CN108157552A - A kind of preparation method of golden camellia tea active material lozenge - Google Patents
A kind of preparation method of golden camellia tea active material lozenge Download PDFInfo
- Publication number
- CN108157552A CN108157552A CN201711458830.9A CN201711458830A CN108157552A CN 108157552 A CN108157552 A CN 108157552A CN 201711458830 A CN201711458830 A CN 201711458830A CN 108157552 A CN108157552 A CN 108157552A
- Authority
- CN
- China
- Prior art keywords
- golden camellia
- camellia tea
- active material
- parts
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
- A23F3/30—Further treatment of dried tea extract; Preparations produced thereby, e.g. instant tea
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
- A23F3/18—Extraction of water soluble tea constituents
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Medicines Containing Plant Substances (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention belongs to Camellia nitidissima processing technique field, specifically a kind of golden camellia tea active material process for preparing buccal lozenge.Preparation method is：First active material is extracted from fresh golden camellia tea, then dry powder is made, in the allotment for carrying out ingredient, golden camellia tea active material powder, trehalose, maltitol, beta-cyclodextrin, Herba Menthae powder are uniformly mixed, then magnesium stearate is added in, powder 5s is beaten in sodium carboxymethylcellulose mixing, obtain mixed-powder, then carry out tabletting, sterilizing, packaging process up to golden camellia tea active material lozenge.The lozenge nutrition of the present invention is high, and stability is good, and palatability is good, is easy to be digested, and it is easy to carry, preserve and edible.
Description
Technical field
The invention belongs to Camellia nitidissima processing technique field, specifically a kind of golden camellia tea active material lozenge preparation side
Method.
Background technology
Camellia nitidissima belongs to Theaceae, Camellia, is all Theaceae Camellia with tea, camellia, South Mountain tea, oil tea, tea plum etc.
Plant.Camellia nitidissima is the distinctive rare ancient tea tree breed in Guangxi.With the gradually development studied Camellia nitidissima, medical value
Also it is more found, is listed in first-grade state protection plant, enjoy the good reputations such as " tea race queen ", " plant kingdom giant panda ".Gold
Contain a variety of chemical compositions such as flavonoids, tea polysaccharide, polyphenol, saponins, liposoluble constituent, trace element in the leaf of jasmine tea.Through
Crossing experiment proves that there is Camellia nitidissima significant antibacterial, anticancer, antioxidant activity, radioresistance, lowering blood pressure and blood fat, reduction courage to consolidate
Alcohol, strengthen immunity and atherosclerosis and other effects.In order to utilize the active material in golden camellia tea, to Camellia nitidissima
Leaf active material is processed extraction.
Golden camellia tea has the health of human body facilitation, and the active substance solution entrance of golden camellia tea extraction has bitter taste
Road, somebody are not easily accepted by, and outgoing carry bothers, and are unfavorable for extending the relevant added value of Camellia nitidissima.
Invention content
The present invention provides a kind of preparation method of golden camellia tea active material lozenge, and the lozenge nutrition being prepared is high, surely
Qualitative good, palatability is good, is easy to be digested, and it is easy to carry, preserve and edible, may advantageously facilitate and Camellia nitidissima phase
The exploitation of product is closed, improves the application value of Camellia nitidissima.
The present invention realizes in this way：A kind of preparation method of golden camellia tea active material lozenge, the preparation
Method and step includes：
(1) extraction of golden camellia tea active material：Fresh golden camellia tea is acquired, is washed with clean water, is drained, is put into reaction kettle
In, liquid nitrogen is passed through, super-pressure is added to carry out impregnation, crushing is then ground and obtains golden camellia tea powder；Toward golden camellia tea
Magnetized water is added in powder, it is 60 ~ 80 DEG C to adjust temperature, then carries out high speed shear, and it is more to add in the absorption of enzyme molecule trace microballoon
Phenol oxidase and catalase filter out insoluble matter, obtain golden camellia tea active ingredient solution；Obtained active material is carried out
Purifying, the surfactant of 0.05% concentration is added in the golden camellia tea active ingredient solution of acquisition, adds 0.2 ~ 0.5%
Then glucono-δ-lactone, 0.4 ~ 0.6% EDETATE SODIUM are filtered to get golden camellia tea active substance solution；
(2) golden camellia tea active material powder：Obtained golden camellia tea active substance solution is subjected to vacuum freeze drying, setting
Vacuum degree is 50 ~ 60Pa, and drying temperature is 60 ~ 65 DEG C, it is dry for 24 hours, it is dry after with clean multifunctional crusher beat powder 20~
The golden camellia tea active material powder that granularity is 200 mesh is made in 30 s；
(3) it allocates：Allotment：Take 30 ~ 40 parts of golden camellia tea active material powders, 10 ~ 12 portions of trehaloses, 5 ~ 8 parts of maltitols, 5 ~
8 parts of cycloheptaamyloses, 10 ~ 15 parts of Herba Menthae powders are uniformly mixed, and then add in 2 ~ 3 parts of magnesium stearates, 2 ~ 3 parts of carboxymethyl celluloses
Powder 5s is beaten in plain sodium mixing, obtains mixed-powder；
(4) tabletting, sterilizing and packaging：By mixed-powder be sent into tablet press machine carry out tabletting forming, and will press tablet be placed on it is ultraviolet
30min is irradiated under line and carries out sterilization treatment, then carries out being vacuum-packed up to golden camellia tea active material lozenge.
