CN104664589B - A kind of atomized liquid containing Korean Ginseng composition and preparation method thereof - Google Patents
A kind of atomized liquid containing Korean Ginseng composition and preparation method thereof Download PDFInfo
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- CN104664589B CN104664589B CN201410855957.4A CN201410855957A CN104664589B CN 104664589 B CN104664589 B CN 104664589B CN 201410855957 A CN201410855957 A CN 201410855957A CN 104664589 B CN104664589 B CN 104664589B
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- korean ginseng
- atomized liquid
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
Abstract
The invention discloses a kind of atomized liquid containing Korean Ginseng composition and preparation method thereof.The described atomized liquid containing Korean Ginseng composition includes following components in percentage by weight: 55 75% propylene glycol, 10 20% glycerol, 5 10% Korean Ginseng compositions and 5 10% distilled water.Atomized liquid formula of the present invention, without tobacco extract, without nicotine, the substitute is and with the addition of Chinese herbal medicine Korean Ginseng medicinal ingredient；Propylene glycol, G & W ratio suitable, atomized liquid smog is dense, to throat nonirritant；Without essence and flavoring agent, the substitute is the pure natural fragrance of Korean Ginseng volatile oil, endanger without second hand smoking；The effect that Korean Ginseng medicinal ingredient has body-building QI invigorating, longevity is prolonged life simultaneously added.
Description
Technical field
The invention belongs to electronic cigarette field, be specifically related to a kind of atomized liquid containing Korean Ginseng composition and preparation thereof
Method.
Background technology
Along with people are more and more deep to the understanding of cigarette harm, smokers are highly desirable there is medicated cigarette substitute
Save their health.Wherein, electronic cigarette is as one of medicated cigarette substitute, and smoking cessation effect is obvious.Healthy
Electronic cigarette without tar, without harmful substances such as carbon monoxide, nitrogen dioxide, arsenic, lead, hydrargyrum, can avoid
" second hand smoking " harm to surrounding population.Through the development of several generations, current electronic cigarette taste can realize many
Sample, meets the demand that different taste is selected by different smoker.But electronic cigarette on the market main the most still with
Tobacco extract, nicotine etc. are given up material as craving for tobacco and are joined in electronic cigarette atomizing liquid, it is impossible to really full
The demand of foot consumer health's smoking cessation, especially can not meet the treatment of smoking cessation of the smoker suffering from some special disease
Demand, has limited to the envelop of function of electronic cigarette product.Electronic cigarette product market potential is huge, electronics on market
Aerosolization liquid function singleness, especially rare with product that Chinese medicine ingredients is tasty.
Korean Ginseng, the root of Araliaceae Radix Ginseng band rhizome, for the key medicine of tonifying five ZANG-organs yang-energy, nourish heart peace of can easily sleeping
God, spleen invigorating can dispel infiltration the pathogenic QI in the body of human five internal organs's six internal organs, hepatoprotective can refreshment eyesight improving, long-term taking then body-building benefit
Gas, longevity are prolonged life.The main active of Korean Ginseng is ginsenoside, and having brain cell activity has by force
The excitation of effect, activates the effect that brain cell two-ways regulation is excited with stable, promotes to keep physiological equilibrium and the heart
Reason state.Korean Ginseng has strongly invigorating primordial QI, promoting the production of body fluid and inducing sedation of the mind etc. to act on, it is adaptable to palpitation with fear insomniac, body void person,
Heart failure, cardiogenic shock etc..
The physiologically active ingredient of Korean Ginseng is ginsenoside, contained by its contained ginsenoside and other kinds
Ginsenoside's character is slightly different, and first, ginsenoside is triterpenes mostly, the distinctive soap of panax species
Glycosides.Second, the saponin found other plant has haemolysis, but ginsenoside is almost without toxicity
Neutrality joins saccharide.3rd, the pharmacological action of ginsenoside and the saponin of other medicinal plants have obvious difference.
4th, from the point of view of the molecular weight of ginsenoside, panoxadiol is 460, and panaxatriol is 478.
