CN105747268A - Hard candy type smokeless tobacco product and preparation method thereof - Google Patents
Hard candy type smokeless tobacco product and preparation method thereof Download PDFInfo
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Abstract
The invention relates to the field of tobacco preparation, in particular to a hard candy type smokeless tobacco product as well as a preparation method and an application thereof. The hard candy type smokeless tobacco product is prepared from components of raw materials in parts by weight as follows: 0.005-25 parts of tobacco powder and/or tobacco extract, 0-10 parts of a traditional Chinese medicine medicament, 70-99 parts of a sugar-free sweetening agent, 0.05-15 parts of a flavoring agent, 0-2 parts of an acid agent, 0-2 parts of a pH regulating agent, 0-1 part of a freshener, 0-15 parts of a thickening agent, 0-2 parts of an emulsifier, 0-0.5 parts of an edible colorant and 0-1 part of an antioxidant. According to the hard candy type smokeless tobacco product, the sugar-free sweetening agent is taken as a sugar substrate, the sun-dried tobacco produced in Guizhou is taken as a main tobacco raw material, the traditional Chinese medicine medicament and the natural flavoring agent are added, nicotine and other effective ingredients can be stably released, proper physical satisfaction and comfort are supplied to a consumer, no residues are left in an oral cavity after use of the hard candy type smokeless tobacco product, and the hard candy type smokeless tobacco product is a novel complementary substitute product of a traditional cigarette and can be used in public places.
Description
Technical field
The present invention relates to field of tobacco preparation, particularly relate to a kind of hard sugar fruit type smoke-free tobacco product and its production and use.
Background technology
Along with people are to going deep into that relation between smoking and health recognizes, government is increasingly stricter to the management and control of traditional cigarette, in China's " administration of sanitation work at public places regulations detailed rules for the implementation ", and clear stipulaties " no smoking for indoor public places ".Smoke-free tobacco product provides the consumer with on-fuel form and is similar to the physiology gratification sucking traditional cigarette, main implementation includes sucking (does not chew, have residue), containing change (do not chew, without residue), chewing tobacco goods etc., preventing the harm of " second hand smoking ", the one being increasingly becoming traditional cigarette supplements substitute products.
At present, smoke-free tobacco product mainly in Europe, North America etc. area sell with the form of in bulk or packed buccal cigarette.But, domestic consumer there is no the tradition using buccal cigarette, and packed buccal cigarette is directly to use in the oral cavity with the form of Nicotiana tabacum L. granule, and nicotine release instability, zest is relatively big, and comfortableness is poor, and the acceptance level of domestic consumer is low.The type smoke-free tobacco product containing change is to be pressed into definite shape after being mixed with other additives by tobacco material, during use under the effects such as saliva, more smoothly discharge the effective ingredient such as nicotine, fragrance matter, zest is little, easy to use, domestic consumer is acceptant, is a kind of market at home Novel smokeless gas tobacco product of having fine development prospect.
Application number is in the patent " hard sugar containing tobacco component " of 200810049285.2, tobacco extract and flavouring essence for tobacco is added in hard sugar substrate, the preparation hard sugar containing tobacco component.But, in this patent, hard sugar substrate is the saccharide such as Saccharum Sinensis Roxb., glucose, and heat is high, and suffering from the crowds such as diabetes, hypertension, hyperlipidemia, obesity should not use；Smoke-free tobacco product uses in the oral cavity, therefore, directly uses the method for flavouring essence for tobacco still to wait to discuss in smoke-free tobacco product.
Summary of the invention
The shortcoming of prior art in view of the above, it is an object of the invention to provide a kind of hard sugar fruit type smoke-free tobacco product and its production and use, is used for solving the problems of the prior art.
For achieving the above object and other relevant purposes, first aspect present invention provides a kind of hard sugar fruit type smoke-free tobacco product, its raw material by weight, including following component:
Preferably, described hard sugar fruit type smoke-free tobacco product, its raw material by weight, including following component:
Preferably, the nicotine content in described hard sugar fruit type smoke-free tobacco product is 0.002-5mg/g.
Preferably, the described Nicotiana tabacum L. one or more combination in flue-cured tobacco, air-curing of tobacco leaves, suncured tabacco, Turkish tobaccos.
It is furthermore preferred that one or more the combination that described air-curing of tobacco leaves is in burley tobaccos, Maryland, cigar, dark tobacco and other air-curing of tobacco leaves, the suncured tabacco one or more combination in Dark sun-cured and Sun cured tobacco and other suncured tabacco.
It is further preferred that the dry in the sun cigarette that described Nicotiana tabacum L. is Guizhou province, or the combination of this dry in the sun cigarette and other Nicotiana tabacum L.s.
It is furthermore preferred that described Nicotiana tabacum L. is one or more the combination in conventional Nicotiana tabacum L. and ecological organic Nicotiana tabacum L..
Preferably, described Nicotiana tabacum L. through natural fermentation, ageing (in a preferred embodiment, digestion time is a year), take out stalk, cleaning, dehydration after carry out flavouring process.
Flavouring processes and refers to spice liquid immersion or infiltrate tobacco-containing material, or is sprayed onto by spice liquid on tobacco powder or tobacco extract.Spice liquid can pass through the pan-fried water of spice material or flavouring agent is formulated.It is furthermore preferred that tobacco powder is that the granularity obtained after tobacco-containing material pulverizing, screening is more than one or more the combination in the Nicotiana tabacum L. fine powder of 100 orders, micropowder, superfine powder.It is further preferred that the granularity of described tobacco powder is 300-2000 order.
It is furthermore preferred that described tobacco extract is liquid tobacco extract or tobacco extract complex fine powder.
Described tobacco extract refers to that tobacco-containing material is after super-dry, pulverizing, screening, by extracting the tobacco extract obtained.Tobacco extract may also pass through the means such as molecular distillation, lyophilization, spray drying, makes tobacco extract complex fine powder under the effect of excipient.
It is furthermore preferred that one or more the combination that described extracting method is in supercritical extraction, extraction, ultrasound on extracting, microwave auxiliary extraction, Simultaneous distillation-extraction and other extracting method.
Preferably, selected from Fructus chebulae immaturus, Radix Isatidis, Herba Menthae, Pericarpium Citri Reticulatae, Herba Ephedrae, Mel, Folium Eriobotryae, Fructus Citri Sarcodactylis, Fructus Fici, Flos Chrysanthemi, Flos Lonicerae, Radix Platycodonis, Radix Scutellariae, Herba mesonae chinensis, Flos Farfarae, Flos Plumeriae Acutifoliae, Fructus Perillae, Folium Microcoris paniculatae, Spica Prunellae, Radix Glycyrrhizae, Folium Mori, the Rhizoma Pinelliae, Fructus Arctii, Herba Taraxaci, Radix Ophiopogonis, Periostracum Cicadae and other heat clearing away wet one's whistle described Chinese medicine, one or more combination in relieving cough and moistening lung Chinese crude drug.
It is furthermore preferred that described Chinese medicine refers to Chinese drugs powder or Chinese medicinal material extract.
nullPreferably，Described sugar-free sweetener is selected from D-mannital、Maltose alcohol、Lactose、Sorbitol、Erythritol、Xylitol、Isomaltulose、Hydrogenated starch hydrolysate、Dextrinosan、Hydroxyl isomaltulose、Oligomeric galactose、Lactulose、Oligofructose、Raffinose、Soybean oligo saccharide、Oligomeric lactulose、Oligomeric xylose、Inulooligosaccharide、LaspartylLphenylalanine methylester、Sucralose、Sodium cyclamate、Acesulfame potassium、Saccharin sodium、Sucralose、Stevioside、Glycyrrhizin、Fructus Momordicae essence、Radix Glycyrrhizae、Ammonium glycyrrhizinate、Glycyrrhizic acid one potassium and tripotassium、NHDC、Africa arrowroot glucin、Rhizoma Curculiginis sweet protein、Synsepalum duleificum monellin、Potato Radix Stephaniae Tetrandrae glucin、Neotame、LaspartylLphenylalanine methylester acesulfame、L-arabinose、L-aspartoyl-N-(2,2,4,4-tetramethyl-3-thietanyl) one or more combination in-D-aminopropanamide and other food sugar-free sweeteners.
