CN102793265A - Preparation method of natural tobacco moisture retaining fumet and applications of natural tobacco moisture retaining fumet in cigarette - Google Patents
Preparation method of natural tobacco moisture retaining fumet and applications of natural tobacco moisture retaining fumet in cigarette Download PDFInfo
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- CN102793265A CN102793265A CN2012103374089A CN201210337408A CN102793265A CN 102793265 A CN102793265 A CN 102793265A CN 2012103374089 A CN2012103374089 A CN 2012103374089A CN 201210337408 A CN201210337408 A CN 201210337408A CN 102793265 A CN102793265 A CN 102793265A
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Abstract
A preparation method of a natural tobacco moisture retaining fumet is characterized in that pittosporum tobira is taken as a raw material, is crushed, subjected to solvent extraction, filtered and concentrated to obtain the natural tobacco moisture retaining fumet. The natural tobacco moisture retaining fumet is added into tobacco shreds, so that the moisture content of the tobacco shreds basically can not be changed along with the environment humidity, the flexibility and the processing resistance of the tobacco shreds can be improved, the dry sensation and the irritation of smoke can be alleviated, the fragrance of the smoke is increased, the smoking smell is improved, and the cigarette smoke is endowed with gentle and slight faint scent. The preparation method has the outstanding characteristics that a new usage of the pittosporum tobira, pericarps and seeds is developed by a common method of a frequently-used solvent, and a new natural tobacco moisture retaining fumet is promoted.
Description
Technical field
The present invention relates to the tobacco additive agent field, specifically is the preparation method of a kind of natural baccy moist-keeping flavouring agent and the application in cigarette thereof, and this moist-keeping flavouring agent is with the cigarette feed liquid or add in the tobacco leaf separately; Can improve the retention ability of tobacco, increase pliability and the anti-processability of tobacco, make the smoker not have dry sensation; Have soft flue gas, dispel assorted gas, reduce excitant; Improve and inhale flavor, the effect that improves the flue gas aroma quality.
Background technology
Production of cigarettes is the process of a complicacy, and operation is various, advanced technology, and quality requirement is strict.The fine quality of cigarette mainly comes from employed raw tobacco material in the prescription, and in the production of cigarettes process to the processing and treating method of tobacco leaf, and each manufacturing procedure also plays an important role.Even prescription, good tobacco leaf preferably are also maybe be because of processed improper or manufacture in a rough and slipshod way and scrap; Otherwise relatively poor tobacco leaf through the processing of meticulous proper process, also can remedy the deficiency of its some aspect and produces better products.So scientific and rational processing technology is the assurance of cigarette quality.In the production of cigarettes process,,, also to feed in raw material and the perfuming processing to tobacco leaf, offal and pipe tobacco in order to improve and improve the smoking quality of cigarette for pliability and the anti-processability that increases tobacco.The additive that cigarette charging is used just is feed liquid.In the cigarette feed liquid except that comprising: cocoa power and/or its extract, licorice powder and/or its extract, corn syrup, high-fructose corn syrup, sucrose, invert sugar, honey, molasses, dried prune concentrate, fig concentrate and the raisins concentrate, also add a certain amount of humectant.The most frequently used application cigarette humectant the earliest is glycerine, propane diols, secondly also has sorbierite, diethylene glycol (DEG) and triethylene glycol etc.Wherein, what the humectation ability was the strongest is glycerine and propane diols, and the two usually is used.Glycerine and propane diols are polyalcohols because of it, stronger water imbibition and have the performance of cigarette humectation preferably.Yet, have stronger water imbibition just because of glycerine, propane diols, and make the moisture content of the cigarette shreds that adds glycerine and propane diols receive the influence of ambient humidity very big usually.Ambient humidity is low, and