CN104687239A - Electronic cigarette liquid rich in ultra-micro green tea powder and tea saponin - Google Patents

Electronic cigarette liquid rich in ultra-micro green tea powder and tea saponin Download PDF

Info

Publication number
CN104687239A
CN104687239A CN201510027674.5A CN201510027674A CN104687239A CN 104687239 A CN104687239 A CN 104687239A CN 201510027674 A CN201510027674 A CN 201510027674A CN 104687239 A CN104687239 A CN 104687239A
Authority
CN
China
Prior art keywords
parts
tobacco
green tea
tea powder
tea
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201510027674.5A
Other languages
Chinese (zh)
Other versions
CN104687239B (en
Inventor
寇明钰
戴亚
冯广林
黄玉川
李国友
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chongqing China Tobacco Industry Co Ltd
Original Assignee
China Tobacco Chuanyu Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Chuanyu Industrial Co Ltd filed Critical China Tobacco Chuanyu Industrial Co Ltd
Priority to CN201510027674.5A priority Critical patent/CN104687239B/en
Publication of CN104687239A publication Critical patent/CN104687239A/en
Application granted granted Critical
Publication of CN104687239B publication Critical patent/CN104687239B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00Systems containing only non-condensed rings
    • C07C2601/12Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14The ring being saturated

Abstract

The invention discloses an electronic cigarette liquid rich in ultra-micro green tea powder and tea saponin. The electronic cigarette liquid comprises, in parts by weight, 50-60 parts of propylene glycol, 10-15 parts of glycerin, 7-10 parts of deionized water, 6-12 parts of a mixture of the ultra-micro green tea powder and the tea saponin, 3-10 parts of a tobacco extract, 1-5 parts of tobacco essence and 1-3 parts of a thickening agent. The electronic cigarette liquid rich in the ultra-micro green tea powder has no high-temperature thermal cracking reaction, and effects on consumers, other people and the environment are reduced while the consumers can have the smoking feeling. The ultra-micro green tea powder can be directly added to the electronic cigarette liquid without microencapsulation, the dissolution rate of effective ingredients is high, the ultra-micro green tea powder can optimize various smoke panel test indexes of the electronic cigarette liquid, improve the color of the electronic cigarette liquid and refresh the breath after added to the electronic cigarette liquid, the tea saponin and the ultra-micro green tea powder are combined to play a good anti-oxidation role, and other antioxidants are not required to be added to tobacco tar.