Preferred, described sugar-free sweetener is selected from D-mannital, maltose alcohol, lactose, Sorbitol, erythritol, xylitol, hydroxyl isomaltulose, hydrogenated starch hydrolysate, dextrinosan, isomaltulose, oligomeric galactose, lactulose, oligofructose, Raffinose, soybean oligo saccharide, oligomeric lactulose, oligomeric xylose, inulooligosaccharide, stevioside, glycyrrhizin, Fructus Momordicae essence, Radix Glycyrrhizae, ammonium glycyrrhizinate, glycyrrhizic acid one potassium and tripotassium, NHDC, one or more combination in the sugar-free sweeteners such as Africa arrowroot glucin.
Preferably, the described flavouring agent one or more combination in coffee bean oil., basil oil, Flos Tagetis Erectae oil, Cardamom oil, oleum Citri sinensis, cognac, wintergreen oil, Flos micheliae Albae oil, Flos Chrysanthemi oil, Fructus Citri Limoniae oil, Oleum Citri grandis, Fructus Mume tincture, black tea tincture, green tea tincture, cocoa tincture, hawthorn fruit tincture, red date tincture, Aloe extract, Flos Lonicerae extract, Folium Nelumbinis extract, rum, coffee powder, Fructus Armeniacae Mume powder, red date powder, cocoa powder, green tea powder, concentrated fruit juice and other food flavouring agents；Concentrated fruit juice can be one or more the combination in the concentrated fruit juice of Fructus Mali pumilae, Fructus Pruni, Fructus Musae, blackberry, Fructus Pruni pseudocerasi, Fructus Jujubae, Fructus Fici, Fructus Citri sinensis, Fructus Persicae, pear, Fructus Pruni salicinae, Fructus Armeniacae Mume, Fructus Vitis viniferae, Prunus mume Sieb. Et Zucc. and other fruit.
Preferably, the described acidic flavoring agent one or more combination in citric acid, gluconic acid, L MALIC ACID, lactic acid, tartaric acid and other food acid taste agent.
Preferably, the described pH adjusting agent one or more combination in sodium carbonate, sodium bicarbonate, potassium carbonate, potassium bicarbonate, sodium citrate, potassium citrate, sodium gluconate and other food pH adjusting agents.
Preferably, described freshener is selected from menthol, mentha piperita oil, asia peppermint oil, asia peppermint vegetable oil, penner oil, Natural menthol, N-to one or more the combination in benzene acetonitrile base Herba Menthae alkyl formamides, N-(2-(pyridine-2-base) ethyl) Herba Menthae alkyl formamides, menthalactone and other Folium Menthae extract or derivant etc..
Preferably, described thickening agent is selected from starch, phosphorylation PASELLI EASYGEL, carboxymethyl starch sodium, starch phosphate sodium, maltodextrin, cyclodextrin, microcrystalline Cellulose, sodium carboxymethyl cellulose, hydroxypropyl cellulose, methylcellulose, ethyl cellulose, hydroxypropyl methylcellulose, gelatin, arabic gum, casein, chitin, Chitosan-phospholipid complex, oligochitosan and derivant thereof, sodium alginate, ammonium alginate, propylene glycol alginate, tara gum, mannitol, Sorbitol, lactose, guar gum, pectin, gloiopeltis glue, trigonella bean gum, locust bean gum, Abelmoschus manihot （L.） Medic glue, xanthan gum, Resina persicae, lac, cassia gum, Tragacanth, carrageenan, curdlan, soluble soybean polysaccharide, tamarind seed polysaccharide glue, pulullan polysaccharide, the combination of one or more in Semen Lini glue and other food grade thickener.
Preferably, the described emulsifying agent one or more combination in single, double, triglyceride, lecithin, soybean phospholipid, degreased cocoa powder, acetylation list bis-fatty acid glyceride, polyglyceryl fatty acid ester, Polyethylene Glycol, polyethylene sorbitan ester, poloxamer, sucrose fatty acid ester and other food emulsifying agents.
It is furthermore preferred that described triglyceride refers to decanoyl/octanoyl glycerides and glyceryl triacetate etc..
Preferably, described edible coloring agent is selected from titanium dioxide, erythrosine, light blue, monascus yellow pigment, tea flavochrome, Tea Green Pigment, Ipomoea batatas(L.)Lam, β-apo--8 '-carotenal, copper chlorophyll, indigo, Pasania cuspidata palm fibre, lycopene, mandarin orange is yellow, Semen sojae atricolor is red, black currant is red, safflower yellow, red rice is red, red yeast rice, Rhizoma Curcumae Longae, burnt sugar coloring, Fructus Rosae Laevigatae palm fibre, coreopsis yellow extract, cacao pigment, chilli orange, radish red, peanut-skin red, Herba basellae rubrae is red, Calyx Hibisci Sabdariffae is red, Pericarpium Vitis viniferae is red, Fructus Mori are red, Ziziphi Spinosae color, natural amaranth, alkermes, Fructus Myricae rubrae is red, phylloxanthin, algae is blue, one or more combination in beta-carotene and other edible coloring agents.
Preferably, the described antioxidant combination of one or more in tea polyphenols, Butylated hydroxyanisole, sodium benzoate, dibenzylatiooluene, propylgallate, sorbic acid and potassium salt, dl-alpha-tocopherol, d-alpha-tocopherol, vitamin C, calcium ascorbate, ascorbyl palmitate, D-araboascorbic acid and sodium salt, carnosic acid, Licorice root antioxidant, AOB, Semen Ginkgo extrac, Folium Camelliae sinensis extract and Semen Vitis viniferae extract and other food antioxidants.
The preparation method that second aspect present invention provides a kind of hard sugar fruit type smoke-free tobacco product, comprises the steps:
(1) take suitable quantity of water and heat to boiling, sugar-free sweetener being added in hot water by proportioning and dissolve, filter；
(2) step (1) gained syrup being proceeded to vacuum sugar boiling machine infusion, control steam pressure is 0.5-0.95atm, and sugar cook temperature is 140-210 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%；
(3) step (2) gained syrup is cooled to 100-140 DEG C, add tobacco powder and/or tobacco extract, Chinese medicine, flavouring agent, acidic flavoring agent, pH adjusting agent, freshener, emulsifying agent, thickening agent, edible coloring agent, antioxidant etc. by proportioning, stir；
(4) step (3) gained syrup is injected into mould, mould disks is cooled down rapidly, make syrup solidification sizing, be cooled to demoulding when 30-40 DEG C, coating, packaging hard sugar fruit type smoke-free tobacco product.
Third aspect present invention provides described hard sugar fruit type smoke-free tobacco product and supplements the purposes of succedaneum preparation field Nicotiana tabacum L..
The hard sugar fruit type smoke-free tobacco product of offer of the present invention, food is selected to be permitted spendable sugar-free sweetener as saccharide matrix, calorific value is low, it is difficult to digested, blood glucose fluctuation will not be caused after edible, and have the growth and breeding promoting bacillus bifidus, maintain the microecological balance of intestinal, promote the absorption of nutrition, promote human body intestinal canal to wriggle, improve body metabolism, enhancing immunity, anti-caries etc. and be conducive to the effect of health, suffer from diabetes, hypertension, hyperlipidemia, obesity crowd can also use.The product of the present invention is a kind of smoke-free tobacco product, tobacco material is selected and is produced dry in the sun cigarette based on Guizhou, cigarette is aromatic strongly fragrant, and processed by fragrance-enhancing tobacco, and select the Chinese medicine that wets one's whistle of heat clearing away and food to be permitted spendable natural flavours, when hard sugar fruit type smoke-free tobacco product slowly dissolves, Stable Release nicotine and other fragrance matters are supplied to the suitable physiology gratification of consumer and comfort.The product of the present invention is a kind of Novel smokeless gas tobacco product that can use in public places.
