae, comprising the following steps:
(1) following raw material: 155 grams of Rhizoma Gastrodiae, 2 grams of Schisandra chinensis, 3 grams of fructus lycii, 1 gram of Radix Astragali, 3 grams of Radix Codonopsis, Fu is weighed
2 grams of Siberian cocklebur, above-mentioned raw materials are cleaned, are drained；
(2) Schisandra chinensis described in step (1), fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos are crushed to 40 mesh, add 50 grams of water, 110
It is decocted 20 minutes at a temperature of DEG C, filters, it is spare to obtain filtrate；
(3) Rhizoma Gastrodiae that step (2) obtains precooling: is placed in -10 DEG C of progress pre-freeze 1 hour；
(4) it is sliced: the Rhizoma Gastrodiae that step (3) obtains is cut into the piece of 3mm；
(5) step (2) resulting filtrate is uniformly sprayed into the Rhizoma Gastrodiae slice surface obtained in step (4)；
(6) it sprays protective agent: chitosan aqueous solution is uniformly sprayed at the Rhizoma Gastrodiae that step (5) obtains in spraying form
Slice surface, the concentration of chitosan aqueous solution are 0.005g/L, and fountain height is that every 1 kilogram of Processed Product of Rhizoma Gastrodiae sprays 40ml chitosan water
Solution；
(7) microwave vacuum freeze is dry: by the Rhizoma Gastrodiae slice that step (6) obtains be put into microwave vacuum freezing dryer into
Row drying is 10Pa in vacuum degree, and microwave power 50W, temperature is -40 DEG C, 3 hours dry；
(8) it packs: the Rhizoma Gastrodiae slice vacuum packaging that step (7) is obtained, and it is put into silica-gel desiccant, silica-gel desiccant
Dosage is to be put into silica-gel desiccant 10g in every 1L vacuum environment, and silica-gel desiccant is by 6 grams of silica gel, 1.6 grams of aluminum oxide, three
Aoxidize two iron 2.4 restrain at.
(9) it stores: the Rhizoma Gastrodiae slice that step (8) obtains is placed in storeroom storage.Indoor temperature control will be stored 5
DEG C, relative humidity is controlled 5%.
Embodiment 2
The processing and storage method of Processed Product of Rhizoma Gastrodiae, comprising the following steps:
(1) following raw material: 160 grams of Rhizoma Gastrodiae, 2 grams of Schisandra chinensis, 4 grams of fructus lycii, 2 grams of Radix Astragali, 4 grams of Radix Codonopsis, Fu is weighed
2 grams of Siberian cocklebur, above-mentioned raw materials are cleaned, are drained；
(2) Schisandra chinensis described in step (1), fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos are crushed to 45 mesh, add 60 grams of water, 115
It is decocted 25 minutes at a temperature of DEG C, filters, it is spare to obtain filtrate；
(3) Rhizoma Gastrodiae that step (2) obtains precooling: is placed in -30 DEG C of progress pre-freeze 2 hours；
(4) it is sliced: the Rhizoma Gastrodiae that step (3) obtains is cut into the piece of 5mm；
(5) step (2) resulting filtrate is uniformly sprayed into the Rhizoma Gastrodiae slice surface obtained in step (4)；
(6) it sprays protective agent: chitosan aqueous solution is uniformly sprayed at the Rhizoma Gastrodiae that step (5) obtains in spraying form
Slice surface, the concentration of chitosan aqueous solution are 0.02g/L, and fountain height is that every 1 kilogram of Processed Product of Rhizoma Gastrodiae sprays 50ml chitosan water
Solution；
(7) microwave vacuum freeze is dry: by the Rhizoma Gastrodiae slice that step (6) obtains be put into microwave vacuum freezing dryer into
Row drying is 10Pa in vacuum degree, and microwave power 50W, temperature is -40 DEG C, 3 hours dry；
(8) it packs: the Rhizoma Gastrodiae slice vacuum packaging that step (7) is obtained, and it is put into silica-gel desiccant, silica-gel desiccant
Dosage is to be put into silica-gel desiccant 10g in every 1L vacuum environment, and silica-gel desiccant is by 6 grams of silica gel, 1.6 grams of aluminum oxide, three
Aoxidize two iron 2.4 restrain at.
