CN103013668A - Tobacco essence extracting solution, extracting method and prepared tobacco essence and tobacco products - Google Patents
Tobacco essence extracting solution, extracting method and prepared tobacco essence and tobacco products Download PDFInfo
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- CN103013668A CN103013668A CN2012105591297A CN201210559129A CN103013668A CN 103013668 A CN103013668 A CN 103013668A CN 2012105591297 A CN2012105591297 A CN 2012105591297A CN 201210559129 A CN201210559129 A CN 201210559129A CN 103013668 A CN103013668 A CN 103013668A
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Abstract
The invention relates to the field of tobacco industries, in particular to a tobacco essence extracting solution, an extracting method and prepared tobacco essence and tobacco products. The extracting solution contains C2-3 alcohol, ester, malic acid and water. The aroma of the tobacco essence prepared by the extracting method provided by the invention is elegant and lingering, which is of harmony with the aroma of tobaccos, so that the tobacco products are endowed with a unique aroma style characteristic. The cigarette containing aquilaria agallocha tobacco flavor and provided by the invention is elegant, sweet, lasting and lingering in aroma, and is very popular among the masses.
Description
Technical field
The present invention relates to the tobacco industry field, particularly a kind of flavouring essence for tobacco extracting solution, extracting method, make flavouring essence for tobacco and tobacco product.
Background technology
Agalloch eaglewood, for agalloch eaglewood Aquilaria agallocha (Lour.) Roxb of dicotyledons medicine thymelaeceae magaphanerophytes or Lignum Aquilariae Resinatum A.sinensis (Lour.) Gilg are being subject to natural injury, (such as thunderbolt, windbreak is damaged by worms etc.) or be subject to after the artificial destruction infection that in the process of self-regeneration oozy grease is subject to fungi and condense and form.
The agalloch eaglewood resource is rare, the effect is extensive, with a long history, as famous and precious medicinal material, the relevant record being arranged in the classic of TCM: claim in the essentials of Matea Medica its " and can descend gas to fall sputum, can fall and also can rise, fragrance enters spleen, in transferring, its look is deceived Gu can manage all gas.The body sun, admittedly enter the right arm gate of vitality, warm essence is supporing yang, promoting the circulation of qi is not felt frustrated, and does not help fire in the temperature "; " large bright book on Chinese herbal medicine " calls it " tonifying the five internal organs in the accent, beneficial able-bodied sun, warm waist knee, ending tendon transfer vomiting and diarrhoea cold air "; The Compendium of Material Medica meaning can " control heat in the upper and cold in the lower, the circulation of vital energy in the wrong direction be breathed heavily urgency, and asthenia of the large intestine closes, and urine gas drenches man's cold sperm ".In a word, agalloch eaglewood is the purging medicine of fragrant stomach invigorating, main hot loose dredging, and in warm stomach qi-activating drug, effect is showing.Control and contrary breathe heavily effectively especially, for retention of urine, the depressed stomach colic of nervosa etc. are all effective.But the most important thing is centre of equilibrium nerve, calm mood, all gas of reason and in transferring, help promoting the circulation of qi to enter fixed.
Ligaloes tea is to win post-treatment by the leaf of rare Chinese medicine agalloch eaglewood to be made, by the made Ligaloes tea of eaglewood leaf, through evidence, identical with the medicines and health protection effect of Chinese medicine agalloch eaglewood, and absorb the property of medicine of agalloch eaglewood uniqueness by the method for drinking tea, in the middle of the reward tea that the delicate health-care effect agalloch eaglewood is dissolved in life is siped tea, the ultimate attainment way to keep in good health especially.Ligaloes tea energy stool, dissipate-swelling gas, the venting grease helps sleep, and skin maintenance more can be locked essence gate, and controlling nocturnal emission with astringent drugs closes, and nourishes kidney water, the shady essence of establishing-Yang.For the busy battle-weary people of modern life work, after the free time, drink one cup of Ligaloes tea, can feel that immediately knowledge is clear and bright, energetic, the long-term drinking body-building of more nourishing heart.