Summary of the invention
In place of shortcoming and defect for solution prior art, the primary and foremost purpose of the present invention is to provide one to contain
The atomized liquid of Korean Ginseng composition.This atomized liquid formula, by regulation water and the ratio of propylene glycol, makes energy after vaporization
Produce dense smog；Adding appropriate Korean Ginseng medicinal ingredient in atomized liquid, smoker is enjoying cigarette simultaneously
Also it can absorb Korean Ginseng medicinal ingredient while mist, play body-building QI invigorating, effect that longevity is prolonged life.
Another object of the present invention is to provide the preparation method of the above-mentioned atomized liquid containing Korean Ginseng composition.
For achieving the above object, the present invention adopts the following technical scheme that
A kind of atomized liquid containing Korean Ginseng composition, including following components in percentage by weight: 55-75% the third two
Alcohol, 10-20% glycerol, 5-10% Korean Ginseng composition and 5-10% distilled water；Described Korean Ginseng composition is Korean Ginseng
Volatile oil and Korean Ginseng extractum, above weight percentages of components sum is 100%.
Preferably, the described atomized liquid containing Korean Ginseng composition includes following components in percentage by weight: 72% the third
Glycol, 15% glycerol, 5% Korean Ginseng composition and 8% distilled water.
Preferably, the described atomized liquid containing Korean Ginseng composition includes following components in percentage by weight: 65% the third
Glycol, 17% glycerol, 8% Korean Ginseng composition and 10% distilled water.
Preferably, the described atomized liquid containing Korean Ginseng composition includes following components in percentage by weight: 63% the third
Glycol, 20% glycerol, 10% Korean Ginseng composition and 7% distilled water.
The preparation method of the above-mentioned atomized liquid containing Korean Ginseng composition, comprises the following steps:
(1) 80 mesh sieves are pulverized and crossed to Korean Ginseng decoction pieces, add distilled water, 75-85 according to solid-liquid ratio 1:10
DEG C extraction 3 times, each 2h, obtain volatile oil compositions and Aqueous extracts；Volatile oil compositions through petroleum ether extraction and
Being concentrated under reduced pressure to give Korean Ginseng volatile oil, Aqueous extracts is through being concentrated under reduced pressure to give Korean Ginseng extractum；
(2) the Korean Ginseng volatile oil and the Korean Ginseng extractum weight sum that prepare in step (1) are calculated as Koryo
The weight of ginseng composition, weighs remaining component raw material according to the percentage by weight of each component；Step (1) is prepared
Korean Ginseng extractum with distilled water dissolve, obtain middle drug solns；It is subsequently adding propylene glycol and glycerol stirring and evenly mixing,
Obtain primary atomization liquid；Add the Korean Ginseng volatile oil that step (1) prepares, 3000-4000rpm's
Emulsifying 5-10min under rotating speed, obtains the described atomized liquid containing Korean Ginseng composition.
Preferably, the temperature of the Aqueous extracts concentrating under reduced pressure described in step (1) is 60 DEG C.
Preferably, the emulsifying temperature described in step (2) is 25-30 DEG C.
Compared with prior art, the present invention has the following advantages and beneficial effect:
(1) traditional electronic cigarette atomizing liquid is the composition that skims the cream off milk from Nicotiana tabacum L., is dissolved in the solvent of food stage
In, add a small amount of essence and flavoring agent simultaneously.The essence of multiple green plants extracted, being inhaled into internal has
The unique effects remove the tobacco poisoning resting in human body, removing craving for tobacco.But, atomized liquid still contains Buddhist nun ancient
The carcinogen such as fourth, the health of harmful to human.
