CN106617277A - Method for preparing tea-fragrance electronic cigarette liquid through wet grinding - Google Patents
Method for preparing tea-fragrance electronic cigarette liquid through wet grinding Download PDFInfo
- Publication number
- CN106617277A CN106617277A CN201611216425.1A CN201611216425A CN106617277A CN 106617277 A CN106617277 A CN 106617277A CN 201611216425 A CN201611216425 A CN 201611216425A CN 106617277 A CN106617277 A CN 106617277A
- Authority
- CN
- China
- Prior art keywords
- tea
- oil
- electronic cigarette
- tea smell
- smell
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
- Tea And Coffee (AREA)
Abstract
The invention provides a method for preparing tea-fragrance electronic cigarette liquid through wet grinding. The method comprises the following steps: (1) accurately weighing dry tea leaves with certain weight, carrying out preliminary grinding, carrying out screening by adopting a 5-50-mesh sieve, adding a solvent into the tea leaves after preliminary grinding according to a certain ratio, carrying out uniform mixing, adding the obtained mixture into a high-speed cutting type wet grinder, carrying out grinding under a certain reaction condition, and after grinding, carrying out material discharging, wherein the discharged liquid is base liquid of the tea-fragrance electronic cigarette liquid; and (2) stirring the base liquid of the tea-fragrance electronic cigarette liquid with the weight percentage being 70-100% and essence and flavor with the weight percentage being 0-30% for uniform mixing, thus obtaining the tea-fragrance electronic cigarette liquid. Compared with the prior art, the method for preparing the tea-fragrance electronic cigarette liquid through wet grinding provided by the invention is rapid, simple and convenient, is easy to operate and high in extraction ratio, and is energy-saving and environmentally friendly. The sensory quality of the electronic cigarette liquid prepared by blending the tea-fragrance base liquid prepared by adopting the method provided by the invention is greatly promoted, so that the overly sweet feeling brought to the mouth cavity by the electronic cigarette liquid is effectively reduced, and the symptoms of parching mouth and scorching tongue caused after smoking are alleviated.
Description
Technical field
The present invention relates to electronic cigarette tobacco tar technical field, more particularly to a kind of waterproof pulverization prepares tea smell electronics ree-oil
Method.
Background technology
In recent years, as international Tobacco Control is increasingly serious and consumer health's consciousness is generally lifted, countries in the world are in succession with vertical
Method form limits traditional cigarette sale, and international Medicated cigarette sales volume maintains 3% speed and glides, in this context, domestic and international Nicotiana tabacum L.
Company constantly advances the development of novel tobacco product, wherein, electronic cigarette is obtained as a kind of important form of novel tobacco product
Fast development.Electronic cigarette is a kind of on-fuel cigarette class substituted type product, there is the outward appearance similar to medicated cigarette, ree-oil
(electronic cigarette liquid) produces fog similar to true cigarette flue gas in the presence of electronic smoke atomizer, full
The pleasant sensation and use habit of sufficient consumer, but different from what medicated cigarette had substantially, does not burn, without tar, carbon monoxide
Deng harmful substance.
