CN104687239B - A kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea - Google Patents
A kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea Download PDFInfo
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- CN104687239B CN104687239B CN201510027674.5A CN201510027674A CN104687239B CN 104687239 B CN104687239 B CN 104687239B CN 201510027674 A CN201510027674 A CN 201510027674A CN 104687239 B CN104687239 B CN 104687239B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Abstract
The invention discloses a kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea, it is by propylene glycol 50��60 parts by weight, glycerol 10��15 parts, deionized water 7��10 parts, 6��12 parts of the mixture of ultrafine green tea powder and tea training element, tobacco extract 3��10 parts, flavouring essence for tobacco 1��5 part, thickening agent 1��3 part composition. The present invention is absent from high temperature pyrolysis reaction rich in the tobacco juice for electronic smoke of ultrafine green tea powder, is meeting while consumer obtains smoking experience, reduce on self, the impact of other people and environment. Ultrafine green tea powder can be directly appended in electronic cigarette liquid without microencapsulation, effective ingredient dissolution rate is high, add to and the every Sensory quality index of electronic cigarette liquid after in electronic cigarette liquid, can be optimized, improve the pool of adding lustre to of tobacco juice for electronic smoke, again can fresh breath, tea training element plays good antioxidation jointly with ultrafine green tea powder, it is not necessary in ree-oil, auxiliary adds other antioxidants.
Description
Technical field
Embodiments of the present invention relate to Field of Tobacco, more specifically, embodiments of the present invention relate to a kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea.
Background technology
Smoking and the healthy problem focus that whole world medical and health circle are paid close attention to always. At present, in the whole world, Tobacco use control continues to strengthen with under the macroeconomic situation of economic growth continued downturn, and World tobacco industry faces a severe challenge. In order to reduce the traditional cigarette impact on consumer, with buccal cigarette be representative smoke-free tobacco product, Medicated cigarette is not burnt in heating and electronic cigarette becomes the main flow of novel tobacco goods.
Electronic cigarette and electronics nicotine delivery device, be by Chinese's innovation and creation. At present, foreign tobacco giant all scolds a huge sum of money to set foot in electronic cigarette field and carry out the research and development of Related product. Tobacco juice for electronic smoke is atomized into mist by atomising device by electronic cigarette allows consumer know from experience the sensation of similar smoking. Because electronic cigarette is absent from Nicotiana tabacum L. high temperature pyrolysis process, therefore tar content is almost nil, it does not have visible side-stream smoke, and surrounding environment influence is less, is approved by consumer gradually. Current electronic cigarette is atomized mainly through propylene glycol and glycerol and nicotine and flavor component etc. is discharged, and also some electronic cigarette is nicotine and flavor component etc. to be discharged by ultrasonic atomizatio water.
After consumer's suction cigarette, usually remaining substantial amounts of tobacco flavor in oral cavity, sensation dry mouth syndrome feel bad, and therefore, pure and fresh oral cavity is the homework that most of smoking population is necessary after suction. But brush teeth after smoking every time and be subject to the restriction in time place, also can bring the pollution of environment with chewing gum, therefore, while suction cigarette, reach the effect in pure and fresh oral cavity, be the target of most of smoker pursuit.
Tea polyphenols is high-efficiency antioxidant agent, general tea powder dissolubility is bad, its effective ingredient is difficult to substantial amounts of dissolution, tea polyphenols is restricted in the application of Field of Tobacco, and green tea has pure and fresh taste, rich in multiple catechin, vitamin, aminoacid, caffeine etc., tea polyphenols therein is the safe and efficient antioxidant generally acknowledged in the world.Additionally, inventor produces from In Xishuangbanna of Yunnan finds the especially significant material tea training element of a kind of antioxidant effect daye tea, and successfully extracting this material, with tea polyphenols coordinative role, be effective good antioxidation, and its structure is as follows:
Because rich in tea polyphenols, alkaloid, aromatic substance etc. in Folium Camelliae sinensis, inventor adopts add in tobacco juice for electronic smoke mix plain with tea training of form of ultrafine green tea powder, all active substances of green tea can be comprehensively utilized, significantly high leaching rate can be reached again, under the synergism of high in antioxidants tea training element, while allowing electronic cigarette consumer obtain higher physiology gratification, pure and fresh oral cavity.
Summary of the invention
Instant invention overcomes the deficiencies in the prior art, it is provided that the embodiment of a kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea, to expect mouthfeel and the quality improving tobacco juice for electronic smoke, the pure and fresh oral cavity when aspirating cigarette simultaneously.