Description

A kind of tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element
Technical field
Embodiments of the present invention relate to Field of Tobacco, and more specifically, embodiments of the present invention relate to a kind of tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element.
Background technology
Smoking and healthy problem be the focus paid close attention to of global medical and health circle always.At present, under the macroeconomic situation that global Tobacco use control continues reinforcement and economic growth continued downturn, World tobacco industry faces a severe challenge.In order to reduce the impact of traditional cigarette on consumer, taking buccal cigarette as the smoke-free tobacco product of representative, do not burn cigarette and electronic cigarette of heating become the main flow of novel tobacco goods.
Electronic cigarette and electronics nicotine delivery device are by Chinese's innovation and creation.At present, foreign tobacco giant all scolds a huge sum of money to set foot in the research and development that electronic cigarette field carries out Related product.Tobacco juice for electronic smoke is atomized into mist by atomising device by electronic cigarette allows consumer know from experience the sensation of similar smoking.Because electronic cigarette does not exist tobacco high temperature pyrolysis process, therefore tar content is almost nil, does not have visible side-stream smoke, less to surrounding environment influence, gradually by consumer acceptance.Nicotine and flavor component etc. discharge mainly through propane diols and glycerine atomization by current electronic cigarette, and also some electronic cigarette nicotine and flavor component etc. is discharged by ultrasonic atomizatio water.
After consumer aspirates cigarette, usually remain a large amount of tobacco flavors in oral cavity, sensation dry mouth syndrome is felt bad, and therefore, pure and fresh oral cavity is the homework that most of smoking population is necessary after suction.But brush teeth after each smoking and be subject to the restriction in time place, also can bring the pollution of environment with chewing gum, therefore, while suction cigarette, reaching the effect in pure and fresh oral cavity, is the target that most of smoker pursues.
Tea Polyphenols is high-efficiency antioxidant agent, general tea powder dissolubility is bad, its active ingredient is difficult to a large amount of strippings, Tea Polyphenols is restricted in the application of Field of Tobacco, and green tea has pure and fresh taste, be rich in multiple catechin, vitamin, amino acid, caffeine etc., Tea Polyphenols is wherein the safe and efficient antioxidant of generally acknowledging in the world.In addition, inventor produces daye tea from In Xishuangbanna of Yunnan and finds the significant especially material of a kind of antioxidant effect---tea training element, and successfully extract this material, with Tea Polyphenols coordinative role, be effective good antioxidation, and its structure is as follows:
Because be rich in Tea Polyphenols, alkaloid, aromatic substance etc. in tealeaves, inventor adopts the form of ultrafine green tea powder and tea to train element to mix and add in tobacco juice for electronic smoke, all active materials of green tea can be fully utilized, very high leaching rate can be reached again, under the synergy of high in antioxidants tea training element, while allowing electronic cigarette consumer obtain higher physiology satisfaction, pure and fresh oral cavity.
Summary of the invention
Instant invention overcomes the deficiencies in the prior art, a kind of embodiment being rich in the tobacco juice for electronic smoke of ultrafine green tea powder and tea training element is provided, to expect the mouthfeel and the quality that improve tobacco juice for electronic smoke, the pure and fresh oral cavity when aspirating cigarette simultaneously.
For solving above-mentioned technical problem, one embodiment of the present invention by the following technical solutions:
Be rich in a tobacco juice for electronic smoke for ultrafine green tea powder and tea training element, it is made up of following component by weight:
Propane diols 50 ~ 60 parts, glycerine 10 ~ 15 parts, deionized water 7 ~ 10 parts, 6 ~ 12 parts, the mixture of ultrafine green tea powder and tea training element, tobacco extract 3 ~ 10 parts, flavouring essence for tobacco 1 ~ 5 part, thickener 1 ~ 3 part.
Further technical scheme is: the described tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element is made up of following component by weight:
Propane diols 55 ~ 60 parts, glycerine 10 ~ 12 parts, deionized water 7 ~ 9 parts, 6 ~ 10 parts, the mixture of ultrafine green tea powder and tea training element, tobacco extract 4 ~ 8 parts, flavouring essence for tobacco 2 ~ 5 parts, thickener 1 ~ 3 part.
According to the present invention one preferred embodiment, the described tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element is made up of following component by weight:
Propane diols 59 parts, glycerine 12 parts, deionized water 9 parts, 6 parts, the mixture of ultrafine green tea powder and tea training element, tobacco extract 6 parts, flavouring essence for tobacco 5 parts, thickener 3 parts.
According to the present invention one preferred embodiment, the described tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element is made up of following component by weight:
Propane diols 59 parts, glycerine 10 parts, deionized water 8 parts, 10 parts, the mixture of ultrafine green tea powder and tea training element, tobacco extract 8 parts, flavouring essence for tobacco 2 parts, thickener 3 parts.
Further technical scheme is: in the mixture of described ultrafine green tea powder and tea training element, the mass ratio of ultrafine green tea powder and tea training element is 5 ~ 8:1.
Further technical scheme is: described tobacco extract is the extract of at least one in flue-cured tobacco, airing cigarette, burley tobaccos, cigar.
Further technical scheme is: described flavouring essence for tobacco is made by being at room temperature uniformly mixed with the following component of parts by weight: cloud and mist absolute oil 2 ~ 3 parts, Peru's medicinal extract 0.5 ~ 1 part, Ethyl vanillin 0.1 ~ 3 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 3 ~ 5 parts, maltol 0.05 ~ 0.1 part, 2-acetyl group pyrazine 0.5 ~ 1.0 part, 2, 3, 5-trimethylpyrazine 0.5 ~ 1 part, iso-amyl iso-valeriate 1.0 ~ 1.5 parts, menthyl acetate 0.1 ~ 0.5 part, the oxidation isophorone of mass concentration 1% 0.5 ~ 1 part, the damascenone of mass concentration 1% 1.0 ~ 2.0 parts, the damascone of mass concentration 1% 0.5 ~ 1 part, the Megastigmatrienone of mass concentration 1% 0.5 ~ 1 part, the lavender oil of mass concentration 1% 1.0 ~ 2.0 parts, the coriander seed oil of mass concentration 1% 1.5 ~ 2.0 parts, vanilla bean tincture 7.0 ~ 8.0 parts, red date tincture 9 ~ 11 parts, angelica grosseserrata root tincture 2.0 ~ 4.0 parts, propane diols 18.0 ~ 22.0 parts, ethanol 40.0 ~ 45.0 parts.
Further technical scheme is: described flavouring essence for tobacco is made by being at room temperature uniformly mixed with the following component of parts by weight: cloud and mist absolute oil 2.2 parts, Peru's medicinal extract 0.6 part, Ethyl vanillin 0.2 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 4.0 parts, maltol 0.05 part, 2-acetyl group pyrazine 1.0 parts, 2, 3, 5-trimethylpyrazine 0.5 part, iso-amyl iso-valeriate 1.0 parts, menthyl acetate 0.2 part, the oxidation isophorone of mass concentration 1% 0.9 part, the damascenone of mass concentration 1% 1.5 parts, the damascone of mass concentration 1% 0.5 part, the Megastigmatrienone of mass concentration 1% 0.5 part, the lavender oil of mass concentration 1% 1.0 parts, the coriander seed oil of mass concentration 1% 1.5 parts, vanilla bean tincture 8.0 parts, red date tincture 10 parts, angelica grosseserrata root tincture 3.0 parts, propane diols 20 parts, ethanol 43.35 parts.
Further technical scheme is: the preparation method of described tea training element is:
(1) extract 3 times with ethanolic solution water-bath under temperature 60 C of the concentration 40% of 5 ~ 10 times of weight portions after being pulverized by tealeaves, extract 2h at every turn, gained extracting liquid filtering concentrates, and obtains medicinal extract;