As the further explanation of the present invention, the super-pressure dip operation parameter is：Pressure is 400 ~ 500MPa, when
Between be 5-10min.
As the further explanation of the present invention, the high speed shear operating parameter is：High-speed shearing machine rotating speed is 10000
~ 12000r/min, extraction time are 1 ~ 2min.
As the further explanation of the present invention, the enzyme molecule trace method for preparing microsphere step includes：
20 ~ 25 parts of golden camellia tea polyphenol oxidase, 15 ~ 18 parts of golden camellia tea catalases, 2 ~ 3 parts of part cyclodextrin is taken to be dissolved in
In 20ml distilled water, ultrasonic dissolution 10min, 2 ~ 4h of prepolymerization add 8 ~ 12 parts of divinylbenzenes, 15 ~ 25 parts of ethyl acetate,
Ultrasonic dissolution 10min is passed through nitrogen after mixing, after ultraviolet light, polymerization 20 ~ for 24 hours, then with 5:1 ethyl alcohol/acetic acid into
Row elution is to get required enzyme molecule trace microballoon.
As the present invention further explanation, the surfactant for sucrose-fatty, sorbic acid monostearate,
The mixture of soybean lecithin.
As the further explanation of the present invention, the golden camellia tea active constituent extracted contains total saposins, flavones, tea
Polyphenol, tea polysaccharide, Tea Pigment, amino acid, vitamin, micro- ferroselenium zinc.
The technical principle that the present invention realizes：Golden camellia tea is carried out at dipping using liquid nitrogen and high pressure united method first
Reason makes golden camellia tea realize the hypervelocity east of low-temperature deep, can preferably ensure golden camellia tea using the cold service of liquid nitrogen
Active material is not damaged.Super-pressure can be such that liquid nitrogen preferably enters in the cell of golden camellia tea, realize deeper into it is cold
Freeze, super-pressure passes through abrupt release pressure after freeze-drying, and the disintegration of golden camellia tea surface pectin composition can be made to promote cell
Wall rupture makes the content dissolution of the inside, after content dissolution the liquid nitrogen that adds in can preferably starvation, inhibit tea polyphenols,
The oxidation of the active ingredients such as tea polysaccharide, super-pressure to polyphenol oxidase, catalase to having effective passivation, superelevation
The synergistic effect of pressure and liquid nitrogen, can preferably protect the active material in golden camellia tea.
Magnetized water has higher osmosis, can penetrate into the histocyte in golden camellia tea, enhances active matter
The exudation ability of matter and improve its solvability in water.High speed shear is the second-time breakage to golden camellia tea, improves golden flower
The sporoderm-broken rate of tea cell wall, magnetized water and high speed shear act on simultaneously, can promote the Fast Stripping of content, save extraction
Time.The active ingredient in golden camellia tea can be made preferably to dissolve out for 1 ~ 2min using shear time, the extension time can destroy
The active ingredients such as polysaccharide reduce the yield of active material instead.
Liquid nitrogen and super-pressure can inhibit the activity of polyphenol oxidase and catalase, make tea polyphenols, tea polysaccharide etc. living
Property substance aoxidized, but be not able to make the activity complete inhibition of polyphenol oxidase, catalase, using enzyme molecule trace
Microballoon detaches catalase and polyphenol oxidase, can better ensure that tea polyphenols, tea polysaccharide etc. in extracting solution
Active material is not oxidized.