Folium Camelliae sinensis nature and flavor sweetness and bitterness is talked about in traditional Chinese medical science medical science, is slightly cold nontoxic；Enter cardiopulmonary stomach, disperse fatigue, improving eyesight is thought clearly；It is raw
Tianjin is quenched the thirst, diuresis antidiarrheal；Control cloperastine to breathe heavily, the effect such as heat-clearing and toxic substances removing.And vitamin C is rich in Folium Camelliae sinensis, and under normal circumstances, Folium Camelliae sinensis
In ascorbic leaching rate can reach 80% or so.Consumer usually drinks tea can supplement the vitamin C caused due to smoking
Deficiency, with keep in human body produce and remove free radical dynamic equilibrium, strengthen human body resistivity.Contain in Folium Camelliae sinensis
Tea polyphenols have (1) blood fat reducing, anti-cardiovascular disease, reduce blood glucose, treatment diabetes；(2) excellent radiation-resisting functional；(3)
The big medicinal health care function of anticancer etc. three.Therefore many developers are added to the extract of Folium Camelliae sinensis in electronic cigarette tobacco tar, to reduce
It is aided with lifting electronic cigarette mouthfeel while the harm that smoking is produced to human body.Steamed using water at atmospheric pressure in patent 201410468818.6
Steam distillation method is extracted to Folium Camelliae sinensis, and concrete operations are first to carry out reduced steam distillation to Folium Camelliae sinensis, and reduced steam is steamed
The distillation for evaporating is discarded, and to the vinasse and Folium Camelliae sinensis therein of reduced steam distillation normal pressure steam distillation is carried out again；Specially
The extracting method of Folium Camelliae sinensis extract is to crush Folium Camelliae sinensis in profit 201410626458.8, at a certain temperature, uses 60% ethanol water
Solution extracts tea-leaf power, and lixiviating solution obtains Folium Camelliae sinensis extract Jing after revolving.Above two method has Folium Camelliae sinensis extract to extract
Rate is low, loss of effective components is big, complex operation, response time length, it is relatively costly the shortcomings of, and prepared by traditional method
The inadequate true nature of fragrance that extract is showed in electronic cigarette tobacco tar, itself and aesthetic quality can not very well meet consumer
Requirement.Simultaneously the discomfort phenomenon such as dry mouth and tougue is had after major part consumer suction electronic cigarette, severe patient is even dizzy, evil
The heart, this problem also urgently makes moderate progress solution.
The content of the invention
In order to overcome the deficiencies in the prior art, the invention provides a kind of waterproof pulverization prepares the side of tea smell electronics ree-oil
Method, the preparation method is fast and convenient, extraction ratio and purity high, low cost, and specific preparation method is comprised the following steps：
(1) accurately weigh and be dried Folium Camelliae sinensis 100g, 5～50 eye mesh screens are crossed after just crushing, solubilization in the Folium Camelliae sinensis to after just crushing
Agent, the Folium Camelliae sinensis are 1 with the mass ratio of solvent:5～10, add after mix homogeneously in high-speed cutting type wet process disintegrator, Yu Yi
Determine to be crushed under reaction condition, discharge after crushing, institute's out-feed liquid is tea smell electronic cigarette oil base oil；
(2) by the tea smell electronic cigarette oil base oil that mass percent is 70～100% and mass percent be 0～
30% essence and flavoring agent stirring and evenly mixing, obtains final product tea smell electronics ree-oil.
Preferably, in step (1), certain reaction condition is that the rotating speed of the high-speed cutting type wet process disintegrator is
2500～8000r/min, it is 5～60 DEG C to crush temperature, and grinding time is 0.5～6h.
Preferably, in step (1), the solvent includes following each component, by mass percentage：Glycerol 20～
70%th, Propylene Glycol 20～75%, ethanol 0～12%, surplus is supplied to 100% weight with deionized water.
Preferably, the rotating speed of the high-speed cutting type wet process disintegrator be 2500～6000r/min, crush temperature be 10～
50 DEG C, grinding time is 1～4h.
Preferably, the rotating speed of the high-speed cutting type wet process disintegrator is 2500～4000r/min, specifically for 2500～
3000r/min, 2500～3500r/min, 3000～3500r/min, 3000～4000r/min, 3500～4000r/min,
2500r/min、2800r/min、3000r/min、3200r/min、3500r/min、3800r/min、4000r/min；Crush temperature
Spend for 15～25 DEG C, be specifically 15～20 DEG C, 20～25 DEG C, 15 DEG C, 18 DEG C, 20 DEG C, 22 DEG C, 25 DEG C；Grinding time be 2～
3h is specifically 2～2.5h, 2.5～3h, 2h, 2.5h, 3h.
Preferably, in step (1), the solvent includes following each component, by mass percentage：Glycerol 30～
70%th, Propylene Glycol 20～60%, ethanol 5～10%, surplus is supplied to 100% weight with deionized water.
Preferably, the tea smell electronic cigarette oil base oil also includes the drug extract with promoting the production of body fluid to quench thirst effect, institute
It is 1～5 that drug extract is stated with the mass ratio of Folium Camelliae sinensis:10, it is more highly preferred to, the mass ratio of the drug extract and Chinese herbal medicine
For 2～4:10, such as 2:10、2.5:10、3:10、3.5:10、4:10.
