CN105907477A - Preparation method of natural flavor - Google Patents
Preparation method of natural flavor Download PDFInfo
- Publication number
- CN105907477A CN105907477A CN201610527829.6A CN201610527829A CN105907477A CN 105907477 A CN105907477 A CN 105907477A CN 201610527829 A CN201610527829 A CN 201610527829A CN 105907477 A CN105907477 A CN 105907477A
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- China
- Prior art keywords
- extraction
- natural perfume
- ethanol
- extract
- preparation
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a preparation method of a natural flavor. The method comprises a raw material pretreatment step of crushing raw materials into 20-40-mesh particles; and the ratio of the raw materials, namely momordica grosvenori to gynostemma pentaphylla to maca is 1 to (1.4-1.8) to (2.2-2.6). Microwave assisted extraction is adopted; and the microwave radiation process is the process that a high-frequency electromagnetic wave penetrates through an extraction medium to reach the inside of the material. Microwave energy is absorbed, so that the temperature in cells rapidly rises, the pressure in the cells exceeds the sustainable pressure for cell walls for expansion, the cells are broken, effective ingredients in the cells freely flow out and are dissolved into the extraction medium at a relatively low temperature, thermosensitive substances are well protected, the extraction time of microwave extraction is very short, and the extraction efficiency is greatly improved. The produced natural flavor is fruity, harmonious, pure and elegant in fragrance, and abundant in fragrance; the problems that a tobacco product is light in smoke and insufficient in fragrance due to the adoption of a method for reducing harmful components in the smoke can be effectively solved; the quality of a cigarette product can also be improved; and the aftertaste is comfortable, sweet and soft.
Description
Technical field
The present invention relates to active ingredients of plants extraction and separation technology field, the preparation method of a kind of natural perfume material.
Background technology
Along with improving constantly of social civilization level, the health perception of people is increasingly stronger, and medicated cigarette is as a kind of special hobby
Product, not only Yao Shi consumer enjoys the enjoyment of smoking, and to reduce the harm to health, therefore reduces medicated cigarette danger
The needs that evil not only tobacco business develops in a healthy way, the demand of consumer's interests especially.
Owing to consumer is more and more higher to the requirement of tobacco product quality, compared with the requirement of consumer, all kinds of tobacco products are also
There is defect in various degree, as the most plentiful in product perfume quantity shortcoming, odor characteristic is notable, mouthfeel, pleasant impression etc. are uncomfortable.
On the other hand, reducing tar and reducing harm has become the direction that domestic and international tobacco product develops, and along with the enforcement of reducing tar and reducing harm technology, in fall
While low smoking is to the harm of human body, also resulting in tobacco product smoke and die down, fragrance is thin out, and product loses original wind
Lattice, it is difficult to accepted by consumer.Interpolation essence and flavoring agent is just had higher requirement by this.
Summary of the invention
It is an object of the invention to provide the preparation method of a kind of natural perfume material, with solve in above-mentioned background technology propose ask
Topic.
For achieving the above object, the present invention provides following technical scheme:
The preparation method of a kind of natural perfume material, it specifically comprises the following steps that
(1) pretreatment of raw material: raw material powder is broken into the granule of 20～40 mesh；
(2) extraction: by raw material according to ratio add in microwave extracting machine, add material quantity 8～the deionized water of 10 times,
Microwave power 300～400 watts, extraction time 6～8 minutes, cross 200～400 mesh filter screens and release extracts, the most again to extraction
Machine adds the deionized water of 6～8 times, microwave power 300～400 watts, extraction time 2～4 minutes, crosses 200～400 mesh filters
Extract released by net；
(3) extract concentrating under reduced pressure: by extract concentrating under reduced pressure in a rotary evaporator, bath temperature 60～65 DEG C, vacuum
Between degree 0.085～0.090Mpa, the concentrate obtained is the 290 ‰～300 ‰ of raw materials quality；
(4) extract concentrated solution precipitate with ethanol: add the ethanol of 88%～90% under stirring in extraction concentrated solution so that precipitate with ethanol
The proportion of liquid is 0.9050～0.9130, continues stirring 60～90 minutes, precipitate with ethanol 32～40h after adding；
(5) alcohol deposit fluid filter centrifugation: take out alcohol deposit fluid supernatant, turbid solution machine by centrifugation in bottom is centrifuged；
(6) precipitate with ethanol clear liquid concentrating under reduced pressure: by sucking filtration clear liquid and centrifugal clear liquid concentrating under reduced pressure in a rotary evaporator, water-bath temperature
Spending 55～65 DEG C, between vacuum 0.088～0.092Mpa, the concentrate obtained is put into raw materials quality 29.3%～30.8%,
It is natural perfume material.