Active material is purified, adding in surfactant can be such that the substance being insoluble in extracting solution preferably dissolves
In water, the EDETATE SODIUM of addition can chelate to form Precipitation with the protein in golden camellia tea active ingredient solution.Portugal
Grape saccharic acid-delta-lactone can act on forming precipitation with pectin, by filtering, can separate protein and pectin substance,
Obtain required golden camellia tea active material extraction solution.
It is added in during film-making（Trehalose, maltitol, cycloheptaamylose, Herba Menthae powder）Trehalose, trehalose can be with
The bitter taste of golden camellia tea active material ingredients can be reduced as sweetener, trehalose can make lozenge after consumption in mouth
Not there are rear taste, there is unique salubrious taste matter, change the eating mouth feel of lozenge, and trehalose also be able to prevent lozenge deterioration,
It keeps the taste and flavor of lozenge, promote the quality of lozenge, can also reduce the hygroscopicity of lozenge, so as to effectively extend the guarantor of lozenge
The matter phase.Sweetener of the maltitol as lozenge, heat content is low, non-saprodontia, can promote absorption of the human body to calcium, while not
Make blood glucose rise, do not increase cholesterol.Cycloheptaamylose can cooperate with trehalose, maltitol eliminate lozenge in peculiar smell, β-
Cyclodextrine is also prevented from the oxidation and decomposition of active material in lozenge, the stability of lozenge is improved, so as to extend lozenge
Shelf-life.Peppermint can also play the role of anti-corrosion and sterilization with fresh breath, also aid digestion, improve the function of lozenge
Value.
In lozenge, magnesium stearate is conducive to as lubricant, sodium carboxymethylcellulose as adhesive, the use of the two
The molding of lozenge.
The present invention has following good result：
1. the present invention can well from golden camellia tea obtain saponin(e, flavones, tea polyphenols, tea polysaccharide, Tea Pigment, amino acid,
Vitamin, trace elements of selenium zinc-iron active material, extraction efficiency higher, extraction is complete, and can effectively inhibit tea polyphenols, tea more
The oxidation of the active ingredients such as sugar, the activity that can preferably retain extraction of substance are not damaged.
2. the lozenge nutrition of the present invention is high, stability is good, and palatability is good, is easy to be digested, and easy to carry,
It preserves and edible.
3. the lozenge of the present invention has certain hardness, elasticity and toughness, refrigerant tasty and refreshing has anti-inflammatory, inhibits aging and drop
Low cholesterol, strengthen immunity and atherosclerosis and other effects are conducive to health, improve Camellia nitidissima and think the attached of pass
It is value added.
Specific embodiment
A kind of preparation method of golden camellia tea active material lozenge of the description present invention with reference to embodiments, these descriptions are simultaneously
It is not that the content of present invention is further limited.
Embodiment 1：
The preparation of enzyme molecule trace microballoon：Take 23 parts of golden camellia tea polyphenol oxidase, 17 parts of golden camellia tea catalases, 2.5
Part part cyclodextrin is dissolved in 20ml distilled water, and ultrasonic dissolution 10min, prepolymerization 4h add 10 parts of divinylbenzenes, 18 parts of second
Acetoacetic ester, ultrasonic dissolution 10min are passed through nitrogen after mixing, after ultraviolet light, polymerize 22h, then with 5:1 ethyl alcohol/second
Acid is eluted to get required enzyme molecule trace microballoon.
The extraction of golden camellia tea active material：Fresh golden camellia tea is acquired, is washed with clean water, is drained, is put into reaction
In kettle, liquid nitrogen is passed through, super-pressure is added to carry out impregnation, pressure 480MPa, dip time 6min.Then it is ground powder
It is broken to obtain golden camellia tea powder；Magnetized water is added in into golden camellia tea powder, it is 60 DEG C to adjust temperature, then carries out cutting at a high speed
It cuts, cutter rotating speed is 10000r/min, extraction time 1.5min, then adds in the oxidation of enzyme molecule trace microballoon adsorbing polyphenols
Enzyme and catalase filter out insoluble matter, obtain golden camellia tea active ingredient solution；Obtained active material is purified,
The surfactant of 0.05% concentration is added in the golden camellia tea active ingredient solution of acquisition, add 0.2% gluconic acid-
Then delta-lactone, 0.4% EDETATE SODIUM are filtered to get golden camellia tea active substance solution.