Preferably, the drug extract with promoting the production of body fluid to quench thirst effect is by Fructus Mori, Punica granatum L., Herba mesonae chinensis, Fructus Mume, Fructus Canarii albi, people
One or two mixed extraction in face, fructus hippophae, Jin Bangchui, precipice beggar are obtained.
Preferably, the Folium Camelliae sinensis are the one kind in black tea, green tea, oolong tea, Ramulus et Folium Mussaendae Pubescentis, yellow tea or postfermented tea.
Another object of the present invention is that offer is a kind of prepares tea smell electronics ree-oil according to a kind of above-mentioned waterproof pulverization
Tea smell electronics ree-oil obtained by method preparation.
Compared with prior art, it is a kind of quick that the waterproof pulverization that the present invention is provided prepares the method for tea smell electronics ree-oil
Easy, the energy-efficient new method for preparing tea smell electronics ree-oil, the method possesses advantages below：
(1) easy to operate, speed is fast, the time is short, remain to greatest extent the bioactive ingredients of Folium Camelliae sinensis and fragrance into
Point, be conducive to making high-quality extract；
(2) it is no longer pass through extracting, distills etc. and processing, reduces the loss of effective ingredient in extraction process, especially fragrance
Composition, improves raw material availability；
(3) bulky grain had both strictly been limited, had turn avoid broken, gained Folium Camelliae sinensis micropowder even particle size distribution, very great Cheng
The specific surface area of micropowder is increased on degree, distance of the Folium Camelliae sinensis component content by tea granule internal diffusion to particle surface is shortened,
So as to increase Folium Camelliae sinensis component content leaching rate；
(4) crushed under closed system, both avoided micropowder pollution environment, can prevent the dust in air from polluting again
Product.
Additionally, the electronic cigarette oil smoke oil phase that the tea powder electronics ree-oil prepared using this method is made with Folium Camelliae sinensis extract
Than aesthetic quality has obtained very big lifting, more meets the requirement of consumer, such as overall tea aroma is stronger, oneself
So, fragrance, to smoker fresh and clean pleasurable sensation is brought；And Herba mesonae chinensis, Fructus Mume etc. are equipped with ree-oil base oil have
The composition of promoting the production of body fluid to quench thirst effect, can effectively reduce Propylene Glycol, the sweet sense that glycerol equal solvent brings, and alleviate consumer and aspirated
The symptom of dry mouth and tougue after electronic cigarette.
Specific embodiment
With reference to specific embodiment, the present invention is described further：
Embodiment 1
(1) accurately weigh and be dried black tea 100g, 5～50 eye mesh screens are crossed after just crushing, add in the black tea to after just crushing
500g solvents, the solvent includes following each component, by mass percentage：Glycerol 60%, Propylene Glycol 30%, surplus is going
Ionized water is supplied to 100% weight, adds Fructus Mori, Punica granatum L. mixed extract 20g, adds high-speed cutting type wet after mix homogeneously
In method pulverizer, the rotating speed for controlling high-speed cutting type wet process disintegrator is 5000r/min, and it is 20 DEG C to crush temperature, grinding time
For 1h, discharge after crushing, institute's out-feed liquid is tea smell electronic cigarette oil base oil；
(2) it is 30% essence by the tea smell electronic cigarette oil base oil that mass percent is 70% and mass percent
Spice stirring and evenly mixing, obtains final product tea smell electronics ree-oil.
Embodiment 2
(1) accurately weigh and be dried green tea 100g, 5～50 eye mesh screens are crossed after just crushing, add in the green tea to after just crushing
1000g solvents, the solvent includes following each component, by mass percentage：Glycerol 35%, Propylene Glycol 50%, ethanol
10%, surplus is supplied to 100% weight with deionized water, adds Fructus Mume, Fructus Canarii albi mixed extract 10g, is added after mix homogeneously
In entering high-speed cutting type wet process disintegrator, the rotating speed for controlling high-speed cutting type wet process disintegrator is 2500r/min, crushes temperature and is
25 DEG C, grinding time is 2h, is discharged after crushing, and institute's out-feed liquid is tea smell electronic cigarette oil base oil；
(2) it is 20% essence by the tea smell electronic cigarette oil base oil that mass percent is 80% and mass percent
Spice stirring and evenly mixing, obtains final product tea smell electronics ree-oil.