Accompanying drawing explanation
Fig. 1 show present invention process flow chart
Detailed description of the invention
It is an object of the invention to provide the supplementary substitute products of a kind of traditional cigarette, i.e. a kind of hard sugar fruit type smoke-free tobacco product.Inventor utilizes Guizhou to produce the aromatic flavor of dry in the sun cigarette, jealous plentiful, feature that strength is sufficient, and process tobacco material by fragrance-enhancing tobacco, add sugar-free sweetener, Chinese medicine, natural flavours etc. further, thus providing the Novel smokeless gas tobacco product of a kind of comfortable taste, safety and environmental protection, complete the present invention on this basis.
The present invention provides a kind of hard sugar fruit type smoke-free tobacco product, its raw material by weight, including following component:
Preferably, the nicotine content in described hard sugar fruit type smoke-free tobacco product is 0.002-5mg/g.
Preferably, in described tobacco powder or tobacco extract, the Nicotiana tabacum L. one or more combination in flue-cured tobacco, air-curing of tobacco leaves, suncured tabacco, Turkish tobaccos.Specifically prepared by positions such as the leaf of Nicotiana tabacum L., flower, stem, seeds.
It is furthermore preferred that one or more the combination that described air-curing of tobacco leaves is in burley tobaccos, Maryland, cigar, dark tobacco etc., the suncured tabacco one or more combination in Dark sun-cured and Sun cured tobacco etc..
It is furthermore preferred that described Nicotiana tabacum L. is selected from the dry in the sun cigarette of Guizhou province, or the combination of this dry in the sun cigarette and other Nicotiana tabacum L.s, in compositions, percentage by weight >=30% of this dry in the sun cigarette.
It is furthermore preferred that described Nicotiana tabacum L. can be conventional Nicotiana tabacum L., it is also possible to be ecological organic Nicotiana tabacum L., or the combination of ecological organic Nicotiana tabacum L. and conventional Nicotiana tabacum L..
Preferably, described Nicotiana tabacum L. through natural fermentation, ageing (in a preferred embodiment, digestion time is a year), take out stalk, cleaning, dehydration after carry out flavouring process.
Flavouring processes and refers to the Nicotiana tabacum L. soaked with spice liquid or before infiltration powdered, or is sprayed onto by spice liquid on tobacco powder or tobacco extract complex.Spice liquid can pass through the pan-fried water of spice material or flavouring agent is formulated, and concrete selectable spice material or flavouring agent include but not limited to one or more the combination in Radix Glycyrrhizae, Flos Lonicerae, Flos Chrysanthemi, Fructus Mume tincture, hawthorn fruit tincture, tobacco extract etc..
It is furthermore preferred that can add adhesive agent in described spice liquid, to improve flavouring effect, concrete alternative adhesive agent includes but not limited to one or more the combination in Sorbitol, poloxamer, beta-schardinger dextrin-, arabic gum, gelatin etc..
Described tobacco powder is that tobacco-containing material forms coarse powder through super-dry, grinding and sieving net, utilizes Ultra-Micro Grinding Equipment to form tobacco powder after coarse powder pulverizing, excessively screen cloth.Described hard sugar fruit type smoke-free tobacco product by weight, including 0.005-10 part tobacco powder, it is preferable that include 0.5-3 part tobacco powder.
It is furthermore preferred that described tobacco powder is that the granularity obtained after Nicotiana tabacum L. pulverizing, screening is more than the combination of one or more in the Nicotiana tabacum L. fine powder of 100 orders, micropowder, superfine powder.
It is further preferred that the granularity of described tobacco powder is 300-2000 order.
In a preferred embodiment, described tobacco powder be Nicotiana tabacum L. through super-dry, pulverize after cross 80 eye mesh screens and form coarse powder, utilize the tobacco powder that Ultra-Micro Grinding Equipment is formed after crossing 300 eye mesh screens after being pulverized by coarse powder.
It is furthermore preferred that described tobacco extract is liquid tobacco extract or tobacco extract complex fine powder.
Described tobacco extract refers to that Nicotiana tabacum L. is after super-dry, pulverizing, screening, by extracting the tobacco extract obtained, one or more the combination in supercritical extraction, extraction, ultrasound on extracting, microwave auxiliary extraction, Simultaneous distillation-extraction etc. of the described extracting method.
In a preferred embodiment, described tobacco extract complex fine powder is that tobacco extract is through the means such as molecular distillation, lyophilization, spray drying, the tobacco extract complex fine powder made under the effect of excipient.Described hard sugar fruit type smoke-free tobacco product by weight, including 0.005-25 part tobacco extract complex fine powder, it is preferable that include 0.8-10 part tobacco extract complex fine powder, more preferably 3.5-5.5 part.Wherein, tobacco extract accounts for 0.05-2 part, it is preferred that ratio is 0.06-0.8 part.
In hard sugar fruit type smoke-free tobacco product provided by the present invention, described Chinese medicine can use various have heat clearing away wet one's whistle, the Chinese crude drug of relieving cough and moistening lung effect and combination.Concrete available Chinese medicine includes but not limited to one or more the combination in Fructus chebulae immaturus, Radix Isatidis, Herba Menthae, Pericarpium Citri Reticulatae, Herba Ephedrae, Mel, Folium Eriobotryae, Fructus Citri Sarcodactylis, Fructus Fici, Flos Chrysanthemi, Flos Lonicerae, Radix Platycodonis, Radix Scutellariae, Herba mesonae chinensis, Flos Farfarae, Flos Plumeriae Acutifoliae, Fructus Perillae, Folium Microcoris paniculatae, Spica Prunellae, Radix Glycyrrhizae, Folium Mori, the Rhizoma Pinelliae, Fructus Arctii, Herba Taraxaci, Radix Ophiopogonis, Periostracum Cicadae etc..Described Chinese medicine refers to Chinese drugs powder or Chinese medicinal material extract.Described hard sugar fruit type smoke-free tobacco product by weight, including 0-10 part Chinese medicine, it is preferable that include 0.5-5 part Chinese medicine.
In hard sugar fruit type smoke-free tobacco product provided by the present invention, described sugar-free sweetener can use is permitted spendable sugar-free sweetener in various food, as long as not producing to limit to the goal of the invention of the present invention.nullConcrete available sugar-free sweetener includes but not limited to D-mannital、Maltose alcohol、Lactose、Sorbitol、Erythritol、Xylitol、Isomaltulose、Hydrogenated starch hydrolysate、Dextrinosan、Hydroxyl isomaltulose、Oligomeric galactose、Lactulose、Oligofructose、Raffinose、Soybean oligo saccharide、Oligomeric lactulose、Oligomeric xylose、Inulooligosaccharide、LaspartylLphenylalanine methylester、Sucralose、Sodium cyclamate、Acesulfame potassium、Saccharin sodium、Sucralose、Stevioside、Glycyrrhizin、Fructus Momordicae essence、Radix Glycyrrhizae、Ammonium glycyrrhizinate、Glycyrrhizic acid one potassium and tripotassium、NHDC、Africa arrowroot glucin、Rhizoma Curculiginis sweet protein、Synsepalum duleificum monellin、Potato Radix Stephaniae Tetrandrae glucin、Neotame、LaspartylLphenylalanine methylester acesulfame、L-arabinose、L-aspartoyl-N-(2,2,4,4-tetramethyl-3-thietanyl) one or more combination in-D-aminopropanamide etc..Preferred, described sugar-free sweetener includes but not limited to D-mannital, maltose alcohol, lactose, Sorbitol, erythritol, xylitol, isomaltulose, hydrogenated starch hydrolysate, dextrinosan, hydroxyl isomaltulose, oligomeric galactose, lactulose, oligofructose, Raffinose, soybean oligo saccharide, oligomeric lactulose, oligomeric xylose, inulooligosaccharide, stevioside, glycyrrhizin, Fructus Momordicae essence, Radix Glycyrrhizae, ammonium glycyrrhizinate, glycyrrhizic acid one potassium and tripotassium, NHDC, one or more combination in the sugar-free sweeteners such as Africa arrowroot glucin.Described hard sugar fruit type smoke-free tobacco product by weight, including 70-99 part sugar-free sweetener, it is preferable that include 80-96 part sugar-free sweetener.
