CN109527643A - A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor - Google Patents
A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor Download PDFInfo
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- CN109527643A CN109527643A CN201811311811.8A CN201811311811A CN109527643A CN 109527643 A CN109527643 A CN 109527643A CN 201811311811 A CN201811311811 A CN 201811311811A CN 109527643 A CN109527643 A CN 109527643A
- Authority
- CN
- China
- Prior art keywords
- siraitia grosvenorii
- filter stick
- cigarettes
- preparation
- chicken flavor
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
Abstract
The present invention provides a kind of preparation methods of filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor, specific step is as follows: 1) crushing Siraitia grosvenorii, it impregnates, Siraitia grosvenorii volatile oil is collected with volatile oil extractor, 5-7h is extracted in distillation, and gained Siraitia grosvenorii volatile oil is extracted with ether, and extractant is dry with anhydrous sodium sulfate, it is concentrated under reduced pressure and removes solvent, obtain Siraitia grosvenorii essential oil；2) Siraitia grosvenorii essential oil is added in triacetyl glycerine, then the triacetyl glycerine added with Siraitia grosvenorii essential oil is sprayed on diacetate fiber, the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor is prepared, wherein Siraitia grosvenorii essential oil adding proportion=0.01-0.05% (mass ratio) in filter stick.Filter stick prepared by the present invention can reduce cigarette irritation and miscellaneous gas, increase perfume quantity, mitigate dry sensation, improves pleasant impression, improves sweet degree.
Description
Technical field
This patent belongs to production of cigarettes field, and in particular to a kind of preparation of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor
Method.
Background technique
Smoking is always the majority of consumers with health problem and is engaged in tobacco business staff focus of interest.Branch gas
Guan Yan is because of one of disease the most apparent caused by smoking.Siraitia grosvenorii has the function such as relieving cough and reducing sputum, clearing heat and detoxicating, clearing away heat and moistening the bowels
Effect, is usually used in treating the diseases such as tracheitis, bronchitis, asthma, sphagitis, and Siraitia grosvenorii essential oil is added in cigarette to be reduced
Harm, 1931039 A of CN brought by cigarette disclose cigarette Chinese herb feed additive, and the weight of Siraitia grosvenorii is in additive
0.2-0.3, prepared by Chinese herb feed additive can reduce disease, reduce flue gas to the pungent thorn of smoker's respiratory system
Swash.
The unique flavor of cigarette can be formed by additional flavouring essence for tobacco, promote organoleptic quality, reduction cigarette bring harm,
Especially essence spice for cigarette has been indispensable raw material in Modern cigarette industry production, and various flavors and fragrancess are added in cigarette
It is the essential process flow of major cigarette enterprise, traditional flavoring and casing mode is that flavors and fragrances is added on pipe tobacco,
Fructus Monordicae extract also has to be applied in cigarette, but Fructus Monordicae extract is also added on pipe tobacco, and is contained in extract
The macromolecular substances such as pectin, protein, fiber, these macromolecular substances can generate not cigarette quality in cigarette combustion enginnering
Benefit influences, and this patent extracts Siraitia grosvenorii volatile oil by volatile oil extractor, and Siraitia grosvenorii essential oil is added on filter stick, can
Cigarette sensory quality is adversely affected with reducing the macromolecular substances such as pectin, protein, fiber in burning.
Summary of the invention
It is an object of the invention to overcome the shortage of prior art, cigarette irritation and miscellaneous gas can be reduced by providing one kind, be increased
Flavoring tolerance mitigates dry sensation, improves pleasant impression, improves sweet degree, the preparation side of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor
Method.The present invention is achieved by the following technical scheme:
A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor, includes the following steps:
Step 1) Siraitia grosvenorii is crushed, Grosvenor Momordica Fruit is set in a round bottom flask, water is added and is impregnated, then
Under electric jacket heating, is distilled using volatile oil extractor and extract Siraitia grosvenorii volatile oil；
Step 2) Siraitia grosvenorii volatile oil is extracted, organic phase is dry with anhydrous sodium sulfate, then removing is concentrated under reduced pressure
Solvent obtains Siraitia grosvenorii essential oil；
Step 3) Siraitia grosvenorii essential oil is uniformly mixed with triacetyl glycerine；
Step 4) use the triacetyl glycerine manufacture filter stick for cigarettes for being mixed with Siraitia grosvenorii essential oil.
It is further to improve, it is 0.01-0.05% by mass fraction of the Siraitia grosvenorii essential oil in filter stick.
Further to improve, the step 1) in the water that is added be deionized water, the matter of Grosvenor Momordica Fruit and deionized water
Amount is than 1:5~6.25.