(9) it stores: the Rhizoma Gastrodiae slice that step (8) obtains is placed in storeroom storage.Indoor temperature control will be stored 5
DEG C, relative humidity is controlled 5%.
Embodiment 3
The processing and storage method of Processed Product of Rhizoma Gastrodiae, comprising the following steps:
(1) following raw material: 165 grams of Rhizoma Gastrodiae, 2 grams of Schisandra chinensis, 4 grams of fructus lycii, 2 grams of Radix Astragali, 4 grams of Radix Codonopsis, Fu is weighed
3 grams of Siberian cocklebur, above-mentioned raw materials are cleaned, are drained；
(2) Schisandra chinensis described in step (1), fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos are crushed to 55 mesh, add 60 grams of water, 115
It is decocted 25 minutes at a temperature of DEG C, filters, it is spare to obtain filtrate；
(3) Rhizoma Gastrodiae that step (2) obtains precooling: is placed in -30 DEG C of progress pre-freeze 2 hours；
(4) it is sliced: the Rhizoma Gastrodiae that step (3) obtains is cut into the piece of 5mm；
(5) step (2) resulting filtrate is uniformly sprayed into the Rhizoma Gastrodiae slice surface obtained in step (4)；
(6) it sprays protective agent: chitosan aqueous solution is uniformly sprayed at the Rhizoma Gastrodiae that step (5) obtains in spraying form
Slice surface, the concentration of chitosan aqueous solution are 0.01g/L, and fountain height is that every 1 kilogram of Processed Product of Rhizoma Gastrodiae sprays 25ml chitosan water
Solution；
(7) microwave vacuum freeze is dry: by the Rhizoma Gastrodiae slice that step (6) obtains be put into microwave vacuum freezing dryer into
Row drying, vacuum degree 60Pa, microwave power 200W, temperature are -45 DEG C, and drying time is 6 hours；
(8) it packs: the Rhizoma Gastrodiae slice vacuum packaging that step (7) is obtained, and it is put into silica-gel desiccant, silica-gel desiccant
Dosage is to be put into silica-gel desiccant 50g in every 1L vacuum environment, and silica-gel desiccant is by 6 grams of silica gel, 1.6 grams of aluminum oxide, three
Aoxidize two iron 2.4 restrain at.
(9) it stores: the Rhizoma Gastrodiae slice that step (8) obtains is placed in storeroom storage.Indoor temperature control will be stored to exist
10 DEG C, relative humidity is controlled 15%.
Embodiment 4
The processing and storage method of Processed Product of Rhizoma Gastrodiae, comprising the following steps:
(1) following raw material: 175 grams of Rhizoma Gastrodiae, 3 grams of Schisandra chinensis, 5 grams of fructus lycii, 3 grams of Radix Astragali, 5 grams of Radix Codonopsis, Fu is weighed
3 grams of Siberian cocklebur, above-mentioned raw materials are cleaned, are drained；
(2) Schisandra chinensis described in step (1), fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos are crushed to 60 mesh, add 80 grams of water, 120
It is decocted 30 minutes at a temperature of DEG C, filters, it is spare to obtain filtrate；
(3) Rhizoma Gastrodiae that step (2) obtains precooling: is placed in -20 DEG C of progress pre-freeze 1.5 hours；
(4) it is sliced: the Rhizoma Gastrodiae that step (3) obtains is cut into the piece of 4mm；
(5) step (2) resulting filtrate is uniformly sprayed into the Rhizoma Gastrodiae slice surface obtained in step (4)；
(6) it sprays protective agent: chitosan aqueous solution is uniformly sprayed at the Rhizoma Gastrodiae that step (5) obtains in spraying form
Slice surface, the concentration of chitosan aqueous solution are 0.01g/L, and fountain height is that every 1 kilogram of Processed Product of Rhizoma Gastrodiae sprays 30ml chitosan water
Solution；
(7) microwave vacuum freeze is dry: by the Rhizoma Gastrodiae slice that step (6) obtains be put into microwave vacuum freezing dryer into
Row drying, vacuum degree 30Pa, microwave power 100W, temperature are -45 DEG C, and drying time is 5 hours；
(8) it packs: the Rhizoma Gastrodiae slice vacuum packaging that step (7) is obtained, and it is put into silica-gel desiccant, silica-gel desiccant
Dosage is to be put into silica-gel desiccant 40g in every 1L vacuum environment, and silica-gel desiccant is by 6 grams of silica gel, 1.6 grams of aluminum oxide, three
Aoxidize two iron 2.4 restrain at.