As the further scheme of the present invention: the raw material in described step (1) includes Fructus Momordicae, Herb Gynostemmae Pentaphylli and Maca.
As the further scheme of the present invention: described Fructus Momordicae: Herb Gynostemmae Pentaphylli: Maca=1:1.4～1.8:2.2～2.6.
As the further scheme of the present invention: in described step (5), centrifuge speed is 3000～4000 rev/min, from
Heart time 15～25 minutes.
As the present invention further scheme: the application of described natural perfume material: in the ratio of 7～the 10 ‰ of tobacco shred weight,
Mixed extract is sprayed on tobacco shred equably, and rolls into the suction of cigarette product.
Compared with prior art, the invention has the beneficial effects as follows: using microwave radiation exaraction, microwave radiation process is high-frequency electrical
Magnetic wave penetrates spe medium and arrives the process within material, and owing to absorbing microwave energy, the temperature of cell interior rises rapidly,
The pressure making cell interior exceedes the ability that cell wall expansion can bear, and makes cell rupture, and its interior effective ingredient is freely
Flow out, and be dissolved at a lower temperature in spe medium, protect heat-sensitive substance well, the extraction of microwave extracting
Time is the shortest, substantially increases extraction efficiency；Precipitate with ethanol can remove impurity invalid in extract, makes effective one-tenth of extract
Divide content height, the purer harmony of fragrance；During concentrating under reduced pressure, operation temperature, less than 65 DEG C, can protect extract well
In thermal sensitivity flavor matter, prevent its oxidation Decomposition at high temperature；The present invention produce the mellow and full harmony of natural perfume material fragrance,
Pure quiet and tastefully laid out, fragrance enriches, and the tobacco product smoke that can not only effectively solve to cause because taking reducing tar and reducing harm is light, perfume quantity
Not enough problem, moreover it is possible to improve cigarette product quality, make pleasant impression comfortable, sweet soft, reduce and stimulate, improve oral cavity and moisten
Degree.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, aobvious
So, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, raw material: Fructus Momordicae: Herb Gynostemmae Pentaphylli: Maca=1:1.4:2.2.
The preparation method of described natural perfume material, it specifically comprises the following steps that
(1) pretreatment of raw material: raw material powder is broken into the granule of 20 mesh；
(2) extraction: by raw material according to ratio add in microwave extracting machine, add the deionized water of material quantity 8 times,
Microwave power 300 watts, extraction time 6 minutes, cross 200 mesh filter screens and release extract, in extracter, add 6 the most again
Deionized water again, microwave power 300 watts, extraction time 2 minutes, cross 200 mesh filter screens and release extracts；
(3) extract concentrating under reduced pressure: by extract concentrating under reduced pressure in a rotary evaporator, bath temperature 60 DEG C, vacuum
Between 0.085Mpa, the concentrate obtained is the 290 ‰ of raw materials quality；
(4) extract concentrated solution precipitate with ethanol: add the ethanol of 88% under stirring in extraction concentrated solution so that alcohol deposit fluid
Proportion is 0.9050, continues stirring 60 minutes, precipitate with ethanol 32h after adding；
(5) alcohol deposit fluid filter centrifugation: taking out alcohol deposit fluid supernatant, turbid solution machine by centrifugation in bottom is centrifuged (centrifuge speed
3000 rev/min, centrifugation time 15 minutes)；
(6) precipitate with ethanol clear liquid concentrating under reduced pressure: by sucking filtration clear liquid and centrifugal clear liquid concentrating under reduced pressure in a rotary evaporator, water-bath temperature
Spending 55 DEG C, between vacuum 0.088Mpa, the concentrate obtained is put into raw materials quality 29.3%, is natural perfume material；
(7) application of natural perfume material: in the ratio of the 7 ‰ of tobacco shred weight, mixed extract is sprayed on tobacco shred equably,
And roll into the suction of cigarette product.
Embodiment 2
In the embodiment of the present invention, raw material: Fructus Momordicae: Herb Gynostemmae Pentaphylli: Maca=1:1.6:2.4.