(2) described medicinal extract is filtered with hot water dissolving, adsorb through macroreticular resin D101, then with pure water, concentration 10% ethanol water, concentration 20% ethanol water, concentration 40% ethanol water gradient elution, collect eluent, with thin-layer chromatography or high-efficient liquid phase analysis, by the partial concentration containing target component, obtain concentrate;
(3) by described concentrate filler be the further chromatography of molecular sieve of sephadex LH20, then use concentration 40% methanol aqueous solution wash-out, collect eluent, with thin-layer chromatography or high-efficient liquid phase analysis, merge and obtain tea training element.Concentration of alcohol refers to the volume fraction of ethanol.
Green tea has pure and fresh taste, and be rich in multiple catechin, vitamin, amino acid, caffeine etc., Tea Polyphenols is wherein the safe and efficient antioxidant of generally acknowledging in the world.And ultrafine green tea powder color is emerald green, quality is fine and smooth, nutritious, can effectively mix with tobacco juice for electronic smoke and abundant stripping active ingredient.Tea training element is the natural products of a kind of high anti-oxidation activity contained in part tealeaves, its structure is made up of a gallic acid and quinolinic acid, jointly antioxidation can be played with the dissolved element in green tea in electronic cigarette liquid, the intermiscibility of tea training element and tobacco juice for electronic smoke is good, the mouthfeel of adjustable tobacco juice for electronic smoke, improves the characteristics such as the pleasant impression of tobacco juice for electronic smoke, harmony and concentration.
Compared with prior art, one of beneficial effect of the present invention is: the tobacco juice for electronic smoke that ultrafine green tea powder is rich in the present invention does not exist high temperature pyrolysis reaction, therefore releasing content of coke tar is almost nil, is meeting while consumer obtains smoking experience, reduce on self, the impact of other people and environment.Simultaneously, ultrafine green tea powder can directly add in electronic cigarette liquid without the need to microencapsulation, active ingredient dissolution rate in ultrafine green tea powder is high, the every Sensory quality index of electronic cigarette liquid can be optimized adding to after in electronic cigarette liquid, improve the color and luster of tobacco juice for electronic smoke, again can fresh breath, tea training element plays good antioxidation jointly with ultrafine green tea powder, add other antioxidants without the need to auxiliary in tobacco tar, simplify tobacco tar composition.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
Flavouring essence for tobacco is made by being at room temperature uniformly mixed with the following component of parts by weight: cloud and mist absolute oil 2.2 parts, Peru's medicinal extract 0.6 part, Ethyl vanillin 0.2 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 4.0 parts, maltol 0.05 part, 2-acetyl group pyrazine 1.0 parts, 2, 3, 5-trimethylpyrazine 0.5 part, iso-amyl iso-valeriate 1.0 parts, menthyl acetate 0.2 part, the oxidation isophorone of mass concentration 1% 0.9 part, the damascenone of mass concentration 1% 1.5 parts, the damascone of mass concentration 1% 0.5 part, the Megastigmatrienone of mass concentration 1% 0.5 part, the lavender oil of mass concentration 1% 1.0 parts, the coriander seed oil of mass concentration 1% 1.5 parts, vanilla bean tincture 8.0 parts, red date tincture 10 parts, angelica grosseserrata root tincture 3.0 parts, propane diols 20 parts, ethanol 43.35 parts.This flavouring essence for tobacco is used for following embodiment.
The preparation of tea training element:
(1) extract 3 times with ethanolic solution water-bath under temperature 60 C of 700g concentration 40% after being pulverized by 100g tealeaves, extract 2h at every turn, gained extracting liquid filtering concentrates, and obtains medicinal extract 30g;
(2) described medicinal extract is filtered with hot water dissolving, adsorb through macroreticular resin D101, then with pure water, concentration 10% ethanol water, concentration 20% ethanol water, concentration 40% ethanol water gradient elution, collect eluent, with thin-layer chromatography or high-efficient liquid phase analysis, by the partial concentration containing target component, obtain concentrate 5.5g;