Elite in the agalloch eaglewood can be distilled and be refined into " heavy oil ", also is called to be coated with perfume (or spice), can directly use for Buddhist, or be applied in the musical instruments used in a Buddhist or Taoist mass beads to reach the purpose of maintenance, also can smear in the people's that practices Buddhism or Taoism body, washs god's hand to circumcise.Sample pure and fresh uniqueness, the effect of tool health care is that kind of perfume (or spice) is altered the medicine of calming the nerves, and fragrance sinks and coagulates, prolonged not loose, invigorating can fall young flat liver, transfer spleen lung, sharp chest stomach, more can wash body for the people that practices Buddhism or Taoism and only read, can keep away again all evil relieving palpitations refreshing, purposes such as ventilation arteries and veins etc., outer without the disturbing of all heresies, only read at a stalemate.
Except being applied to above-mentioned field, agalloch eaglewood also can be used for smoked combustion, and fragrance is elegant, has promoting the circulation of QI to relieve pain, warming middle-JIAO to arrest vomiting, the effect of helping inspiration to relieve asthma.Smoked combustion agalloch eaglewood, incense drug gas fills the air, and can purify air, the fragrance dehumidifying, and the taste agalloch eaglewood is calmed the nerves, with all worries set aside, gives free and natural and gentle enjoyment, the taste boundary of life is purified and distils, and can help to improve the sleep quality.But the utensil that needs in traditional stacte process is more, and process is loaded down with trivial details.
Summary of the invention
In view of this, the invention provides a kind of flavouring essence for tobacco extracting solution, extracting method, make flavouring essence for tobacco and tobacco product.This extracting solution comprises C
2-3Alcohol, ester, oxysuccinic acid and water.The fragrance of the flavouring essence for tobacco that extracting method provided by the invention makes and tobacco aroma harmony, graceful and long, can give the aromatic style feature of tobacco product uniqueness.
In order to realize the foregoing invention purpose, the invention provides following technical scheme:
The invention provides a kind of extracting solution of flavouring essence for tobacco, comprise C
2-3Alcohol, ester, oxysuccinic acid and water.
As preferably, C in the extracting solution of flavouring essence for tobacco provided by the invention
2-3The mass ratio of alcohol, ester, oxysuccinic acid and water be 65～90:35～50:0.05～0.2:4.95～6.
As preferably, C in the extracting solution of flavouring essence for tobacco provided by the invention
2-3Alcohol be ethanol or propylene glycol.
As preferably, ester is glyceryl ester in the extracting solution of flavouring essence for tobacco provided by the invention.
As preferably, glyceryl ester is vanay in the extracting solution of flavouring essence for tobacco provided by the invention.
The present invention also provides a kind of said extracted liquid to be used for extracting the application of agalloch eaglewood flavouring essence for tobacco; This extracting solution comprises C
2-3Alcohol, ester, oxysuccinic acid and water.As preferably, C
2-3Alcohol be ethanol or propylene glycol.As preferably, ester is glyceryl ester.As preferably, glyceryl ester is vanay.
The present invention also provides a kind of method of extracting the agalloch eaglewood flavouring essence for tobacco, gets agalloch eaglewood and obtains after crushed eaglewood powder, extract to obtain the agalloch eaglewood extracting solution after mixing with extracting solution provided by the invention, again behind vacuum filtration, ethanol constant volume and get final product; Extracting solution provided by the invention comprises C
2-3Alcohol, ester, oxysuccinic acid and water.As preferably, C in the extracting solution of flavouring essence for tobacco provided by the invention
2-3The mass ratio of alcohol, ester, oxysuccinic acid and water be 65～90:35～50:0.05～0.2:4.95～6.As preferably, C
2-3Alcohol be ethanol or propylene glycol.As preferably, ester is glyceryl ester.As preferably, glyceryl ester is vanay.
As preferably, the mass ratio that extracts the extracting solution of eaglewood powder and flavouring essence for tobacco provided by the invention in the method for agalloch eaglewood flavouring essence for tobacco is 1:(5～15).
As preferably, be extracted as supersound extraction, the frequency of supersound extraction is 40～80KHz, the temperature of supersound extraction is 35～45 ℃.
As preferably, the number of times of extraction is at least 3 times.