The preparation method of described natural perfume material, it specifically comprises the following steps that
(1) pretreatment of raw material: raw material powder is broken into the granule of 30 mesh；
(2) extraction: by raw material according to ratio add in microwave extracting machine, add the deionized water of material quantity 9 times,
Microwave power 350 watts, extraction time 7 minutes, cross 300 mesh filter screens and release extract, in extracter, add 7 the most again
Deionized water again, microwave power 350 watts, extraction time 3 minutes, cross 300 mesh filter screens and release extracts；
(3) extract concentrating under reduced pressure: by extract concentrating under reduced pressure in a rotary evaporator, bath temperature 62.5 DEG C, vacuum
Between degree 0.0875Mpa, the concentrate obtained is the 295 ‰ of raw materials quality；
(4) extract concentrated solution precipitate with ethanol: add the ethanol of 89% under stirring in extraction concentrated solution so that alcohol deposit fluid
Proportion is 0.9090, continues stirring 70 minutes, precipitate with ethanol 36h after adding；
(5) alcohol deposit fluid filter centrifugation: taking out alcohol deposit fluid supernatant, turbid solution machine by centrifugation in bottom is centrifuged (centrifuge speed
3500 rev/min, centrifugation time 20 minutes)；
(6) precipitate with ethanol clear liquid concentrating under reduced pressure: by sucking filtration clear liquid and centrifugal clear liquid concentrating under reduced pressure in a rotary evaporator, water-bath temperature
Spending 60 DEG C, between vacuum 0.090Mpa, the concentrate obtained is put into raw materials quality 30.05%, is natural perfume material；
(7) application of natural perfume material: in the ratio of the 8.5 ‰ of tobacco shred weight, is sprayed at tobacco shred equably by mixed extract
On, and roll into the suction of cigarette product.
Embodiment 3
In the embodiment of the present invention, raw material: Fructus Momordicae: Herb Gynostemmae Pentaphylli: Maca=1:1.8:2.6.
The preparation method of described natural perfume material, it specifically comprises the following steps that
(1) pretreatment of raw material: raw material powder is broken into the granule of 40 mesh；
(2) extraction: by raw material according to ratio add in microwave extracting machine, add the deionized water of material quantity 10 times,
Microwave power 400 watts, extraction time 8 minutes, cross 400 mesh filter screens and release extract, in extracter, add 8 the most again
Deionized water again, microwave power 400 watts, extraction time 4 minutes, cross 400 mesh filter screens and release extracts；
(3) extract concentrating under reduced pressure: by extract concentrating under reduced pressure in a rotary evaporator, bath temperature 65 DEG C, vacuum
Between 0.090Mpa, the concentrate obtained is the 300 ‰ of raw materials quality；
(4) extract concentrated solution precipitate with ethanol: add the ethanol of 90% under stirring in extraction concentrated solution so that alcohol deposit fluid
Proportion is 0.9130, continues stirring 90 minutes, precipitate with ethanol 40h after adding；
(5) alcohol deposit fluid filter centrifugation: taking out alcohol deposit fluid supernatant, turbid solution machine by centrifugation in bottom is centrifuged (centrifuge speed
4000 rev/min, centrifugation time 25 minutes)；
(6) precipitate with ethanol clear liquid concentrating under reduced pressure: by sucking filtration clear liquid and centrifugal clear liquid concentrating under reduced pressure in a rotary evaporator, water-bath temperature
Spending 65 DEG C, between vacuum 0.092Mpa, the concentrate obtained is put into raw materials quality 30.8%, is natural perfume material；
(7) application of natural perfume material: in the ratio of the 10 ‰ of tobacco shred weight, is sprayed at tobacco shred equably by mixed extract
On, and roll into the suction of cigarette product.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and do not carrying on the back
In the case of the spirit or essential attributes of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter from
From the point of view of which point, all should regard embodiment as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all by fall in the implication of equivalency and scope of claim
Change is included in the present invention.
Although moreover, it will be appreciated that this specification is been described by according to embodiment, but the most each embodiment only comprises
One independent technical scheme, this narrating mode of description is only the most for clarity sake, and those skilled in the art should be by
Description is as an entirety, and the technical scheme in each embodiment can also be through appropriately combined, and forming those skilled in the art can
With other embodiments understood.