The present invention, without tobacco extract, without nicotine, the substitute is and with the addition of Chinese herbal medicine Koryo
Ginseng medicinal ingredient.The present invention, by selecting the Korean Ginseng decoction pieces of high-quality, uses abstraction technique, from Korean Ginseng
Main active is isolated in extraction, and ginsenoside contained in Korean Ginseng has multiple medicinal function, passes through
Atomization suck entrance internal after the most strongly fragrant while can produce drug effect, reach body-building QI invigorating, longevity is prolonged life
Effect；Obtained Korean Ginseng volatile oil abnormal smells from the patient is aromatic, can replace Nicotiana tabacum L. elite.
(2) atomized liquid formula of the present invention, propylene glycol, G & W ratio suitable, atomized liquid smog is dense,
To throat nonirritant；Without essence and flavoring agent, the substitute is the pure natural fragrance of Korean Ginseng volatile oil,
Endanger without second hand smoking；The effect that Korean Ginseng medicinal ingredient has body-building QI invigorating, longevity is prolonged life simultaneously added.
Accompanying drawing explanation
Fig. 1 is the embodiment of the present invention 1 Korean Ginseng constituents extraction process chart；
Fig. 2 is the embodiment of the present invention 1 atomized liquid preparation technology flow chart containing Korean Ginseng composition.
Detailed description of the invention
Below in conjunction with embodiment and accompanying drawing, the present invention is described in further detail, but the embodiment party of the present invention
Formula is not limited to this.
The invention discloses a kind of atomized liquid containing Korean Ginseng composition, it includes the group of following percentage by weight
Point: 55-75% propylene glycol, 10-20% glycerol, 5-10% Korean Ginseng composition and 5-10% distilled water.Should be containing height
The preparation process of the atomized liquid of Radix Ginseng Rubra composition is as follows:
(1) Korean Ginseng decoction pieces was pulverized 80 mesh sieves, according to solid-liquid ratio 1:10 add distilled water, 75-85 DEG C
Extract 3 times, each 2h, obtain volatile oil compositions and Aqueous extracts；Volatile oil compositions is through petroleum ether extraction and subtracts
Pressure is concentrated to give Korean Ginseng volatile oil, and Aqueous extracts is concentrated under reduced pressure to give Korean Ginseng extractum through 55-60 DEG C；
(2) the Korean Ginseng volatile oil and the Korean Ginseng extractum weight sum that prepare in step (1) are calculated as Koryo
The weight of ginseng composition, weighs remaining component raw material according to the percentage by weight of each component；Step (1) is prepared
Korean Ginseng extractum with distilled water dissolve, obtain middle drug solns；It is subsequently adding propylene glycol and glycerol stirring and evenly mixing,
Obtain primary atomization liquid；Add the Korean Ginseng volatile oil that step (1) prepares, the rotating speed of 3000-4000rpm
Lower emulsifying 5-10min, obtains the described atomized liquid containing Korean Ginseng composition.The atomized liquid bottling envelope obtained
Gai Hou, sterilized, lamp inspection, finally packaging warehouse-in stores.
The preparation process of above-mentioned atomized liquid is after determining rational formula, by abstraction technique and emulsifying technology
Realize, electronic atomized liquid will be made to have medicinal health function and reach optimal atomizing effect, separation must be extracted
Going out the main active of Korean Ginseng and prepare good properties and stable atomized liquid, its each composition is especially
Korean Ginseng volatile oil can be uniformly distributed with aqueous phase, without effects such as composition delays during atomization.Character to be prepared is excellent
Good and stable electronic atomized liquid, needs to solve the difficult problem in stirring and emulsifying hybrid technology, designs optimal parameter,
Wherein temperature, emulsification times, mixing speed all play vital effect.
Being found by experiment that, the atomized liquid water-oil phase prepared after using emulsifying stirring is uniformly dispersed, and
Can keep stable, biphase being not easy separates again.This system water oil is liquid, the most i.e. can reach
Good emulsifying effectiveness, higher than this temperature (40-70 DEG C) emulsifying effectiveness without writing change, the energy that high temperature consumes
More, from cost-effective angle, emulsifying temperature is set to 25-30 DEG C.