In hard sugar fruit type smoke-free tobacco product provided by the present invention, described flavouring agent can use is permitted spendable spice in various food, as long as not producing to limit to the goal of the invention of the present invention.Concrete spendable flavouring agent includes but not limited to one or more the combination in coffee bean oil., basil oil, Flos Tagetis Erectae oil, Cardamom oil, oleum Citri sinensis, cognac, wintergreen oil, Flos micheliae Albae oil, Flos Chrysanthemi oil, Fructus Citri Limoniae oil, Oleum Citri grandis, Fructus Mume tincture, black tea tincture, green tea tincture, cocoa tincture, hawthorn fruit tincture, red date tincture, Aloe extract, Flos Lonicerae extract, Folium Nelumbinis extract, rum, coffee powder, Fructus Armeniacae Mume powder, red date powder, cocoa powder, green tea powder, concentrated fruit juice etc.；Concentrated fruit juice can be one or more the combination in the concentrated fruit juice of the fruit such as Fructus Mali pumilae, Fructus Pruni, Fructus Musae, blackberry, Fructus Pruni pseudocerasi, Fructus Jujubae, Fructus Fici, Fructus Citri sinensis, Fructus Persicae, pear, Fructus Pruni salicinae, Fructus Armeniacae Mume, Fructus Vitis viniferae, Prunus mume Sieb. Et Zucc..Described hard sugar fruit type smoke-free tobacco product by weight, including 0.5-15 part flavouring agent, it is preferable that include 1-8 part flavouring agent.
In hard sugar fruit type smoke-free tobacco product provided by the present invention, described acidic flavoring agent can use is permitted spendable acidic flavoring agent in various food, as long as not producing to limit to the goal of the invention of the present invention.Concrete spendable acidic flavoring agent includes but not limited to one or more the combination in citric acid, gluconic acid, L MALIC ACID, lactic acid, tartaric acid etc..Described hard sugar fruit type smoke-free tobacco product by weight, including 0-2 part acidic flavoring agent.
In hard sugar fruit type smoke-free tobacco product provided by the present invention, described pH adjusting agent can use is permitted spendable pH adjusting agent in various food, as long as not producing to limit to the goal of the invention of the present invention.Concrete available pH adjusting agent includes but not limited to one or more the combination in sodium carbonate, sodium bicarbonate, potassium carbonate, potassium bicarbonate, sodium citrate, potassium citrate, sodium gluconate etc..Described hard sugar fruit type smoke-free tobacco product by weight, including 0-2 part pH adjusting agent.
In hard sugar fruit type smoke-free tobacco product provided by the present invention, described freshener can use is permitted spendable freshener in various food, as long as not producing to limit to the goal of the invention of the present invention.Concrete spendable freshener includes but not limited to that menthol, mentha piperita oil, asia peppermint oil, asia peppermint vegetable oil, penner oil, Natural menthol, N-are to one or more the combination in Folium Menthae extract or the derivants etc. such as benzene acetonitrile base Herba Menthae alkyl formamides, N-(2-(pyridine-2-base) ethyl) Herba Menthae alkyl formamides, menthalactone.Described hard sugar fruit type smoke-free tobacco product by weight, including 0-1 part freshener.
In hard sugar fruit type smoke-free tobacco product provided by the present invention, described thickening agent can use is permitted spendable thickening agent in various food, as long as not producing to limit to the goal of the invention of the present invention.Concrete spendable thickening agent includes but not limited to starch, phosphorylation PASELLI EASYGEL, carboxymethyl starch sodium, starch phosphate sodium, maltodextrin, cyclodextrin, microcrystalline Cellulose, sodium carboxymethyl cellulose, hydroxypropyl cellulose, methylcellulose, ethyl cellulose, hydroxypropyl methylcellulose, gelatin, arabic gum, casein, chitin, Chitosan-phospholipid complex, oligochitosan and derivant thereof, sodium alginate, ammonium alginate, propylene glycol alginate, tara gum, mannitol, Sorbitol, lactose, guar gum, pectin, gloiopeltis glue, trigonella bean gum, locust bean gum, Abelmoschus manihot （L.） Medic glue, xanthan gum, Resina persicae, lac, cassia gum, Tragacanth, carrageenan, curdlan, soluble soybean polysaccharide, tamarind seed polysaccharide glue, pulullan polysaccharide, the combination of one or more in Semen Lini glue etc..It is furthermore preferred that spendable thickening agent includes but not limited to one or more the combination in maltodextrin, cyclodextrin, gelatin, arabic gum, sodium alginate, ammonium alginate, mannitol, Sorbitol, lactose, xanthan gum, Resina persicae, lac, cassia gum, Tragacanth, carrageenan, soluble soybean polysaccharide, pulullan polysaccharide.Described hard sugar fruit type smoke-free tobacco product by weight, including 0-15 part thickening agent, it is preferable that include 3-11 part thickening agent.
In hard sugar fruit type smoke-free tobacco product provided by the present invention, described emulsifying agent can use is permitted spendable emulsifying agent in various food, as long as not producing to limit to the goal of the invention of the present invention.Concrete spendable emulsifying agent includes but not limited to one or more the combination in single, double, triglyceride, lecithin, soybean phospholipid, degreased cocoa powder, acetylation list bis-fatty acid glyceride, polyglyceryl fatty acid ester, Polyethylene Glycol, polyethylene sorbitan ester, poloxamer, sucrose fatty acid ester etc..It is furthermore preferred that described triglyceride refers to decanoyl/octanoyl glycerides and glyceryl triacetate etc..Described hard sugar fruit type smoke-free tobacco product by weight, including 0-2 part emulsifying agent.
In hard sugar fruit type smoke-free tobacco product provided by the present invention, described edible coloring agent can use is permitted spendable edible coloring agent in various food, as long as not producing to limit to the goal of the invention of the present invention.Concrete spendable edible coloring agent includes but not limited to titanium dioxide, erythrosine, light blue, monascus yellow pigment, tea flavochrome, Tea Green Pigment, Ipomoea batatas(L.)Lam, β-apo--8 '-carotenal, copper chlorophyll, indigo, Pasania cuspidata palm fibre, lycopene, mandarin orange is yellow, Semen sojae atricolor is red, black currant is red, safflower yellow, red rice is red, red yeast rice, Rhizoma Curcumae Longae, burnt sugar coloring, Fructus Rosae Laevigatae palm fibre, coreopsis yellow extract, cacao pigment, chilli orange, radish red, peanut-skin red, Herba basellae rubrae is red, Calyx Hibisci Sabdariffae is red, Pericarpium Vitis viniferae is red, Fructus Mori are red, Ziziphi Spinosae color, natural amaranth, alkermes, Fructus Myricae rubrae is red, phylloxanthin, algae is blue, one or more combination in beta-carotene etc..Described hard sugar fruit type smoke-free tobacco product by weight, including 0-0.5 part edible coloring agent, it is preferable that include 0.01-0.05 part edible coloring agent.
In hard sugar fruit type smoke-free tobacco product provided by the present invention, described antioxidant can use is permitted spendable antioxidant in various food, as long as not producing to limit to the goal of the invention of the present invention.Concrete spendable antioxidant includes but not limited to the combination of one or more in tea polyphenols, Butylated hydroxyanisole, sodium benzoate, dibenzylatiooluene, propylgallate, sorbic acid and potassium salt, dl-alpha-tocopherol, d-alpha-tocopherol, vitamin C, calcium ascorbate, ascorbyl palmitate, D-araboascorbic acid and sodium salt, carnosic acid, Licorice root antioxidant, AOB, Semen Ginkgo extrac, Folium Camelliae sinensis extract and Semen Vitis viniferae extract etc..Described hard sugar fruit type smoke-free tobacco product by weight, including 0-1 part antioxidant, it is preferable that include 0.005-0.1 part antioxidant.
The preparation method that the present invention also provides for a kind of hard sugar fruit type smoke-free tobacco product, comprises the steps:
(1) in sugar dissolving kettle, add suitable quantity of water and heat to boiling, sugar-free sweetener added in hot water by proportioning dissolve, filtration；
(2) step (1) gained syrup being proceeded to vacuum sugar boiling machine infusion, control steam pressure is 0.5-0.95atm, and sugar cook temperature is 140-210 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%；
(3) step (2) gained syrup is cooled to 100-140 DEG C, add tobacco powder and/or tobacco extract complex fine powder, Chinese medicine, flavouring agent, acidic flavoring agent, freshener, emulsifying agent, thickening agent, edible coloring agent, antioxidant etc. by proportioning, stir；
(4) step (3) gained syrup is injected into mould, mould disks is cooled down rapidly, make syrup solidification sizing, be cooled to demoulding when 30-40 DEG C, coating, packaging hard sugar fruit type smoke-free tobacco product.
The shape of hard sugar fruit type smoke-free tobacco product can be spherical, elliposoidal, taper, cylinder, prismatic, regular polygon shape, platform turriform, capsule shape, the shape such as leaf, flower-shape, fruit shape, product surface can carry out characters cut in intaglio or characters cut in relief embossing, such as enterprise name, enterprise mark, letter, leaves, flower, fruit etc..
Present invention also offers described hard sugar fruit type smoke-free tobacco product and supplement the purposes of succedaneum preparation field Nicotiana tabacum L..
Hard sugar fruit type smoke-free tobacco product provided by the present invention is the supplementary substitute products of a kind of novel traditional cigarette that can use in public places.Described hard sugar fruit type smoke-free tobacco product can, as a kind of non-staple food, occur slowly to dissolve in the oral cavity, and Stable Release nicotine and other fragrance matters are supplied to the suitable physiology gratification of consumer and comfort；Hard boiled candy base is sugar-free sweetener, will not cause blood glucose fluctuation, also has anti-caries simultaneously, regulates the effects such as digestive function.The product of the present invention is smoke-free tobacco product, it is possible to use in public places；Tobacco material adopts cigarette aromatic strongly fragrant, it is main that dry in the sun cigarette is produced in the Guizhou of comfortable taste, and processed by fragrance-enhancing tobacco, flavouring agent selects food to be permitted spendable natural flavor material, and with the addition of the Chinese medicine that heat clearing away wets one's whistle, therefore, this product is the Novel smokeless gas tobacco product of a kind of comfortable taste, safety and environmental protection.
Below by way of specific instantiation, embodiments of the present invention being described, those skilled in the art the content disclosed by this specification can understand other advantages and effect of the present invention easily.The present invention can also be carried out by additionally different detailed description of the invention or apply, and the every details in this specification based on different viewpoints and application, can also carry out various modification or change under the spirit without departing from the present invention.
It should be clear that the not concrete process equipment indicated or device all adopt the conventional equipment in this area or device in the following example；All force value and scope are all referring to absolute pressure.
Can also there is additive method step before and after described combination step in addition, it is to be understood that the one or more method steps mentioned in the present invention do not repel or additive method step can also be inserted between these steps specifically mentioned, except as otherwise noted；Will also be understood that, combination annexation between the one or more equipment/devices mentioned in the present invention is not repelled and can also be there are other equipment/devices before and after described unit equipment/device or can also insert other equipment/devices between these two equipment/devices specifically mentioned, except as otherwise noted.And, except as otherwise noted, the numbering of various method steps is only the convenient tool differentiating various method steps, but not for limiting the ordering of various method steps or limiting the enforceable scope of the present invention, the change of its relativeness or adjustment, when changing technology contents without essence, when being also considered as the enforceable category of the present invention.
Embodiment 1:
Weight ratio shared by each component is as follows: dry in the sun cigarette (originate from Guizhou, lower with) 0.83 part, Chinese medicine 3 parts, hydroxyl isomaltulose 72 parts (sugar-free sweetener), dextrinosan 21 parts (sugar-free sweetener), stevioside 0.15 part (sugar-free sweetener), Prunus mume Sieb. Et Zucc. extract 1.5 parts (flavouring agent), citric acid 1 part (acidic flavoring agent), 0.5 part of lecithin (emulsifying agent), Fructus Rosae Laevigatae palm fibre 0.01 part of (edible coloring agent), potassium sorbate 0.01 part (antioxidant).Wherein, the weight ratio of each component of Chinese medicine formula is as follows: Folium Microcoris paniculatae 19.6 parts, Herba mesonae chinensis 19.6 parts, Flos Plumeriae Acutifoliae 19.6 parts, Flos Chrysanthemi 13.7 parts, Flos Lonicerae 11.8 parts, Spica Prunellae 11.8 parts, 3.9 parts of Radix Glycyrrhizae.
Preparation process is as follows:
A, fragrance-enhancing tobacco: by dry in the sun cigarette natural fermentation, ageing 1 year, carry out taking out stalk, cleaning, processed.According to Radix Glycyrrhizae: after the mixing of the ratio of water=1:10, under fluidized state fried 1 hour, cooling, after filtration, adding weight ratio in filtrate was that 5% sorbitol syrup is configured to spice liquid, is infiltrated 24-72 hour by dry in the sun cigarette with spice liquid, carries out flavouring process.
B, prepare tobacco powder: dry in the sun cigarette carries out flash baking to moisture less than 3wt% at 120-140 DEG C after taking out.Dried tobacco-containing material is pulverized, crosses 80 mesh sieves and obtain Nicotiana tabacum L. coarse powder.Then carry out secondary micronizing, sieve and obtain order granularity more than 300 order dry in the sun tobacco powder ends.
C, prepare Chinese medicine: weigh Chinese crude drug by formula, after drying, pulverize and obtain Chinese crude drug granule.According to Chinese crude drug: the ratio of water=1:10-20, being soaked 30 minutes by Chinese crude drug granule, then fried 30 minutes, the secondary that adds water was fried, and filtration, concentration obtain Chinese crude drug water decoction.
D, change sugar: add enough water in jacketed pan, heating, to seething with excitement, weighs hydroxyl isomaltulose, dextrinosan by formula, adds in hot water and fully dissolves, and 80 eye mesh screens proceed to holding vessel and store after filtering.
E, sugar cook: the syrup changed proceeds to vacuum sugar boiling machine infusion, and control steam pressure is 0.85-0.9atm, and sugar cook temperature is 160-175 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%.
F, the syrup that is in harmonious proportion: the syrup concentrated is cooled to 130-140 DEG C, adds dry in the sun tobacco powder end, Chinese medicine, stevioside, Prunus mume Sieb. Et Zucc. extract, citric acid, lecithin, Fructus Rosae Laevigatae palm fibre, potassium sorbate etc., stir to mix homogeneously.
G, moulding by casting: the syrup being in harmonious proportion quantitatively is injected into mould, cool down rapidly whole mould disks, makes syrup solidification sizing.Be cooled to demoulding when 30-40 DEG C, utilize hydroxyl isomaltulose to carry out coating, packaging hard sugar fruit type smoke-free tobacco product.The specification of hard sugar fruit type smoke-free tobacco product is every 3.0 ± 0.1g, shape can be spherical, elliposoidal, taper, cylinder, prismatic, regular polygon shape, platform turriform, capsule shape, the shape such as leaf, flower-shape, fruit shape, product surface can carry out characters cut in intaglio or characters cut in relief embossing, such as enterprise name, enterprise mark, letter, leaves, flower, fruit etc..
Embodiment 2:
Weight ratio shared by each component is as follows: 0.59 part of 1.18 parts of flue-cured tobacco powder, dry in the sun tobacco powder end, maltose alcohol 25 parts (sugar-free sweetener), hydroxyl isomaltulose 25 parts (sugar-free sweetener), xylitol 30 parts (sugar-free sweetener), green tea powder 7 parts (flavouring agent), sodium carbonate 1 part (pH adjusting agent), 10 parts of gelatin (thickening agent), menthol 0.18 part (freshener), sodium D-isoascorbate 0.05 part (antioxidant).
Preparation process is as follows:
A, fragrance-enhancing tobacco: by dry in the sun cigarette natural fermentation, ageing 1 year, carry out taking out stalk, cleaning, processed, and flue-cured tobacco carries out baking, ageing 1 year, carries out taking out stalk, cleaning, processed.According to Flos Jasmini Sambac: Flos Lonicerae: Flos Chrysanthemi: the ratio of water=2:5:3:100 at 80-90 DEG C fried 0.5-2 hour, after filtration, filtrate adds the poloxamer that weight ratio is 5% and is configured to spice liquid.According to flue-cured tobacco: the ratio of dry in the sun cigarette=2:1 is mixed and joined, immerse in spice liquid, soak 24-48 hour at 30-60 DEG C, carry out flavouring process.