Golden camellia tea active material powder：Obtained golden camellia tea active substance solution is subjected to vacuum freeze drying, if
Vacuum degree is put as 50Pa, drying temperature is 65 DEG C, and drying for 24 hours, is beaten powder 25s with clean multifunctional crusher after drying, is made
Granularity is the golden camellia tea active material powder of 200 mesh
Allotment：Take 40 parts of golden camellia tea active material powders, 11 portions of trehaloses, 7 parts of maltitols, 6 parts of cycloheptaamyloses, 14 parts
Herba Menthae powder is uniformly mixed, and powder 5s is beaten in then 3 parts of magnesium stearates of addition, 2.5 parts of sodium carboxymethylcelluloses mixing, is mixed
Powder.
Tabletting, sterilizing and packaging：By mixed-powder be sent into tablet press machine carry out tabletting forming, and will press tablet be placed on it is ultraviolet
30min is irradiated under line and carries out sterilization treatment, then carries out being vacuum-packed up to golden camellia tea active material lozenge.
Embodiment 2
The preparation of enzyme molecule trace microballoon：Take 20 parts of golden camellia tea polyphenol oxidase, 18 parts of golden camellia tea catalases, 2 parts
Part cyclodextrin is dissolved in 20ml distilled water, and ultrasonic dissolution 10min, prepolymerization 3.5h add 9 parts of divinylbenzenes, 20 parts of second
Acetoacetic ester, ultrasonic dissolution 10min are passed through nitrogen after mixing, after ultraviolet light, polymerize 20h, then with 5:1 ethyl alcohol/second
Acid is eluted to get required enzyme molecule trace microballoon.
The extraction of golden camellia tea active material：Fresh golden camellia tea is acquired, is washed with clean water, is drained, is put into reaction
In kettle, liquid nitrogen is passed through, super-pressure is added to carry out impregnation, pressure 400MPa, dip time 10min.Then it is ground
Crushing obtains golden camellia tea powder；Magnetized water is added in into golden camellia tea powder, it is 75 DEG C to adjust temperature, then carries out cutting at a high speed
It cuts, cutter rotating speed is 11000r/min, and extraction time is 1 min, then adds in the oxidation of enzyme molecule trace microballoon adsorbing polyphenols
Enzyme and catalase filter out insoluble matter, obtain golden camellia tea active ingredient solution；Obtained active material is purified,
The surfactant of 0.05% concentration is added in the golden camellia tea active ingredient solution of acquisition, add 0.3% gluconic acid-
Then delta-lactone, 0.5% EDETATE SODIUM are filtered to get golden camellia tea active substance solution.
Golden camellia tea active material powder：Obtained golden camellia tea active substance solution is subjected to vacuum freeze drying, if
Vacuum degree is put as 60Pa, drying temperature is 62 DEG C, and drying for 24 hours, is beaten powder 20s with clean multifunctional crusher after drying, is made
Granularity is the golden camellia tea active material powder of 200 mesh.
Allotment：Take 35 parts of golden camellia tea active material powders, 12 portions of trehaloses, 8 parts of maltitols, 5 parts of cycloheptaamyloses,
13 parts of Herba Menthae powders are uniformly mixed, and powder 5s is beaten in then 2 parts of magnesium stearates of addition, 3 parts of sodium carboxymethylcelluloses mixing, is mixed
Close powder.
Tabletting, sterilizing and packaging：By mixed-powder be sent into tablet press machine carry out tabletting forming, and will press tablet be placed on it is ultraviolet
30min is irradiated under line and carries out sterilization treatment, then carries out being vacuum-packed up to golden camellia tea active material lozenge.
Embodiment 3
The preparation of enzyme molecule trace microballoon：Take 24 parts of golden camellia tea polyphenol oxidase, 16 parts of golden camellia tea catalases, 2.5
Part part cyclodextrin is dissolved in 20ml distilled water, and ultrasonic dissolution 10min, prepolymerization 2h add 10 parts of divinylbenzenes, 23 parts of second
Acetoacetic ester, ultrasonic dissolution 10min are passed through nitrogen after mixing, after ultraviolet light, polymerize for 24 hours, then with 5:1 ethyl alcohol/second
Acid is eluted to get required enzyme molecule trace microballoon.
