CN103013668B - A kind of flavouring essence for tobacco extract, extracting method, obtained flavouring essence for tobacco and tobacco product - Google Patents
A kind of flavouring essence for tobacco extract, extracting method, obtained flavouring essence for tobacco and tobacco product Download PDFInfo
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- CN103013668B CN103013668B CN201210559129.7A CN201210559129A CN103013668B CN 103013668 B CN103013668 B CN 103013668B CN 201210559129 A CN201210559129 A CN 201210559129A CN 103013668 B CN103013668 B CN 103013668B
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Abstract
The present invention relates to tobacco industry field, particularly a kind of flavouring essence for tobacco extract, extracting method, obtained flavouring essence for tobacco and tobacco product.This extract comprises C
2-3alcohol, ester, malic acid and water.The fragrance of the flavouring essence for tobacco that extracting method provided by the invention obtains and tobacco aroma harmony, graceful and long, the aromatic style feature of tobacco product uniqueness can be given.Cigarette containing agalloch eaglewood flavouring essence for tobacco provided by the invention, elegant fragrance, sweet note, fragrance is lasting and long, the dark welcome by broad masses of the people.
Description
Technical field
The present invention relates to tobacco industry field, particularly a kind of flavouring essence for tobacco extract, extracting method, obtained flavouring essence for tobacco and tobacco product.
Background technology
Agalloch eaglewood, for dicotyledon medicine Thymelaeceae magaphanerophytes agalloch eaglewood Aquilaria agallocha (Lour.) Roxb or suspension culture of Aquilaria sinensis A.sinensis (Lour.) Gilg is being subject to natural injury, (as thunderbolt, windbreak, damages by worms) or to be subject to after artificial destruction the infection condensation that oozy grease in the process of self-regeneration is subject to fungi and to form.
Agalloch eaglewood resource is rare, it is extensive, with a long history to act on, and as famous and precious medicinal material, having relevant description in the classic of TCM: claim in essentials of Matea Medica its " and gas can be descended to fall sputum, can fall and also can rise, fragrance enters spleen, Gu can manage all gas and in adjusting, its look black.Body sun, admittedly enter the right arm gate of vitality, warm essence is supporing yang, and promoting the circulation of qi is not felt frustrated, and does not help fire in temperature "; " large bright book on Chinese herbal medicine " is called it " tonifying five zang organs in tune, beneficial able-bodied sun, warm waist knee, ending tendon transfer vomiting and diarrhoea cold air "; Compendium of Material Medica meaning can " control heat in the upper and cold in the lower, the circulation of vital energy in the wrong direction breathes heavily urgency, and large intestine void is closed, urine gas drench, man's cold sperm ".In a word, agalloch eaglewood is the purging medicine of fragrant stomach invigorating, and main pungent loose dredging, in warm stomach qi-activating drug, effect shows.Control inverse breathing heavily especially effectively, for retention of urine, neurotic depression gastric colic etc. are all effective.The most important thing is can centre of equilibrium nerve, calm mood, manage all gas and in adjusting, help promoting the circulation of qi to enter fixed.
Ligaloes tea wins aft-loaded airfoil by the leaf of rare Chinese medicine agalloch eaglewood to be made, Ligaloes tea made by eaglewood leaf, prove through test, identical with the medicines and health protection effect of Chinese medicine agalloch eaglewood, and the property of medicine of agalloch eaglewood uniqueness is absorbed by the method for drinking tea, in the middle of the delicate reward tea health-care effect of agalloch eaglewood being dissolved in life is siped tea, the way to keep in good health ultimate attainment especially.Ligaloes tea energy stool, dissipate-swelling gas, venting grease, helps sleep, skin maintenance, more can lock essence gate, and controlling nocturnal emission with astringent drugs closes, and nourishes kidney water, the shady essence of establishing-Yang.For the busy battle-weary people of modern life work, after the free time, drink one cup of Ligaloes tea, can feel that knowledge is clear and bright immediately, energetic, drink body-building of more nourishing heart for a long time.