(9) it stores: the Rhizoma Gastrodiae slice that step (8) obtains is placed in storeroom storage.Indoor temperature control will be stored 8
DEG C, relative humidity is controlled 10%.
Test example 1
Gastrodin and p-Hydroxybenzylalcohol detection method of content:
Chromatographic condition and system suitability test are using octadecylsilane chemically bonded silica as filler；With acetonitrile -0.05%
Phosphoric acid solution (3:97) is mobile phase；Detection wavelength is 220nm.Number of theoretical plate is calculated by Gastrodin peak should be not less than 5000.It is right
Preparation according to product solution takes Gastrodin reference substance, p-Hydroxybenzylalcohol reference substance appropriate, accurately weighed, adds acetonitrile water (3:97) mixed
Close solution be made mixed solution of every 1ml containing 50 μ g of Gastrodin, 25 μ g of p-Hydroxybenzylalcohol to get.The preparation of test solution
This product powder (crossing No. three sieves) about 2g is taken, it is accurately weighed, it sets in stuffed conical flask, precision addition Diluted Alcohol 50ml, weighed weight,
It is ultrasonically treated (power 120W, frequency 40kHz) 30 minutes, lets cool, then weighed weight, the weight of less loss is supplied with Diluted Alcohol, filter
It crosses, precision measures subsequent filtrate 10ml, is concentrated into and closely does without alcohol taste, and residue adds acetonitrile-water (3:97) mixed solution to dissolve, and is transferred to
In 25ml measuring bottle, be diluted to scale with acetonitrile-water (3:97) mixed solution, shake up, filter, take subsequent filtrate to get.Measuring method point
It is accurate to draw reference substance solution and each 5 μ l of test solution, inject liquid chromatograph, measurement to get.Testing result such as table one
It is shown.
One Gastrodin of table and p-Hydroxybenzylalcohol content detection result statistics
Testing result proves, maintains original mode of appearance completely through the dry Processed Product of Rhizoma Gastrodiae of this method, Gastrodin, to hydroxyl
Base benzyl alcohol isoreactivity component damages are few, and the reservation of best available component content can achieve 98.4%.
Test example 2
Comparative example 1 is set, and comparative example 1 does not spray chitosan aqueous solution, other steps are same as Example 4, and observation is being store
Deposit 6 months, 12 months, 18 each, the mouldy snake situations of each embodiment, comparative example 1 and Rhizoma Gastrodiae drying piece.Observe result such as table 2
It is shown.