B, prepare tobacco powder: from spice liquid, take out tobacco-containing material, rotating cage elimination moisture, dry to moisture less than 3wt% at 50-60 DEG C.Dried tobacco-containing material is pulverized, crosses 80 mesh sieves and obtain Nicotiana tabacum L. coarse powder.Then carrying out secondary micronizing, sieve the tobacco powder obtaining order granularity more than 400 orders.The order granularity green tea powder more than 400 orders is prepared in the same manner after tea-drying.
C, change sugar: add enough water in jacketed pan, heating, to seething with excitement, weighs maltose alcohol, hydroxyl isomaltulose by formula, adds in hot water and fully dissolves, and 80 eye mesh screens proceed to holding vessel and store after filtering.
D, sugar cook: the syrup changed proceeds to vacuum sugar boiling machine infusion, and control steam pressure is 0.85-0.9atm, and sugar cook temperature is 150-160 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%.
E, the syrup that is in harmonious proportion: the syrup concentrated is cooled to 120-130 DEG C, adds xylitol, tobacco powder, green tea powder, gelatin, menthol, sodium carbonate, sodium D-isoascorbate etc., stir to mix homogeneously.
F, moulding by casting: the syrup being in harmonious proportion quantitatively is injected into mould, cool down rapidly whole mould disks, makes syrup solidification sizing.Be cooled to demoulding when 30-40 DEG C, utilize hydroxyl isomaltulose to carry out coating, packaging hard sugar fruit type smoke-free tobacco product.The specification of hard sugar fruit type smoke-free tobacco product is every 3.0 ± 0.1g, shape can be spherical, elliposoidal, taper, cylinder, prismatic, regular polygon shape, platform turriform, capsule shape, the shape such as leaf, flower-shape, fruit shape, product surface can carry out characters cut in intaglio or characters cut in relief embossing, such as enterprise name, enterprise mark, letter, leaves, flower, fruit etc..
Embodiment 3:
Weight ratio shared by each component is as follows: 0.8 part of dry in the sun tobacco powder end, 0.2 part of Turkish tobaccos powder, Chinese medicine 4 parts, D-mannital 15 parts (sugar-free sweetener), oligomeric xylose 25 parts (sugar-free sweetener), lactose 33 parts (sugar-free sweetener), soybean oligo saccharide 13 parts (sugar-free sweetener), ammonium glycyrrhizinate 0.2 part (sugar-free sweetener), oleum Citri sinensis 0.76 part (flavouring agent), Fructus Vitis viniferae concentrated juice 4 parts (flavouring agent), AJC 3 parts (flavouring agent), soybean phospholipid 1 part (emulsifying agent), black currant red 0.03 part (edible coloring agent), carnosic acid 0.01 part (antioxidant).Wherein, the weight ratio of each component of Chinese medicine formula is as follows: Radix Isatidis 28.6 parts, Flos Lonicerae 22.8 parts, Spica Prunellae 14.3 parts, Flos Chrysanthemi 14.3 parts, Herba mesonae chinensis 14.3 parts, 5.7 parts of Radix Glycyrrhizae.
Preparation process is as follows:
A, preparing tobacco powder: by dry in the sun cigarette natural fermentation, ageing 1 year, carry out taking out stalk, cleaning, processed, then heat treatment 1 hour in 80-90 DEG C of water, after taking-up, rotating cage elimination moisture, dries at 40-60 DEG C.According to dry in the sun cigarette: the weight ratio mixing of Turkish tobaccos=4:1, pulverizing, cross 80 mesh sieves and obtain Nicotiana tabacum L. coarse powder.Then carrying out secondary micronizing, sieve the tobacco powder obtaining order granularity more than 500 orders.
B, fragrance-enhancing tobacco: by weight ratio be 1% Fructus Mume tincture, 1% hawthorn fruit tincture, 5% beta-schardinger dextrin-disperse in ethanol, strong stirring, mix homogeneously make spice liquid, are uniformly sprayed in tobacco powder, are as the criterion not lump, and namely obtain flavouring tobacco powder after balance.
Prepared by c, Chinese crude drug agent: weigh Chinese crude drug by formula, and after drying, pulverizing, screening obtain 400-500 order Chinese drugs powder.
D, change sugar: enough water in jacketed pan, heating, to boiling, weighs D-mannital, oligomeric xylose, lactose by formula, fully dissolves in addition hot water, and 80 eye mesh screens proceed to holding vessel and store after filtering.
E, sugar cook: the syrup changed proceeds to vacuum sugar boiling machine infusion, and control steam pressure is 0.6-0.8atm, and sugar cook temperature is 170-200 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%.
F, the syrup that is in harmonious proportion: the syrup concentrated is cooled to 130-140 DEG C, add tobacco powder, Chinese medicine, soybean oligo saccharide, ammonium glycyrrhizinate, oleum Citri sinensis, Fructus Vitis viniferae concentrated juice, AJC, soybean phospholipid, red, the carnosic acid of black currant etc., stirring to mix homogeneously, dehydration to moisture less than 2wt%.
G, moulding by casting: the syrup being in harmonious proportion quantitatively is injected into mould, cool down rapidly whole mould disks, makes syrup solidification sizing.Be cooled to demoulding when 30-40 DEG C, utilize D-mannital to carry out coating, packaging hard sugar fruit type smoke-free tobacco product.The specification of hard sugar fruit type smoke-free tobacco product is every 5.0 ± 0.1g, shape can be spherical, elliposoidal, taper, cylinder, prismatic, regular polygon shape, platform turriform, capsule shape, the shape such as leaf, flower-shape, fruit shape, product surface can carry out characters cut in intaglio or characters cut in relief embossing, such as enterprise name, enterprise mark, letter, leaves, flower, fruit etc..
Embodiment 4:
Weight ratio shared by each component is as follows: tobacco extract complex fine powder 3.5 parts, inulooligosaccharide 49.85 parts (sugar-free sweetener), oligofructose 30 parts (sugar-free sweetener), hydrogenated starch hydrolysate 10 parts (sugar-free sweetener), Momordia grosvenori aglycone 0.15 part (sugar-free sweetener), cocoa tincture 1 part (flavouring agent), cocoa powder 2 parts (flavouring agent), arabic gum 3 parts (thickening agent), glyceryl triacetate 0.495 part (emulsifying agent), AOB 0.005 part (antioxidant).
Preparation process is as follows:
A, prepare tobacco extract: by dry in the sun cigarette natural fermentation, ageing 1 year, flue-cured tobacco baking, ageing 1 year, carry out taking out stalk, cleaning, processed.Then heat treatment 1 hour in 85 DEG C of water by flue-cured tobacco and dry in the sun cigarette, after taking-up, rotating cage elimination moisture, dries at 40-60 DEG C.Turkish tobaccos are dried at 40-60 DEG C.According to there being flue-cured tobacco: dry in the sun cigarette: the weight ratio mixing of Turkish tobaccos=5:3:2, pulverizing, solvent extraction method is utilized to prepare tobacco extract.
B, prepare tobacco extract complex: according to tobacco extract: beta-schardinger dextrin-: gelatin: the weight ratio of arabic gum=1:3:1:1 weighs each component, dispersion is in deionized water, strong stirring is emulsion uniformly, and spray drying forms tobacco extract complex fine powder.
C, change sugar: add suitable quantity of water in jacketed pan, heating, to seething with excitement, weighs inulooligosaccharide, oligofructose, hydrogenated starch hydrolysate by formula, adds in hot water and fully dissolves, and 80 eye mesh screens proceed to holding vessel and store after filtering.
D, sugar cook: the syrup changed proceeds to vacuum sugar boiling machine infusion, and control steam pressure is 0.6-0.8atm, and sugar cook temperature is 170-200 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%.