the moisture content of cigarette shreds is low, the soft property variation of cigarette smoke; Ambient humidity is big, and the moisture content of cigarette shreds is high, and cigarette shreds may go mouldy, especially at China's south plum rain season.Therefore; In order to seek better humectant; Tobacco business since the eighties in 20th century just reduce the developmental research of the moist-keeping agent for tobacco of consumption or the alternative glycerine of glycerine in cigarette; So far developed multiple tobacco humectant, such as the water soluble pectin extract of complex, pomace and the orange skin of modified starch, KSAP-T (konjaku glucomannan and acrylic acid a kind of graft copolymer), CPL-NR (a kind of natural polysaccharide), lactic acid and lactate, citric acid, malic acid, lactic acid and Fe III, Mn II, Zn II, Ce III etc.Though some tobacco humectant propane diols, glycerine and sorbierite etc. that are superior to using always of the humectation performance of these humectants; But adding to when burning in the pipe tobacco, it may bring adverse influence to cigarette smoke; For example the water soluble pectin extract of modified starch, KSAP-T, CPL-NR and pomace, orange skin etc. all belongs to natural polysaccharide; Not only can increase the releasing content of coke tar of flue gas in the adding cigarette shreds, but also the excitant of flue gas is increased, inhale the flavor variation; The complex of citric acid, malic acid, lactic acid and Fe III, Mn II, Zn II, Ce III may bring Fe III, Mn II, Zn II, Ce III to cigarette smoke.Therefore, the development of new tobacco humectant remains one of heat subject of tobacco business research so far.
Pittosporum tobira, pittosporum tobira section pittosporum tobira belongs to, formal name used at school
Pittosporum tobiraAit, English name Seatung, another name daphne odera, mountain winter daphne, mountain alum.Pittosporum tobira is evergreen dungarunga or shrub, reaches as high as 3 m.The most consor branches of leaf top, narrow obovate, long 5～12 cm, wide 1～4 cm, full edge, blunt circle in top or indent, the base portion wedge shape, the normal outer volume in edge has handle.Give birth on the cyme top; Floral white or band yellow green have mentally refreshing fragrance, long 0.8～1.5 cm of anthocaulus; Sepal, petal, stamen each 5; Ovary is upper, close living pubescence.Capsule is subsphaeroidal, and corner angle are arranged, and reaches 1.5 cm, and 3 lobes split when ripe, and the fruit lobe is wooden, flows out the oil-based liquid of transparent thickness in the fruit lobe, and gives out a kind of simple and elegant delicate fragrance; The seed cerise, one deck oily liquids is also wrapped up in the seed outside, so its seed is glossy shinny, color is red gorgeous.May at florescence, fructescence October.Main component in the oriental variegated coralbean leaf volatile oil is viridiflorol (40.09%), hexadecane (15.13%); Main component in the tobira volatile oil is green grey dried layer alcohol (60.33%), myristicin (17.40%), ledol (5.69%), also has hendecane, nonane, α-cubebene, α-pepper alkene, α-farnesene, beta-myrcene, verbenene etc. in addition.The sea Oleum Verniciae fordii contains 6 kinds of aliphatic acid, main aliphatic acid be palmitic acid (C16: 0) and oleic acid (C18: 1), its content is respectively palmitic acid 29.66%～34.72%, oleic acid 66.43%～62.54%; All contain phenolic constituent, tannin, sugar, polysaccharide and glucoside, saponin, steroidal, ter penoids in pittosporum tobira seed and the pericarp; Compositions such as flavones and glucoside thereof, lactone, cumarin and glucoside thereof, amino acid, polypeptide, protein, volatile oil, grease class; All do not contain anthraquinone and glucoside thereof, also detected alkaloid, cupreol, the pure and mild oleanolic acid of fan beans in the pittosporum tobira seed.And do not detect in the pericarp.Pittosporum tobira root, leaf and seed can be used as medicine.Root can dispelling, collateral-activating, blood stasis removing analgesic; Leaf can detoxify, stop blooding; Seed can puckery intestines, controlling nocturnal emission with astringent drugs.Pittosporum tobira has stronger resistance to toxic gases such as sulfur dioxide.Yet except that above-mentioned these researchs, the research for application and development of solvent extractable matter in the cigarette moist-keeping flavouring of relevant paulownia leaf, flower, seed and pericarp still do not have report.