Claims (5)
1. the preparation method of a natural perfume material, it is characterised in that it specifically comprises the following steps that
(1) pretreatment of raw material: raw material powder is broken into the granule of 20～40 mesh；
(2) extraction: by raw material according to ratio add in microwave extracting machine, add material quantity 8～the deionized water of 10 times,
Microwave power 300～400 watts, extraction time 6～8 minutes, cross 200～400 mesh filter screens and release extracts, the most again to extraction
Machine adds the deionized water of 6～8 times, microwave power 300～400 watts, extraction time 2～4 minutes, crosses 200～400 mesh filters
Extract released by net；
(3) extract concentrating under reduced pressure: by extract concentrating under reduced pressure in a rotary evaporator, bath temperature 60～65 DEG C, vacuum
Between degree 0.085～0.090Mpa, the concentrate obtained is the 290 ‰～300 ‰ of raw materials quality；
(4) extract concentrated solution precipitate with ethanol: add the ethanol of 88%～90% under stirring in extraction concentrated solution so that precipitate with ethanol
The proportion of liquid is 0.9050～0.9130, continues stirring 60～90 minutes, precipitate with ethanol 32～40h after adding；
(5) alcohol deposit fluid filter centrifugation: take out alcohol deposit fluid supernatant, turbid solution machine by centrifugation in bottom is centrifuged；
(6) precipitate with ethanol clear liquid concentrating under reduced pressure: by sucking filtration clear liquid and centrifugal clear liquid concentrating under reduced pressure in a rotary evaporator, water-bath temperature
Spending 55～65 DEG C, between vacuum 0.088～0.092Mpa, the concentrate obtained is put into raw materials quality 29.3%～30.8%,
It is natural perfume material.
The preparation method of natural perfume material the most according to claim 1, it is characterised in that former in described step (1)
Material includes Fructus Momordicae, Herb Gynostemmae Pentaphylli and Maca.
The preparation method of natural perfume material the most according to claim 2, it is characterised in that described Fructus Momordicae: Herb Gynostemmae Pentaphylli:
Maca=1:1.4～1.8:2.2～2.6.
The preparation method of natural perfume material the most according to claim 1, it is characterised in that centrifugal in described step (5)
Machine rotating speed is 3000～4000 rev/min, centrifugation time 15～25 minutes.
Natural perfume material the most according to claim 1, it is characterised in that the application of described natural perfume material: by tobacco shred weight
The ratio of 7～the 10 ‰ of amount, is sprayed on tobacco shred equably by mixed extract, and rolls into the suction of cigarette product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610527829.6A CN105907477A (en) | 2016-07-06 | 2016-07-06 | Preparation method of natural flavor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610527829.6A CN105907477A (en) | 2016-07-06 | 2016-07-06 | Preparation method of natural flavor |
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| Publication Number | Publication Date |
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| CN105907477A true CN105907477A (en) | 2016-08-31 |
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ID=56754498
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610527829.6A Pending CN105907477A (en) | 2016-07-06 | 2016-07-06 | Preparation method of natural flavor |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109222213A (en) * | 2018-08-03 | 2019-01-18 | 云南瑞升烟草技术（集团）有限公司 | The green Extraction and enrichment and isolation and purification method of neophytadiene in a kind of tobacco material |
| CN109527643A (en) * | 2018-11-05 | 2019-03-29 | 广西中烟工业有限责任公司 | A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101928640A (en) * | 2010-09-16 | 2010-12-29 | 无锡华海香料有限公司 | Method for extracting natural perfume and application of extract |
| CN102321503A (en) * | 2011-08-30 | 2012-01-18 | 无锡华海香料有限公司 | Preparation method of fructus momordicae condensate and application thereof |
| CN102526295A (en) * | 2012-03-07 | 2012-07-04 | 江南大学 | Method for comprehensively utilizing dried orange peel |
| CN103396888A (en) * | 2013-08-09 | 2013-11-20 | 湖北中烟工业有限责任公司 | Preparation method of corn stigma extract for cigarettes |
-
2016
- 2016-07-06 CN CN201610527829.6A patent/CN105907477A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101928640A (en) * | 2010-09-16 | 2010-12-29 | 无锡华海香料有限公司 | Method for extracting natural perfume and application of extract |
| CN102321503A (en) * | 2011-08-30 | 2012-01-18 | 无锡华海香料有限公司 | Preparation method of fructus momordicae condensate and application thereof |
| CN102526295A (en) * | 2012-03-07 | 2012-07-04 | 江南大学 | Method for comprehensively utilizing dried orange peel |
| CN103396888A (en) * | 2013-08-09 | 2013-11-20 | 湖北中烟工业有限责任公司 | Preparation method of corn stigma extract for cigarettes |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109222213A (en) * | 2018-08-03 | 2019-01-18 | 云南瑞升烟草技术（集团）有限公司 | The green Extraction and enrichment and isolation and purification method of neophytadiene in a kind of tobacco material |
| CN109222213B (en) * | 2018-08-03 | 2021-08-20 | 云南瑞升烟草技术（集团）有限公司 | Green extraction, enrichment, separation and purification method of neophytadiene in tobacco raw material |
| CN109527643A (en) * | 2018-11-05 | 2019-03-29 | 广西中烟工业有限责任公司 | A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor |
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Application publication date: 20160831 |
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