The extraction of golden camellia tea active material：Fresh golden camellia tea is acquired, is washed with clean water, is drained, is put into reaction
In kettle, liquid nitrogen is passed through, super-pressure is added to carry out impregnation, pressure 500MPa, dip time 5min.Then it is ground powder
It is broken to obtain golden camellia tea powder；Magnetized water is added in into golden camellia tea powder, it is 70 DEG C to adjust temperature, then carries out cutting at a high speed
It cuts, cutter rotating speed is 12000r/min, extraction time 2min, then adds in enzyme molecule trace microballoon adsorbing polyphenols oxidizing ferment
And catalase, insoluble matter is filtered out, obtains golden camellia tea active ingredient solution；Obtained active material is purified,
The surfactant of 0.05% concentration is added in the golden camellia tea active ingredient solution of acquisition, add 0.5% gluconic acid-δ-
Then lactone, 0.6% EDETATE SODIUM are filtered to get golden camellia tea active substance solution.
Golden camellia tea active material powder：Obtained golden camellia tea active substance solution is subjected to vacuum freeze drying, if
Vacuum degree is put as 52Pa, drying temperature is 64 DEG C, and drying for 24 hours, is beaten powder 28s with clean multifunctional crusher after drying, is made
Granularity is the golden camellia tea active material powder of 200 mesh.
Allotment：Take 30 parts of golden camellia tea active material powders, 10.5 portions of trehaloses, 5 parts of maltitols, 7 parts of β-ring-type paste
Essence, 10 parts of Herba Menthae powders are uniformly mixed, and powder 5s is beaten in then 2.5 parts of magnesium stearates of addition, 2 parts of sodium carboxymethylcelluloses mixing,
Obtain mixed-powder.
Tabletting, sterilizing and packaging：By mixed-powder be sent into tablet press machine carry out tabletting forming, and will press tablet be placed on it is ultraviolet
30min is irradiated under line and carries out sterilization treatment, then carries out being vacuum-packed up to golden camellia tea active material lozenge.
Embodiment 4
The preparation of enzyme molecule trace microballoon：Take 25 parts of golden camellia tea polyphenol oxidase, 16 parts of golden camellia tea catalases, 3 parts
Part cyclodextrin is dissolved in 20ml distilled water, and ultrasonic dissolution 10min, prepolymerization 3h add 8 parts of divinylbenzenes, 15 parts of acetic acid
Ethyl ester, ultrasonic dissolution 10min are passed through nitrogen after mixing, after ultraviolet light, polymerize 23h, then with 5:1 ethyl alcohol/acetic acid
It is eluted to get required enzyme molecule trace microballoon.
The extraction of golden camellia tea active material：Fresh golden camellia tea is acquired, is washed with clean water, is drained, is put into reaction
In kettle, liquid nitrogen is passed through, super-pressure is added to carry out impregnation, pressure 420MPa, dip time 9min.Then it is ground powder
It is broken to obtain golden camellia tea powder；Magnetized water is added in into golden camellia tea powder, it is 80 DEG C to adjust temperature, then carries out cutting at a high speed
It cuts, cutter rotating speed is 11500r/min, and extraction time is 2 min, then adds in the oxidation of enzyme molecule trace microballoon adsorbing polyphenols
Enzyme and catalase filter out insoluble matter, obtain golden camellia tea active ingredient solution；Obtained active material is purified,
The surfactant of 0.05% concentration is added in the golden camellia tea active ingredient solution of acquisition, add 0.4% gluconic acid-
Then delta-lactone, 0.5% EDETATE SODIUM are filtered to get golden camellia tea active material.
Golden camellia tea active material powder：Obtained golden camellia tea active substance solution is subjected to vacuum freeze drying, if
Vacuum degree is put as 58Pa, drying temperature is 60 DEG C, and drying for 24 hours, is beaten powder 30s with clean multifunctional crusher after drying, is made
Granularity is the golden camellia tea active material powder of 200 mesh.
Allotment：Take 38 parts of golden camellia tea active material powders, 11.5 portions of trehaloses, 6 parts of maltitols, 8 parts of β-ring-type paste
Essence, 15 parts of Herba Menthae powders are uniformly mixed, and powder 5s is beaten in then 3 parts of magnesium stearates of addition, 2.5 parts of sodium carboxymethylcelluloses mixing,
Obtain mixed-powder.
Tabletting, sterilizing and packaging：By mixed-powder be sent into tablet press machine carry out tabletting forming, and will press tablet be placed on it is ultraviolet
30min is irradiated under line and carries out sterilization treatment, then carries out being vacuum-packed up to golden camellia tea active material lozenge.