Embodiment 3
(1) accurately weigh and be dried Ramulus et Folium Mussaendae Pubescentis 100g, 5～50 eye mesh screens are crossed after just crushing, add in the Ramulus et Folium Mussaendae Pubescentis to after just crushing
600g solvents, the solvent includes following each component, by mass percentage：Glycerol 40%, Propylene Glycol 45%, ethanol
12%, surplus is supplied to 100% weight with deionized water, Herba mesonae chinensis, Fructus Dracontomeli Duperreani mixed extract 50g is added, after mix homogeneously
In adding high-speed cutting type wet process disintegrator, the rotating speed for controlling high-speed cutting type wet process disintegrator is 8000r/min, crushes temperature
For 5 DEG C, grinding time is 6h, is discharged after crushing, and institute's out-feed liquid is tea smell electronic cigarette oil base oil；
(2) it is 10% essence by the tea smell electronic cigarette oil base oil that mass percent is 90% and mass percent
Spice stirring and evenly mixing, obtains final product tea smell electronics ree-oil.
Embodiment 4
(1) accurately weigh and be dried postfermented tea 100g, 5～50 eye mesh screens are crossed after just crushing, add in the postfermented tea to after just crushing
800g solvents, the solvent includes following each component, by mass percentage：Glycerol 70%, Propylene Glycol 25%, ethanol 5%,
Fructus hippophae, golden rod hammer mixed extract 30g are added, is added after mix homogeneously in high-speed cutting type wet process disintegrator, control is high
The rotating speed of fast cutting-type wet process disintegrator is 4000r/min, and it is 10 DEG C to crush temperature, and grinding time is 3h, is discharged after crushing, nothing
Essence and flavoring agent, institute's out-feed liquid need to be added to be tea smell electronics ree-oil.
Embodiment 5
(1) accurately weigh and be dried yellow tea 100g, 5～50 eye mesh screens are crossed after just crushing, add in the yellow tea to after just crushing
700g solvents, the solvent includes following each component, by mass percentage：Glycerol 30%, Propylene Glycol 60%, ethanol 8%,
Surplus is supplied to 100% weight with deionized water, adds Jin Bangchui, precipice beggar mixed extract 40g, is added after mix homogeneously
In high-speed cutting type wet process disintegrator, the rotating speed for controlling high-speed cutting type wet process disintegrator is 2500r/min, and it is 50 to crush temperature
DEG C, grinding time is 1.5h, is discharged after crushing, and institute's out-feed liquid is tea smell electronic cigarette oil base oil；
(2) it is 25% essence by the tea smell electronic cigarette oil base oil that mass percent is 75% and mass percent
Spice stirring and evenly mixing, obtains final product tea smell electronics ree-oil.
Embodiment 6
(1) drying oolong 100g is accurately weighed, 5～50 eye mesh screens is crossed after just crushing, added in the black tea to after just crushing
550g solvents, the solvent includes following each component, by mass percentage：Glycerol 20%, Propylene Glycol 75%, surplus is going
Ionized water is supplied to 100% weight, adds Punica granatum L. extract 15g, and high-speed cutting type wet process disintegrator is added after mix homogeneously
In, the rotating speed for controlling high-speed cutting type wet process disintegrator is 4500r/min, and it is 30 DEG C to crush temperature, and grinding time is 2.5h, powder
Discharging after broken, institute's out-feed liquid is tea smell electronic cigarette oil base oil；
(2) it is 15% essence by the tea smell electronic cigarette oil base oil that mass percent is 85% and mass percent
Spice stirring and evenly mixing, obtains final product tea smell electronics ree-oil.
Embodiment 7
(1) accurately weigh and be dried black tea 100g, 5～50 eye mesh screens are crossed after just crushing, add in the black tea to after just crushing
750g solvents, the solvent includes following each component, by mass percentage：Glycerol 60%, Propylene Glycol 20%, ethanol 3%,
Surplus is supplied to 100% weight with deionized water, adds Herba mesonae chinensis, precipice beggar mixed extract 25g, is added after mix homogeneously high
In fast cutting-type wet process disintegrator, the rotating speed for controlling high-speed cutting type wet process disintegrator is 3000r/min, and it is 40 to crush temperature
DEG C, grinding time is 0.5h, is discharged after crushing, and institute's out-feed liquid is tea smell electronic cigarette oil base oil；
(2) it is 5% essence by the tea smell electronic cigarette oil base oil that mass percent is 95% and mass percent
Spice stirring and evenly mixing, obtains final product tea smell electronics ree-oil.