Elite in agalloch eaglewood can be distilled and refined into " heavy oil ", is also called to be coated with fragrant, directly with for Buddhist, or can be applied in musical instruments used in a Buddhist or Taoist mass beads to reach the object of maintenance, also can smear the body in the people that practices Buddhism or Taoism, wash the hand of god to circumcise.Sample pure and fresh uniqueness, the effect of tool health care is that the medicine of calming the nerves altered by kind of perfume (or spice), and fragrance is heavy and coagulate, prolongedly not fall apart, invigorating, can fall young flat liver, adjust spleen lung, sharp chest stomach, more can wash body only read for the people that practices Buddhism or Taoism, all evil relieving palpitation god can be kept away again, the purposes such as ventilation arteries and veins, outer disturbing without all heresies, clean thought is at a stalemate.
Except being applied to above-mentioned field, agalloch eaglewood also can be used for smoked combustion, and fragrance is elegant, has promoting qi circulation and relieving pain, warming middle energizer to arrest vomiting, effect of promoting inspiration to relieve asthma.Smoked combustion agalloch eaglewood, incense drug gas fills the air, and can purify air, fragrance dehumidifying, taste agalloch eaglewood, is calmed the nerves, with all worries set aside, gives free and natural and gentle enjoyment, makes the taste boundary of life be purified and distil, and can contribute to improving sleep quality.But the utensil needed in traditional stacte process is more, and process is loaded down with trivial details.
Summary of the invention
In view of this, the invention provides a kind of flavouring essence for tobacco extract, extracting method, obtained flavouring essence for tobacco and tobacco product.This extract comprises C
2-3alcohol, ester, malic acid and water.The fragrance of the flavouring essence for tobacco that extracting method provided by the invention obtains and tobacco aroma harmony, graceful and long, the aromatic style feature of tobacco product uniqueness can be given.
In order to realize foregoing invention object, the invention provides following technical scheme:
The invention provides a kind of extract of flavouring essence for tobacco, comprise C
2-3alcohol, ester, malic acid and water.
As preferably, C in the extract of flavouring essence for tobacco provided by the invention
2-3alcohol, ester, malic acid and water mass ratio be 65 ~ 90:35 ~ 50:0.05 ~ 0.2:4.95 ~ 6.
As preferably, C in the extract of flavouring essence for tobacco provided by the invention
2-3alcohol be ethanol or propane diols.
As preferably, in the extract of flavouring essence for tobacco provided by the invention, ester is glyceride.
As preferably, in the extract of flavouring essence for tobacco provided by the invention, glyceride is glyceryl triacetate.
Present invention also offers a kind of said extracted liquid for extracting the application of agalloch eaglewood flavouring essence for tobacco; This extract comprises C
2-3alcohol, ester, malic acid and water.As preferably, C
2-3alcohol be ethanol or propane diols.As preferably, ester is glyceride.As preferably, glyceride is glyceryl triacetate.
Present invention also offers a kind of method extracting agalloch eaglewood flavouring essence for tobacco, get agalloch eaglewood and obtain eaglewood powder after crushed, extract and obtain agalloch eaglewood extract after mixing with extract provided by the invention, then after vacuum filtration, ethanol constant volume and get final product; Extract provided by the invention comprises C
2-3alcohol, ester, malic acid and water.As preferably, C in the extract of flavouring essence for tobacco provided by the invention
2-3alcohol, ester, malic acid and water mass ratio be 65 ~ 90:35 ~ 50:0.05 ~ 0.2:4.95 ~ 6.As preferably, C
2-3alcohol be ethanol or propane diols.As preferably, ester is glyceride.As preferably, glyceride is glyceryl triacetate.
As preferably, the mass ratio extracting the extract of eaglewood powder and flavouring essence for tobacco provided by the invention in the method for agalloch eaglewood flavouring essence for tobacco is 1:(5 ~ 15).
As preferably, be extracted as ultrasonic extraction, the frequency of ultrasonic extraction is 40 ~ 80KHz, and the temperature of ultrasonic extraction is 35 ~ 45 DEG C.
As preferably, the number of times of extraction is at least 3 times.
Preferably, the number of times of extraction is at least 4 times.
As preferably, the vacuum of vacuum filtration is 0.07MPa.
As preferably, in ethanol constant volume, the mass ratio of eaglewood powder and ethanol is 1: 10 ~ 14.
The agalloch eaglewood flavouring essence for tobacco that the method that present invention also offers said extracted agalloch eaglewood flavouring essence for tobacco prepares; The method is got agalloch eaglewood and is obtained eaglewood powder after crushed, extracts and obtains agalloch eaglewood extract after mixing with extract provided by the invention, then after vacuum filtration, ethanol constant volume and get final product; Extract provided by the invention comprises C
2-3alcohol, ester, malic acid and water.As preferably, C
2-3alcohol be ethanol or propane diols.As preferably, ester is glyceride.As preferably, glyceride is glyceryl triacetate.
Present invention also offers a kind of cigarette, the agalloch eaglewood flavouring essence for tobacco that the method comprising extraction agalloch eaglewood flavouring essence for tobacco provided by the invention prepares.
The invention provides a kind of flavouring essence for tobacco extract, extracting method, obtained flavouring essence for tobacco and tobacco product.This extract comprises C
2-3alcohol, ester, malic acid and water.The fragrance of the flavouring essence for tobacco that extracting method provided by the invention obtains and tobacco aroma harmony, graceful and long, the aromatic style feature of tobacco product uniqueness can be given.Cigarette containing agalloch eaglewood flavouring essence for tobacco provided by the invention, elegant fragrance, sweet note, fragrance is lasting and long, the dark welcome by broad masses of the people.
Detailed description of the invention
The invention discloses a kind of flavouring essence for tobacco extract, extracting method, obtained flavouring essence for tobacco and tobacco product, those skilled in the art can use for reference present disclosure, and suitable improving technique parameter realizes.Special needs to be pointed out is, all similar replacements and change apparent to those skilled in the art, they are all deemed to be included in the present invention.Method of the present invention and application are described by preferred embodiment, related personnel obviously can not depart from content of the present invention, spirit and scope methods and applications as herein described are changed or suitably change with combination, realize and apply the technology of the present invention.
In flavouring essence for tobacco extract provided by the invention, extracting method, obtained flavouring essence for tobacco and tobacco product, raw materials used and reagent all can be buied by market.
Below in conjunction with embodiment, set forth the present invention further:
The preparation of embodiment 1 agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood and make agalloch eaglewood juggle, juggle size is less than 1cm, agalloch eaglewood meal is ground into accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after filtration is poured in single tank planetary ball mill, continue grinding, milling time is 10 minutes, crosses 200 order mesh screens and obtain agalloch eaglewood fine powder after grinding.
Extract is made into by the ratio that absolute ethyl alcohol, propane diols, glyceryl triacetate, malic acid, ultra-pure water are 50:15:50:0.05:6 according to mass ratio.
In the agalloch eaglewood fine powder of 100g, add the extract of 500g, be 60KHz in frequency, and temperature is ultrasonic under the condition of 35 DEG C, is to stir under the condition of 360r/min to extract in speed, obtained extract solution for the first time by vacuum filtration.
Collect the extract that filter residue adds 500g again, be 60KHz in frequency, temperature is ultrasonic under the condition of 35 DEG C, is to stir under the condition of 360r/min to extract in speed, obtains second time extract solution by vacuum filtration.
Collect filter residue and repeat above-mentioned steps again 1 time, merge the agalloch eaglewood extract of three times, quantitatively arrive 15 times that agalloch eaglewood extract is agalloch eaglewood fine powder weight with absolute ethyl alcohol, namely obtain agalloch eaglewood flavouring essence for tobacco.
The preparation of embodiment 2 agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood and make agalloch eaglewood juggle, juggle size is less than 1cm, agalloch eaglewood meal is ground into accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after filtration is poured in single tank planetary ball mill, continue grinding, milling time is 10 minutes, crosses 200 order mesh screens and obtain agalloch eaglewood fine powder after grinding.Extract is made into by the ratio that absolute ethyl alcohol, propane diols, glyceryl triacetate, malic acid, ultra-pure water are 70:20:35:0.1:4.95 according to mass ratio.
In the agalloch eaglewood fine powder of 100g, add the extract of 125g, be 70KHz in frequency, and temperature is ultrasonic under the condition of 40 DEG C, is to stir under the condition of 360r/min to extract in speed, obtained extract solution for the first time by vacuum filtration.
Collect the extract that filter residue adds 125g again, be 70KHz in frequency, temperature is ultrasonic under the condition of 40 DEG C, is to stir under the condition of 360r/min to extract in speed, obtains second time extract solution by vacuum filtration.
Collect filter residue and repeat said extracted step, number of repetition is 2 times, merges four agalloch eaglewood extracts, quantitatively arrives 5 times that agalloch eaglewood extract is agalloch eaglewood fine powder weight, namely obtain agalloch eaglewood flavouring essence for tobacco with absolute ethyl alcohol.