Preferably, the number of times of extraction is at least 4 times.
As preferably, the vacuum tightness of vacuum filtration is 0.07MPa.
As preferably, in the ethanol constant volume, the mass ratio of eaglewood powder and ethanol is 1: 10～14.
The agalloch eaglewood flavouring essence for tobacco that the present invention also provides the method for said extracted agalloch eaglewood flavouring essence for tobacco to prepare; The method is got agalloch eaglewood and is obtained after crushed eaglewood powder, extract to obtain the agalloch eaglewood extracting solution after mixing with extracting solution provided by the invention, again behind vacuum filtration, ethanol constant volume and get final product; Extracting solution provided by the invention comprises C
2-3Alcohol, ester, oxysuccinic acid and water.As preferably, C
2-3Alcohol be ethanol or propylene glycol.As preferably, ester is glyceryl ester.As preferably, glyceryl ester is vanay.
The present invention also provides a kind of cigarette, comprises the agalloch eaglewood flavouring essence for tobacco that the method for extraction agalloch eaglewood flavouring essence for tobacco provided by the invention prepares.
The invention provides a kind of flavouring essence for tobacco extracting solution, extracting method, make flavouring essence for tobacco and tobacco product.This extracting solution comprises C
2-3Alcohol, ester, oxysuccinic acid and water.The fragrance of the flavouring essence for tobacco that extracting method provided by the invention makes and tobacco aroma harmony, graceful and long, can give the aromatic style feature of tobacco product uniqueness.The cigarette that contains the agalloch eaglewood flavouring essence for tobacco provided by the invention, fragrance is graceful, sweet note, and fragrance is lasting and long, deeply is subjected to broad masses of the people's welcome.
Embodiment
The invention discloses a kind of flavouring essence for tobacco extracting solution, extracting method, make flavouring essence for tobacco and tobacco product, those skilled in the art can use for reference this paper content, suitably improve processing parameter and realize.Special needs to be pointed out is, all similarly replace and change apparent to those skilled in the art, and they all are deemed to be included in the present invention.Method of the present invention and application are described by preferred embodiment, the related personnel obviously can change or suitably change and combination methods and applications as herein described within not breaking away from content of the present invention, spirit and scope, realizes and use the technology of the present invention.
Flavouring essence for tobacco extracting solution provided by the invention, extracting method, make raw materials used in flavouring essence for tobacco and the tobacco product and reagent all can be buied by market.
Below in conjunction with embodiment, further set forth the present invention:
The preparation of embodiment 1 agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood and make the agalloch eaglewood juggle, the juggle size is less than 1cm, be ground into the agalloch eaglewood meal with accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after the filtration is poured in single tank planetary ball mill, continue to grind, milling time is 10 minutes, crosses 200 order mesh screens after grinding and obtains the agalloch eaglewood fine powder.
Be that the ratio of 50:15:50:0.05:6 is made into extracting solution with dehydrated alcohol, propylene glycol, vanay, oxysuccinic acid, ultrapure water according to mass ratio.
Adding the extracting solution of 500g in the agalloch eaglewood fine powder of 100g, is 60KHz in frequency, and temperature is ultrasonic under 35 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the first time solution by vacuum filtration.
Collecting the extracting solution that filter residue adds 500g again, is 60KHz in frequency, and temperature is ultrasonic under 35 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the second time solution by vacuum filtration.
Collecting filter residue and repeat above-mentioned steps 1 time again, merge three times agalloch eaglewood extracting solution, is 15 times of agalloch eaglewood fine powder weight to the agalloch eaglewood extracting solution quantitatively with dehydrated alcohol, namely obtains the agalloch eaglewood flavouring essence for tobacco.
The preparation of embodiment 2 agalloch eaglewood flavouring essence for tobaccos
Get agalloch eaglewood and make the agalloch eaglewood juggle, the juggle size is less than 1cm, be ground into the agalloch eaglewood meal with accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after the filtration is poured in single tank planetary ball mill, continue to grind, milling time is 10 minutes, crosses 200 order mesh screens after grinding and obtains the agalloch eaglewood fine powder.Be that the ratio of 70:20:35:0.1:4.95 is made into extracting solution with dehydrated alcohol, propylene glycol, vanay, oxysuccinic acid, ultrapure water according to mass ratio.