Summary of the invention
The object of the invention just to the cigarette shreds moisture content that adds the glycerine humectant in the above-mentioned existing cigarette charging technology with the leaf of the variation issue of ambient humidity and pittosporum tobira, problem that fruit does not have other purposes and the oriental variegated coralbean leaf of development and preparation, the extract of fruit--a kind of natural baccy moist-keeping flavouring agent, to substitute or the alternative existing cigarette humectant glycerine of part.
The objective of the invention is to realize through following technical scheme:
The preparation method of natural baccy moist-keeping flavouring of the present invention agent is to be raw material with the pittosporum tobira, and warp pulverizing → solvent extraction → filtration → concentrate obtains the agent of natural baccy moist-keeping flavouring.
Said pittosporum tobira is the pittosporum tobira leaf or the pittosporum tobira fruit of ripe and fresh or baking, and said pittosporum tobira fruit is the pittosporum tobira seed of fruit shell and its parcel.Said baking pittosporum tobira leaf or pittosporum tobira fruit are that ripe and fresh pittosporum tobira leaf or pittosporum tobira fruit toasted 1～24 hour down in 50～300 ℃, are preferably 100～130 ℃ and toast 3～5 hours down.
The powder size of raw material pulverizing is 40～300 orders, is preferably 100～200 orders.
In the solvent extraction process; Said solvent be in water, ethanol, propane diols, glycerine, ether, ethyl acetate, acetonitrile, acetone, carrene, chloroform, cyclohexane, the supercritical carbon dioxide any one or its mix, be preferably any one or its mixing in water, ethanol, the propane diols.
In the solvent extraction process; Said extracting mode be leave standstill immersion, mechanical oscillation, ultrasonic, reflux, heating using microwave under the room temperature, distillation extraction, Suo Shi extract or supercritical fluid extraction simultaneously, be preferably to leave standstill soaking and extracting under the room temperature and combine the reflux extraction.
Said concentration process is that distillation concentrates or decompression distillation concentrates under the normal pressure, is preferably decompression distillation and concentrates.
Natural baccy moist-keeping flavouring of the present invention agent is added in the cigarette shreds; Can make add cigarette shreds moisture content do not change basically with ambient humidity; Increase the pliability of cigarette shreds, reduce the dry sensation and the excitant of flue gas, strengthen the fragrance of flue gas; Improve and inhale flavor, and give the light delicate fragrance of a kind of gracefulness of cigarette smoke.The consumption of natural baccy moist-keeping flavouring agent is 0.01%～1% of tobacco leaf or a tobacco quality, is preferably 0.1%～0.5%, during use after the mixture diluted of water, ethanol or ethanol and water spray be added on the tobacco leaf smoked sheet or in the pipe tobacco.Said concentration of alcohol is 50%～70%.
Outstanding feature of the present invention is: use the common method of solvent commonly used to develop the new purposes of a kind of oriental variegated coralbean leaf, pericarp and seed, released a kind of new natural baccy moist-keeping flavouring agent.This moist-keeping flavouring agent is with the cigarette feed liquid or add separately in the tobacco leaf, can improve the retention ability of tobacco, increases pliability and the anti-processability of tobacco; It is broken to reduce making of tobacco in the process, can also effectively stop scattering and disappearing of production of cigarettes, transportation, storage, selling period cigarette shreds moisture simultaneously, makes the smoker not have dry sensation; Has soft flue gas; Dispel assorted gas, reduce excitant, improve and inhale flavor; Improve the effect of flue gas aroma quality, and give the light delicate fragrance of a kind of gracefulness of cigarette smoke.
The specific embodiment
The present invention further describes below in conjunction with embodiment but does not limit the present invention.