Test finding, the water-oil phase dispersion effect of the prepared atomized liquid of high rotating speed (4000-6000rpm) is good,
But the foam produced during high speed emulsifying is more, and the stirring at low speed of 3000rpm can eliminate bubble.Rotating speed is too small
(1000-2000rpm) shearing force is not enough so that the biphase of atomized liquid completes dispersion uniform, fine and smoothly.
Emulsification times will also result in impact to the quality of atomized liquid, owing to volatilizing in the atomized liquid formula of the present invention
The component content of oil is less, and viscosity is relatively low, can complete dispersion within a short period of time.5-10min, is atomized vacuole
The few oil slick of foam is few, emulsion-stabilizing.Less than 3min, owing to the time is too short, the not up to effect of stable dispersion.
Embodiment 1
The preparation method of a kind of atomized liquid containing Korean Ginseng composition, as illustrated in fig. 1 and 2, including following step
Rapid:
(1) 100g Korean Ginseng decoction pieces was pulverized 80 mesh sieves, according to solid-liquid ratio 1:10 add distilled water, 80
DEG C extraction 3 times, each 2h, obtain volatile oil compositions and Aqueous extracts；Volatile oil compositions through petroleum ether extraction and
Being concentrated under reduced pressure to give Korean Ginseng volatile oil, Aqueous extracts is concentrated under reduced pressure to give Korean Ginseng extractum through 60 DEG C；
(2) the Korean Ginseng volatile oil and the Korean Ginseng extractum weight sum that prepare in step (1) are calculated as Koryo
The weight of ginseng composition, weighs remaining component raw material according to the percentage by weight of each component；Step (1) is prepared
Korean Ginseng extractum with distilled water dissolve, obtain middle drug solns；It is subsequently adding propylene glycol and glycerol stirring and evenly mixing,
Obtain primary atomization liquid；Add the Korean Ginseng volatile oil that step (1) prepares, under the rotating speed of 3000rpm
Emulsifying 5min, emulsifying temperature is room temperature (25-30 DEG C), obtains the described atomization containing Korean Ginseng composition
Liquid.After the atomized liquid bottling capping obtained, sterilized, lamp inspection, finally packaging warehouse-in stores.
The most above-mentioned atomized liquid containing Korean Ginseng composition includes following components in percentage by weight: 72% the third two
Alcohol, 15% glycerol, 5% Korean Ginseng composition and 8% distilled water；Described Korean Ginseng composition is system in step (1)
The Korean Ginseng volatile oil obtained and Korean Ginseng extractum.
In this embodiment, Korean Ginseng medicinal ingredient ratio is less than normal, and smog is dense, and be suitable for just having given up smoking crowd.
Embodiment 2
The preparation method of a kind of atomized liquid containing Korean Ginseng composition, comprises the following steps:
(1) Korean Ginseng decoction pieces is pulverized 80 mesh sieves, add distilled water, 75 DEG C of leachings according to solid-liquid ratio 1:10
Carry 3 times, each 2h, obtain volatile oil compositions and Aqueous extracts；Volatile oil compositions is through petroleum ether extraction and decompression
Being concentrated to give Korean Ginseng volatile oil, Aqueous extracts is concentrated under reduced pressure to give Korean Ginseng extractum through 55 DEG C；
(2) the Korean Ginseng volatile oil and the Korean Ginseng extractum weight sum that prepare in step (1) are calculated as Koryo
The weight of ginseng composition, weighs remaining component raw material according to the percentage by weight of each component；Step (1) is prepared
Korean Ginseng extractum with distilled water dissolve, obtain middle drug solns；It is subsequently adding propylene glycol and glycerol stirring and evenly mixing,
Obtain primary atomization liquid；Add the Korean Ginseng volatile oil that step (1) prepares, under the rotating speed of 4000rpm
Emulsifying 5min, emulsifying temperature is room temperature (25-30 DEG C), obtains the described atomization containing Korean Ginseng composition
Liquid.After the atomized liquid bottling capping obtained, sterilized, lamp inspection, finally packaging warehouse-in stores.