Adding the extracting solution of 125g in the agalloch eaglewood fine powder of 100g, is 70KHz in frequency, and temperature is ultrasonic under 40 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the first time solution by vacuum filtration.
Collecting the extracting solution that filter residue adds 125g again, is 70KHz in frequency, and temperature is ultrasonic under 40 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the second time solution by vacuum filtration.
Collect filter residue and repeat the said extracted step, multiplicity is 2 times, merges four times the agalloch eaglewood extracting solution, is 5 times of agalloch eaglewood fine powder weight to the agalloch eaglewood extracting solution quantitatively with dehydrated alcohol, namely obtains the agalloch eaglewood flavouring essence for tobacco.
The preparation of embodiment 3 agalloch eaglewood flavouring essence for tobaccos
Get agalloch eaglewood and make the agalloch eaglewood juggle, the juggle size is less than 1cm, be ground into the agalloch eaglewood meal with accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after the filtration is poured in single tank planetary ball mill, continue to grind, milling time is 10 minutes, crosses 200 order mesh screens after grinding and obtains the agalloch eaglewood fine powder.
Be that the ratio of 50:25:40:0.2:5.25 is made into extracting solution with dehydrated alcohol, propylene glycol, vanay, oxysuccinic acid, ultrapure water according to mass ratio.
Adding the extracting solution of 220g in the agalloch eaglewood fine powder of 100g, is 50KHz in frequency, and temperature is ultrasonic under 45 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the first time solution by vacuum filtration.
Collecting the extracting solution that filter residue adds 220g again, is 50KHz in frequency, and temperature is ultrasonic under 45 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the second time solution by vacuum filtration.
Collect filter residue and repeat above-mentioned steps again, multiplicity is 3 times, merges five times the agalloch eaglewood extracting solution, is 12 times of agalloch eaglewood fine powder weight to the agalloch eaglewood extracting solution quantitatively with dehydrated alcohol, namely obtains the agalloch eaglewood flavouring essence for tobacco.
The preparation of embodiment 4 agalloch eaglewood flavouring essence for tobaccos
Get agalloch eaglewood and make the agalloch eaglewood juggle, the juggle size is less than 1cm, be ground into the agalloch eaglewood meal with accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after the filtration is poured in single tank planetary ball mill, continue to grind, milling time is 10 minutes, crosses 200 order mesh screens after grinding and obtains the agalloch eaglewood fine powder.
Be that the ratio of 50:30:45:0.15:5.75 is made into extracting solution with dehydrated alcohol, propylene glycol, vanay, oxysuccinic acid, ultrapure water according to mass ratio.
Adding the extracting solution of 190g in the agalloch eaglewood fine powder of 100g, is 60KHz in frequency, and temperature is ultrasonic under 35 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the first time solution by vacuum filtration.
Collecting the extracting solution that filter residue adds 190g again, is 60KHz in frequency, and temperature is ultrasonic under 35 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the second time solution by vacuum filtration.
Collect filter residue and repeat above-mentioned steps again, multiplicity is 4 times, merges six times the agalloch eaglewood extracting solution, is 13 times of agalloch eaglewood fine powder weight to the agalloch eaglewood extracting solution quantitatively with dehydrated alcohol, namely obtains the agalloch eaglewood flavouring essence for tobacco.
The preparation of embodiment 5 agalloch eaglewood flavouring essence for tobaccos
Get agalloch eaglewood and make the agalloch eaglewood juggle, the juggle size is less than 1cm, be ground into the agalloch eaglewood meal with accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after the filtration is poured in single tank planetary ball mill, continue to grind, milling time is 10 minutes, crosses 200 order mesh screens after grinding and obtains the agalloch eaglewood fine powder.
Be that the ratio of 50:22:42:0.16:5.5 is made into extracting solution with dehydrated alcohol, propylene glycol, vanay, oxysuccinic acid, ultrapure water according to mass ratio.