For solving above-mentioned technical problem, one embodiment of the present invention by the following technical solutions:
A kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea, it is made up of following components by weight:
Propylene glycol 50��60 parts, glycerol 10��15 parts, deionized water 7��10 parts, 6��12 parts of the mixture of ultrafine green tea powder and tea training element, tobacco extract 3��10 parts, flavouring essence for tobacco 1��5 part, thickening agent 1��3 part.
Further technical scheme is: the described tobacco juice for electronic smoke rich in ultrafine green tea powder and tea training element is made up of following components by weight:
Propylene glycol 55��60 parts, glycerol 10��12 parts, deionized water 7��9 parts, 6��10 parts of the mixture of ultrafine green tea powder and tea training element, tobacco extract 4��8 parts, flavouring essence for tobacco 2��5 parts, thickening agent 1��3 part.
According to one preferred embodiment of the invention, the described tobacco juice for electronic smoke rich in ultrafine green tea powder and tea training element is made up of following components by weight:
Propylene glycol 59 parts, glycerol 12 parts, deionized water 9 parts, 6 parts of the mixture of ultrafine green tea powder and tea training element, tobacco extract 6 parts, flavouring essence for tobacco 5 parts, thickening agent 3 parts.
According to one preferred embodiment of the invention, the described tobacco juice for electronic smoke rich in ultrafine green tea powder and tea training element is made up of following components by weight:
Propylene glycol 59 parts, glycerol 10 parts, deionized water 8 parts, 10 parts of the mixture of ultrafine green tea powder and tea training element, tobacco extract 8 parts, flavouring essence for tobacco 2 parts, thickening agent 3 parts.
Further technical scheme is: in the mixture of described ultrafine green tea powder and tea training element, the mass ratio of ultrafine green tea powder and tea training element is 5��8:1.
Further technical scheme is: described tobacco extract is extract at least one in flue-cured tobacco, dry in the sun cigarette, burley tobaccos, cigar.
Further technical scheme is: described flavouring essence for tobacco is at room temperature stirred by the following components with parts by weight and is mixed: cloud and mist absolute oil 2��3 parts, Peru's extractum 0.5��1 part, ethyl vanillin 0.1��3 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 3��5 parts, maltol 0.05��0.1 part, 2-acetyl group pyrazine 0.5��1.0 part, 2, 3, 5-trimethylpyrazine 0.5��1 part, iso-amyl iso-valeriate 1.0��1.5 parts, menthyl acetate 0.1��0.5 part, the oxidation isophorone of mass concentration 1% 0.5��1 part, the damascenone of mass concentration 1% 1.0��2.0 parts, the damascone of mass concentration 1% 0.5��1 part, the Megastigmatrienone of mass concentration 1% 0.5��1 part, the Oleum lavandula angustifolia of mass concentration 1% 1.0��2.0 parts, the coriander seed oil of mass concentration 1% 1.5��2.0 parts, vanilla bean tincture 7.0��8.0 parts, red date tincture 9��11 parts, angelica grosseserrata root tincture 2.0��4.0 parts, propylene glycol 18.0��22.0 parts, ethanol 40.0��45.0 parts.
Further technical scheme is: described flavouring essence for tobacco is at room temperature stirred by the following components with parts by weight and is mixed: cloud and mist absolute oil 2.2 parts, Peru's extractum 0.6 part, ethyl vanillin 0.2 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 4.0 parts, maltol 0.05 part, 2-acetyl group pyrazine 1.0 parts, 2, 3, 5-trimethylpyrazine 0.5 part, iso-amyl iso-valeriate 1.0 parts, menthyl acetate 0.2 part, the oxidation isophorone of mass concentration 1% 0.9 part, the damascenone of mass concentration 1% 1.5 parts, the damascone of mass concentration 1% 0.5 part, the Megastigmatrienone of mass concentration 1% 0.5 part, the Oleum lavandula angustifolia of mass concentration 1% 1.0 parts, the coriander seed oil of mass concentration 1% 1.5 parts, vanilla bean tincture 8.0 parts, red date tincture 10 parts, angelica grosseserrata root tincture 3.0 parts, propylene glycol 20 parts, ethanol 43.35 parts.