The most above-mentioned atomized liquid containing Korean Ginseng composition includes following components in percentage by weight: 65% the third two
Alcohol, 17% glycerol, 8% Korean Ginseng composition and 10% distilled water；Described Korean Ginseng composition is system in step (1)
The Korean Ginseng volatile oil obtained and Korean Ginseng extractum.
In this embodiment, Korean Ginseng component ratio is moderate, can play a role in health care.
Embodiment 3
The preparation method of a kind of atomized liquid containing Korean Ginseng composition, comprises the following steps:
(1) Korean Ginseng decoction pieces is pulverized 80 mesh sieves, add distilled water, 80 DEG C of leachings according to solid-liquid ratio 1:10
Carry 3 times, each 2h, obtain volatile oil compositions and Aqueous extracts；Volatile oil compositions is through petroleum ether extraction and decompression
Being concentrated to give Korean Ginseng volatile oil, Aqueous extracts is concentrated under reduced pressure to give Korean Ginseng extractum through 60 DEG C；
(2) the Korean Ginseng volatile oil and the Korean Ginseng extractum weight sum that prepare in step (1) are calculated as Koryo
The weight of ginseng composition, weighs remaining component raw material according to the percentage by weight of each component；Step (1) is prepared
Korean Ginseng extractum with distilled water dissolve, obtain middle drug solns；It is subsequently adding propylene glycol and glycerol stirring and evenly mixing,
Obtain primary atomization liquid；Add the Korean Ginseng volatile oil that step (1) prepares, under the rotating speed of 3000rpm
Emulsifying 10min, emulsifying temperature is room temperature (25-30 DEG C), obtains the described atomization containing Korean Ginseng composition
Liquid.After the atomized liquid bottling capping obtained, sterilized, lamp inspection, finally packaging warehouse-in stores.
The most above-mentioned atomized liquid containing Korean Ginseng composition includes following components in percentage by weight: 63% the third two
Alcohol, 20% glycerol, 10% Korean Ginseng composition and 7% distilled water；Described Korean Ginseng composition is system in step (1)
The Korean Ginseng volatile oil obtained and Korean Ginseng extractum.
In this embodiment, Korean Ginseng medicinal ingredient ratio is higher, and health-care effect is obvious and smog is dense.
For verifying smoking cessation effect and the health-care effect of atomized liquid of the present invention, the atomized liquid in embodiment 3 is used to join
Side tests after making electronic cigarette, randomly draws 100 example smokers, all has palpitation with fear insomnia, body void, mental and physical efforts
The ill symptomses such as exhaustion.Put into electronic cigarette atomizing inhaler with 5ml atomized liquid, suck 10 every day, 2
The moon draws 80ml altogether.Test effect 92% craving for tobacco is remarkably decreased, and 65% body is empty, the symptoms such as insomnia of palpitating with fear all have
Improved, illustrated that atomized liquid of the present invention has remarkable result to smoking cessation, had the health-care effect calmed the nerves of easily sleeping simultaneously.
Above-described embodiment is the present invention preferably embodiment, but embodiments of the present invention are not by above-mentioned reality
Execute the restriction of example, the change made under other any spirit without departing from the present invention and principle, modification,
Substitute, combine, simplify, all should be the substitute mode of equivalence, within being included in protection scope of the present invention.