Instance 1
Get the fresh oriental variegated coralbean leaf of 50g, be crushed to 100～200 orders, add 50mL water in the slurries that obtain; Stir, dipping is 1 hour under the room temperature, filters; Filter residue repeats to extract 2 times under similarity condition with the water with amount; Merge No. 3 times extract, normal pressure distillation down is concentrated into thickness, obtains natural baccy moist-keeping flavouring agent I.
Instance 2
Get the fresh pittosporum tobira pericarp of 50g, be crushed to 100～200 orders, add 50 mL, 70% ethanol in the powder that obtains; Stir, reflux 0.5～1 hour is filtered; Filter residue repeats to extract 2 times under similarity condition with 70% ethanol with amount; Merge No. 3 times extract, decompression distillation is concentrated into thickness, obtains natural baccy moist-keeping flavouring agent II.
Instance 3
Get the fresh pittosporum tobira seed of 100g, 105 ℃ were toasted 3 hours down, pulverized, and crossed 100～200 mesh sieves; Add 80 mL water, ethanol and 1 in the powder that obtains, the mixture of 2-propane diols, water, ethanol and 1, the mass fraction of 2-propane diols is respectively 30%; 65% and 5%, stir, sonic oscillation is 1 hour under the room temperature; Filter, filter residue is with measuring water, the ethanol and 1 of composition and division in a proportion on the same group together, and the 2-propylene glycol mixtures repeats to extract 2 times under similarity condition; Merge No. 3 times extract, decompression distillation is concentrated into thickness, obtains natural baccy moist-keeping flavouring agent III.
Use comparative example
Get natural baccy moist-keeping flavouring agent I, II, each 10g of III, glycerine, propane diols, sorbierite and modified starch, with the dilution of 90g 50% ethanol, dilution is halved, and is sprayed on 0.5 equably respectively, on the 1kg flue-cured tobacco pipe tobacco respectively.Contrast adds the same amount flue-cured tobacco pipe tobacco of 50g 50% ethanol for spray.Spray adds natural baccy moist-keeping flavouring agent I, II, the pipe tobacco of III, glycerine, propane diols and sorbierite and contrast pipe tobacco in temperature (22 ± 1) ℃ and relative humidity (60 ± 2) % environment in adjusting 48 hours, its equilibrium moisture content of employing oven method measuring.This method was divided into for 3 steps: vessel culture dish constant weight is surveyed in (1).The culture dish of writing number is put into same baking oven, and 100 ℃ were dried by the fire 2 hours down, took out, and put into silica gel drier and were cooled to room temperature, weighed immediately
m 0, repetitive operation, until claim the culture dish constant mass; (2) measure balance mass.Get the 10g tobacco sample, be spread out in equably in the surface plate, respectively at 22 ℃ of temperature, balance is 48 hours in relative humidity (RH) 40%, 80% environment, rapidly in the culture dish with pipe tobacco impouring constant weight, adds a cover and weighs immediately
m b(3) measure balance shredded tobacco baking quality.Balance pipe tobacco after weighing is put into same baking oven, open the lid of culture dish, 100 ℃ were dried by the fire 2 hours down, covered the lid of culture dish, took out, and put into silica gel drier rapidly, were cooled to room temperature, weighed immediately
m BakingAccording to computes pipe tobacco equilibrium moisture content:
The pipe tobacco equilibrium moisture content=[(
m b-
m 0)-(
m Baking-
m 0)]/(
m b-
m 0) * 100%
=[(
m b-
m Baking)/(
m b-
m 0)] * 100%