Adding the extracting solution of 130g in the agalloch eaglewood fine powder of 100g, is 40KHz in frequency, and temperature is ultrasonic under 45 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the first time solution by vacuum filtration.
Collecting the extracting solution that filter residue adds 130g again, is 40KHz in frequency, and temperature is ultrasonic under 45 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the second time solution by vacuum filtration.
Collect filter residue and repeat above-mentioned steps again, multiplicity is 6 times, merges eight times the agalloch eaglewood extracting solution, is 11 times of agalloch eaglewood fine powder weight to the agalloch eaglewood extracting solution quantitatively with dehydrated alcohol, namely obtains the agalloch eaglewood flavouring essence for tobacco.
The preparation of embodiment 6 agalloch eaglewood flavouring essence for tobaccos
Get agalloch eaglewood and make the agalloch eaglewood juggle, the juggle size is less than 1cm, be ground into the agalloch eaglewood meal with accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after the filtration is poured in single tank planetary ball mill, continue to grind, milling time is 10 minutes, crosses 200 order mesh screens after grinding and obtains the agalloch eaglewood fine powder.
Be that the ratio of 50:33:46:0.14:5.35 is made into extracting solution with dehydrated alcohol, propylene glycol, vanay, oxysuccinic acid, ultrapure water according to mass ratio.
Adding the extracting solution of 100g in the agalloch eaglewood fine powder of 100g, is 80KHz in frequency, and temperature is ultrasonic under 40 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the first time solution by vacuum filtration.
Collecting the extracting solution that filter residue adds 100g again, is 80KHz in frequency, and temperature is ultrasonic under 40 ℃ the condition, in speed is to stir under the condition of 360r/min to extract, and obtains to extract for the second time solution by vacuum filtration.
Collect filter residue and repeat above-mentioned steps again, multiplicity is 5 times, merges seven times the agalloch eaglewood extracting solution, is 8 times of agalloch eaglewood fine powder weight to the agalloch eaglewood extracting solution quantitatively with dehydrated alcohol, namely obtains the agalloch eaglewood flavouring essence for tobacco.
Embodiment 7 contains the preparation of the cigarette of agalloch eaglewood flavouring essence for tobacco
Get the agalloch eaglewood flavouring essence for tobacco of the embodiment of the invention 1 preparation, add acceptable auxiliary material in the cigarette, adopt ordinary method to prepare cigarette.
Embodiment 8 contains the preparation of the cigarette of agalloch eaglewood flavouring essence for tobacco
Get the agalloch eaglewood flavouring essence for tobacco of the embodiment of the invention 2 preparations, add acceptable auxiliary material in the cigarette, adopt ordinary method to prepare cigarette.
Embodiment 9 contains the preparation of the cigarette of agalloch eaglewood flavouring essence for tobacco
Get the agalloch eaglewood flavouring essence for tobacco of the embodiment of the invention 3 preparations, add acceptable auxiliary material in the cigarette, adopt ordinary method to prepare cigarette.
Embodiment 10 contains the preparation of the cigarette of agalloch eaglewood flavouring essence for tobacco
Get the agalloch eaglewood flavouring essence for tobacco of the embodiment of the invention 4 preparations, add acceptable auxiliary material in the cigarette, adopt ordinary method to prepare cigarette.
Embodiment 11 contains the preparation of the cigarette of agalloch eaglewood flavouring essence for tobacco
Get the agalloch eaglewood flavouring essence for tobacco of the embodiment of the invention 5 preparations, add acceptable auxiliary material in the cigarette,
Adopt ordinary method to prepare cigarette.
Embodiment 12 contains the preparation of the cigarette of agalloch eaglewood flavouring essence for tobacco
Get the agalloch eaglewood flavouring essence for tobacco of the embodiment of the invention 6 preparations, add acceptable auxiliary material in the cigarette, adopt ordinary method to prepare cigarette.
The sensory quality assessment of the cigarette of embodiment 13 the present invention preparation
Carry out aesthetic quality's examination according to standard GB/T 5606.4-2005, the sensory quality assessment standard sees Table 1.
Table 1 Sensory Quality of Cigarette judgement criteria
Carry out the main flume examination according to standard GB/T 5606.5-2005.