(3) by described concentrate filler be the further chromatography of molecular sieve of sephadex LH20, then use concentration 40% methanol aqueous solution wash-out, collect eluent, with thin-layer chromatography or high-efficient liquid phase analysis, merge and obtain tea and train plain 0.3g.
Ultrafine green tea powder is commercially available conventional products.
Thickener is the commercially available conventional products of Field of Tobacco.
Embodiment 1
By weight, get propane diols 59 parts, glycerine 12 parts, deionized water 9 parts, ultrafine green tea powder 5 parts, tea training element 1 part, flue-cured tobacco extract 6 parts, flavouring essence for tobacco 5 parts, thickener 3 parts is configured to the tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element.
Comparative example 1
By weight, get propane diols 65 parts, glycerine 12 parts, deionized water 9 parts, flue-cured tobacco extract 6 parts, flavouring essence for tobacco 5 parts, thickener 3 parts configuration tobacco juice for electronic smoke, not containing ultrafine green tea powder and tea training element in this tobacco juice for electronic smoke.
Embodiment 2
By weight, get propane diols 59 parts, glycerine 10 parts, deionized water 8 parts, ultrafine green tea powder 8.5 parts, tea training element 1.5 parts, burley tobaccos extract 8 parts, flavouring essence for tobacco 2 parts, thickener 3 parts is configured to the tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element.
Comparative example 2
By weight, get propane diols 66 parts, glycerine 10 parts, deionized water 8 parts, burley tobaccos extract 8 parts, flavouring essence for tobacco 5 parts, thickener 3 parts configuration tobacco juice for electronic smoke, not containing ultrafine green tea powder and tea training element in this tobacco juice for electronic smoke.
Using embodiment 1 and comparative example 1 as one group, embodiment 2 and comparative example 2 are as one group, carry out electronic cigarette sensory evaluating smoking, evaluation method is with reference to consolidating the big method of effect (CN 201310031800.5), the evaluation criteria of indices is as table 1, embodiment 1,2, the smoking result of comparative example 1,2 is as table 2:
Table 1 individual event sensory evaluation index 9 points of point system quantitative descriptions processed
Note: minimum score standard is 0.5.
Table 2 embodiment and comparative example sensory evaluating smoking results contrast
As shown in Table 2, embodiment 1 sensory evaluating smoking must be divided into 51 points, be better than comparative example 1, wherein embodiment 1 fragrance, harmony, assorted gas, excitant, pleasant impression are all better than comparative example 1, especially pleasant impression and harmony, owing to having the pure and fresh implication of green tea, pleasant impression improves obviously, be used in tobacco juice for electronic smoke because tea training element and ultrafine green tea powder combine, the harmony of tobacco juice for electronic smoke significantly improves; Embodiment 2 sensory evaluating smoking must be divided into 50.0, is better than comparative example 2, and wherein, embodiment 2 harmony, assorted gas, excitant, pleasant impression are better than comparative example 2.In addition, in outward appearance, the tobacco juice for electronic smoke adding ultrafine green tea powder is green transparent shape, and color and luster pleasant, excites the desire that consumer sucks.
Although with reference to multiple explanatory embodiment of the present invention, invention has been described here, but, should be appreciated that, those skilled in the art can design a lot of other amendment and embodiment, these amendments and embodiment will drop within spirit disclosed in the present application and spirit.More particularly, in the scope of and claim open in the application, multiple modification and improvement can be carried out to the building block of subject combination layout and/or layout.Except the modification of carrying out building block and/or layout is with except improvement, to those skilled in the art, other purposes also will be obvious.