Claims (6)
1. the atomized liquid containing Korean Ginseng composition, it is characterised in that by following components in percentage by weight
Composition: 63-75% propylene glycol, 10-20% glycerol, 5-10% Korean Ginseng composition and 5-10% distilled water；Described height
Radix Ginseng Rubra composition is Korean Ginseng volatile oil and Korean Ginseng extractum, and above weight percentages of components sum is 100%；
The described atomized liquid containing Korean Ginseng composition is prepared by following steps:
(1) 80 mesh sieves are pulverized and crossed to Korean Ginseng decoction pieces, according to solid-liquid ratio 1:10 add distilled water, 75-85 DEG C
Extract 3 times, each 2h, obtain volatile oil compositions and Aqueous extracts；Volatile oil compositions is through petroleum ether extraction and subtracts
Pressure is concentrated to give Korean Ginseng volatile oil, and Aqueous extracts is through being concentrated under reduced pressure to give Korean Ginseng extractum；
(2) the Korean Ginseng volatile oil and the Korean Ginseng extractum weight sum that prepare in step (1) are calculated as Koryo
The weight of ginseng composition, weighs remaining component raw material according to the percentage by weight of each component；Step (1) is prepared
Korean Ginseng extractum with distilled water dissolve, obtain middle drug solns；It is subsequently adding propylene glycol and glycerol stirring and evenly mixing,
Obtain primary atomization liquid；Add the Korean Ginseng volatile oil that step (1) prepares, 3000-4000rpm's
Emulsifying 5-10min under rotating speed, obtains the described atomized liquid containing Korean Ginseng composition.
Atomized liquid containing Korean Ginseng composition the most according to claim 1, it is characterised in that this atomization
Liquid consists of the following components in percentage by weight: 72% propylene glycol, 15% glycerol, 5% Korean Ginseng composition and 8%
Distilled water.
Atomized liquid containing Korean Ginseng composition the most according to claim 1, it is characterised in that this atomization
Liquid consists of the following components in percentage by weight: 65% propylene glycol, 17% glycerol, 8% Korean Ginseng composition and 10%
Distilled water.
Atomized liquid containing Korean Ginseng composition the most according to claim 1, it is characterised in that this atomization
Liquid consists of the following components in percentage by weight: 63% propylene glycol, 20% glycerol, 10% Korean Ginseng composition and 7%
Distilled water.
Atomized liquid containing Korean Ginseng composition the most according to claim 1, it is characterised in that step (1)
The temperature of described Aqueous extracts concentrating under reduced pressure is 60 DEG C.
Atomized liquid containing Korean Ginseng composition the most according to claim 1, it is characterised in that step (2)
Described emulsifying temperature is 25-30 DEG C.
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| CN1994159A (en) * | 2006-12-15 | 2007-07-11 | 姜志荣 | Kidney-strengthening mind-refreshing tobacco liquid for electronic atomized cigarette |
| CN101194752A (en) * | 2006-12-29 | 2008-06-11 | 河南农业大学 | Oriental tobacco leaf concrete extracting method and use method thereof |
| CN101933653A (en) * | 2010-08-09 | 2011-01-05 | 深圳市如烟生物科技有限公司 | Officinal health-care solid electronic aerosolization liquid and preparation method thereof |
| CN102140388A (en) * | 2011-01-20 | 2011-08-03 | 深圳市如烟生物科技有限公司 | Preparation method for solid essence for tobaccos |
| CN103564647A (en) * | 2012-07-31 | 2014-02-12 | 马瑞 | Preparation method of traditional Chinese medicine spices for tobaccos |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ITMI20130214A1 (en) * | 2013-02-15 | 2014-08-16 | Pharmaday S R L | COMPOSITION FOR ELECTRONIC CIGARETTE |
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2014
- 2014-12-31 CN CN201410855957.4A patent/CN104664589B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1994159A (en) * | 2006-12-15 | 2007-07-11 | 姜志荣 | Kidney-strengthening mind-refreshing tobacco liquid for electronic atomized cigarette |
| CN101194752A (en) * | 2006-12-29 | 2008-06-11 | 河南农业大学 | Oriental tobacco leaf concrete extracting method and use method thereof |
| CN101933653A (en) * | 2010-08-09 | 2011-01-05 | 深圳市如烟生物科技有限公司 | Officinal health-care solid electronic aerosolization liquid and preparation method thereof |
| CN102140388A (en) * | 2011-01-20 | 2011-08-03 | 深圳市如烟生物科技有限公司 | Preparation method for solid essence for tobaccos |
| CN103564647A (en) * | 2012-07-31 | 2014-02-12 | 马瑞 | Preparation method of traditional Chinese medicine spices for tobaccos |
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