The preparation of embodiment 3 agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood and make agalloch eaglewood juggle, juggle size is less than 1cm, agalloch eaglewood meal is ground into accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after filtration is poured in single tank planetary ball mill, continue grinding, milling time is 10 minutes, crosses 200 order mesh screens and obtain agalloch eaglewood fine powder after grinding.
Extract is made into by the ratio that absolute ethyl alcohol, propane diols, glyceryl triacetate, malic acid, ultra-pure water are 50:25:40:0.2:5.25 according to mass ratio.
In the agalloch eaglewood fine powder of 100g, add the extract of 220g, be 50KHz in frequency, and temperature is ultrasonic under the condition of 45 DEG C, is to stir under the condition of 360r/min to extract in speed, obtained extract solution for the first time by vacuum filtration.
Collect the extract that filter residue adds 220g again, be 50KHz in frequency, temperature is ultrasonic under the condition of 45 DEG C, is to stir under the condition of 360r/min to extract in speed, obtains second time extract solution by vacuum filtration.
Collect filter residue and repeat above-mentioned steps again, number of repetition is 3 times, merges five agalloch eaglewood extracts, quantitatively arrives 12 times that agalloch eaglewood extract is agalloch eaglewood fine powder weight, namely obtain agalloch eaglewood flavouring essence for tobacco with absolute ethyl alcohol.
The preparation of embodiment 4 agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood and make agalloch eaglewood juggle, juggle size is less than 1cm, agalloch eaglewood meal is ground into accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after filtration is poured in single tank planetary ball mill, continue grinding, milling time is 10 minutes, crosses 200 order mesh screens and obtain agalloch eaglewood fine powder after grinding.
Extract is made into by the ratio that absolute ethyl alcohol, propane diols, glyceryl triacetate, malic acid, ultra-pure water are 50:30:45:0.15:5.75 according to mass ratio.
In the agalloch eaglewood fine powder of 100g, add the extract of 190g, be 60KHz in frequency, and temperature is ultrasonic under the condition of 35 DEG C, is to stir under the condition of 360r/min to extract in speed, obtained extract solution for the first time by vacuum filtration.
Collect the extract that filter residue adds 190g again, be 60KHz in frequency, temperature is ultrasonic under the condition of 35 DEG C, is to stir under the condition of 360r/min to extract in speed, obtains second time extract solution by vacuum filtration.
Collect filter residue and repeat above-mentioned steps again, number of repetition is 4 times, merges six agalloch eaglewood extracts, quantitatively arrives 13 times that agalloch eaglewood extract is agalloch eaglewood fine powder weight, namely obtain agalloch eaglewood flavouring essence for tobacco with absolute ethyl alcohol.
The preparation of embodiment 5 agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood and make agalloch eaglewood juggle, juggle size is less than 1cm, agalloch eaglewood meal is ground into accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after filtration is poured in single tank planetary ball mill, continue grinding, milling time is 10 minutes, crosses 200 order mesh screens and obtain agalloch eaglewood fine powder after grinding.
Extract is made into by the ratio that absolute ethyl alcohol, propane diols, glyceryl triacetate, malic acid, ultra-pure water are 50:22:42:0.16:5.5 according to mass ratio.
In the agalloch eaglewood fine powder of 100g, add the extract of 130g, be 40KHz in frequency, and temperature is ultrasonic under the condition of 45 DEG C, is to stir under the condition of 360r/min to extract in speed, obtained extract solution for the first time by vacuum filtration.
Collect the extract that filter residue adds 130g again, be 40KHz in frequency, temperature is ultrasonic under the condition of 45 DEG C, is to stir under the condition of 360r/min to extract in speed, obtains second time extract solution by vacuum filtration.
Collect filter residue and repeat above-mentioned steps again, number of repetition is 6 times, merges eight agalloch eaglewood extracts, quantitatively arrives 11 times that agalloch eaglewood extract is agalloch eaglewood fine powder weight, namely obtain agalloch eaglewood flavouring essence for tobacco with absolute ethyl alcohol.
The preparation of embodiment 6 agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood and make agalloch eaglewood juggle, juggle size is less than 1cm, agalloch eaglewood meal is ground into accurate whirlwind type crushing machine, cross 100 order mesh screens, agalloch eaglewood meal after filtration is poured in single tank planetary ball mill, continue grinding, milling time is 10 minutes, crosses 200 order mesh screens and obtain agalloch eaglewood fine powder after grinding.