Claims (9)

1. be rich in a tobacco juice for electronic smoke for ultrafine green tea powder and tea training element, it is characterized in that it is made up of following component by weight:
Propane diols 50 ~ 60 parts, glycerine 10 ~ 15 parts, deionized water 7 ~ 10 parts, 6 ~ 12 parts, the mixture of ultrafine green tea powder and tea training element, tobacco extract 3 ~ 10 parts, flavouring essence for tobacco 1 ~ 5 part, thickener 1 ~ 3 part.
2. the tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element according to claim 1, is characterized in that it is made up of following component by weight:
Propane diols 55 ~ 60 parts, glycerine 10 ~ 12 parts, deionized water 7 ~ 9 parts, 6 ~ 10 parts, the mixture of ultrafine green tea powder and tea training element, tobacco extract 4 ~ 8 parts, flavouring essence for tobacco 2 ~ 5 parts, thickener 1 ~ 3 part.
3. the tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element according to claim 2, is characterized in that it is made up of following component by weight:
Propane diols 59 parts, glycerine 12 parts, deionized water 9 parts, 6 parts, the mixture of ultrafine green tea powder and tea training element, tobacco extract 6 parts, flavouring essence for tobacco 5 parts, thickener 3 parts.
4. the tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element according to claim 2, is characterized in that it is made up of following component by weight:
Propane diols 59 parts, glycerine 10 parts, deionized water 8 parts, 10 parts, the mixture of ultrafine green tea powder and tea training element, tobacco extract 8 parts, flavouring essence for tobacco 2 parts, thickener 3 parts.
5. the tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element according to Claims 1 to 4 any one, is characterized in that the mass ratio of ultrafine green tea powder and tea training element in the mixture of described ultrafine green tea powder and tea training element is 5 ~ 8:1.
6. the tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element according to Claims 1 to 4 any one, is characterized in that described tobacco extract is the extract of at least one in flue-cured tobacco, airing cigarette, burley tobaccos, cigar.
7. the tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element according to Claims 1 to 4 any one, it is characterized in that described flavouring essence for tobacco is made by being at room temperature uniformly mixed with the following component of parts by weight: cloud and mist absolute oil 2 ~ 3 parts, Peru's medicinal extract 0.5 ~ 1 part, Ethyl vanillin 0.1 ~ 3 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 3 ~ 5 parts, maltol 0.05 ~ 0.1 part, 2-acetyl group pyrazine 0.5 ~ 1.0 part, 2, 3, 5-trimethylpyrazine 0.5 ~ 1 part, iso-amyl iso-valeriate 1.0 ~ 1.5 parts, menthyl acetate 0.1 ~ 0.5 part, the oxidation isophorone of mass concentration 1% 0.5 ~ 1 part, the damascenone of mass concentration 1% 1.0 ~ 2.0 parts, the damascone of mass concentration 1% 0.5 ~ 1 part, the Megastigmatrienone of mass concentration 1% 0.5 ~ 1 part, the lavender oil of mass concentration 1% 1.0 ~ 2.0 parts, the coriander seed oil of mass concentration 1% 1.5 ~ 2.0 parts, vanilla bean tincture 7.0 ~ 8.0 parts, red date tincture 9 ~ 11 parts, angelica grosseserrata root tincture 2.0 ~ 4.0 parts, propane diols 18.0 ~ 22.0 parts, ethanol 40.0 ~ 45.0 parts.
8. the tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element according to claim 7 any one, it is characterized in that described flavouring essence for tobacco is made by being at room temperature uniformly mixed with the following component of parts by weight: cloud and mist absolute oil 2.2 parts, Peru's medicinal extract 0.6 part, Ethyl vanillin 0.2 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 4.0 parts, maltol 0.05 part, 2-acetyl group pyrazine 1.0 parts, 2, 3, 5-trimethylpyrazine 0.5 part, iso-amyl iso-valeriate 1.0 parts, menthyl acetate 0.2 part, the oxidation isophorone of mass concentration 1% 0.9 part, the damascenone of mass concentration 1% 1.5 parts, the damascone of mass concentration 1% 0.5 part, the Megastigmatrienone of mass concentration 1% 0.5 part, the lavender oil of mass concentration 1% 1.0 parts, the coriander seed oil of mass concentration 1% 1.5 parts, vanilla bean tincture 8.0 parts, red date tincture 10 parts, angelica grosseserrata root tincture 3.0 parts, propane diols 20 parts, ethanol 43.35 parts.
9. the tobacco juice for electronic smoke being rich in ultrafine green tea powder and tea training element according to Claims 1 to 4 any one, is characterized in that the preparation method of described tea training element is:
(1) extract 3 times with ethanolic solution water-bath under temperature 60 C of the concentration 40% of 5 ~ 10 times of weight portions after being pulverized by tealeaves, extract 2h at every turn, gained extracting liquid filtering concentrates, and obtains medicinal extract;
(2) described medicinal extract is filtered with hot water dissolving, adsorb through macroreticular resin D101, then with pure water, concentration 10% ethanol water, concentration 20% ethanol water, concentration 40% ethanol water gradient elution, collect eluent, with thin-layer chromatography or high-efficient liquid phase analysis, by the partial concentration containing target component, obtain concentrate;
(3) by described concentrate filler be the further chromatography of molecular sieve of sephadex LH20, then use concentration 40% methanol aqueous solution wash-out, collect eluent, with thin-layer chromatography or high-efficient liquid phase analysis, merge and obtain tea training element.
CN201510027674.5A 2015-01-20 2015-01-20 A kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea Active CN104687239B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510027674.5A CN104687239B (en) 2015-01-20 2015-01-20 A kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510027674.5A CN104687239B (en) 2015-01-20 2015-01-20 A kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea

Publications (2)

Publication Number Publication Date
CN104687239A true CN104687239A (en) 2015-06-10
CN104687239B CN104687239B (en) 2016-06-08

Family

ID=53335129

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510027674.5A Active CN104687239B (en) 2015-01-20 2015-01-20 A kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea

Country Status (1)

Country Link
CN (1) CN104687239B (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105011352A (en) * 2015-08-06 2015-11-04 云南中烟工业有限责任公司 Green tea scent type electronic cigarette liquid
CN105962426A (en) * 2016-07-29 2016-09-28 福建中烟工业有限责任公司 Composition containing Tie Guanyin tea extracts and electronic cigarette fluid
CN106617277A (en) * 2016-12-26 2017-05-10 颐中(青岛)实业有限公司 Method for preparing tea-fragrance electronic cigarette liquid through wet grinding
CN113749276A (en) * 2021-09-11 2021-12-07 深圳市真味生物科技有限公司 Electronic atomized liquid capable of freshening oral cavity and having good smoke amount

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106307602A (en) * 2016-09-12 2017-01-11 三峡大学 Electronic cigarette liquid for freshening breath

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002091866A1 (en) * 2001-05-11 2002-11-21 Thione International, Inc. Glutathione, green tea, grape seed extract to neutralize tobacco free radicals
CN1903087A (en) * 2005-07-26 2007-01-31 株式会社梦烟草技术 Green tea-based cigarette and method for manufacturing the same
CN102771884A (en) * 2012-07-31 2012-11-14 普瑞斯生物科技(湖南)有限公司 Tobacco juice of electronic cigarette having functions of antioxidation, softening blood vessels and refreshing breath
CN102813278A (en) * 2012-08-09 2012-12-12 深圳瀚星翔科技有限公司 Mixed electronic cigarette tobacco liquid
CN103054173A (en) * 2013-01-25 2013-04-24 红云红河烟草(集团)有限责任公司 Electronic cigarette liquid prepared from discarded tobacco
CN103070472A (en) * 2013-01-25 2013-05-01 红云红河烟草(集团)有限责任公司 Electronic cigarette liquid capable of effectively improving sensory quality of electronic cigarette
CN104068467A (en) * 2014-07-01 2014-10-01 安徽中烟工业有限责任公司 Electronic cigarette liquid rich in plant flavone

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002091866A1 (en) * 2001-05-11 2002-11-21 Thione International, Inc. Glutathione, green tea, grape seed extract to neutralize tobacco free radicals
CN1903087A (en) * 2005-07-26 2007-01-31 株式会社梦烟草技术 Green tea-based cigarette and method for manufacturing the same
CN102771884A (en) * 2012-07-31 2012-11-14 普瑞斯生物科技(湖南)有限公司 Tobacco juice of electronic cigarette having functions of antioxidation, softening blood vessels and refreshing breath
CN102813278A (en) * 2012-08-09 2012-12-12 深圳瀚星翔科技有限公司 Mixed electronic cigarette tobacco liquid
CN103054173A (en) * 2013-01-25 2013-04-24 红云红河烟草(集团)有限责任公司 Electronic cigarette liquid prepared from discarded tobacco
CN103070472A (en) * 2013-01-25 2013-05-01 红云红河烟草(集团)有限责任公司 Electronic cigarette liquid capable of effectively improving sensory quality of electronic cigarette
CN104068467A (en) * 2014-07-01 2014-10-01 安徽中烟工业有限责任公司 Electronic cigarette liquid rich in plant flavone

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
陈宗懋: "《中国茶叶大辞典》", 31 December 2000 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105011352A (en) * 2015-08-06 2015-11-04 云南中烟工业有限责任公司 Green tea scent type electronic cigarette liquid
CN105011352B (en) * 2015-08-06 2016-06-01 云南中烟工业有限责任公司 A kind of green tea flavor electronic cigarette tobacco tar
CN105962426A (en) * 2016-07-29 2016-09-28 福建中烟工业有限责任公司 Composition containing Tie Guanyin tea extracts and electronic cigarette fluid
CN105962426B (en) * 2016-07-29 2019-07-16 福建中烟工业有限责任公司 Composition and tobacco juice for electronic smoke containing extra-strong tea extract
CN106617277A (en) * 2016-12-26 2017-05-10 颐中(青岛)实业有限公司 Method for preparing tea-fragrance electronic cigarette liquid through wet grinding
CN113749276A (en) * 2021-09-11 2021-12-07 深圳市真味生物科技有限公司 Electronic atomized liquid capable of freshening oral cavity and having good smoke amount

Also Published As

Publication number Publication date
CN104687239B (en) 2016-06-08

Similar Documents

Publication Publication Date Title
CN102304428B (en) Formula of tobacco flavoring essence with sweet fragrance
CN104687239B (en) A kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea
CN103070472A (en) Electronic cigarette liquid capable of effectively improving sensory quality of electronic cigarette
CN104770863A (en) Electronic cigarette smoke solution with herbal tea flavor
CN103989245A (en) Chinese flue-cured tobacco type electronic cigarette liquid capable of effectively reducing oral cavity sweet greasy feeling
CN104397871B (en) A kind of electronic cigarette tobacco tar containing tea extract and preparation method thereof
CN103768435B (en) A kind of fresh breath type tobacco oral spray agent and preparation method thereof
CN104544552A (en) Electronic cigarette smoke solution prepared through oolong leaf extract
CN104544549A (en) Electronic cigarette smoke solution prepared through green tea leaf extract
CN102304423A (en) Fragrance-enhancing tobacco essence
CN104544543A (en) Electronic cigarette smoke solution prepared through black tea leaf extract
CN103054172A (en) Electronic cigarette liquid prepared from strong-flavor tobacco
CN111671134A (en) Mint flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid
CN104531356A (en) Honeyed-sweet additive and electronic cigarette liquid with same
CN104970445B (en) A kind of spacetabs type aerosol mouth cigarette
CN107343668A (en) A kind of purposes of the electronics tobacco tar for lifting fragrance texture and preparation method thereof with it
CN102154060A (en) Formula of tobacco additive essence of hami melon fragrance
CN104585864B (en) A kind of tobacco juice for electronic smoke containing Fructus Hippophae polysaccharide
CN104544544A (en) Electronic cigarette smoke solution prepared through white tea leaf extract
CN103478888B (en) A kind of quid of plum flavor
CN105361237A (en) Electronic cigarette tobacco juice with cholesterol reducing function and preparation method thereof
CN104544548A (en) Electronic cigarette smoke solution prepared through yellow tea leaf extract
CN102994229B (en) Cigarette flavor prepared by utilizing red date extract and preparation and application method thereof
CN102031198A (en) Tobacco feeding essence for replenishing bean-flavor
CN103734904B (en) A kind of nourishing Yin and falling fire type tobacco oral spray agent and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20210601

Address after: Nanping Nan'an District of Chongqing City Road 400060 No. 2

Patentee after: CHONGQING CHINA TOBACCO INDUSTRY Co.,Ltd.

Address before: 610000 No. 2 Jackie Chan Road, Chengdu new economic and Technological Development Zone, Longquanyi District, Chengdu, Sichuan

Patentee before: CHINA TOBACCO SICHUAN INDUSTRIAL Co.,Ltd.

TR01 Transfer of patent right