Further to improve, the step 1) in soaking time be the 12h or 10-30min under ultrasound on extracting.
Further to improve, state step 1) in electric jacket be heated to water to slightly boiled, flowed back using volatile oil extractor
Extract 5-7h.
Further to improve, the step 1) in use a small amount of washed with ether volatile oil extractor, pour into sieve that extraction obtains
In Chinese fruit volatile oil.
Further to improve, the step 2) in Siraitia grosvenorii volatile oil is extracted twice using ether, merging is twice
It is dry using anhydrous sodium sulfate after the organic phase of extraction.
Further to improve, the step 2) in it is dry for 24 hours with anhydrous sodium sulfate.
Further to improve, the step 2) in be concentrated under reduced pressure using rotary evaporator, rotary evaporator is first 30
It is concentrated at DEG C, falls behind under dripless and heating temperature is raised to 60 DEG C of removal solvents.
The beneficial effects of the invention are that: the present invention extracts Siraitia grosvenorii essence using Siraitia grosvenorii as raw material, by volatile oil extractor
Oil, and Siraitia grosvenorii essential oil is applied on filter stick for cigarettes.The Siraitia grosvenorii essential oil of extraction contains compared with traditional Fructus Monordicae extract
There are the macromolecular substances such as pectin, protein, pectin seldom, and Siraitia grosvenorii essential oil is added to reduction pectin, albumen on filter stick
The macromolecular substances such as matter, pectin are in combustion to the adverse effect of cigarette sensory quality.
Siraitia grosvenorii essential oil adds in triacetyl glycerine, then the triacetyl glycerine containing Siraitia grosvenorii essential oil is added to fibre
It ties up on tow, Siraitia grosvenorii essential oil is distributed more uniform in filter stick for cigarettes.Filter stick prepared by the present invention is reducing cigarette to human body
Harm while, additionally it is possible to reduce cigarette irritation and miscellaneous gas, increase perfume quantity, mitigate dry sensation, improve pleasant impression, improve sweet tea
Humidity promotes cigarette sensory quality.
Specific embodiment
The present invention is further explained combined with specific embodiments below.Following embodiment is only used for further tool of the invention
Body description.
Embodiment 1
Grosvenor Momordica Fruit 80g is weighed in 1000mL round-bottomed flask, 500mL deionized water is added and impregnates 12h, electric jacket adds
Heat collects Siraitia grosvenorii essential oil, refluxing extraction 5h to slightly boiled, with volatile oil extractor, and reflux terminates, and is volatilized with a small amount of washed with ether
Oil extractor, mixed liquor are collected into 50mL triangular flask, are then extracted 2 times with 30mL ether, are merged and are collected organic phase in 150mL
In triangular flask, organic phase is dry for 24 hours with anhydrous sodium sulfate, is concentrated under reduced pressure and removes solvent (Rotary Evaporators initial heating temperature is
30 DEG C, in the case where drop under no liquid, temperature is raised to 60 DEG C, keeps 15min in the case where drop under no liquid.)
Obtain Siraitia grosvenorii essential oil.
Embodiment 2
Grosvenor Momordica Fruit 90g is weighed in 1000mL round-bottomed flask, 500mL deionized water is added and impregnates 12h, electric jacket adds
Heat collects Siraitia grosvenorii essential oil to slightly boiled, with volatile oil extractor, and refluxing extraction 6h after reflux, is waved with a small amount of washed with ether
Hair oil extractor, mixed liquor are collected into 50mL triangular flask, then with 30mL ether extract 2 times, merge collect organic phase in
In 150mL triangular flask, organic phase is dry for 24 hours with anhydrous sodium sulfate, is concentrated under reduced pressure and removes solvent (Rotary Evaporators initial heating temperature
Degree is 30 DEG C, and in the case where drop under no liquid, temperature is raised to 60 DEG C, is kept in the case where drop under no liquid
15min.) obtain Siraitia grosvenorii essential oil.
Embodiment 3
Grosvenor Momordica Fruit 100g is weighed in 1000mL round-bottomed flask, 500mL deionized water is added and impregnates 12h, electric jacket
Be heated to it is slightly boiled, with volatile oil extractor collect Siraitia grosvenorii essential oil, refluxing extraction 7h, after reflux, with a small amount of washed with ether
Volatile oil extractor, mixed liquor are collected into 50mL triangular flask, then with 30mL ether extract 2 times, merge collect organic phase in
In 150mL triangular flask, organic phase is dry for 24 hours with anhydrous sodium sulfate, is concentrated under reduced pressure and removes solvent (Rotary Evaporators initial heating temperature
Degree is 30 DEG C, and in the case where drop under no liquid, temperature is raised to 60 DEG C, is kept in the case where drop under no liquid
15min.) obtain Siraitia grosvenorii essential oil.
Embodiment 4
The Siraitia grosvenorii essential oil being prepared in above-described embodiment is added in triacetyl glycerine and is stirred evenly, will be added
There is the triacetyl glycerine of Siraitia grosvenorii essential oil to be sprayed on fibre bundle, prepares the cigarette filter with Siraitia grosvenorii characteristic chicken flavor
Stick is put into spicing machine and is produced, and is prepared with Siraitia grosvenorii characteristic chicken flavor cigarette.Personnel smoke panel test according to " GB5606.4-
2005 tobaccos and tobacco product sensory evaluation method " sensory evaluating smoking is carried out, smoking result is as shown in table 1.
Influence of the 1 Siraitia grosvenorii essential oil Different adding amount of table to Sensory Quality of Cigarette
1#: conventional cigarette；2#: Siraitia grosvenorii essential oil additive amount is 0.01%；3#: Siraitia grosvenorii essential oil additive amount is 0.03%；
4# Siraitia grosvenorii essential oil additive amount is 0.05%.
From smoking result: when additive amount is 0.01% to Siraitia grosvenorii essential oil in filter stick, only irritation is declined,
Do not influence on the indices of other cigarette: when additive amount is 0.03% to Siraitia grosvenorii essential oil in filter stick, application effect is most
Good, the most obvious to cigarette quality promotion, perfume quantity increased, and irritation decreases, and pleasant impression has sweet sense, and
And there is the characteristic chicken flavor of apparent arhat.When additive amount is 0.05% to Siraitia grosvenorii essential oil in filter stick, perfume quantity be increased,
But harmony decreases.
Claims (9)
1. a kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor, which comprises the steps of:
Step 1) Siraitia grosvenorii is crushed, Grosvenor Momordica Fruit is set in a round bottom flask, water is added and is impregnated, then in electricity
Under hot jacket heating, is distilled using volatile oil extractor and extract Siraitia grosvenorii volatile oil；
Step 2) Siraitia grosvenorii volatile oil is extracted, organic phase is dry with anhydrous sodium sulfate, then be concentrated under reduced pressure remove it is molten
Agent obtains Siraitia grosvenorii essential oil；
Step 3) Siraitia grosvenorii essential oil is uniformly mixed with triacetyl glycerine；
Step 4) use the triacetyl glycerine manufacture filter stick for cigarettes for being mixed with Siraitia grosvenorii essential oil.
2. a kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor as described in claim 1, it is characterised in that
It is 0.01-0.05% by mass fraction of the Siraitia grosvenorii essential oil in filter stick.
3. a kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor as described in claim 1, it is characterised in that
The step 1) in be added water be deionized water, mass ratio 1:5~6.25 of Grosvenor Momordica Fruit and deionized water.
4. a kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor as described in claim 1, it is characterised in that
The step 1) in soaking time be the 12h or 10-30min under ultrasound on extracting.
5. a kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor as described in claim 1, it is characterised in that
The step 1) in electric jacket be heated to water to slightly boiled, use volatile oil extractor refluxing extraction 5-7h.
6. a kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor as described in claim 1, it is characterised in that
The step 1) in use a small amount of washed with ether volatile oil extractor, pour into the obtained Siraitia grosvenorii volatile oil of extraction.
7. a kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor as described in claim 1, it is characterised in that
The step 2) in Siraitia grosvenorii volatile oil is extracted twice using ether, use nothing after merging the organic phase extracted twice
Aqueous sodium persulfate is dry.
8. a kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor as described in claim 1, it is characterised in that
The step 2) in it is dry for 24 hours with anhydrous sodium sulfate.
9. a kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor as described in claim 1, it is characterised in that
The step 2) in be concentrated under reduced pressure using rotary evaporator, rotary evaporator is first concentrated at 30 DEG C, falls behind under dripless
Heating temperature is raised to 60 DEG C of removal solvents.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811311811.8A CN109527643A (en) | 2018-11-05 | 2018-11-05 | A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811311811.8A CN109527643A (en) | 2018-11-05 | 2018-11-05 | A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor |
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| CN109527643A true CN109527643A (en) | 2019-03-29 |
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| CN201811311811.8A Pending CN109527643A (en) | 2018-11-05 | 2018-11-05 | A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor |
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Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101862027A (en) * | 2010-06-07 | 2010-10-20 | 中国烟草总公司郑州烟草研究院 | Preparation method of rhododendron fastigiatum extracts and application of rhododendron fastigiatum extracts in cigarettes |
| CN102321503A (en) * | 2011-08-30 | 2012-01-18 | 无锡华海香料有限公司 | Preparation method of fructus momordicae condensate and application thereof |
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