Embodiment 8
(1) accurately weigh and be dried postfermented tea 100g, 5～50 eye mesh screens are crossed after just crushing, add in the black tea to after just crushing
500g solvents, the solvent includes following each component, by mass percentage：Glycerol 50%, Propylene Glycol 40%, ethanol 4%,
Surplus is supplied to 100% weight with deionized water, adds Fructus Mume, Fructus Mori mixed extract 35g, is added at a high speed after mix homogeneously
In cutting-type wet process disintegrator, the rotating speed for controlling high-speed cutting type wet process disintegrator is 6000r/min, and it is 10 DEG C to crush temperature,
Grinding time is 4h, is discharged after crushing, and institute's out-feed liquid is tea smell electronic cigarette oil base oil；
(2) it is 25% essence by the tea smell electronic cigarette oil base oil that mass percent is 75% and mass percent
Spice stirring and evenly mixing, obtains final product tea smell electronics ree-oil.
Comparative example 1
Proportioning according to each component of embodiment 1 is obtained tea smell electronics ree-oil, and simply black tea extract adopts water at atmospheric pressure
Vapor distillation method is extracted, and Fructus Mori, Punica granatum L. mixed extract are added without in base oil.Specifically：Black tea extract 100g, to
500g solvents, the solvent is added to include following each component in black tea extract, by mass percentage：Glycerol 60%, the third two
Alcohol 30%, surplus is supplied to 100% weight with deionized water, and tea smell electronic cigarette oil base oil is after mix homogeneously；By matter
Amount percentage ratio is the 70% tea smell electronic cigarette oil base oil and mass percent is 30% essence and flavoring agent stirring and evenly mixing, i.e.,
Obtain tea smell electronics ree-oil.Comparative example 2
Proportioning according to each component of embodiment 2 is obtained tea smell electronics ree-oil, and simply green tea extract adopts ethanol water
Solution extraction, revolving are extracted, and Fructus Mume, Fructus Canarii albi mixed extract are added without in base oil.Specifically：Green tea extract
100g, adds 1000g solvents, the solvent to include following each component, by mass percentage in green tea extract：Glycerol
35%th, Propylene Glycol 50%, ethanol 10%, surplus is supplied to 100% weight with deionized water, and tea smell electricity is after mix homogeneously
Sub- ree-oil base oil；It is 20% fragrant by the tea smell electronic cigarette oil base oil that mass percent is 80% and mass percent
Smart spice stirring and evenly mixing, obtains final product tea smell electronics ree-oil.
Electronic cigarette tobacco tar in above-described embodiment and comparative example is added in electronic cigarette device and carry out respectively sensory effects
Evaluate.
Sensory effects evaluation methodology is comprised the following steps：
(1) 6 evaluation indexes, including zest, gratification, dry sensation, feature style, aroma quality and fragrance are provided with
Amount, and give different score values to the Different Effects degree of electronic cigarette tobacco tar aesthetic quality according to every evaluation index.
The zest is referred to：The flue gas that suction electronic cigarette tobacco tar Jing atomization is produced includes oral cavity, throat to sensory organ
The discomfort produced with nasal cavity is received.
The gratification is referred to：Flue gas strength, concentration and the note that the atomization of electronic cigarette tobacco tar Jing is produced is on sensory organ
The comprehensive impression of generation.
The dry sensation is referred to：Electronic cigarette tobacco tar Jing atomization produce flue gas Jing suction oral cavity and exhalation after to xerostomia
The impact of degree.
The feature style is referred to：A kind of electronic cigarette tobacco tar is different from the sense of other homogeneous e cigarette ree-oil in pleasant feeling
Official's Main Differences are showed.
The aroma quality is referred to：The good and bad degree of pleasant breath is felt during smokeing panel test by olfactory sensation and the sense of taste.