The mouldy snake situation result statistical graph of table 2
| 6 months | 12 months | 18 months | |
| Embodiment 1 | Non- snake is mouldy | Non- snake is mouldy | Have slight mouldy |
| Embodiment 2 | Non- snake is mouldy | Non- snake is mouldy | Non- snake is mouldy |
| Embodiment 3 | Non- snake is mouldy | Non- snake is mouldy | Non- snake is mouldy |
| Embodiment 4 | Non- snake is mouldy | Non- snake is mouldy | Non- snake is mouldy |
| Rhizoma Gastrodiae dries piece | Non- snake is mouldy | Slight snake is mouldy | Serious snake is mouldy |
| Comparative example 1 | Non- snake is mouldy | Have slight mouldy | There is slight snake mouldy |
Statistical result shows that the processing and storage method of Processed Product of Rhizoma Gastrodiae of the present invention has apparent mildew and insect proof effect, comparison
Chitosan aqueous solution is not sprayed in example 1, the effect of mildew and insect proof can not show a candle to embodiment 1-4, and chitosan has good film forming
Property, it is possible to reduce the loss of medicinal material effective component, and it is inhibited to a variety of common bacterias, it both will not influence drug effect,
It can prevent medicinal material infested mouldy again, extend storage period, play an important role in the processing and storage method of Processed Product of Rhizoma Gastrodiae of the present invention.
Test example 3
Be arranged comparative example 2, comparative example 2 do not spray Schisandra chinensis, fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos extracting solution, other steps
It is same as Example 4, select the age 40-60 years old male or female region it is unlimited with rheumatic pain volunteer 100, point
It is 2 groups, every group of 50 people.The Processed Product of Rhizoma Gastrodiae of comparative example 2 and embodiment 4+ are impregnated 10 minutes, the 1st group is drunk embodiment the 4, the 2nd
Group drinks comparative example 2, and after one month, what first group of pain symptom mitigated has 48 people, and what second group of pain symptom mitigated has 29 people.
Test example 4
Select the age 30-50 years old male or female region it is unlimited with neurasthenia or neurasthenia syndrome volunteer
200, it is divided into 2 groups, every group of 100 people.The Processed Product of Rhizoma Gastrodiae of above-mentioned comparative example 2 and embodiment 4 is impregnated 10 minutes, the 1st group is drunk
Embodiment 4, after the 2nd group is drunk comparative example 2,20 days, what first group of neurasthenia symptom mitigated has 95 people, second group of neurasthenia
What symptom mitigated has 60 people.
The results show, Rhizoma Gastrodiae of the present invention slice spray Schisandra chinensis, fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos extracting solution, can
To enhance the drug effect of Rhizoma Gastrodiae, make Rhizoma Gastrodiae slice healthcare function enhancing of the present invention.
Claims (9)
1. a kind of processing and storage method of Processed Product of Rhizoma Gastrodiae, which comprises the following steps:
(1) following raw material: 150-180 parts of Rhizoma Gastrodiae, 2-3 parts of Schisandra chinensis, 3-5 parts of fructus lycii, 1-3 parts of Radix Astragali, Radix Codonopsis is weighed
3-5 parts, 2-3 parts of Poria cocos, above-mentioned raw materials are cleaned, are drained；
(2) Schisandra chinensis described in step (1), fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos is broken, it adds water to cook, filters, it is standby to obtain filtrate
With；
(3) by the Rhizoma Gastrodiae precooling of step (1)；
(4) Rhizoma Gastrodiae for obtaining step (3) is sliced；
(5) step (2) resulting filtrate is uniformly sprayed into the Rhizoma Gastrodiae slice surface obtained in step (4)；
(6) chitosan aqueous solution is uniformly sprayed into the Rhizoma Gastrodiae slice surface obtained in step (5) in spraying form；
(7) microwave vacuum freeze is dry: the Rhizoma Gastrodiae slice that step (6) obtains being put into microwave vacuum freezing dryer and is done
It is dry；
(8) it packs: the Rhizoma Gastrodiae slice vacuum packaging that step (7) is obtained, and it is put into silica-gel desiccant.
(9) it stores: the Rhizoma Gastrodiae slice that step (8) obtains is placed in storeroom storage.
