CN105011368A - Glycerol triacetate extract of momordica grosvenori and application thereof to cigarette - Google Patents
Glycerol triacetate extract of momordica grosvenori and application thereof to cigarette Download PDFInfo
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- CN105011368A CN105011368A CN201510336402.3A CN201510336402A CN105011368A CN 105011368 A CN105011368 A CN 105011368A CN 201510336402 A CN201510336402 A CN 201510336402A CN 105011368 A CN105011368 A CN 105011368A
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- momordica grosvenori
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- glycerol triacetate
- triacetyl glycerine
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Abstract
The invention discloses a glycerol triacetate extract of momordica grosvenori and application thereof to a cigarette.The method for preparing the glycerol triacetate extract of momordica grosvenori comprises following steps of: utilizing coarse powder of momordica grosvenori dried fruits with moisture content of 6% to 8 % and particle size of 20 to 60 meshes as raw materials and utilizing glycerol triacetate as an extraction agent; carrying out extraction operation by adoption of a heating reflux mode; preparing the glycerol triacetate extract of momordica grosvenori by ultrasonic extraction; preparing the glycerol triacetate extract of momordica grosvenori as a solution with a concentration of 3% to 5% by utilizing glycerol triacetate as a solvent; and uniformly spraying the solution to filter stick tows based on the weight of cellulose acetate tows in a ratio in the range of 7% to 8% in order to prepare a cigarette filter containing effective components of momordica grosvenori. The extract has capabilities of heightening a sense of sweetness of cigarette smoke, improving richness and tenderness of smoke, reducing irritation and improving sapor and offensive odor and has fine suction comfortableness. The glycerol triacetate extract of momordica grosvenori and application thereof to the cigarette have following beneficial effects: simple production technology is obtained; high operationality and standardability are achieved; raw materials are easily available and low in cost; industrial-scale production is conveniently realized; and a broad application prospect is obtained.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of Momordica grosvenori triacetyl glycerine extract.Meanwhile, the invention still further relates to the described application of Momordica grosvenori triacetyl glycerine extract in cigarette.
Background technology
Momordica grosvenori is a kind of traditional medicine food dual purpose plant, the fruit of its drying is cool in nature, taste is sweet, nontoxic, have promote the production of body fluid to quench thirst, the effect such as moistening lung for removing phlegm, clearing heat, relieving sore-throat, can be used for the diseases such as treatment pulmonary tuberculosis, asthma, pertussis, tracheitis and tonsillitis clinically.The functional mass extracted from Momordica grosvenori can be used as low calorie sweetener and makes an addition in varieties of food items, also can be processed into the Foods or drinks that wets one's whistle.The primary bioactive components of Momordica grosvenori is mogroside, is a kind of sweet substance low in calories, and with health role to respiratory system.In addition, also the various bioactivators such as flavone compound, natural fructose, several amino acids and aliphatic acid, vitamin and trace element are contained in Lo Han Guo fruit.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But the reduction of tar content in cigarette also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus of each tobacco productive corporation research and development.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.Such as a kind of containing Momordica grosvenori porous particle composite filter (CN 203709250U), the application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN103271441A) thereof, a kind of filter stick fiber base material additive and application (CN 103126073A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN 104161303A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582A) etc., but the filter stick additive described in above-mentioned patent mainly first by extract or allocate additive again in triacetyl glycerine dissolve add in cigarette, or the additive some being insoluble in triacetyl glycerine is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the solvability of triacetyl glycerine to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in triacetyl glycerine, limit the application of spices in cigarette filter rod.On the other hand, if be not that medium carries out filter stick perfuming by triacetyl glycerine, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco business in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide a kind of Fructus Monordicae extract prepared using triacetyl glycerine as extractant, this extract is applied to cigarette effectively can be strengthened cigarette sweet moisture feeling and exquisiteness, enrich the fresh and clean cigarette perfume of cigarette.
The present invention also aims to provide the described application of Momordica grosvenori triacetyl glycerine extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage adopted in the present invention is mass percent.