The perfume quantity is referred to：During smokeing panel test by oral cavity and nasal cavity weigh pleasant breath amount number.
(2) member of smoking of 10 people, everyone a electronic cigarette tobacco tar sensory quality assessment table, using the scoring side secretly commented are set
Formula, using overall method of smokeing panel test is circulated, and electronic cigarette tobacco tar is aspirated, according to 6 sensory quality assessment index score values in table 1
Implication, each project full marks is 9 points, and full marks are 54 points, and projects with 1 point as scoring unit, be shown in by the explanation of each score value meaning
Table 1.
The score value implication table of the electronic cigarette tobacco tar sensory quality assessment index of table 1
| Score value | Zest | Gratification | Dry sensation | Feature style | Aroma quality | Perfume quantity |
| 9 | Nothing | Very well | It is very light | Please very much | Very well | It is very sufficient |
| 8 | Seemingly have | It is good | Gently | Pleasure | It is good | It is sufficient |
| 7 | It is micro- to have | Preferably | It is lighter | Relatively please | Preferably | It is more sufficient |
| 6 | Slightly | It is slightly good | It is still light | Slightly please | It is slightly good | It is slightly sufficient |
| 5 | Have | Typically | In | Typically | Typically | Typically |
| 4 | It is bigger | It is slightly poor | Slightly weigh | Slightly do not please | It is slightly poor | Slightly |
| 3 | It is larger | It is poor | It is heavier | Less please | It is poor | It is micro- to have |
| 2 | Greatly | Difference | Weight | Do not please | Difference | Seemingly have |
| 1 | It is very big | It is very poor | It is very heavy | Do not please very much | It is very poor | Nothing |
(3) result statistics：The smoking result of all members of smoking is effective, and the individual event smoking result of each member of smoking is asked into arithmetic
Meansigma methodss, as a result retain to a decimal, and the arithmetic mean of instantaneous value of each individual event is added and, obtain total score, as a result retain to one
Decimal.
The electronic cigarette tobacco tar prepared in the electronic cigarette tobacco tar prepared in embodiment 1-8 and comparative example 1-2 is added on into electronics
Sensory quality assessment is carried out in cigarette.Concrete evaluation result is shown in Table 2, and the scoring of every evaluation index in table 2 has for 10 members of smoking
The arithmetic average point of effect scoring.
The electronic cigarette tobacco tar sensory effects evaluation result of table 2
As shown in Table 2, compared with two comparative examples, the electronic cigarette tobacco tar total score of the present invention is higher, and advantage is main
It is embodied in：(1) add the aesthetic quality of overall flue gas after Folium Camelliae sinensis extract good, this is because Folium Camelliae sinensis obtained in waterproof pulverization are extracted
Thing remains the effective ingredient of Folium Camelliae sinensis to greatest extent and Folium Camelliae sinensis component content leaching rate is high；(2) after aspirating the ree-oil of the present invention
Dry sensation substantially mitigates, and this is the work that the extracts such as Herba mesonae chinensis, Fructus Mume due to adding in electronic cigarette base oil have promoting the production of body fluid to quench thirst
With.
The above, is only presently preferred embodiments of the present invention, is not the restriction for making other forms to the present invention, is appointed
What those skilled in the art changed possibly also with the technology contents of the disclosure above or be modified as equivalent variations etc.
Effect embodiment.But it is every without departing from technical solution of the present invention content, according to the technical spirit of the present invention to above example institute
Any simple modification, equivalent variations and the remodeling made, still falls within the protection domain of technical solution of the present invention.
Claims (10)
1. a kind of method that waterproof pulverization prepares tea smell electronics ree-oil, it is characterised in that comprise the following steps：
（1）Accurately weigh and be dried the g of Folium Camelliae sinensis 100,5 ~ 50 eye mesh screens are crossed after just crushing, solubilizer in the Folium Camelliae sinensis to after just crushing, institute
It is 1 that Folium Camelliae sinensis are stated with the mass ratio of solvent:5 ~ 10, add after mix homogeneously in high-speed cutting type wet process disintegrator, in certain reaction
Under the conditions of crush, discharge after crushing, institute's out-feed liquid is tea smell electronic cigarette oil base oil；
（2）For 70 ~ 100% tea smell electronic cigarette oil base oil and mass percent it is 0 ~ 30% essence by mass percent
Spice stirring and evenly mixing, obtains final product tea smell electronics ree-oil.