Extract is made into by the ratio that absolute ethyl alcohol, propane diols, glyceryl triacetate, malic acid, ultra-pure water are 50:33:46:0.14:5.35 according to mass ratio.
In the agalloch eaglewood fine powder of 100g, add the extract of 100g, be 80KHz in frequency, and temperature is ultrasonic under the condition of 40 DEG C, is to stir under the condition of 360r/min to extract in speed, obtained extract solution for the first time by vacuum filtration.
Collect the extract that filter residue adds 100g again, be 80KHz in frequency, temperature is ultrasonic under the condition of 40 DEG C, is to stir under the condition of 360r/min to extract in speed, obtains second time extract solution by vacuum filtration.
Collect filter residue and repeat above-mentioned steps again, number of repetition is 5 times, merges seven agalloch eaglewood extracts, quantitatively arrives 8 times that agalloch eaglewood extract is agalloch eaglewood fine powder weight, namely obtain agalloch eaglewood flavouring essence for tobacco with absolute ethyl alcohol.
The preparation of the cigarette of embodiment 7 containing agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood flavouring essence for tobacco prepared by the embodiment of the present invention 1, add acceptable auxiliary material in cigarette, adopt conventional method to prepare cigarette.
The preparation of the cigarette of embodiment 8 containing agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood flavouring essence for tobacco prepared by the embodiment of the present invention 2, add acceptable auxiliary material in cigarette, adopt conventional method to prepare cigarette.
The preparation of the cigarette of embodiment 9 containing agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood flavouring essence for tobacco prepared by the embodiment of the present invention 3, add acceptable auxiliary material in cigarette, adopt conventional method to prepare cigarette.
The preparation of the cigarette of embodiment 10 containing agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood flavouring essence for tobacco prepared by the embodiment of the present invention 4, add acceptable auxiliary material in cigarette, adopt conventional method to prepare cigarette.
The preparation of the cigarette of embodiment 11 containing agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood flavouring essence for tobacco prepared by the embodiment of the present invention 5, add acceptable auxiliary material in cigarette,
Conventional method is adopted to prepare cigarette.
The preparation of the cigarette of embodiment 12 containing agalloch eaglewood flavouring essence for tobacco
Get agalloch eaglewood flavouring essence for tobacco prepared by the embodiment of the present invention 6, add acceptable auxiliary material in cigarette, adopt conventional method to prepare cigarette.
The sensory quality assessment of cigarette prepared by embodiment 13 the present invention
Carry out aesthetic quality's examination according to standard GB/T 5606.4-2005, sensory quality assessment standard is in table 1.
Table 1 Sensory Quality of Cigarette evaluation criterion
Main flume examination is carried out according to standard GB/T 5606.5-2005.
Tar content:
Tar content class and corresponding box mark tar content are in table 2.
Tar content class and corresponding box mark tar content standard in table 2 cigarette
| Tar content class | Low | In | High |
| Box mark tar content/mg | ≤10 | 11～15 | ＞15 |
Tar content franchise:
When box mark tar content is less than or equal to 4mg, then ︱ surveys tar content-box mark tar content ︱≤1.0mg.
When box mark tar content is at 5mg ~ 10mg, then ︱ surveys tar content-box mark tar content ︱≤2.0mg.
When box mark tar content is more than or equal to 11mg, then ︱ surveys tar content-box mark tar content ︱≤2.5mg.
Nicotine content in smoke:
When box mark nicotine content in smoke is less than or equal to 0.4mg, then ︱ surveys nicotine content in smoke-box mark nicotine content in smoke ︱≤0.10mg.
When box mark nicotine content in smoke is at 0.5mg ~ 1.0mg, then ︱ surveys nicotine content in smoke-box mark nicotine content in smoke ︱≤0.20mg.
When box mark nicotine content in smoke is more than or equal to 1.1mg, then ︱ surveys nicotine content in smoke-box mark nicotine content in smoke ︱≤0.30mg.
Carbon monoxide in flue gas amount:
Carbon monoxide in flue gas amount class and corresponding box mark CO content are in table 3.