The equilibrium moisture content testing result such as the table 1 of tobacco sample.Found out that by table 1 equilibrium moisture content of contrast, interpolation glycerine, propane diols, sorbierite and modified starch tobacco sample all receives the influence of equilibrium humidity bigger, equilibrium humidity is little, and the pipe tobacco equilibrium moisture content is low, and equilibrium humidity is big, and the pipe tobacco equilibrium moisture content is high.Compare with it, the equilibrium moisture content of adding 3 kinds of moist-keeping flavouring agent tobacco sample of the present invention's preparation receives the influence of equilibrium humidity less, and along with the increase influence degree of addition diminishes.Possibly be because, the natural baccy moist-keeping flavouring agent I of the present invention preparation, II; III all contains a certain amount of plant wax; These plant waxs have formed one deck cere on the pipe tobacco surface, and this cere is hydrophobic, and it can stop the moisture loss in the pipe tobacco; Can stop the aqueous vapor in the environment to get in the pipe tobacco, again so it has humectation performance preferably.In addition, the natural baccy moist-keeping flavouring agent I of the present invention preparation, II, III is compared, the humectation effect of II number is best, the III number it, I is number poor slightly.Possibly be that to contain the plant wax in the preparation raw material oriental variegated coralbean leaf of I number less, and these plant waxs are insoluble to the cause that it extracts aqueous solvent; Though the preparation raw material pittosporum tobira seed surface of III number is coated with a large amount of plant wax and grease, possibly partly be destroyed between baking, so its humectation proterties is poor slightly.In the preparation raw material pittosporum tobira fruit shell of II number a large amount of plant wax and grease are arranged, and be not destroyed during extracting, so its humectation effect is best.
The equilibrium moisture content of the tobacco sample of balance under 2 kinds of humidity of table 1
Humectant addition/% equilibrium moisture content/%
Under the RH40% under the RH80%
Contrast (water) 0.5 7.26 22.85
1.0 7.26 22.85
Propane diols 0.5 7.59 23.60
1.0 7.78 24.46
Sorbierite 0.5 7.35 23.42
1.0 7.97 24.67
Glycerine 0.5 7.34 23.18
1.0 7.88 24.46
Modified starch 0.5 7.54 24.26
1.0 7.83 24.62
Moist-keeping flavouring agent I 0.5 9.96 15.85
1.0 10.73 14.56
Moist-keeping flavouring agent II 0.5 10.24 14.97
1.0 12.35 13.87
Moist-keeping flavouring agent III 0.5 10.06 15.25
1.0 11.69 14.23
Claims (10)
1. the preparation method of natural baccy moist-keeping flavouring agent is characterized in that: be to be raw material with the pittosporum tobira, through pulverizings → solvent extraction → filtration → concentrated, obtain the agent of natural baccy moist-keeping flavouring.
2. the preparation method of natural baccy moist-keeping flavouring according to claim 1 agent is characterized in that: said pittosporum tobira is the pittosporum tobira leaf or the pittosporum tobira fruit of ripe and fresh or baking, and said pittosporum tobira fruit is the pittosporum tobira seed of fruit shell and shell parcel.
3. the preparation method of natural baccy moist-keeping flavouring according to claim 2 agent; It is characterized in that: said baking pittosporum tobira leaf or pittosporum tobira fruit are that ripe and fresh pittosporum tobira leaf or pittosporum tobira fruit toasted 1～24 hour down in 50～300 ℃, are preferably 100～130 ℃ and toast 3～5 hours down.
4. the preparation method of natural baccy moist-keeping flavouring according to claim 1 agent is characterized in that: the powder size of raw material pulverizing is 40～300 orders, is preferably 100～200 orders.
5. the preparation method of natural baccy moist-keeping flavouring according to claim 1 agent; It is characterized in that: in the solvent extraction process; Said solvent be in water, ethanol, propane diols, glycerine, ether, ethyl acetate, acetonitrile, acetone, carrene, chloroform, cyclohexane, the supercritical carbon dioxide any one or its mix, be preferably any one or its mixing in water, ethanol, the propane diols.