A kind of Momordica grosvenori triacetyl glycerine extract, is obtained by the method for following steps:
(1) by after dried fructus momordicae fragmentation, under 50 ~ 70 DEG C of conditions, be dried to moisture is 6 ~ 8%, then pulverizing is 20 ~ 60 object meal, for subsequent use;
(2) take 8 ~ 10 parts of Grosvenor Momordica Fruits according to weight portion and be placed in round-bottomed flask, add 80 ~ 120 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 4 ~ 6 hours, refluxing extraction is carried out under 70 ~ 120 DEG C of conditions, 5 ~ 10 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 600 ~ 800W, 40kHZ condition, extract 30 ~ 60 minutes, obtain settled solution after excessively filtering filter residue and be required Momordica grosvenori triacetyl glycerine extraction ester thing.
The described application of Momordica grosvenori triacetyl glycerine extract in cigarette, it is characterized in that: be that described Momordica grosvenori triacetyl glycerine extract is mixed with the solution that concentration is 3 ~ 5% by solvent with triacetyl glycerine, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the Momordica grosvenori triacetyl glycerine extract prepared by the present invention, can dissolve each other in any proportion with triacetyl glycerine, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that Momordica grosvenori exists by prior art when filter stick additive is mixed and is fitted in plasticizer.
2. adopt triacetyl glycerine to be that extractant extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in triacetyl glycerine in Momordica grosvenori fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to triacetyl glycerine time, the loss of effective efficiency composition.
3. gained Momordica grosvenori triacetyl glycerine extract can strengthen cigarette sweet moisture feeling, to enrich nature cigarette fragrant, has soft flue gas simultaneously, reduces excitant and improves effect of pleasant impression.
4. material used herein is food-grade, has higher safety in utilization.
5. production technology of the present invention is simple, operability and normative strong, and raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
Dried fructus momordicae is carried out preliminary fragmentation, and under 70 DEG C of conditions, be dried to moisture is 8%, then is crushed to 20 object meal.Take 10 parts of Grosvenor Momordica Fruits according to weight portion and be placed in round-bottomed flask, add 100 parts of glycerol triacetate for tobacco and make extractant, soaking at room temperature is after 5 hours, refluxing extraction is carried out under 120 DEG C of conditions, extraction time is 10 hours, after being cooled to room temperature, Momordica grosvenori after refluxing extraction and triacetyl glycerine mixture are placed in ultrasonic extractor (800W, 40kHZ), extract 55 minutes, cross after filtering filter residue and obtain settled solution, required Momordica grosvenori triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, Momordica grosvenori triacetyl glycerine extract is mixed with the solution that concentration is 3%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains Momordica grosvenori active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and add the cigarette fragrance exquisiteness of above-mentioned Momordica grosvenori triacetyl glycerine extract, coordinate, there is sweet sense in oral cavity, and excitant reduces, and assorted gas and pleasant impression improve.
Embodiment 2
Dried fructus momordicae is carried out preliminary fragmentation, and under 50 DEG C of conditions, be dried to moisture is 7%, then pulverizing is 60 object meal.Take 8 parts of Grosvenor Momordica Fruits according to weight portion and be placed in round-bottomed flask, the glycerol triacetate for tobacco adding 120 parts makes extractant, soaking at room temperature is after 4 hours, refluxing extraction is carried out under 70 DEG C of conditions, extraction time is 5 hours, to be cooled to room temperature, Momordica grosvenori after refluxing extraction and triacetyl glycerine mixture are placed in ultrasonic extractor (600W, 40kHZ), extract 40 minutes, cross after filtering filter residue and obtain settled solution, required Momordica grosvenori triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, Momordica grosvenori triacetyl glycerine extract is mixed with the solution that concentration is 5%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains Momordica grosvenori active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and add the rich increase of cigarette cigarette perfume of above-mentioned Momordica grosvenori triacetyl glycerine extract, cigarette perfume is coordinated, and flue gas excitant and assorted gas reduce, and pleasant impression improves, and time sweet sense is obvious.
Embodiment 3
Dried fructus momordicae is carried out preliminary fragmentation, and under 70 DEG C of conditions, be dried to moisture is 6%, then pulverizing is 20 object meal.Take 8 parts of Grosvenor Momordica Fruits according to weight portion and be placed in round-bottomed flask, the glycerol triacetate for tobacco adding 80 parts makes extractant, soaking at room temperature is after 4 hours, refluxing extraction is carried out under 90 DEG C of conditions, extraction time is 7 hours, to be cooled to room temperature, Momordica grosvenori after refluxing extraction and triacetyl glycerine mixture are placed in ultrasonic extractor (700W, 40kHZ), extract 60 minutes, cross after filtering filter residue and obtain settled solution, required Momordica grosvenori triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, Momordica grosvenori triacetyl glycerine extract is mixed with the solution that concentration is 4%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8% and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains Momordica grosvenori active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and add the cigarette flue gas delicate fragrance of above-mentioned Momordica grosvenori triacetyl glycerine extract, harmonious, flue gas exquisiteness is soft, and excitant and assorted gas obviously reduce, and pleasant impression is clean, and sweet sense and comfort level strengthen.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a Momordica grosvenori triacetyl glycerine extract, is obtained by the method for following steps:
(1) by after dried fructus momordicae fragmentation, under 50 ~ 70 DEG C of conditions, be dried to moisture is 6 ~ 8%, then pulverizing is 20 ~ 60 object meal, for subsequent use;
(2) take 8 ~ 10 parts of Grosvenor Momordica Fruits according to weight portion and be placed in round-bottomed flask, add 80 ~ 120 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 4 ~ 6 hours, refluxing extraction is carried out under 70 ~ 120 DEG C of conditions, 5 ~ 10 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 600 ~ 800W, 40kHZ condition, extract 30 ~ 60 minutes, obtain settled solution after excessively filtering filter residue and be required Momordica grosvenori triacetyl glycerine extraction ester thing.
2. the application of Momordica grosvenori triacetyl glycerine extract according to claim 1 in cigarette, it is characterized in that: be that described Momordica grosvenori triacetyl glycerine extract is mixed with the solution that concentration is 3 ~ 5% by solvent with triacetyl glycerine, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510336402.3A CN105011368A (en) | 2015-06-17 | 2015-06-17 | Glycerol triacetate extract of momordica grosvenori and application thereof to cigarette |
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| CN201510336402.3A CN105011368A (en) | 2015-06-17 | 2015-06-17 | Glycerol triacetate extract of momordica grosvenori and application thereof to cigarette |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105614947A (en) * | 2016-03-28 | 2016-06-01 | 云南养瑞科技集团有限公司 | Filter stick additive and application thereof |
| CN109527643A (en) * | 2018-11-05 | 2019-03-29 | 广西中烟工业有限责任公司 | A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor |
| CN112075661A (en) * | 2020-09-07 | 2020-12-15 | 广西中烟工业有限责任公司 | Preparation method of persimmon leaf flavonoid cigarette filter stick |
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| CN102952635A (en) * | 2012-11-12 | 2013-03-06 | 湖北中烟工业有限责任公司 | Cigarette spice for enhancing fragrance and relaxing throat and application |
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| CN104068391A (en) * | 2014-06-05 | 2014-10-01 | 桂林三宝生物科技有限公司 | Aloe and momordica grosvenori compound capsule with high mogroside IV content |
| CN104403794A (en) * | 2014-09-24 | 2015-03-11 | 云南中烟工业有限责任公司 | Preparation method and application of Pu'er tea extract to cigarettes |
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2015
- 2015-06-17 CN CN201510336402.3A patent/CN105011368A/en active Pending
Patent Citations (6)
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| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| CN102321503A (en) * | 2011-08-30 | 2012-01-18 | 无锡华海香料有限公司 | Preparation method of fructus momordicae condensate and application thereof |
| CN102952635A (en) * | 2012-11-12 | 2013-03-06 | 湖北中烟工业有限责任公司 | Cigarette spice for enhancing fragrance and relaxing throat and application |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105614947A (en) * | 2016-03-28 | 2016-06-01 | 云南养瑞科技集团有限公司 | Filter stick additive and application thereof |
| CN109527643A (en) * | 2018-11-05 | 2019-03-29 | 广西中烟工业有限责任公司 | A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor |
| CN112075661A (en) * | 2020-09-07 | 2020-12-15 | 广西中烟工业有限责任公司 | Preparation method of persimmon leaf flavonoid cigarette filter stick |
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