Tar content:
Tar content class and corresponding box mark tar content see Table 2.
The coal-tar middle oil amount class of table 2 cigarette and corresponding box mark tar content standard
| The tar content class | Low | In | High |
| Box mark tar content/mg | ≤10 | 11～15 | ＞15 |
The tar content franchise:
When box mark tar content during less than or equal to 4mg, ︱ actual measurement tar content-box mark tar content ︱≤1.0mg then.
When box mark tar content during at 5mg～10mg, ︱ actual measurement tar content-box mark tar content ︱≤2.0mg then.
When box mark tar content during more than or equal to 11mg, ︱ actual measurement tar content-box mark tar content ︱≤2.5mg then.
Nicotine content in smoke:
When box mark nicotine content in smoke during less than or equal to 0.4mg, ︱ actual measurement nicotine content in smoke-box mark nicotine content in smoke ︱≤0.10mg then.
When box mark nicotine content in smoke during at 0.5mg～1.0mg, ︱ actual measurement nicotine content in smoke-box mark nicotine content in smoke ︱≤0.20mg then.
When box mark nicotine content in smoke during more than or equal to 1.1mg, ︱ actual measurement nicotine content in smoke-box mark nicotine content in smoke ︱≤0.30mg then.
The carbon monoxide in flue gas amount:
Carbon monoxide in flue gas amount class and corresponding box mark CO content see Table 3.
Carbon monoxide in flue gas amount class and corresponding box mark CO content standard in table 3 cigarette
| The CO content class | Low | In | High |
| Box mark CO content/mg | ≤10 | 11～15 | ＞15 |
Carbon monoxide in flue gas amount franchise:
When box mark carbon monoxide in flue gas amount during less than or equal to 4mg, ︱ actual measurement carbon monoxide in flue gas amount-box mark carbon monoxide in flue gas amount ︱≤1.0mg then.
When box mark carbon monoxide in flue gas amount during at 5mg～10mg, ︱ actual measurement carbon monoxide in flue gas amount-box mark carbon monoxide in flue gas amount ︱≤2.0mg then.
When box mark carbon monoxide in flue gas amount during more than or equal to 11mg, ︱ actual measurement carbon monoxide in flue gas amount-box mark carbon monoxide in flue gas amount ︱≤3.0mg then.
The cigarette that the embodiment of the invention 7 to 12 provides is test group, the cigarette that does not add agalloch eaglewood flavouring essence for tobacco provided by the invention is control group, above cigarette sample is had smoke panel test 21 professional and technical personnel of qualification certificate of country or provincial Sensory Quality of Cigarette and is smoked panel test by domestic, the results are shown in Table 4.
Table 4 smoking result
| Project | Gloss | Fragrance | Harmony | Assorted gas | Stimulate | Pleasant impression | Add up to |
| Control group | 5.0 | 29.00 | 5.0 | 10.50 | 17.70 | 21.60 | 88.80 |
| Test group example 7 | 5.0 | 30.65 | 5.0 | 11.05 | 17.85 | 22.10 | 91.65 |
| Test group example 8 | 5.0 | 30.95 | 5.0 | 11.04 | 17.83 | 21.86 | 91.68 |
| Test group example 9 | 5.0 | 30.75 | 5.0 | 11.15 | 17.98 | 22.08 | 91.96 |
| Test group example 10 | 5.0 | 30.38 | 5.0 | 11.17 | 17.81 | 22.01 | 91.37 |
| Test group example 11 | 5.0 | 30.72 | 5.0 | 10.85 | 17.88 | 21.88 | 91.33 |
| Test group example 12 | 5.0 | 30.58 | 5.0 | 11.09 | 17.92 | 21.94 | 91.53 |
The cigarette that contains the agalloch eaglewood flavouring essence for tobacco that the embodiment of the invention 7 to 12 provides, fragrance is graceful, sweet note, and fragrance is lasting and long, deeply is subjected to broad masses of the people's welcome.
The cigarette sample that the embodiment of the invention 7 to 12 provides, tar content are 8mg, and nicotine content in smoke is 0.8mg, and the carbon monoxide in flue gas amount is 10mg.