Further technical scheme is: the preparation method of described tea training element is:
(1) extract 3 times with the water-bath under temperature 60 C of the alcoholic solution of the concentration 40% of 5��10 times of weight portions after Folium Camelliae sinensis being pulverized, extract 2h, gained extracting solution filtering and concentrating every time, obtain extractum;
(2) described extractum is filtered with hot water dissolving, adsorb through macroporous resin D101, then with pure water, concentration 10% ethanol water, concentration 20% ethanol water, concentration 40% ethanol water gradient elution, collect eluent, with thin layer chromatography or high-efficient liquid phase analysis, by the partial concentration containing target component, it is thus achieved that concentrate;
(3) by the further chromatography of molecular sieve that described concentrate filler is polydextran gel LH20, then with concentration 40% methanol aqueous solution eluting, collect eluent, with thin layer chromatography or high-efficient liquid phase analysis, merge and obtain tea training element. Concentration of alcohol refers to the volume fraction of ethanol.
Green tea has pure and fresh taste, and rich in multiple catechin, vitamin, aminoacid, caffeine etc., tea polyphenols therein is the safe and efficient antioxidant generally acknowledged in the world. And ultrafine green tea powder color is emerald green, exquisite quality, nutritious, it is possible to effectively mix with tobacco juice for electronic smoke and be fully dissolved out effective ingredient. Tea training element is the natural product of a kind of high anti-oxidation activity contained in part Folium Camelliae sinensis, its structure is made up of a gallic acid and quinolinic acid, electronic cigarette liquid can play antioxidation jointly with the dissolved element in green tea, the intermiscibility of tea training element and tobacco juice for electronic smoke is good, the mouthfeel of scalable tobacco juice for electronic smoke, improves the characteristics such as the pleasant impression of tobacco juice for electronic smoke, harmony and concentration.
Compared with prior art, one of beneficial effects of the present invention is: the present invention is absent from high temperature pyrolysis reaction rich in the tobacco juice for electronic smoke of ultrafine green tea powder, therefore releasing content of coke tar is almost nil, obtains while smoking experience meeting consumer, reduce on self, the impact of other people and environment. Simultaneously, ultrafine green tea powder can be directly appended in electronic cigarette liquid without microencapsulation, effective ingredient dissolution rate in ultrafine green tea powder is high, the every Sensory quality index of electronic cigarette liquid can be optimized after in electronic cigarette liquid adding to, improve the color and luster of tobacco juice for electronic smoke, again can fresh breath, tea training element with ultrafine green tea powder jointly plays good antioxidation, add other antioxidants without auxiliary in ree-oil, simplify ree-oil composition.
Detailed description of the invention
In order to make the purpose of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein is only in order to explain the present invention, is not intended to limit the present invention.
Flavouring essence for tobacco is at room temperature stirred by the following components with parts by weight and is mixed: cloud and mist absolute oil 2.2 parts, Peru's extractum 0.6 part, ethyl vanillin 0.2 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 4.0 parts, maltol 0.05 part, 2-acetyl group pyrazine 1.0 parts, 2, 3, 5-trimethylpyrazine 0.5 part, iso-amyl iso-valeriate 1.0 parts, menthyl acetate 0.2 part, the oxidation isophorone of mass concentration 1% 0.9 part, the damascenone of mass concentration 1% 1.5 parts, the damascone of mass concentration 1% 0.5 part, the Megastigmatrienone of mass concentration 1% 0.5 part, the Oleum lavandula angustifolia of mass concentration 1% 1.0 parts, the coriander seed oil of mass concentration 1% 1.5 parts, vanilla bean tincture 8.0 parts, red date tincture 10 parts, angelica grosseserrata root tincture 3.0 parts, propylene glycol 20 parts, ethanol 43.35 parts. this flavouring essence for tobacco is used for following embodiment.
The preparation of tea training element:
(1) extract 3 times with the water-bath under temperature 60 C of the alcoholic solution of 700g concentration 40% after 100g Folium Camelliae sinensis being pulverized, extract 2h, gained extracting solution filtering and concentrating every time, obtain extractum 30g;
(2) described extractum is filtered with hot water dissolving, adsorb through macroporous resin D101, then with pure water, concentration 10% ethanol water, concentration 20% ethanol water, concentration 40% ethanol water gradient elution, collect eluent, with thin layer chromatography or high-efficient liquid phase analysis, by the partial concentration containing target component, it is thus achieved that concentrate 5.5g;
(3) by the further chromatography of molecular sieve that described concentrate filler is polydextran gel LH20, then with concentration 40% methanol aqueous solution eluting, collect eluent, with thin layer chromatography or high-efficient liquid phase analysis, merge and obtain tea training element 0.3g.
Ultrafine green tea powder is commercially available conventional products.