2. a kind of processing and storage method of Processed Product of Rhizoma Gastrodiae according to claim 1, which is characterized in that in the step (2),
Schisandra chinensis, fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos are crushed to 40-60 mesh, add Schisandra chinensis, fructus lycii, Radix Astragali, Radix Codonopsis, Poria cocos total weight
4-5 times of water, decocting temperature is 110-120 DEG C, and decocting time is 20-30 minutes.
3. a kind of processing and storage method of Processed Product of Rhizoma Gastrodiae according to claim 1, which is characterized in that in the step (3),
The temperature of precooling is -10 DEG C~-30 DEG C, and the time of precooling is 1-2 hours.
4. a kind of processing and storage method of Processed Product of Rhizoma Gastrodiae according to claim 1, which is characterized in that in the step (4),
Rhizoma Gastrodiae slice with a thickness of 3-5mm.
5. a kind of processing and storage method of Processed Product of Rhizoma Gastrodiae according to claim 1, which is characterized in that in the step (6),
The concentration of chitosan aqueous solution is 0.005-0.02g/L, and fountain height is that every 1000g Rhizoma Gastrodiae slice sprinkling 0.01-0.05ml shell is poly-
Sugar aqueous solution.
6. a kind of processing and storage method of Processed Product of Rhizoma Gastrodiae according to claim 1, which is characterized in that in the step (7),
Gastrodia elata slice is put into microwave vacuum freezing dryer and is dried, vacuum degree 10-60Pa, microwave power 50-200W, temperature
Degree is -40 DEG C~-45 DEG C, and drying time is 3-6 hours.
7. a kind of processing and storage method of Processed Product of Rhizoma Gastrodiae according to claim 1, which is characterized in that in the step (8),
The dosage of silica-gel desiccant is to be put into silica-gel desiccant 10-50g in every 1L vacuum environment.
8. a kind of processing and storage method of Processed Product of Rhizoma Gastrodiae according to claim 7, which is characterized in that the silica-gel desiccant
It is made of raw material from the following weight: 30-40 parts of silica gel, 8-10 parts of aluminum oxide, 12-14 parts of di-iron trioxide.
9. a kind of processing and storage method of Processed Product of Rhizoma Gastrodiae according to claim 1, which is characterized in that in the step (9),
Controlled at 5-10 DEG C in storeroom, relative humidity 5-15%.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115120677A (en) * | 2022-07-16 | 2022-09-30 | 陕西康惠制药股份有限公司 | Traditional Chinese medicine composition for tonifying kidney and soothing nerves and preparation method thereof |
| CN115120678A (en) * | 2022-07-16 | 2022-09-30 | 陕西康惠制药股份有限公司 | Traditional Chinese medicine composition for treating neurasthenia, insomnia and dreaminess and preparation method thereof |
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| CN107308350A (en) * | 2017-07-15 | 2017-11-03 | 浙江尖峰健康科技有限公司 | A kind of rhizoma Gastrodiae microwave vacuum freeze drying means |
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| CN107308350A (en) * | 2017-07-15 | 2017-11-03 | 浙江尖峰健康科技有限公司 | A kind of rhizoma Gastrodiae microwave vacuum freeze drying means |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115120677A (en) * | 2022-07-16 | 2022-09-30 | 陕西康惠制药股份有限公司 | Traditional Chinese medicine composition for tonifying kidney and soothing nerves and preparation method thereof |
| CN115120678A (en) * | 2022-07-16 | 2022-09-30 | 陕西康惠制药股份有限公司 | Traditional Chinese medicine composition for treating neurasthenia, insomnia and dreaminess and preparation method thereof |
| CN115120678B (en) * | 2022-07-16 | 2023-05-26 | 陕西康惠制药股份有限公司 | Preparation method of traditional Chinese medicine composition for neurasthenia, insomnia and dreaminess |
| CN115120677B (en) * | 2022-07-16 | 2023-05-26 | 陕西康惠制药股份有限公司 | Traditional Chinese medicine composition for tonifying kidney and soothing nerves and preparation method thereof |
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