The above only is preferred implementation of the present invention; should be pointed out that for those skilled in the art, under the prerequisite that does not break away from the principle of the invention; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (12)
1. the extracting solution of a flavouring essence for tobacco is characterized in that, comprises C
2-3Alcohol, ester, oxysuccinic acid and water.
2. extracting solution according to claim 1 is characterized in that, described C
2-3The mass ratio of alcohol, described ester, described oxysuccinic acid and described water be 65～90:35～50:0.05～0.2:4.95～6.
3. extracting solution according to claim 1 is characterized in that, described C
2-3Alcohol be ethanol and/or propylene glycol.
4. extracting solution according to claim 1 is characterized in that, described ester is glyceryl ester.
5. extracting solution according to claim 4 is characterized in that, described glyceryl ester is vanay.
6. application that is used for extracting according to claim 1 the agalloch eaglewood flavouring essence for tobacco to 5 each described extracting solutions.
7. method of extracting the agalloch eaglewood flavouring essence for tobacco, it is characterized in that, get agalloch eaglewood and obtain after crushed eaglewood powder, with mix such as each described extracting solution of claim 1 to 5 after extract to obtain the agalloch eaglewood extracting solution, again behind vacuum filtration, ethanol constant volume and get final product.
8. method according to claim 7 is characterized in that, the mass ratio of described eaglewood powder and described extracting solution is 1:(5～15).
9. method according to claim 7 is characterized in that, the described supersound extraction that is extracted as, the frequency of described supersound extraction are 40～80KHz, and the temperature of described supersound extraction is 35～45 ℃.
10. method according to claim 7 is characterized in that, the number of times of described extraction is at least 3 times.
11. the agalloch eaglewood flavouring essence for tobacco for preparing to 10 each described methods according to claim 7.
12. a cigarette is characterized in that, comprises agalloch eaglewood flavouring essence for tobacco as claimed in claim 11.
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| CN103361176A (en) * | 2013-07-31 | 2013-10-23 | 广州市澳键丰泽生物科技有限公司 | Aroma compound |
| CN103361176B (en) * | 2013-07-31 | 2014-12-10 | 广州市澳键丰泽生物科技有限公司 | Aroma compound |
| CN104171157A (en) * | 2014-09-10 | 2014-12-03 | 嘉兴市得百科新材料科技有限公司 | Green tea extract as well as preparation method and application thereof |
| CN104171157B (en) * | 2014-09-10 | 2016-06-15 | 河源市绿环生物科技有限公司 | A kind of green tea extract and preparation method thereof, application |
| CN104830537A (en) * | 2015-04-30 | 2015-08-12 | 东莞波顿香料有限公司 | Preparation method and application of aquilaria wood hydrolat |
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| CN104886769A (en) * | 2015-05-06 | 2015-09-09 | 湖北中烟工业有限责任公司 | Low-tar cigarette and manufacturing method thereof |
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| CN105011368A (en) * | 2015-06-17 | 2015-11-04 | 云南中烟工业有限责任公司 | Glycerol triacetate extract of momordica grosvenori and application thereof to cigarette |
| CN105062686A (en) * | 2015-07-17 | 2015-11-18 | 王再青 | Method for extracting lavender essential oil |
| CN110699179A (en) * | 2018-07-10 | 2020-01-17 | 湖南中烟工业有限责任公司 | Solvent system of surface fragrance essence for cigarettes and surface fragrance essence for cigarettes |
| CN109907357A (en) * | 2019-04-03 | 2019-06-21 | 中烟施伟策（云南）再造烟叶有限公司 | Reconstituted tobacco and preparation method thereof |
| CN110403236A (en) * | 2019-07-04 | 2019-11-05 | 江西中烟工业有限责任公司 | A kind of dry pearl mouth stick of cigarette for sending out function thoroughly with promotion flue gas |
| CN110403236B (en) * | 2019-07-04 | 2021-07-27 | 江西中烟工业有限责任公司 | Cigarette dry bead filter rod with function of improving smoke permeation |
| CN116349909A (en) * | 2023-04-21 | 2023-06-30 | 云南中烟工业有限责任公司 | Tobacco column |
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