Carbon monoxide in flue gas amount class and corresponding box mark CO content standard in table 3 cigarette
| CO content class | Low | In | High |
| Box mark CO content/mg | ≤10 | 11～15 | ＞15 |
Carbon monoxide in flue gas amount franchise:
When box mark carbon monoxide in flue gas amount is less than or equal to 4mg, then ︱ surveys carbon monoxide in flue gas amount-box mark carbon monoxide in flue gas amount ︱≤1.0mg.
When box mark carbon monoxide in flue gas amount is at 5mg ~ 10mg, then ︱ surveys carbon monoxide in flue gas amount-box mark carbon monoxide in flue gas amount ︱≤2.0mg.
When box mark carbon monoxide in flue gas amount is more than or equal to 11mg, then ︱ surveys carbon monoxide in flue gas amount-box mark carbon monoxide in flue gas amount ︱≤3.0mg.
The cigarette that the embodiment of the present invention 7 to 12 provides is test group, the cigarette not adding agalloch eaglewood flavouring essence for tobacco provided by the invention is control group, above cigarette sample is had smoke panel test 21 professional and technical personnel of credentials of country or provincial Sensory Quality of Cigarette smoked panel test by domestic, the results are shown in Table 4.
Table 4 smoking result
| Project | Gloss | Fragrance | Harmony | Assorted gas | Stimulate | Pleasant impression | Add up to |
| Control group | 5.0 | 29.00 | 5.0 | 10.50 | 17.70 | 21.60 | 88.80 |
| Test group example 7 | 5.0 | 30.65 | 5.0 | 11.05 | 17.85 | 22.10 | 91.65 |
| Test group example 8 | 5.0 | 30.95 | 5.0 | 11.04 | 17.83 | 21.86 | 91.68 |
| Test group example 9 | 5.0 | 30.75 | 5.0 | 11.15 | 17.98 | 22.08 | 91.96 |
| Test group example 10 | 5.0 | 30.38 | 5.0 | 11.17 | 17.81 | 22.01 | 91.37 |
| Test group example 11 | 5.0 | 30.72 | 5.0 | 10.85 | 17.88 | 21.88 | 91.33 |
| Test group example 12 | 5.0 | 30.58 | 5.0 | 11.09 | 17.92 | 21.94 | 91.53 |
The cigarette containing agalloch eaglewood flavouring essence for tobacco that the embodiment of the present invention 7 to 12 provides, elegant fragrance, sweet note, fragrance is lasting and long, the dark welcome by broad masses of the people.
The cigarette sample that the embodiment of the present invention 7 to 12 provides, tar content is 8mg, and nicotine content in smoke is 0.8mg, and carbon monoxide in flue gas amount is 10mg.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (7)
1. extract a method for agalloch eaglewood flavouring essence for tobacco, it is characterized in that, get agalloch eaglewood and obtain eaglewood powder after crushed, extract and obtain agalloch eaglewood extract after mixing with flavouring essence for tobacco extract, then after vacuum filtration, ethanol constant volume and get final product;
Described flavouring essence for tobacco extract is by C
2-3alcohol, glyceride, malic acid and water composition; Described C
2-3alcohol be ethanol and propane diols; Described glyceride is glyceryl triacetate.
2. method according to claim 1, is characterized in that, described C
2-3alcohol, described ester, described malic acid and described water mass ratio be 65 ~ 90:35 ~ 50:0.05 ~ 0.2:4.95 ~ 6.
3. method according to claim 1, is characterized in that, the mass ratio of described eaglewood powder and described extract is 1:(5 ~ 15).
4. method according to claim 1, is characterized in that, described in be extracted as ultrasonic extraction, the frequency of described ultrasonic extraction is 40 ~ 80KHz, and the temperature of described ultrasonic extraction is 35 ~ 45 DEG C.
5. method according to claim 1, is characterized in that, the number of times of described extraction is at least 3 times.
6. the agalloch eaglewood flavouring essence for tobacco that the method according to any one of claim 1 to 5 prepares.
7. a cigarette, is characterized in that, comprises agalloch eaglewood flavouring essence for tobacco as claimed in claim 6.
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| CN101518358A (en) * | 2009-04-01 | 2009-09-02 | 红云红河烟草(集团)有限责任公司 | Cigarette perfume solvent and preparation method thereof |
| EP2514320A1 (en) * | 2009-12-16 | 2012-10-24 | Kaneka Corporation | Method for producing flavoring agent, and flavoring agent |
| CN102488315A (en) * | 2011-12-13 | 2012-06-13 | 吴伟銮 | Health-care perfume combination for cigarettes |
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