Thickening agent is the commercially available conventional products of Field of Tobacco.
Embodiment 1
By weight, taking propylene glycol 59 parts, glycerol 12 parts, deionized water 9 parts, ultrafine green tea powder 5 parts, tea training element 1 part, flue-cured tobacco extract 6 parts, flavouring essence for tobacco 5 parts, thickening agent 3 parts is configured to train the tobacco juice for electronic smoke of element rich in ultrafine green tea powder and tea.
Comparative example 1
By weight, take propylene glycol 65 parts, glycerol 12 parts, deionized water 9 parts, flue-cured tobacco extract 6 parts, flavouring essence for tobacco 5 parts, thickening agent 3 parts configuration tobacco juice for electronic smoke, this tobacco juice for electronic smoke trains element without ultrafine green tea powder and tea.
Embodiment 2
By weight, taking propylene glycol 59 parts, glycerol 10 parts, deionized water 8 parts, ultrafine green tea powder 8.5 parts, tea training element 1.5 parts, burley tobaccos extract 8 parts, flavouring essence for tobacco 2 parts, thickening agent 3 parts is configured to train the tobacco juice for electronic smoke of element rich in ultrafine green tea powder and tea.
Comparative example 2
By weight, take propylene glycol 66 parts, glycerol 10 parts, deionized water 8 parts, burley tobaccos extract 8 parts, flavouring essence for tobacco 5 parts, thickening agent 3 parts configuration tobacco juice for electronic smoke, this tobacco juice for electronic smoke trains element without ultrafine green tea powder and tea.
Using embodiment 1 and comparative example 1 as one group, embodiment 2 and comparative example 2 are as one group, carry out electronic cigarette sensory evaluating smoking, evaluation methodology imitates big method (CN201310031800.5) with reference to consolidating, the evaluation criteria of indices such as table 1, embodiment 1,2, smoking result such as table 2 of comparative example 1,2:
9 points of point system quantitative descriptions processed of table 1 individual event sensory evaluation index
Note: minimum score standard is 0.5.
Table 2 embodiment and comparative example's sensory evaluating smoking's results contrast
As shown in Table 2, embodiment 1 sensory evaluating smoking must be divided into 51 points, it is better than comparative example 1, wherein embodiment 1 fragrance, harmony, miscellaneous QI, zest, pleasant impression are all better than comparative example 1, especially pleasant impression and harmony, the implication pure and fresh owing to having green tea, pleasant impression improves substantially, owing to tea training element and ultrafine green tea powder combine in tobacco juice for electronic smoke, the harmony of tobacco juice for electronic smoke significantly improves; Embodiment 2 sensory evaluating smoking must be divided into 50.0, is better than comparative example 2, and wherein, embodiment 2 harmony, miscellaneous QI, zest, pleasant impression are better than comparative example 2. Additionally, in outward appearance, the tobacco juice for electronic smoke adding ultrafine green tea powder is green transparent shape, color and luster pleasant excites the desire that consumer sucks.
Although reference be made herein to invention has been described for the multiple explanatory embodiment of the present invention, but, it should be understood that those skilled in the art can be designed that a lot of other amendments and embodiment, these amendments and embodiment will drop within spirit disclosed in the present application and spirit. More specifically, in disclosure and scope of the claims, it is possible to building block and/or layout to theme composite configuration carry out multiple modification and improvement. Except the modification that building block and/or layout are carried out and improvement, to those skilled in the art, other purposes also will be apparent from.
Claims (7)
1. the tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea, it is characterised in that it is made up of following components by weight:
Propylene glycol 50��60 parts, glycerol 10��15 parts, deionized water 7��10 parts, 6��12 parts of the mixture of ultrafine green tea powder and tea training element, tobacco extract 3��10 parts, flavouring essence for tobacco 1��5 part, thickening agent 1��3 part, in the mixture of described ultrafine green tea powder and tea training element, the mass ratio of ultrafine green tea powder and tea training element is 5��8:1, described flavouring essence for tobacco is at room temperature stirred by the following components with parts by weight and is mixed: cloud and mist absolute oil 2��3 parts, Peru's extractum 0.5��1 part, ethyl vanillin 0.1��3 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 3��5 parts, maltol 0.05��0.1 part, 2-acetyl group pyrazine 0.5��1.0 part, 2, 3, 5-trimethylpyrazine 0.5��1 part, iso-amyl iso-valeriate 1.0��1.5 parts, menthyl acetate 0.1��0.5 part, the oxidation isophorone of mass concentration 1% 0.5��1 part, the damascenone of mass concentration 1% 1.0��2.0 parts, the damascone of mass concentration 1% 0.5��1 part, the Megastigmatrienone of mass concentration 1% 0.5��1 part, the Oleum lavandula angustifolia of mass concentration 1% 1.0��2.0 parts, the coriander seed oil of mass concentration 1% 1.5��2.0 parts, vanilla bean tincture 7.0��8.0 parts, red date tincture 9��11 parts, angelica grosseserrata root tincture 2.0��4.0 parts, propylene glycol 18.0��22.0 parts, ethanol 40.0��45.0 parts.