2. the method that a kind of waterproof pulverization as claimed in claim 1 prepares tea smell electronics ree-oil, it is characterised in that in step
（1）In, it is 2500 ~ 8000 r/min that certain reaction condition is the rotating speed of the high-speed cutting type wet process disintegrator, is crushed
Temperature is 5 ~ 60 DEG C, and grinding time is 0.5 ~ 6 h.
3. the method that a kind of waterproof pulverization as claimed in claim 2 prepares tea smell electronics ree-oil, it is characterised in that in step
（1）In, the solvent includes following each component, by mass percentage：Glycerol 20 ~ 70%, Propylene Glycol 20 ~ 75%, ethanol 0 ~
12%, surplus is supplied to 100% weight with deionized water.
4. the method that a kind of waterproof pulverization as claimed in claim 2 prepares tea smell electronics ree-oil, it is characterised in that the height
The rotating speed of fast cutting-type wet process disintegrator is 2500 ~ 6000 r/min, and it is 10 ~ 50 DEG C to crush temperature, and grinding time is 1 ~ 4 h.
5. the method that a kind of waterproof pulverization as claimed in claim 4 prepares tea smell electronics ree-oil, it is characterised in that the height
The rotating speed of fast cutting-type wet process disintegrator is 2500 ~ 4000 r/min, and it is 15 ~ 25 DEG C to crush temperature, and grinding time is 2 ~ 3 h.
6. the method that a kind of waterproof pulverization as claimed in claim 3 prepares tea smell electronics ree-oil, it is characterised in that in step
（1）In, the solvent includes following each component, by mass percentage：Glycerol 30 ~ 70%, Propylene Glycol 20 ~ 60%, ethanol 5 ~
10%, surplus is supplied to 100% weight with deionized water.
7. the method that a kind of waterproof pulverization as claimed in claim 1 prepares tea smell electronics ree-oil, it is characterised in that the tea
Fragrance electronic cigarette oil base oil also includes the matter of the drug extract with promoting the production of body fluid to quench thirst effect, the drug extract and Folium Camelliae sinensis
Amount is than being 1 ~ 5:10.
8. the method that a kind of waterproof pulverization as claimed in claim 7 prepares tea smell electronics ree-oil, it is characterised in that the tool
There is the drug extract of promoting the production of body fluid to quench thirst effect by Fructus Mori, Punica granatum L., Herba mesonae chinensis, Fructus Mume, Fructus Canarii albi, Fructus Dracontomeli Duperreani, fructus hippophae, Jin Bangchui, precipice
One or two mixed extraction in beggar are obtained.
9. the method that a kind of waterproof pulverization as described in claim 1-8 is arbitrary prepares tea smell electronics ree-oil, it is characterised in that
The Folium Camelliae sinensis are the one kind in black tea, green tea, oolong tea, Ramulus et Folium Mussaendae Pubescentis, yellow tea or postfermented tea.