Embodiment 5
The preparation of enzyme molecule trace microballoon：Take 21 parts of golden camellia tea polyphenol oxidase, 15 parts of golden camellia tea catalases, 3 parts
Part cyclodextrin is dissolved in 20ml distilled water, and ultrasonic dissolution 10min, prepolymerization 2.5h add 12 parts of divinylbenzenes, 25 parts of second
Acetoacetic ester, ultrasonic dissolution 10min are passed through nitrogen after mixing, after ultraviolet light, polymerize 21h, then with 5:1 ethyl alcohol/second
Acid is eluted to get required enzyme molecule trace microballoon.
The extraction of golden camellia tea active material：Fresh golden camellia tea is acquired, is washed with clean water, is drained, is put into reaction
In kettle, liquid nitrogen is passed through, super-pressure is added to carry out impregnation, pressure 450MPa, dip time 8min.Then it is ground powder
It is broken to obtain golden camellia tea powder；Magnetized water is added in into golden camellia tea powder, it is 65 DEG C to adjust temperature, then carries out cutting at a high speed
It cuts, cutter rotating speed is 10500r/min, and extraction time is 1 min, then adds in the oxidation of enzyme molecule trace microballoon adsorbing polyphenols
Enzyme and catalase filter out insoluble matter, obtain golden camellia tea active ingredient solution；Obtained active material is purified,
The surfactant of 0.05% concentration is added in the golden camellia tea active ingredient solution of acquisition, add 0.3% gluconic acid-
Then delta-lactone, 0.6% EDETATE SODIUM are filtered to get golden camellia tea active material.
Golden camellia tea active material powder：Obtained golden camellia tea active substance solution is subjected to vacuum freeze drying, if
Vacuum degree is put as 55Pa, drying temperature is 63 DEG C, and drying for 24 hours, is beaten powder 22s with clean multifunctional crusher after drying, is made
Granularity is the golden camellia tea active material powder of 200 mesh.
Allotment：Take 35 parts of golden camellia tea active material powders, 12 portions of trehaloses, 8 parts of maltitols, 5 parts of cycloheptaamyloses,
13 parts of Herba Menthae powders are uniformly mixed, and powder 5s is beaten in then 2 parts of magnesium stearates of addition, 3 parts of sodium carboxymethylcelluloses mixing, is mixed
Close powder.
Tabletting, sterilizing and packaging：By mixed-powder be sent into tablet press machine carry out tabletting forming, and will press tablet be placed on it is ultraviolet
30min is irradiated under line and carries out sterilization treatment, then carries out being vacuum-packed up to golden camellia tea active material lozenge.
The lozenge that embodiment is prepared is measured and is referred to using leaching time, tablet hardness, mouthfeel and appearance as evaluation
Mark.Evaluation method and standard are as shown in table 1.
1 evaluation method of table and standard
2 evaluation result of table
The above embodiment of the present invention scheme is only the description of the invention and cannot limit the present invention, this is indicated in claim
Invention product form ingredient, component ratio, the range of preparation method parameter, and above-mentioned explanation does not point out parameter of the present invention
Range, therefore, any change within the meaning and scope equivalent to the claims of the present invention, be all considered to be including
In the range of claims.
The present invention be by multidigit Camellia nitidissima processing staff's long-term work experience accumulation, and by creative work create and
Go out, lozenge nutrition of the invention is high, and stability is good, and palatability is good, is easy to be digested, and it is easy to carry, preserve and
It is edible.
Claims (6)
1. a kind of preparation method of golden camellia tea active material lozenge, which is characterized in that the preparation method step includes：
The extraction of step 1) golden camellia tea active material：Fresh golden camellia tea is acquired, is washed with clean water, is drained, is put into anti-
It answers in kettle, is passed through liquid nitrogen, super-pressure is added to carry out impregnation, crushing is then ground and obtains golden camellia tea powder；Toward golden flower
Magnetized water is added in tea-leaf power, it is 60 ~ 80 DEG C to adjust temperature, then carries out high speed shear, adds in enzyme molecule trace microballoon and inhales
Attached polyphenol oxidase and catalase filter out insoluble matter, obtain golden camellia tea active ingredient solution；The active material that will be obtained
It is purified, the surfactant of 0.05% concentration is added in the golden camellia tea active ingredient solution of acquisition, add 0.2 ~
Then 0.5% glucono-δ-lactone, 0.4 ~ 0.6% EDETATE SODIUM are filtered to get golden camellia tea active substance solution；
Step 2) golden camellia tea active material powder：Obtained golden camellia tea active substance solution is subjected to vacuum freeze drying,
Setting vacuum degree is 50 ~ 60Pa, and drying temperature is 60 ~ 65 DEG C, and drying for 24 hours, powder is beaten after drying with clean multifunctional crusher
The golden camellia tea active material powder that granularity is 200 mesh is made in 20~30 s；
Step 3) is allocated：Take 30 ~ 40 parts of golden camellia tea active material powders, 10 ~ 12 portions of trehaloses, 5 ~ 8 parts of maltitols, 5 ~ 8
Part cycloheptaamylose, 10 ~ 15 parts of Herba Menthae powders are uniformly mixed, and then add in 2 ~ 3 parts of magnesium stearates, 2 ~ 3 parts of carboxymethyl celluloses
Powder 5s is beaten in plain sodium mixing, obtains mixed-powder；
Step 4) tabletting, sterilizing and packaging：Mixed-powder is sent into tablet press machine and carries out tabletting forming, and tablet will be pressed and be placed on purple
30min is irradiated under outside line and carries out sterilization treatment, then carries out being vacuum-packed up to golden camellia tea active material lozenge.
2. the preparation method of a kind of golden camellia tea active material lozenge according to claim 1, which is characterized in that described
Super-pressure dip operation parameter is：Pressure is 400 ~ 500MPa, time 5-10min.
3. the preparation method of a kind of golden camellia tea active material lozenge according to claim 1, which is characterized in that described
High speed shear operating parameter is：High-speed shearing machine rotating speed is 10000 ~ 12000r/min, and extraction time is 1 ~ 2min.
4. the preparation method of a kind of golden camellia tea active material lozenge according to claim 1, which is characterized in that described
Enzyme molecule trace method for preparing microsphere step includes：
20 ~ 25 parts of golden camellia tea polyphenol oxidase, 15 ~ 18 parts of golden camellia tea catalases, 2 ~ 3 parts of part cyclodextrin is taken to be dissolved in
In 20ml distilled water, ultrasonic dissolution 10min, 2 ~ 4h of prepolymerization add 8 ~ 12 parts of divinylbenzenes, 15 ~ 25 parts of ethyl acetate,
Ultrasonic dissolution 10min is passed through nitrogen after mixing, after ultraviolet light, polymerization 20 ~ for 24 hours, then with 5:1 ethyl alcohol/acetic acid into
Row elution is to get required enzyme molecule trace microballoon.
5. the preparation method of a kind of golden camellia tea active material lozenge according to claim 1, which is characterized in that described
Surfactant is sucrose-fatty, the mixture of sorbic acid monostearate, soybean lecithin.
6. the preparation method of a kind of golden camellia tea active material lozenge according to claim 1, which is characterized in that extracted
Obtained golden camellia tea active substance solution contain total saposins, flavones, tea polyphenols, tea polysaccharide, Tea Pigment, amino acid, vitamin,
Micro- ferroselenium zinc active constituent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711458830.9A CN108157552A (en) | 2017-12-28 | 2017-12-28 | A kind of preparation method of golden camellia tea active material lozenge |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711458830.9A CN108157552A (en) | 2017-12-28 | 2017-12-28 | A kind of preparation method of golden camellia tea active material lozenge |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108157552A true CN108157552A (en) | 2018-06-15 |
Family
ID=62519067
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711458830.9A Pending CN108157552A (en) | 2017-12-28 | 2017-12-28 | A kind of preparation method of golden camellia tea active material lozenge |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108157552A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108951269A (en) * | 2018-07-05 | 2018-12-07 | 常州思宇知识产权运营有限公司 | A kind of preparation method of cigarette tipping paper |
| CN116725106A (en) * | 2023-07-17 | 2023-09-12 | 广西国茗金花茶科技有限公司 | High-pressure carbon dioxide fixation method and processing method for golden camellia flowers |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101427772A (en) * | 2008-12-16 | 2009-05-13 | 广西中港高科国宝金花茶产业有限公司 | Camellia chrysantha beverage and producing method thereof |
| CN101485789A (en) * | 2009-02-06 | 2009-07-22 | 广西桂人堂金花茶产业集团股份有限公司 | Camellia chrysantha polysaccharide lozenge and method for producing the same |
| CN104140494A (en) * | 2014-07-17 | 2014-11-12 | 陕西师范大学 | Method for preparing mimic enzyme molecularly imprinted polymer microsphere for hydrolyzing organophosphorus |
| CN106582985A (en) * | 2016-12-13 | 2017-04-26 | 郑红芹 | Ultramicro wall breaking and smashing method for rhizomatic traditional Chinese medicine |
| CN106622165A (en) * | 2016-10-19 | 2017-05-10 | 中国科学技术大学 | Magnetic catalase molecularly imprinted microspheres and preparation method thereof as well as catalase inhibitor |
-
2017
- 2017-12-28 CN CN201711458830.9A patent/CN108157552A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101427772A (en) * | 2008-12-16 | 2009-05-13 | 广西中港高科国宝金花茶产业有限公司 | Camellia chrysantha beverage and producing method thereof |
| CN101485789A (en) * | 2009-02-06 | 2009-07-22 | 广西桂人堂金花茶产业集团股份有限公司 | Camellia chrysantha polysaccharide lozenge and method for producing the same |
| CN104140494A (en) * | 2014-07-17 | 2014-11-12 | 陕西师范大学 | Method for preparing mimic enzyme molecularly imprinted polymer microsphere for hydrolyzing organophosphorus |
| CN106622165A (en) * | 2016-10-19 | 2017-05-10 | 中国科学技术大学 | Magnetic catalase molecularly imprinted microspheres and preparation method thereof as well as catalase inhibitor |
| CN106582985A (en) * | 2016-12-13 | 2017-04-26 | 郑红芹 | Ultramicro wall breaking and smashing method for rhizomatic traditional Chinese medicine |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108951269A (en) * | 2018-07-05 | 2018-12-07 | 常州思宇知识产权运营有限公司 | A kind of preparation method of cigarette tipping paper |
| CN116725106A (en) * | 2023-07-17 | 2023-09-12 | 广西国茗金花茶科技有限公司 | High-pressure carbon dioxide fixation method and processing method for golden camellia flowers |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100401925C (en) | Making method of health-care beverage for efficient preventing and treating asthma | |
| CN101797045B (en) | Honey raisin tree oral liquid and processing method thereof | |
| CN108552369A (en) | A kind of tea-drinking preparation method for material of the active material containing golden camellia tea | |
| CN106668144B (en) | Chinese herbal medicine tea for reducing blood pressure and preparation method thereof | |
| CN104997091B (en) | Cordyceps militaris instant solid beverage | |
| CN104547045A (en) | Compound moringa oleifera instant granules and preparation method thereof | |
| CN106343343A (en) | Lithocarpus polystachyus (DC.) Rehd tartarian buckwheat composition for reducing three-high and application thereof | |
| CN108157552A (en) | A kind of preparation method of golden camellia tea active material lozenge | |
| CN104783180A (en) | Chewable tablet containing freeze-dried anoectochilus roxburghii powder and preparation method of chewable tablet | |
| KR20130092652A (en) | Natural tea having an effect on the hangover | |
| CN101972025B (en) | Bamboo vinegar health care beverage and preparation method thereof | |
| KR20190112498A (en) | Whole Ginseng Composition Using Ginseng Roots, Leaves and Berries and Method of Preparing the Same | |
| CN105851764B (en) | A kind of Qingqian Willow leaf solid beverage and its preparation method and application | |
| CN102972815A (en) | Onion health beverage and production method thereof | |
| CN107801993A (en) | The preparation method of mulberry alkali piece | |
| CN101884408B (en) | Ginkgo leaf leaching liquor and preparation method thereof | |
| CN102972838A (en) | Chestnut flower health drink and preparation method thereof | |
| CN104206582B (en) | A kind of Aquilaria sinensis leaf tea beverage and processing technology thereof | |
| CN105495214A (en) | Anoectochilus roxburghii (Wall.) Lindl and strawbaeery juice beverage and making method thereof | |
| CN107912567A (en) | A kind of extracting method of golden camellia tea active material | |
| CN107125376A (en) | A kind of Inonotus obliquus electuary（Tea） | |
| CN106511471B (en) | A kind of fig oral spray and preparation method thereof | |
| KR20040081943A (en) | Bio-Natural Fresh Apple(Happy Tea) Tea | |
| CN110585260A (en) | Single-ingredient freeze-dried powder and preparation method thereof | |
| CN110663787A (en) | Tea beverage containing tea hair and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20190507 Address after: No. 25 Xinzhu Road, Qingxiu District, Nanning City, Guangxi Zhuang Autonomous Region, 530022 Applicant after: Chen Yanrong Address before: 530700 Guliang Village, Baoan Township, Duan Yao Autonomous County, Hechi City, Guangxi Zhuang Autonomous Region Applicant before: Tang Xiuting |
|
| TA01 | Transfer of patent application right | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180615 |
|
| RJ01 | Rejection of invention patent application after publication |