2. the tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea according to claim 1, it is characterised in that it is made up of following components by weight:
Propylene glycol 55��60 parts, glycerol 10��12 parts, deionized water 7��9 parts, 6��10 parts of the mixture of ultrafine green tea powder and tea training element, tobacco extract 4��8 parts, flavouring essence for tobacco 2��5 parts, thickening agent 1��3 part.
3. the tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea according to claim 2, it is characterised in that it is made up of following components by weight:
Propylene glycol 59 parts, glycerol 12 parts, deionized water 9 parts, 6 parts of the mixture of ultrafine green tea powder and tea training element, tobacco extract 6 parts, flavouring essence for tobacco 5 parts, thickening agent 3 parts.
4. the tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea according to claim 2, it is characterised in that it is made up of following components by weight:
Propylene glycol 59 parts, glycerol 10 parts, deionized water 8 parts, 10 parts of the mixture of ultrafine green tea powder and tea training element, tobacco extract 8 parts, flavouring essence for tobacco 2 parts, thickening agent 3 parts.
5. the tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea according to Claims 1 to 4 any one, it is characterised in that described tobacco extract is extract at least one in flue-cured tobacco, dry in the sun cigarette, burley tobaccos, cigar.
6. the tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea according to claim 1 any one, it is characterized in that described flavouring essence for tobacco is at room temperature stirred by the following components with parts by weight to be mixed: cloud and mist absolute oil 2.2 parts, Peru's extractum 0.6 part, ethyl vanillin 0.2 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 4.0 parts, maltol 0.05 part, 2-acetyl group pyrazine 1.0 parts, 2, 3, 5-trimethylpyrazine 0.5 part, iso-amyl iso-valeriate 1.0 parts, menthyl acetate 0.2 part, the oxidation isophorone of mass concentration 1% 0.9 part, the damascenone of mass concentration 1% 1.5 parts, the damascone of mass concentration 1% 0.5 part, the Megastigmatrienone of mass concentration 1% 0.5 part, the Oleum lavandula angustifolia of mass concentration 1% 1.0 parts, the coriander seed oil of mass concentration 1% 1.5 parts, vanilla bean tincture 8.0 parts, red date tincture 10 parts, angelica grosseserrata root tincture 3.0 parts, propylene glycol 20 parts, ethanol 43.35 parts.
7. the tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea according to Claims 1 to 4 any one, it is characterised in that the preparation method of described tea training element is:
(1) extract 3 times with the water-bath under temperature 60 C of the alcoholic solution of the concentration 40% of 5��10 times of weight portions after Folium Camelliae sinensis being pulverized, extract 2h, gained extracting solution filtering and concentrating every time, obtain extractum;
(2) described extractum is filtered with hot water dissolving, adsorb through macroporous resin D101, then with pure water, concentration 10% ethanol water, concentration 20% ethanol water, concentration 40% ethanol water gradient elution, collect eluent, with thin layer chromatography or high-efficient liquid phase analysis, by the partial concentration containing target component, it is thus achieved that concentrate;
(3) by the further chromatography of molecular sieve that described concentrate filler is polydextran gel LH20, then with concentration 40% methanol aqueous solution eluting, collect eluent, with thin layer chromatography or high-efficient liquid phase analysis, merge and obtain tea training element.
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| CN105962426B (en) * | 2016-07-29 | 2019-07-16 | 福建中烟工业有限责任公司 | Composition and tobacco juice for electronic smoke containing extra-strong tea extract |
| CN106617277B (en) * | 2016-12-26 | 2018-07-27 | 颐中（青岛）实业有限公司 | A kind of tea smell electronics tobacco tar and its wet pulverizing preparation method |
| CN113749276B (en) * | 2021-09-11 | 2023-04-25 | 深圳市真味生物科技有限公司 | Electronic atomized liquid capable of refreshing oral cavity and having good smoke quantity |
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