6. the preparation method of natural baccy moist-keeping flavouring according to claim 1 agent; It is characterized in that: in the solvent extraction process; Said extracting mode be leave standstill immersion, mechanical oscillation, ultrasonic, reflux, heating using microwave under the room temperature, distillation extraction, Suo Shi extract or supercritical fluid extraction simultaneously, be preferably and leave standstill soaking and extracting or reflux extraction under the room temperature.
7. the preparation method of natural baccy moist-keeping flavouring according to claim 1 agent is characterized in that: said concentration process is that distillation concentrates or decompression distillation concentrates under the normal pressure, is preferably decompression distillation and concentrates.
8. the application of natural baccy moist-keeping flavouring agent in cigarette of preparing according to claim 1 preparation method; It is characterized in that: this natural baccy moist-keeping flavouring agent is added in the cigarette shreds, can be kept the moisture of cigarette shreds, increase the pliability of cigarette shreds; Reduce the dry sensation and the excitant of flue gas; Strengthen the fragrance of flue gas, improve and inhale flavor, and give the light delicate fragrance of a kind of gracefulness of cigarette smoke.
9. the application of natural baccy moist-keeping flavouring according to claim 8 agent in cigarette; It is characterized in that: the consumption of natural baccy moist-keeping flavouring agent is 0.01%～1% of tobacco leaf or a tobacco quality; Be preferably 0.1%～0.5%, during use after the mixture diluted of water, ethanol or ethanol and water spray be added on the tobacco leaf smoked sheet or in the pipe tobacco.
10. the application of natural baccy moist-keeping flavouring according to claim 9 agent in cigarette is characterized in that: said concentration of alcohol is 50%～70%.
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| CN106174686A (en) * | 2016-07-15 | 2016-12-07 | 福建中烟工业有限责任公司 | A kind of preparation method of long column winter daphne extract |
| CN106977359A (en) * | 2017-05-03 | 2017-07-25 | 淮海工学院 | A kind of preparation method and purposes of pittosporum tobira fruit extract |
| CN107361398A (en) * | 2017-06-26 | 2017-11-21 | 河南中烟工业有限责任公司 | A kind of tea extraction in May and preparation method thereof and the application in cigarette |
| CN109280580A (en) * | 2018-09-13 | 2019-01-29 | 云南中烟工业有限责任公司 | A kind of tealeaves baking Studies of The Aromatic Substances and the preparation method and application thereof |
| CN110913864A (en) * | 2018-08-17 | 2020-03-24 | 邦泰生物工程(深圳)有限公司 | Stable nicotinamide riboside composition and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106174686A (en) * | 2016-07-15 | 2016-12-07 | 福建中烟工业有限责任公司 | A kind of preparation method of long column winter daphne extract |
| CN106977359A (en) * | 2017-05-03 | 2017-07-25 | 淮海工学院 | A kind of preparation method and purposes of pittosporum tobira fruit extract |
| CN107361398A (en) * | 2017-06-26 | 2017-11-21 | 河南中烟工业有限责任公司 | A kind of tea extraction in May and preparation method thereof and the application in cigarette |
| CN110913864A (en) * | 2018-08-17 | 2020-03-24 | 邦泰生物工程(深圳)有限公司 | Stable nicotinamide riboside composition and preparation method thereof |
| CN110913864B (en) * | 2018-08-17 | 2022-12-13 | 邦泰生物工程(深圳)有限公司 | Stable nicotinamide ribose composition and preparation method thereof |
| CN109280580A (en) * | 2018-09-13 | 2019-01-29 | 云南中烟工业有限责任公司 | A kind of tealeaves baking Studies of The Aromatic Substances and the preparation method and application thereof |
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| CN102793265B (en) | 2015-01-07 |
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Inventor after: Liu Liquan Inventor after: Wang Yuexia Inventor after: Liu Yali Inventor after: Zhou Yaning Inventor after: Hong Guangfeng Inventor after: Hong Qunye Inventor after: Jia Nan Inventor after: Wang Zhibo Inventor before: Liu Liquan Inventor before: Wang Yuexia |
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