E, the syrup that is in harmonious proportion: the syrup concentrated is cooled to 140-160 DEG C, adds tobacco extract complex fine powder, Momordia grosvenori aglycone, cocoa tincture, glyceryl triacetate, cocoa powder, arabic gum, AOB etc., stir to mix homogeneously.
F, moulding by casting: the syrup being in harmonious proportion quantitatively is injected into mould, cool down rapidly whole mould disks, makes syrup solidification sizing.Be cooled to demoulding when 30-40 DEG C, utilize erythritol etc. to carry out coating, packaging hard sugar fruit type smoke-free tobacco product.The specification of hard sugar fruit type smoke-free tobacco product is every 5.0 ± 0.1g, shape can be spherical, elliposoidal, taper, cylinder, prismatic, regular polygon shape, platform turriform, capsule shape, the shape such as leaf, flower-shape, fruit shape, product surface can carry out characters cut in intaglio or characters cut in relief embossing, such as enterprise name, enterprise mark, letter, leaves, flower, fruit etc..
Embodiment 5:
Weight ratio shared by each component is as follows: tobacco extract complex fine powder 5.3 parts, oligomeric galactose 30 parts (sugar-free sweetener), xylitol 50 parts (sugar-free sweetener), lactulose 8 parts (sugar-free sweetener), cognac 1 part (flavouring agent), rum 4.7 parts (flavouring agent), decanoyl/octanoyl glycerides 1 part (emulsifying agent).
Preparation process is as follows:
A, prepare tobacco extract: by dry in the sun cigarette natural fermentation, ageing 1 year, flue-cured tobacco baking, ageing 1 year, carry out taking out stalk, cleaning, processed, dry at 40-60 DEG C.Turkish tobaccos are dried at 40-60 DEG C.According to flue-cured tobacco: dry in the sun cigarette: the weight ratio mixing of Turkish tobaccos=5:3:2, pulverizing, supercritical extraction is utilized to prepare tobacco extract.
B, preparing tobacco extract complex: according to tobacco extract: xanthan gum: the weight ratio of using carboxyl chitosan=1:2:2 weighs each component, in deionized water, strong stirring is emulsion uniformly in dispersion, and spray drying forms tobacco extract complex fine powder.
C, change sugar: add suitable quantity of water in jacketed pan, heating, to seething with excitement, weighs oligomeric galactose, lactulose by formula, adds in hot water and fully dissolves, and 80 eye mesh screens proceed to holding vessel and store after filtering.
D, sugar cook: the syrup changed proceeds to vacuum sugar boiling machine infusion, and control steam pressure is 0.85-0.9atm, and sugar cook temperature is 150-170 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%.
E, the syrup that is in harmonious proportion: the syrup concentrated is cooled to 110-130 DEG C, adds tobacco extract complex fine powder, xylitol, cognac, rum, decanoyl/octanoyl glycerides etc., stir to mix homogeneously.
F, moulding by casting: the syrup being in harmonious proportion quantitatively is injected into mould, cool down rapidly whole mould disks, makes syrup solidification sizing.Be cooled to demoulding when 30-40 DEG C, utilize hydroxypropyl cellulose etc. to carry out coating, packaging hard sugar fruit type smoke-free tobacco product.The specification of hard sugar fruit type smoke-free tobacco product is every 5.0 ± 0.1g, shape can be spherical, elliposoidal, taper, cylinder, prismatic, regular polygon shape, platform turriform, capsule shape, the shape such as leaf, flower-shape, fruit shape, product surface can carry out characters cut in intaglio or characters cut in relief embossing, such as enterprise name, enterprise mark, letter, leaves, flower, fruit etc..
Comparative example:
By flue-cured tobacco natural fermentation, ageing 1 year, carry out taking out stalk, cleaning, processed.Dry to moisture less than 3wt% at 120-140 DEG C.Being pulverized by dried tobacco-containing material, screening obtains the order granularity flue-cured tobacco powder more than 300 orders.Other preparation processes, technological parameter, formula composition is identical with embodiment 1, the kind of tobacco powder is only changed to flue-cured tobacco, and does not carry out flavouring process, and the weight portion of dextrinosan is changed to 24 parts, is not added with Chinese medicine in comparative example.
Hard sugar fruit type smoke-free tobacco product prepared by embodiment 1-5 and comparative example is carried out sensory evaluation test, each metrics evaluation grade is divided into 6 grades, respectively 0 point=be almost not felt by, 1 point=very low, 2 points=relatively low, 3 points=general, 4 points=stronger, 5 points=very strong, minimum score unit is 0.5 point.After entrance mouthfeel refers to that hard sugar fruit type smoke-free tobacco product puts into oral cavity, the initial synthetic impression of user.Physiological strength refers in use, the physiology gratification that user is experienced, i.e. strength.Balsamic refers in use, the amount of the flavouring agent that user is experienced and matter.Nicotiana tabacum L. perfume (or spice) refers in use, amount that Nicotiana tabacum L. that user is experienced is fragrant and matter.Excitement refers in use, and the zest impressions such as pungent, uncomfortable are experienced at the position such as user oral cavity, throat, esophagus.Comfort refers in use, the experienced smell coordination of user, comfortableness, without the impression of the fragrance such as residue foreign body sensation.Release uniformity refers in use, the release stability in time such as the experienced fragrance of user, physiological strength.Release persistency refers in use, the persistent period length such as the experienced fragrance of user, physiological strength.Oral cavity pleasant impression refers to after use procedure, the taste perception that user oral cavity is remaining.Excitement is more strong, and score is more low；Oral cavity pleasant impression impression is more good, and score is more high；Sundry item is to experience more strong, and score is more high；Final score is added by the arithmetic of each subitem score and is obtained.Concrete outcome is as shown in table 1:
The nicotine burst size of table 1 hard sugar fruit type smoke-free tobacco product and sensory evaluation index comparing result
From table 1, producing hard sugar fruit type smoke-free tobacco product prepared by dry in the sun cigarette based on Guizhou and have that comfortable taste, zest be little, the feature of good after-taste, aggregative indicator evaluation is better than based on the hard sugar fruit type smoke-free tobacco product prepared by conventional flue-cured tobacco.
In sum, the present invention effectively overcomes various shortcoming of the prior art and has high industrial utilization.
Above-described embodiment is illustrative principles of the invention and effect thereof only, not for the restriction present invention.Above-described embodiment all under the spirit and category of the present invention, can be modified or change by any those skilled in the art.Therefore, art has usually intellectual such as modifying without departing from all equivalences completed under disclosed spirit and technological thought or change, must be contained by the claim of the present invention.
Claims (16)
1. a hard sugar fruit type smoke-free tobacco product, its raw material by weight, including following component:
2. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 1, it is characterised in that the nicotine content in described hard sugar fruit type smoke-free tobacco product is 0.002-5mg/g.
3. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 1, it is characterised in that the described Nicotiana tabacum L. one or more combination in flue-cured tobacco, air-curing of tobacco leaves, suncured tabacco, Turkish tobaccos.
4. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 3, it is characterized in that, the air-curing of tobacco leaves one or more combination in burley tobaccos, Maryland, cigar, dark tobacco, the suncured tabacco one or more combination in Dark sun-cured and Sun cured tobacco.
5. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 4, it is characterised in that described Nicotiana tabacum L. is the dry in the sun cigarette of Guizhou province, or the combination of this dry in the sun cigarette and other Nicotiana tabacum L.s.
6. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 1, it is characterised in that described Nicotiana tabacum L. is one or more the combination in conventional Nicotiana tabacum L. and ecological organic Nicotiana tabacum L..
7. hard sugar fruit type smoke-free tobacco product as claimed in claim 1 a kind of, it is characterised in that described Nicotiana tabacum L. through natural fermentation, ageing, take out stalk, cleaning, dehydration after carry out flavouring process.
8. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 7, it is characterised in that described flavouring processes and refers to spice liquid immersion or infiltrate tobacco-containing material, or is sprayed onto by spice liquid on tobacco powder or tobacco extract.
9. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 1, it is characterised in that described tobacco powder is that Nicotiana tabacum L. is pulverized, sieves the granularity obtained more than one or more the combination in the Nicotiana tabacum L. fine powder of 100 orders, micropowder, superfine powder.
10. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 1, it is characterised in that described tobacco extract is liquid tobacco extract or tobacco extract complex fine powder.
11. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 1, it is characterized in that, one or more the combination in Fructus chebulae immaturus, Radix Isatidis, Herba Menthae, Pericarpium Citri Reticulatae, Herba Ephedrae, Mel, Folium Eriobotryae, Fructus Citri Sarcodactylis, Fructus Fici, Flos Chrysanthemi, Flos Lonicerae, Radix Platycodonis, Radix Scutellariae, Herba mesonae chinensis, Flos Farfarae, Flos Plumeriae Acutifoliae, Fructus Perillae, Folium Microcoris paniculatae, Spica Prunellae, Radix Glycyrrhizae, Folium Mori, the Rhizoma Pinelliae, Fructus Arctii, Herba Taraxaci, Radix Ophiopogonis, Periostracum Cicadae of the described Chinese medicine.
null12. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 1，It is characterized in that，Described sugar-free sweetener is selected from D-mannital、Maltose alcohol、Lactose、Sorbitol、Erythritol、Xylitol、Isomaltulose、Hydrogenated starch hydrolysate、Dextrinosan、Hydroxyl isomaltulose、Oligomeric galactose、Lactulose、Oligofructose、Raffinose、Soybean oligo saccharide、Oligomeric lactulose、Oligomeric xylose、Inulooligosaccharide、LaspartylLphenylalanine methylester、Sucralose、Sodium cyclamate、Acesulfame potassium、Saccharin sodium、Sucralose、Stevioside、Glycyrrhizin、Fructus Momordicae essence、Radix Glycyrrhizae、Ammonium glycyrrhizinate、Glycyrrhizic acid one potassium and tripotassium、NHDC、Africa arrowroot glucin、Rhizoma Curculiginis sweet protein、Synsepalum duleificum monellin、Potato Radix Stephaniae Tetrandrae glucin、Neotame、LaspartylLphenylalanine methylester acesulfame、L-arabinose、L-aspartoyl-N-(2,2,4,4-tetramethyl-3-thietanyl) one or more combination in-D-aminopropanamide，Described flavouring agent is selected from coffee bean oil.、Basil oil、Flos Tagetis Erectae oil、Cardamom oil、Oleum Citri sinensis、Cognac、Wintergreen oil、Flos micheliae Albae oil、Flos Chrysanthemi oil、Fructus Citri Limoniae oil、Oleum Citri grandis、Fructus Mume tincture、Black tea tincture、Green tea tincture、Cocoa tincture、Hawthorn fruit tincture、Red date tincture、Aloe extract、Flos Lonicerae extract、Folium Nelumbinis extract、Rum、Coffee powder、Fructus Armeniacae Mume powder、Red date powder、Cocoa powder、Green tea powder、One or more combination in concentrated fruit juice；Concentrated fruit juice is one or more the combination in the fruit such as Fructus Mali pumilae, Fructus Pruni, Fructus Musae, blackberry, Fructus Pruni pseudocerasi, Fructus Jujubae, Fructus Fici, Fructus Citri sinensis, Fructus Persicae, pear, Fructus Pruni salicinae, Fructus Armeniacae Mume, Fructus Vitis viniferae, Prunus mume Sieb. Et Zucc..
13. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 1, it is characterized in that, one or more the combination in citric acid, gluconic acid, L MALIC ACID, lactic acid, tartaric acid of the described acidic flavoring agent, described freshener is selected from menthol, mentha piperita oil, asia peppermint oil, asia peppermint vegetable oil, penner oil, Natural menthol, N-to one or more the combination in benzene acetonitrile base Herba Menthae alkyl formamides, N-(2-(pyridine-2-base) ethyl) Herba Menthae alkyl formamides, menthalactone.
null14. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 1，It is characterized in that，Described thickening agent is selected from starch、Phosphorylation PASELLI EASYGEL、Carboxymethyl starch sodium、Starch phosphate sodium、Maltodextrin、Cyclodextrin、Microcrystalline Cellulose、Sodium carboxymethyl cellulose、Hydroxypropyl cellulose、Methylcellulose、Ethyl cellulose、Hydroxypropyl methylcellulose、Gelatin、Arabic gum、Casein、Chitin、Chitosan-phospholipid complex、Oligochitosan and derivant thereof、Sodium alginate、Ammonium alginate、Propylene glycol alginate、Tara gum、Mannitol、Sorbitol、Lactose、Guar gum、Pectin、Gloiopeltis glue、Trigonella bean gum、Locust bean gum、Abelmoschus manihot （L.） Medic glue、Xanthan gum、Resina persicae、Lac、Cassia gum、Tragacanth、Carrageenan、Curdlan、Soluble soybean polysaccharide、Tamarind seed polysaccharide glue、Pulullan polysaccharide、The combination of one or more in Semen Lini glue，Described emulsifying agent is selected from single、Double; two、Triglyceride、Lecithin、Soybean phospholipid、Degreased cocoa powder、Acetylation list bis-fatty acid glyceride、Polyglyceryl fatty acid ester、Polyethylene Glycol、Polyethylene sorbitan ester、Poloxamer、One or more combination in sucrose fatty acid ester.
null15. a kind of hard sugar fruit type smoke-free tobacco product as claimed in claim 1，It is characterized in that，Described pH adjusting agent is selected from sodium carbonate、Sodium bicarbonate、Potassium carbonate、Potassium bicarbonate、Sodium citrate、Potassium citrate、One or more combination in sodium gluconate，Described edible coloring agent is selected from titanium dioxide、Erythrosine、Light blue、Monascus yellow pigment、Tea flavochrome、Tea Green Pigment、Ipomoea batatas(L.)Lam、β-apo--8 '-carotenal、Copper chlorophyll、Indigo、Pasania cuspidata palm fibre、Lycopene、Mandarin orange is yellow、Semen sojae atricolor is red、Black currant is red、Safflower yellow、Red rice is red、Red yeast rice、Rhizoma Curcumae Longae、Burnt sugar coloring、Fructus Rosae Laevigatae palm fibre、Coreopsis yellow extract、Cacao pigment、Chilli orange、Radish red、Peanut-skin red、Herba basellae rubrae is red、Calyx Hibisci Sabdariffae is red、Pericarpium Vitis viniferae is red、Fructus Mori are red、Ziziphi Spinosae color、Natural amaranth、Alkermes、Fructus Myricae rubrae is red、Phylloxanthin、Algae is blue、One or more combination in beta-carotene，Described antioxidant is selected from tea polyphenols、Butylated hydroxyanisole、Sodium benzoate、Dibenzylatiooluene、Propylgallate、Sorbic acid and potassium salt thereof、Dl-alpha-tocopherol、D-alpha-tocopherol、Vitamin C、Calcium ascorbate、Ascorbyl palmitate、D-araboascorbic acid and sodium salt thereof、Carnosic acid、Licorice root antioxidant、AOB、Semen Ginkgo extrac、The combination of one or more in Folium Camelliae sinensis extract and Semen Vitis viniferae extract.
16. the hard sugar fruit type smoke-free tobacco product as described in claim 1-15 any claim supplements the purposes of succedaneum preparation field Nicotiana tabacum L..
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| CN108739975A (en) * | 2018-06-08 | 2018-11-06 | 四川理工学院 | A kind of natural and preparation method thereof for Saute beef with cayenne pepper |
| CN109393547A (en) * | 2017-08-16 | 2019-03-01 | 上海晶橡商务咨询有限公司 | A kind of Jasmine cigar and preparation method thereof |
| CN109619252A (en) * | 2018-10-25 | 2019-04-16 | 上海兰明食品科技有限公司 | A kind of clearing lung-heat, the function candy for adsorbing nicotine |
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| CN108739975A (en) * | 2018-06-08 | 2018-11-06 | 四川理工学院 | A kind of natural and preparation method thereof for Saute beef with cayenne pepper |
| CN109619252A (en) * | 2018-10-25 | 2019-04-16 | 上海兰明食品科技有限公司 | A kind of clearing lung-heat, the function candy for adsorbing nicotine |
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Application publication date: 20160713 |