CN108951269A - A kind of preparation method of cigarette tipping paper - Google Patents
A kind of preparation method of cigarette tipping paper Download PDFInfo
- Publication number
- CN108951269A CN108951269A CN201810727014.1A CN201810727014A CN108951269A CN 108951269 A CN108951269 A CN 108951269A CN 201810727014 A CN201810727014 A CN 201810727014A CN 108951269 A CN108951269 A CN 108951269A
- Authority
- CN
- China
- Prior art keywords
- tipping paper
- reaction kettle
- cigarette tipping
- preparation
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H11/00—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
- D21H11/12—Pulp from non-woody plants or crops, e.g. cotton, flax, straw, bagasse
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21B—FIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
- D21B1/00—Fibrous raw materials or their mechanical treatment
- D21B1/04—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
- D21B1/12—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
- D21B1/30—Defibrating by other means
- D21B1/36—Explosive disintegration by sudden pressure reduction
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C5/00—Other processes for obtaining cellulose, e.g. cooking cotton linters ; Processes characterised by the choice of cellulose-containing starting materials
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21F—PAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
- D21F13/00—Making discontinuous sheets of paper, pulpboard or cardboard, or of wet web, for fibreboard production
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H11/00—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
- D21H11/16—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only modified by a particular after-treatment
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/03—Non-macromolecular organic compounds
- D21H17/05—Non-macromolecular organic compounds containing elements other than carbon and hydrogen only
- D21H17/14—Carboxylic acids; Derivatives thereof
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/68—Water-insoluble compounds, e.g. fillers, pigments siliceous, e.g. clays
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Mechanical Engineering (AREA)
- Paper (AREA)
Abstract
The present invention relates to a kind of preparation methods of cigarette tipping paper, belong to paper products preparation technical field.The present invention is first using the tealeaves rich in phenolic group as raw material, ammonia explosion treatment is carried out to it, again by after ammonia explosion treatment tealeaves and tartaric acid solution mix after it is spare, then zeolite granular is taken, with freezing and ball milling after water retting, obtain zeolite powder, zeolite powder and ammonia explosion tealeaves are mixed with the mixture of tartaric acid again, high-temperature high-voltage reaction is carried out under the action of sodium citrate and calgon, it is beaten after reaction and molding of manufacturing paper with pulp can be prepared by cigarette tipping paper, cigarette tipping paper organic matter volatile quantity produced by the present invention is small, it will not influence environment, it has broad application prospects.
Description
Technical field
The present invention relates to a kind of preparation methods of cigarette tipping paper, belong to paper products preparation technical field.
Background technique
Tipping paper is a kind of cigarette packaging material, specializes in the outer packing that cigar mill is used as filter tip, belongs to special industrial and uses
Paper, general tipping paper are a kind of decoration paper by obtain after printing coating and other modes processing to body paper.To reach
Improve the effect of cigarette external appearance, what the intaglio printing process of general tipping paper was mainly used has coating (mill base) or ink.
This virtually increases the consumption and carrying capacity of environment of chemicals, exists simultaneously potential chemicals and endangers the contact of human body.And
The transparent tipping paper aesthetic dim since appearance itself has does not need the post-processings such as printing, so to human body and environment
Harm minimize.Tobacco factory's mouthpieces attacter is very high to the performance requirements of tipping paper.Page characteristic is bad can be in very great Cheng
The difficulty for increasing process on degree, causes various problems, influences quality, increases consumption of raw materials.
Existing tipping paper is made of alcohol ink or the printing of ester soluble ink, and tipping paper surface can remain a certain amount of
Volatile organic compounds, connect filter tip and cigarette with this paper, be packaged and be sealed in cigarette case, in tipping paper
Remaining volatile organic compounds can inevitably be diffused into pipe tobacco and go, and during smoking property of cigarette, just have the feeling of taint of odour,
The suction taste for affecting flue gas, increases the oxious component in flue gas；In addition, printing tipping paper using alcohols, esters solvent ink
During, the organic exhaust gas containing these solvents can be largely discharged, not only causes burden to environment, and also resulted in
The waste of solvent resource；In addition, printing tipping paper compared with water-based ink using alcohols, esters solvent ink, also will increase
Production cost also affects Business Economic Benefit.
Therefore, a kind of cigarette tipping paper that can reduce organic matter volatile quantity in tipping paper is invented, prepared by skill to paper products
Art field has positive meaning.
Summary of the invention
Present invention mainly solves the technical issues of, can largely discharge organic compound for current existing cigarette tipping paper
Object provides a kind of preparation of cigarette tipping paper the problem of not only affecting the suction taste of flue gas, while causing burden to environment
Method.
In order to solve the above-mentioned technical problem, the technical scheme adopted by the invention is that:
A kind of preparation method of cigarette tipping paper, it is characterised in that specific preparation step are as follows:
(1) it weighs fresh tea leaf to be put into the reaction kettle with relief valve, preheats, liquid ammonia is added after preheating into reaction kettle,
After sealing reaction kettle, high temperature high pressure process；
(2) after to above-mentioned high temperature high pressure process, the relief valve of reaction kettle is opened, reaction kettle is taken out in moment pressure release to normal pressure
In product, obtain ammonia explosion fiber, by obtained ammonia explosion fiber and mass fraction be 10% tartaric acid solution be mixed to get
Mixture, it is spare；
(3) it weighs zeolite granular and is put into 10~15min of dipping in deionized water, be removed and placed in refrigerator, freeze after dipping, then
Zeolite after freezing is taken out immediately and is put into ball grinder, is that zirconium oxide ball milling is added into ball grinder by 20:1 by ball material mass ratio
Pearl, 200 meshes are crossed after 2~3h of ball-milling treatment, and collection obtains sieving zeolite powder；
(4) will above-mentioned sieving zeolite powder and spare mixture mix after be fitted into high-temperature high-pressure reaction kettle, then to reaction kettle
Middle addition sodium citrate and calgon, are stirred 15~20min；
(5) after to above-mentioned be stirred, reaction kettle is sealed, high-temperature high-voltage reaction discharges after reaction, obtains prefabricated paper
Slurry；
(6) above-mentioned prefabricated paper pulp is moved into hydrabeating machine after being beaten 20~30min and obtains paper pulp, paper pulp is poured into copy and is tried to please
In device, the type of being made is copied, up to cigarette tipping paper after being dried with vacuum desiccator.
The temperature of preheating as described in step (1) is 60~80 DEG C, and the time of preheating is 5~10min, high temperature high pressure process
Pressure be 1900~2000kPa, the temperature of high temperature high pressure process is 85~90 DEG C, the time of high temperature high pressure process is 10~
15min。
The mass ratio for the tartaric acid solution that ammonia explosion fiber described in step (2) and mass fraction are 10% is 1:2.
The temperature of freezing described in step (3) is -15~-10 DEG C, and the time of freezing is 10~12h.
The mass ratio of sieving zeolite powder and spare mixture described in step (4) is 1:5, the addition of sodium citrate
Amount is the 1% of sieving zeolite powder quality, and the additional amount of calgon is the 3% of sieving powder quality.
The pressure of high-temperature high-voltage reaction described in step (5) is 1.3~1.5MPa, and the temperature of high-temperature high-voltage reaction is
200~220 DEG C, the time of high-temperature high-voltage reaction is 10~12h.
Molding copy of system is copied described in step (6) takes quantification of 130~150g/m2, the drying temperature of vacuum desiccator
It is 105~110 DEG C, drying time is 3~5min.
The beneficial effects of the present invention are:
The present invention using the tealeaves rich in phenolic group as raw material, carries out ammonia explosion treatment to it first, then by the tea after ammonia explosion treatment
It is spare after leaf and tartaric acid solution mixing, zeolite granular is then taken, with freezing and ball milling after water retting, obtains zeolite powder, then
Zeolite powder and ammonia explosion tealeaves are mixed with the mixture of tartaric acid, under the action of sodium citrate and calgon into
Row high-temperature high-voltage reaction, is beaten after reaction and molding of manufacturing paper with pulp can be prepared by cigarette tipping paper, and the present invention is first to be rich in phenol
The tealeaves of base is raw material, makes lignin dissolution in tealeaves, half using the generation of physicochemical collective effect by ammonia explosion treatment
The effect that cellulose hydrolysis, cellulose crystallity reduce is conducive to making full use of for tealeaves fiber to increase specific surface area,
Then by after ammonia explosion treatment tealeaves and organic carboxyl acid mix, then zeolite interior hole widened by the ice effect of splitting, will mixed
After object and zeolite powder mixing, high-temperature high-voltage reaction is carried out jointly, there are two the purposes of high-temperature high-voltage reaction, one of them is logical
It crosses high-temperature high-voltage reaction and makes ammonia explosion tealeaves fibre composition, absorb thermal energy, and in hydrothermal and organic carboxyl acid effect
The furfural that hydrolysis, hydrolysis can promote furfural to generate, and generate lower further can be under subsequent effect and ammonia explosion tealeaves table
Face phenolic group contact abundant, according to reactive modified phenolic resin principle, so that part phenolic group and furfurol reaction, production network structure is multiple
Miscellaneous, the compound of the huge polyphenol base of molecule, more carboxyls can be in strong adsorption tipping paper with huge specific surface area
Organic volatile, fixed organic volatile substance reduces the volatile performance of organic compound in tipping paper；Second acts on
In under the influence of high pressure and temperature, organic carboxyl acid can be by the part metals Ion release in zeolite powder, then there is complexing to make
These complexing of metal ion are removed under the action of sodium citrate and calgon, to generate gold in zeolite surface
Belong to hole, these holes have and the positive charge of removed metal ion same charge, obtain electronic capability raising, therefore it is aoxidized
Property be largely increased, the strong adsorptivity of bound zeolite molecular sieve can first adsorb the volatile organic matter in tipping paper solid
, recycle the strong oxidizing property of itself by these volatile organic matter oxidative degradations, to be further reduced tipping paper of the present invention
The volatility of middle organic matter, has broad application prospects.
Specific embodiment
It weighs fresh tea leaf to be put into the reaction kettle with relief valve, is heated to 60~80 DEG C, preheat 5~10min
The liquid ammonia of the quality such as fresh tea leaf is added in backward reaction kettle, is forced into 1900~2000kPa after sealing reaction kettle, and improve
Temperature of reaction kettle is to 85~90 DEG C, 10~15min of high temperature high pressure process；After to high temperature high pressure process, reaction kettle is opened
Relief valve, moment pressure release to normal pressure take out the product in reaction kettle, obtain ammonia explosion fiber, by obtained ammonia explosion fiber and
The tartaric acid solution that mass fraction is 10% is that 1:2 is mixed to get mixture in mass ratio, spare；Zeolite granular is weighed to be put into
10~15min is impregnated in ionized water, is removed and placed in refrigerator after dipping, 10~12h is freezed at -15~-10 DEG C, then will be cold
Zeolite after jelly takes out immediately to be put into ball grinder, is that zirconium oxide ball milling pearl is added into ball grinder by 20:1 by ball material mass ratio,
200 meshes are crossed after 2~3h of ball-milling treatment, collection obtains sieving zeolite powder；Sieving zeolite powder and spare mixture are pressed
Mass ratio is to be fitted into high-temperature high-pressure reaction kettle after 1:5 is mixed, then the lemon of sieving zeolite powder quality 1% is added into reaction kettle
The calgon of lemon acid sodium and sieving powder quality 3%, is stirred 15~20min；It is to be mixed after mixing, sealing is anti-
It answers kettle, increases and increase reactor temperature after reactor pressure to 1.3~1.5MPa again to 200~220 DEG C, high-temperature high-voltage reaction
10~12h discharges after reaction, obtains prefabricated paper pulp；Prefabricated paper pulp is moved into hydrabeating machine after being beaten 20~30min
Paper pulp is obtained, paper pulp is poured into and is copied in extracting container, takes quantification of 130~150g/m by copying2The type of being made is copied, is existed with vacuum desiccator
Up to cigarette tipping paper after dry 3~5min at 105~110 DEG C.
Example 1
It weighs fresh tea leaf to be put into the reaction kettle with relief valve, is heated to 60 DEG C, preheat after 5min into reaction kettle
The liquid ammonia of the quality such as fresh tea leaf is added, is forced into 1900kPa after sealing reaction kettle, and improves temperature of reaction kettle to 85 DEG C,
High temperature high pressure process 10min；After to high temperature high pressure process, the relief valve of reaction kettle is opened, moment pressure release to normal pressure is taken out
Product in reaction kettle obtains ammonia explosion fiber, by obtained ammonia explosion fiber and mass fraction be 10% tartaric acid solution by
Mass ratio is that 1:2 is mixed to get mixture, spare；It weighs zeolite granular and is put into deionized water and impregnate 10min, taken out after dipping
And be put into refrigerator, 10h is freezed at -15 DEG C, then the zeolite after freezing is taken out immediately and is put into ball grinder, by ball material quality
Than zirconium oxide ball milling pearl is added into ball grinder for 20:1,200 meshes are crossed after ball-milling treatment 2h, collection obtains sieving zeolite powder
End；It is in mass ratio to be fitted into high-temperature high-pressure reaction kettle after 1:5 is mixed by sieving zeolite powder and spare mixture, then to anti-
The calgon for answering the sodium citrate that sieving zeolite powder quality 1% is added in kettle and sieving powder quality 3%, is stirred
15min；It is to be mixed to seal reaction kettle after mixing, reactor temperature is increased again after increasing reactor pressure to 1.3MPa
To 200 DEG C, high-temperature high-voltage reaction 10h discharges after reaction, obtains prefabricated paper pulp；Prefabricated paper pulp is moved into hydrabeating machine
Paper pulp is obtained after middle mashing 20min, paper pulp is poured into and is copied in extracting container, takes quantification of 130g/m by copying2The type of being made is copied, vacuum is used
Drier is at 105 DEG C up to cigarette tipping paper after dry 3min.
Example 2
It weighs fresh tea leaf to be put into the reaction kettle with relief valve, is heated to 70 DEG C, preheat after 8min into reaction kettle
The liquid ammonia of the quality such as fresh tea leaf is added, is forced into 1950kPa after sealing reaction kettle, and improves temperature of reaction kettle to 88 DEG C,
High temperature high pressure process 13min；After to high temperature high pressure process, the relief valve of reaction kettle is opened, moment pressure release to normal pressure is taken out
Product in reaction kettle obtains ammonia explosion fiber, by obtained ammonia explosion fiber and mass fraction be 10% tartaric acid solution by
Mass ratio is that 1:2 is mixed to get mixture, spare；It weighs zeolite granular and is put into deionized water and impregnate 13min, taken out after dipping
And be put into refrigerator, 11h is freezed at -13 DEG C, then the zeolite after freezing is taken out immediately and is put into ball grinder, by ball material quality
Than zirconium oxide ball milling pearl is added into ball grinder for 20:1,200 meshes are crossed after ball-milling treatment 2h, collection obtains sieving zeolite powder
End；It is in mass ratio to be fitted into high-temperature high-pressure reaction kettle after 1:5 is mixed by sieving zeolite powder and spare mixture, then to anti-
The calgon for answering the sodium citrate that sieving zeolite powder quality 1% is added in kettle and sieving powder quality 3%, is stirred
18min；It is to be mixed to seal reaction kettle after mixing, reactor temperature is increased again after increasing reactor pressure to 1.4MPa
To 210 DEG C, high-temperature high-voltage reaction 11h discharges after reaction, obtains prefabricated paper pulp；Prefabricated paper pulp is moved into hydrabeating machine
Paper pulp is obtained after middle mashing 25min, paper pulp is poured into and is copied in extracting container, takes quantification of 140g/m by copying2The type of being made is copied, vacuum is used
Drier is at 108 DEG C up to cigarette tipping paper after dry 4min.
Example 3
It weighs fresh tea leaf to be put into the reaction kettle with relief valve, is heated to 70 DEG C, preheat after 8min into reaction kettle
The liquid ammonia of the quality such as fresh tea leaf is added, is forced into 1950kPa after sealing reaction kettle, and improves temperature of reaction kettle to 88 DEG C,
High temperature high pressure process 13min；After to high temperature high pressure process, the relief valve of reaction kettle is opened, moment pressure release to normal pressure is taken out
Product in reaction kettle obtains ammonia explosion fiber, by obtained ammonia explosion fiber and mass fraction be 10% tartaric acid solution by
Mass ratio is that 1:2 is mixed to get mixture, spare；It weighs zeolite granular and is put into deionized water and impregnate 13min, taken out after dipping
And be put into refrigerator, 11h is freezed at -13 DEG C, then the zeolite after freezing is taken out immediately and is put into ball grinder, by ball material quality
Than zirconium oxide ball milling pearl is added into ball grinder for 20:1,200 meshes are crossed after ball-milling treatment 2h, collection obtains sieving zeolite powder
End；It is in mass ratio to be fitted into high-temperature high-pressure reaction kettle after 1:5 is mixed by sieving zeolite powder and spare mixture, then to anti-
The calgon for answering the sodium citrate that sieving zeolite powder quality 1% is added in kettle and sieving powder quality 3%, is stirred
18min；It is to be mixed to seal reaction kettle after mixing, reactor temperature is increased again after increasing reactor pressure to 1.4MPa
To 210 DEG C, high-temperature high-voltage reaction 11h discharges after reaction, obtains prefabricated paper pulp；Prefabricated paper pulp is moved into hydrabeating machine
Paper pulp is obtained after middle mashing 25min, paper pulp is poured into and is copied in extracting container, takes quantification of 140g/m by copying2The type of being made is copied, vacuum is used
Drier is at 108 DEG C up to cigarette tipping paper after dry 4min.
Reference examples
Using the tipping paper that Changzhou company produces as reference examples
Tipping paper in tipping paper produced by the present invention and reference examples is cut into 20cm × 4cm scraps of paper, tubular is rolled into, sets immediately
Accurate that 0.1mL glyceryl triacetate solution is added in the dedicated ml headspace bottle of 20mL, sealing is placed in Static Headspace equilibristat,
After balancing 45min at 80 DEG C, to ml headspace bottle pressurization 1min, inserting needle sampling, control sample introduction needle temperature is 100 DEG C, and sample injection time is
0.2min, samples taken directly carry out gas chromatography/mass spectrometry by transmission line and are measured organic matter volatile quantity, specific to examine
Survey the results are shown in Table 1.
1 testing result of table
Cigarette tipping paper organic matter volatile quantity produced by the present invention is small it can be seen from detection data in upper table, will not influence ring
Border has broad application prospects.
Claims (7)
1. a kind of preparation method of cigarette tipping paper, it is characterised in that specific preparation step are as follows:
(1) it weighs fresh tea leaf to be put into the reaction kettle with relief valve, preheats, liquid ammonia is added after preheating into reaction kettle,
After sealing reaction kettle, high temperature high pressure process；
(2) after to above-mentioned high temperature high pressure process, the relief valve of reaction kettle is opened, reaction kettle is taken out in moment pressure release to normal pressure
In product, obtain ammonia explosion fiber, by obtained ammonia explosion fiber and mass fraction be 10% tartaric acid solution be mixed to get
Mixture, it is spare；
(3) it weighs zeolite granular and is put into 10~15min of dipping in deionized water, be removed and placed in refrigerator, freeze after dipping, then
Zeolite after freezing is taken out immediately and is put into ball grinder, is that zirconium oxide ball milling is added into ball grinder by 20:1 by ball material mass ratio
Pearl, 200 meshes are crossed after 2~3h of ball-milling treatment, and collection obtains sieving zeolite powder；
(4) will above-mentioned sieving zeolite powder and spare mixture mix after be fitted into high-temperature high-pressure reaction kettle, then to reaction kettle
Middle addition sodium citrate and calgon, are stirred 15~20min；
(5) after to above-mentioned be stirred, reaction kettle is sealed, high-temperature high-voltage reaction discharges after reaction, obtains prefabricated paper
Slurry；
(6) above-mentioned prefabricated paper pulp is moved into hydrabeating machine after being beaten 20~30min and obtains paper pulp, paper pulp is poured into copy and is tried to please
In device, the type of being made is copied, up to cigarette tipping paper after being dried with vacuum desiccator.
2. a kind of preparation method of cigarette tipping paper according to claim 1, it is characterised in that: as described in step (1)
The temperature of preheating is 60~80 DEG C, and the time of preheating is 5~10min, and the pressure of high temperature high pressure process is 1900~2000kPa,
The temperature of high temperature high pressure process is 85~90 DEG C, and the time of high temperature high pressure process is 10~15min.
3. a kind of preparation method of cigarette tipping paper according to claim 1, it is characterised in that: described in step (2)
The mass ratio for the tartaric acid solution that ammonia explosion fiber and mass fraction are 10% is 1:2.
4. a kind of preparation method of cigarette tipping paper according to claim 1, it is characterised in that: described in step (3)
The temperature of freezing is -15~-10 DEG C, and the time of freezing is 10~12h.
5. a kind of preparation method of cigarette tipping paper according to claim 1, it is characterised in that: described in step (4)
The mass ratio of sieving zeolite powder and spare mixture is 1:5, and the additional amount of sodium citrate is sieving zeolite powder quality
1%, the additional amount of calgon is the 3% of sieving powder quality.
6. a kind of preparation method of cigarette tipping paper according to claim 1, it is characterised in that: described in step (5)
The pressure of high-temperature high-voltage reaction is 1.3~1.5MPa, and the temperature of high-temperature high-voltage reaction is 200~220 DEG C, high-temperature high-voltage reaction
Time is 10~12h.
7. a kind of preparation method of cigarette tipping paper according to claim 1, it is characterised in that: described in step (6)
It copies molding copy of system and takes quantification of 130~150g/m2, the drying temperature of vacuum desiccator is 105~110 DEG C, drying time 3
~5min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810727014.1A CN108951269A (en) | 2018-07-05 | 2018-07-05 | A kind of preparation method of cigarette tipping paper |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810727014.1A CN108951269A (en) | 2018-07-05 | 2018-07-05 | A kind of preparation method of cigarette tipping paper |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108951269A true CN108951269A (en) | 2018-12-07 |
Family
ID=64485605
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810727014.1A Withdrawn CN108951269A (en) | 2018-07-05 | 2018-07-05 | A kind of preparation method of cigarette tipping paper |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108951269A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014117964A1 (en) * | 2013-01-31 | 2014-08-07 | Glatfelter Gernsbach Gmbh & Co. Kg | Crosslinking/functionalization system for a paper or non-woven web |
| CN104789035A (en) * | 2015-05-06 | 2015-07-22 | 湖北中烟工业有限责任公司 | Tipping paper for tobacco and preparation method thereof |
| CN106280949A (en) * | 2016-08-17 | 2017-01-04 | 张静 | A kind of preparation method of aging resistance strong attached type exterior wall heat-insulating paint |
| CN106436445A (en) * | 2016-10-21 | 2017-02-22 | 吴迪 | Preparation method of double-layer antimicrobial breathable tipping paper for cigarettes |
| CN106567276A (en) * | 2015-10-08 | 2017-04-19 | 日本制纸巴比利亚股份有限公司 | Roll paper for smoking articles |
| CN107619962A (en) * | 2017-08-31 | 2018-01-23 | 常州道博化工有限公司 | A kind of preparation method of silver-based electric contact material |
| CN108157552A (en) * | 2017-12-28 | 2018-06-15 | 唐秀廷 | A kind of preparation method of golden camellia tea active material lozenge |
-
2018
- 2018-07-05 CN CN201810727014.1A patent/CN108951269A/en not_active Withdrawn
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014117964A1 (en) * | 2013-01-31 | 2014-08-07 | Glatfelter Gernsbach Gmbh & Co. Kg | Crosslinking/functionalization system for a paper or non-woven web |
| CN104789035A (en) * | 2015-05-06 | 2015-07-22 | 湖北中烟工业有限责任公司 | Tipping paper for tobacco and preparation method thereof |
| CN106567276A (en) * | 2015-10-08 | 2017-04-19 | 日本制纸巴比利亚股份有限公司 | Roll paper for smoking articles |
| CN106280949A (en) * | 2016-08-17 | 2017-01-04 | 张静 | A kind of preparation method of aging resistance strong attached type exterior wall heat-insulating paint |
| CN106436445A (en) * | 2016-10-21 | 2017-02-22 | 吴迪 | Preparation method of double-layer antimicrobial breathable tipping paper for cigarettes |
| CN107619962A (en) * | 2017-08-31 | 2018-01-23 | 常州道博化工有限公司 | A kind of preparation method of silver-based electric contact material |
| CN108157552A (en) * | 2017-12-28 | 2018-06-15 | 唐秀廷 | A kind of preparation method of golden camellia tea active material lozenge |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1106805C (en) | Tabacco sheet producing process by using the leftover of cigarette factory | |
| Wang et al. | Effect of stepwise lignin removal on the enzymatic hydrolysis and cellulase adsorption | |
| CN106511403B (en) | A kind of ganoderma lucidum tablet and preparation method thereof | |
| CN106942783B (en) | A method of improving papermaking-method reconstituted tobaccos appearance luster | |
| CN102524934A (en) | Reconstructed tobacco coating liquid component-component group chemical kitchen combination, coupling preparation, and coupling preparation process | |
| Yuan et al. | Dissolution of Bamboo Hemicellulose in 1-Butyl-3-Methylimidazolium Halide-based Ionic Liquids. | |
| CN108308693A (en) | A kind of preparation method of papermaking-method reconstituted tobaccos and improve method of the paper-process reconstituted tobacco to coating fluid absorbability | |
| CN109053821B (en) | Method for extracting tea polyphenol, total amino acids and flavone compounds from momordica grosvenori leaves | |
| CN1290453C (en) | Making process of creped tobacco sheet | |
| CN105505998A (en) | Method for preparing alcohol and biochar from traditional Chinese medicine residues in gradient mode | |
| CN116616483A (en) | Preparation method of reconstituted tobacco with fragrance-preserving function | |
| CN103704872B (en) | A kind of have reconstituted tobacco of fragrant and sweet style and uses thereof | |
| CN108951269A (en) | A kind of preparation method of cigarette tipping paper | |
| CN112641126A (en) | Circumferential heating tobacco cigarette core material and preparation method of heating tobacco cigarette core material | |
| CN105670793B (en) | Preparation method and application of cigarette cracking incense | |
| CN100525660C (en) | Method for preparing reproduced tobacco concentrated liquid | |
| CN113713766B (en) | Preparation method of biochar with excellent adsorption performance | |
| CN100999880A (en) | Process and product of pulping and mfg. sheet using low tar tabacco straw by biotransferring and swelling | |
| CN114540112B (en) | A kind of gardenia oil rich in crocin-I and its preparation method and application | |
| CN108560299B (en) | Preparation method of high-retention papermaking filler | |
| CN114468342A (en) | A steam explosion method for improving the quality of tobacco stems | |
| CN115336781A (en) | Reconstituted tobacco and preparation method and application thereof | |
| WO2022160397A1 (en) | Shanzhuang lipid-lowering micropellet and preparation method therefor | |
| CN106185915B (en) | A kind of method that nitrogen carbon molecular sieve is prepared by bagasse | |
| CN106723278A (en) | A kind of preparation method of tobacco humectant |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20181207 |