10. prepared by a kind of method for preparing tea smell electronics ree-oil according to a kind of arbitrary described waterproof pulverization of claim 1-8
The tea smell electronics ree-oil of gained.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611216425.1A CN106617277B (en) | 2016-12-26 | 2016-12-26 | A kind of tea smell electronics tobacco tar and its wet pulverizing preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611216425.1A CN106617277B (en) | 2016-12-26 | 2016-12-26 | A kind of tea smell electronics tobacco tar and its wet pulverizing preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106617277A true CN106617277A (en) | 2017-05-10 |
| CN106617277B CN106617277B (en) | 2018-07-27 |
Family
ID=58827924
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611216425.1A Active CN106617277B (en) | 2016-12-26 | 2016-12-26 | A kind of tea smell electronics tobacco tar and its wet pulverizing preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106617277B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109757763A (en) * | 2019-02-01 | 2019-05-17 | 福建绿色黄金生物科技有限公司 | A kind of tabletting method of tealeaves and its preparing the application in tea smoke grenade |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104687239A (en) * | 2015-01-20 | 2015-06-10 | 川渝中烟工业有限责任公司 | Electronic cigarette liquid rich in ultra-micro green tea powder and tea saponin |
| CN105343203A (en) * | 2015-11-04 | 2016-02-24 | 深圳瀚星翔科技有限公司 | Tobacco tar of electronic cigarette and preparation method of tobacco tar |
| CN105559136A (en) * | 2015-12-30 | 2016-05-11 | 立场电子科技发展（上海）有限公司 | Method for preparing electronic cigarette juice fragrance from green tea enzyme |
-
2016
- 2016-12-26 CN CN201611216425.1A patent/CN106617277B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104687239A (en) * | 2015-01-20 | 2015-06-10 | 川渝中烟工业有限责任公司 | Electronic cigarette liquid rich in ultra-micro green tea powder and tea saponin |
| CN105343203A (en) * | 2015-11-04 | 2016-02-24 | 深圳瀚星翔科技有限公司 | Tobacco tar of electronic cigarette and preparation method of tobacco tar |
| CN105559136A (en) * | 2015-12-30 | 2016-05-11 | 立场电子科技发展（上海）有限公司 | Method for preparing electronic cigarette juice fragrance from green tea enzyme |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109757763A (en) * | 2019-02-01 | 2019-05-17 | 福建绿色黄金生物科技有限公司 | A kind of tabletting method of tealeaves and its preparing the application in tea smoke grenade |
| CN109757763B (en) * | 2019-02-01 | 2024-01-23 | 泉州禾知科技有限公司 | Tea tabletting method and application thereof in preparing tea tobacco cartridges |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106617277B (en) | 2018-07-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104397871B (en) | A kind of electronic cigarette tobacco tar containing tea extract and preparation method thereof | |
| CN106174684A (en) | The preparation method of a kind of natural perfume material superfine powder and the application in reconstituted tobacoo thereof | |
| CN103211054B (en) | Tea bag of jasmine white tea and preparation method thereof | |
| CN103989245A (en) | Chinese flue-cured tobacco type electronic cigarette liquid capable of effectively reducing oral cavity sweet greasy feeling | |
| WO2013097164A1 (en) | Alternative cut tobacco composition and preparation method thereof | |
| CN104645204A (en) | Electronic atomized liquid having functions of detoxifying and de-inebriating and preparation method thereof | |
| CN105747267A (en) | Dissolvable smoke-free tobacco product and preparation method thereof | |
| CN103013668A (en) | Tobacco essence extracting solution, extracting method and prepared tobacco essence and tobacco products | |
| CN104544543A (en) | Electronic cigarette smoke solution prepared through black tea leaf extract | |
| CN106262671A (en) | Seasoning sauce and preparation method thereof | |
| CN106723303B (en) | A kind of method that wet pulverizing prepares tobacco flavor electronics tobacco tar | |
| CN106539048A (en) | Edible selenium-rich areca-nut brine and method for preparing areca-nuts by using edible selenium-rich areca-nut brine | |
| CN105747268A (en) | Hard candy type smokeless tobacco product and preparation method thereof | |
| CN109123764A (en) | A kind of preparation method of Bin phenol cigarette | |
| CN106820270A (en) | A kind of electronic cigarette tobacco tar and preparation method thereof | |
| CN106617276B (en) | A kind of method that Chinese herbal medicine electronics tobacco tar and wet pulverizing prepare Chinese herbal medicine electronics tobacco tar | |
| CN106617277A (en) | Method for preparing tea-fragrance electronic cigarette liquid through wet grinding | |
| CN104664588B (en) | Nebulized liquid containing ginseng | |
| CN106867667A (en) | The preparation and its application of a kind of essence spice for cigarette | |
| CN107057856B (en) | Preparation method of liquorice sweetening and moisturizing essence for filter tip | |
| CN104544548A (en) | Electronic cigarette smoke solution prepared through yellow tea leaf extract | |
| CN107746748A (en) | A kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and the application in cigarette | |
| CN108992539A (en) | A kind of Poria cocos tea granule and preparation method thereof | |
| CN105768194A (en) | Fermented buccal tobacco | |
| CN107224005B (en) | One kind drinks formula tobacco product |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |