CN106221935A - The preparation method of a kind of Pericarpium Citri Reticulatae absolute oil and the application in Medicated cigarette thereof - Google Patents
The preparation method of a kind of Pericarpium Citri Reticulatae absolute oil and the application in Medicated cigarette thereof Download PDFInfo
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- CN106221935A CN106221935A CN201610732174.6A CN201610732174A CN106221935A CN 106221935 A CN106221935 A CN 106221935A CN 201610732174 A CN201610732174 A CN 201610732174A CN 106221935 A CN106221935 A CN 106221935A
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- pericarpium citri
- citri reticulatae
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
Abstract
The present invention discloses the preparation method of a kind of Pericarpium Citri Reticulatae absolute oil, size-reduced Pericarpium Citri Reticulatae, fermentation Pericarpium Citri Reticulatae, extraction Pericarpium Citri Reticulatae, extracts and filters, concentrates, precipitate with ethanol, is concentrated to give Pericarpium Citri Reticulatae absolute oil.The flavonoids such as Hesperidin in gained Pericarpium Citri Reticulatae absolute oil of the present invention, Nobiletin, Pericarpium Citri tangerinae element, the volatile oil content such as limonene is higher, effectively maintains the peculiar fragrance of Pericarpium Citri Reticulatae so that it is be applied to natural flavor in Medicated cigarette apparent.And the range of application of absolute oil can be more extensive, solving state and the dissolubility of Pericarpium Citri Reticulatae extract, absolute oil can preferably be applied in Medicated cigarette.Reparation technology is simple, workable, makes whole production process efficient, is suitable to industrializing implementation.On the other hand, Pericarpium Citri Reticulatae absolute oil the inventive method prepared is applied in Medicated cigarette, can improve the mouthfeel pleasant impression of cigarette smoking, gives the natural flavor that Medicated cigarette is special, promotes flue gas quality.
Description
Technical field
The present invention relates to plant extract and applied technical field thereof, particularly relate to a kind of Pericarpium Citri Reticulatae absolute oil preparation method and
Its application in Medicated cigarette.
Background technology
Pericarpium Citri Reticulatae, Chinese medicine name.It is again Pericarpium Citri tangerinae, expensive old, Folium Styracis Suberifoliae, Fructus Citri tangerinae skin, wide Pericarpium Citri tangerinae, Pericarpium Citri tangerinae, Citrus chachiensis Hort. C. Suavissima Tanaka, Pericarpium citri reticuatae chachiensis.It it is rue
Savoury herb Fructus Citri tangerinae and the mature peel of variety thereof, take fruit, strip peel, dries in the shade or aeration-drying.Peel is with old person
Good, therefore named.Pericarpium Citri Reticulatae acrid in the mouth is bitter, warm in nature, has effect of warming stomach for dispelling cold, regulating qi-flowing for strengthening spleen, is suitable for stomach distension, dyspepsia, food
The people being intended to the symptoms such as depressed, cough ant phlegm eats.
Pericarpium Citri Reticulatae has appetizing of regulating the flow of vital energy, drying dampness to eliminate phlegm, controls effect of the spleen-stomach disease.Because Pericarpium Citri Reticulatae contains limonoid, this
Limonoid taste is gentle, is easily soluble in water, additionally, Pericarpium Citri Reticulatae contains the compositions such as volatile oil, hesperidin, vitamin B, C, contained by it
Volatile oil gastrointestinal tract is had gentle stimulation, can the secretion of facilitating digestion liquid, get rid of pneumatosis in intestinal tube.Pericarpium Citri Reticulatae is the most normal
With Chinese medicine, there is ventilation spleen invigorating, drying dampness to eliminate phlegm, the greasy lasting of solution, effect of stopping nausea and vomiting by lowering the adverse flow of QI.It is suitable for stomach distension, dyspepsia, food
The people being intended to the symptoms such as depressed, cough ant phlegm eats.
In recent years, for the extraction of effective ingredient in Pericarpium Citri Reticulatae, microwave extracting, ultrasonic extraction, conventional returning occur
The technology such as stream extraction produce Pericarpium Citri Reticulatae extractum, and result shows, its yield of Pericarpium Citri Reticulatae extractum is higher, but ultrasonic extraction, microwave extracting skill
Art produces Pericarpium Citri Reticulatae extractum, the heat-sensitive substance being easily destroyed in Pericarpium Citri Reticulatae, causes this perfume (or spice) of Pericarpium Citri Reticulatae impaired, reduces Pericarpium Citri Reticulatae extractum quality.
And Pericarpium Citri Reticulatae extractum is vulnerable to the impact of extractum state, dissolubility etc., it is limited in scope in application process.At present for Pericarpium Citri Reticulatae has
The extraction of effect composition, mainly carries with water in traditional handicraft, alcohol extraction, and the process of reconcentration obtains.The method is the longest, and easily
Destroy the aroma component in Pericarpium Citri Reticulatae, owing to Pericarpium Citri Reticulatae containing a large amount of pectin, cellulose etc., make the flavonoid in Pericarpium Citri Reticulatae, volatile oil
Class can not get fully extracting, and makes quality reduce.
In order to expand the range of application of Pericarpium Citri Reticulatae extract, promoting the added value of Pericarpium Citri Reticulatae, research worker makes great efforts to change always simultaneously
Enter technique, to obtain the Pericarpium Citri Reticulatae extract of high this perfume (or spice) of Pericarpium Citri Reticulatae.On the other hand, present stage, because the pharmacological action of Pericarpium Citri Reticulatae, domestic have
The applied research closing Pericarpium Citri Reticulatae is concentrated mainly on medicines and health protection field, and application in other respects is less, and the application on Medicated cigarette
The most less.
Summary of the invention
For solving above-mentioned the deficiencies in the prior art, the present invention provides the preparation method of a kind of Pericarpium Citri Reticulatae absolute oil and in Medicated cigarette
Application, the Pericarpium Citri Reticulatae absolute oil of high this perfume of Pericarpium Citri Reticulatae, high added value can be obtained to greatest extent；The Pericarpium Citri Reticulatae extract obtained is applied to
In Medicated cigarette, the interior quality of Medicated cigarette can be improved.
The present invention is realized by following technical proposal: the preparation method of a kind of Pericarpium Citri Reticulatae absolute oil, through following each step:
(1) Pericarpium Citri Reticulatae is pulverized: pulverize dry Pericarpium Citri Reticulatae for Pericarpium Citri Reticulatae grain；
(2) fermentation Pericarpium Citri Reticulatae: 0.1～5% by Pericarpium Citri Reticulatae grain quality take pectase, by 0.1～5% extracting cellulose of Pericarpium Citri Reticulatae grain quality
Enzyme；Step (1) gained Pericarpium Citri Reticulatae grain is placed in the environment of constant temperature and humidity, then adds pectase in material spray mode and cellulase enters
Row fermentation 1～10 day, turning in every 1～2 day once, makes the pectin in Pericarpium Citri Reticulatae and cellulose fully decompose；
(3) extraction Pericarpium Citri Reticulatae: the petroleum ether mixing adding 2～15 times of volumes in the Pericarpium Citri Reticulatae grain after step (2) gained ferments stirs evenly,
Obtain mixed material；
(4) extract and filter: step (3) gained mixed material be heated at 30～150 DEG C and be incubated 0.5～12h, then passing through
Filter obtains lixiviating solution；
(5) concentrate: step (5) gained lixiviating solution, through being evaporated to extractum, is obtained extract；
(6) precipitate with ethanol: in the extract obtained middle addition 1 of step (5)～the ethanol of 30 times of volumes, seal the most afterwards, then 0
～at-50 DEG C, stand 0.5～48h, obtain mixed liquor；
(7) concentrate: step (6) gained mixed liquor is carried out sucking filtration, concentrates filtrate to oily, obtain Pericarpium Citri Reticulatae absolute oil.
The Pericarpium Citri Reticulatae water content of described step (1) is 7～20%.
The granularity of described step (1) Pericarpium Citri Reticulatae grain is 0.1～5mm.
In described step (2) constant temperature and humidity be temperature be 30～60 DEG C, humidity be 60～90%.
The filtration of described step (4) is that the filter screen using 10～1000 mesh filters.
In described step (5) and (7), the vacuum pressure of concentrating under reduced pressure is 0.01～0.1MPa.
In described step (6), concentration of alcohol is 70v/v%～dehydrated alcohol.
The application in Medicated cigarette of the above-mentioned gained Pericarpium Citri Reticulatae absolute oil, individually prepares described Pericarpium Citri Reticulatae absolute oil or allocates conventional tobacco into
In spice, it is sprayed in tobacco in the way of perfuming or charging.
It is Pericarpium Citri Reticulatae absolute oil nontoxic non-stimulated solvent dilution 2～100 times to be allocated that described Pericarpium Citri Reticulatae absolute oil is individually prepared
Liquid.
Described solvent is one or any several in ethanol, propylene glycol, sorbitol, xylitol and glycerol.
Described ethanol, propylene glycol, sorbitol, xylitol and glycerol are commercial analytical pure.
Described sprinkling is by tobacco quality 0.01～2% to be sprayed in tobacco by seasoning liquid.
The present invention is compared with the prior art and provides the benefit that: although the backflow of microwave extracting, ultrasonic extraction and routine
Extracting the Pericarpium Citri Reticulatae yield of extract prepared high, active constituent content is the highest, but ultrasonic extraction, microwave-assisted extraction technique produce Pericarpium Citri Reticulatae leaching
Cream, the heat-sensitive substance in destructible Pericarpium Citri Reticulatae, cause this perfume (or spice) of Pericarpium Citri Reticulatae impaired, reduce Pericarpium Citri Reticulatae extract quality, and Pericarpium Citri Reticulatae extractum is attached
Value added the highest.In Pericarpium Citri Reticulatae, the main aroma component of fragrance is volatile oil, the highest with limonene content again in volatile oil, but lemon
Lemon alkene is volatile, easily decompose, and easily loses during extracting.The present invention carries out fermentation process to Pericarpium Citri Reticulatae, certain by adding
The pectase of ratio, cellulase ferment Pericarpium Citri Reticulatae under the conditions of constant temperature and humidity, fully decompose the unfavorable composition in Pericarpium Citri Reticulatae, make Pericarpium Citri Reticulatae
In effective aroma component leach to greatest extent.In conjunction with petroleum ether as solvent extraction Pericarpium Citri Reticulatae absolute oil, directly absolute oil is separated
Out, extracting efficiency is high, obtains the absolute oil of high added value, it is to avoid microwave, the ultrasound wave destruction to Pericarpium Citri Reticulatae, carries to greatest extent
Rise the quality of Pericarpium Citri Reticulatae extract.The flavonoids such as Hesperidin in gained Pericarpium Citri Reticulatae absolute oil of the present invention, Nobiletin, Pericarpium Citri tangerinae element, limonene
Higher Deng volatile oil content, effectively maintain the peculiar fragrance of Pericarpium Citri Reticulatae so that it is be applied to natural flavor in Medicated cigarette apparent.
And the range of application of absolute oil can be more extensive, solving state and the dissolubility of Pericarpium Citri Reticulatae extract, absolute oil can preferably be applied to
In Medicated cigarette.Organic solvent extraction Pericarpium Citri Reticulatae absolute oil, compensate for microwave, ultrasound wave, the deficiency of normal reflux extraction, it is ensured that Pericarpium Citri Reticulatae extracts
Article matter.The preparation method of Pericarpium Citri Reticulatae absolute oil of the present invention, in addition to using petroleum ether, water and ethanol, carries out auxiliary without other reagent
Helping extraction, reparation technology is simple, workable, makes whole production process efficient, is suitable to industrializing implementation.On the other hand, will
The Pericarpium Citri Reticulatae absolute oil that the inventive method prepares is applied in Medicated cigarette, can improve the mouthfeel pleasant impression of cigarette smoking, gives Medicated cigarette special
Different natural flavor, promotes flue gas quality.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the present invention is described in further details.But they are not the limit to the present invention
Fixed.
Embodiment 1
(1) Pericarpium Citri Reticulatae is pulverized: the tangerine peel powder that water content is 10% is broken to the Pericarpium Citri Reticulatae grain that granularity is 5mm；
(2) fermentation Pericarpium Citri Reticulatae: take pectase by the 1.5% of Pericarpium Citri Reticulatae grain quality, by 1.5% extracting cellulose enzyme of Pericarpium Citri Reticulatae grain quality；Will step
Suddenly (1) gained Pericarpium Citri Reticulatae grain be placed in temperature be 301 DEG C, humidity be 65% the environment of constant temperature and humidity in, then add fruit in material spray mode
Glue enzyme and cellulase carry out fermenting 3 days, and turning in every 1～2 day once, makes the pectin in Pericarpium Citri Reticulatae and cellulose fully decompose；
(3) extraction Pericarpium Citri Reticulatae: the petroleum ether mixing adding 10 times of volumes in the Pericarpium Citri Reticulatae grain after step (2) gained ferments stirs evenly,
To mixed material；
(4) extract and filter: step (3) gained mixed material being heated at 100 DEG C and be incubated 5h, then uses the filter of 100 mesh
Net carries out being filtrated to get lixiviating solution；
(5) concentrate: by step (5) gained lixiviating solution through vacuum pressure be 0.06MPa be evaporated to extractum, extracted
Thing；
(6) precipitate with ethanol: the concentration in the extract obtained middle 20 times of volumes of addition of step (5) is 80v/v% ethanol, by evenly mixing after
Seal, then at-30 DEG C, stand 24h, obtain mixed liquor；
(7) concentrate: step (6) gained mixed liquor is carried out sucking filtration, concentrates filtrate to oily, obtain Pericarpium Citri Reticulatae absolute oil.
Above-mentioned gained Pericarpium Citri Reticulatae absolute oil ethanol dilution 5 obtains seasoning liquid, again by the 0.1% of tobacco quality by seasoning liquid
It is sprayed in tobacco.
Embodiment 2
(1) Pericarpium Citri Reticulatae is pulverized: the tangerine peel powder that water content is 20% is broken to the Pericarpium Citri Reticulatae grain that granularity is 4mm；
(2) fermentation Pericarpium Citri Reticulatae: take pectase by the 5% of Pericarpium Citri Reticulatae grain quality, by 5% extracting cellulose enzyme of Pericarpium Citri Reticulatae grain quality；By step (1)
Gained Pericarpium Citri Reticulatae grain be placed in temperature be 40 DEG C, humidity be 90% the environment of constant temperature and humidity in, then with material spray mode add pectase and
Cellulase carries out fermenting 10 days, and turning in every 1～2 day once, makes the pectin in Pericarpium Citri Reticulatae and cellulose fully decompose；
(3) extraction Pericarpium Citri Reticulatae: the petroleum ether mixing adding 2 times of volumes in the Pericarpium Citri Reticulatae grain after step (2) gained ferments stirs evenly, and obtains
Mixed material；
(4) extract and filter: step (3) gained mixed material being heated at 30 DEG C and be incubated 12h, then uses the filter screen of 10 mesh
Carry out being filtrated to get lixiviating solution；
(5) concentrate: by step (5) gained lixiviating solution through vacuum pressure be 0.01MPa be evaporated to extractum, extracted
Thing；
(6) precipitate with ethanol: the concentration in the extract obtained middle 1 times of volume of addition of step (5) is 70v/v% ethanol, rear close by evenly mixing
Envelope, then at 0 DEG C, stand 0.5h, obtain mixed liquor；
(7) concentrate: step (6) gained mixed liquor is carried out sucking filtration, concentrates filtrate to oily, obtain Pericarpium Citri Reticulatae absolute oil.
Above-mentioned gained Pericarpium Citri Reticulatae absolute oil propylene glycol and sorbitol dilute 2 times and obtain seasoning liquid, by tobacco quality
Seasoning liquid is sprayed in tobacco by 0.01%.
Embodiment 3
(1) Pericarpium Citri Reticulatae is pulverized: the tangerine peel powder that water content is 7% is broken to the Pericarpium Citri Reticulatae grain that granularity is 0.1mm；
(2) fermentation Pericarpium Citri Reticulatae: take pectase by the 0.1% of Pericarpium Citri Reticulatae grain quality, by 0.1% extracting cellulose enzyme of Pericarpium Citri Reticulatae grain quality；Will step
Suddenly (1) gained Pericarpium Citri Reticulatae grain be placed in temperature be 60 DEG C, humidity be 60% the environment of constant temperature and humidity in, then add fruit in material spray mode
Glue enzyme and cellulase carry out fermenting 1 day, and turning in every 1～2 day once, makes the pectin in Pericarpium Citri Reticulatae and cellulose fully decompose；
(3) extraction Pericarpium Citri Reticulatae: the petroleum ether mixing adding 15 times of volumes in the Pericarpium Citri Reticulatae grain after step (2) gained ferments stirs evenly,
To mixed material；
(4) extract and filter: step (3) gained mixed material being heated at 150 DEG C and be incubated 0.5h, then uses 1000 purposes
Filter screen carries out being filtrated to get lixiviating solution；
(5) concentrate: by step (5) gained lixiviating solution through vacuum pressure be 0.1MPa be evaporated to extractum, obtain extract；
(6) precipitate with ethanol: the concentration in the extract obtained middle 30 times of volumes of addition of step (5) is dehydrated alcohol, rear close by evenly mixing
Envelope, then at-50 DEG C, stand 48h, obtain mixed liquor；
(7) concentrate: step (6) gained mixed liquor is carried out sucking filtration, concentrates filtrate to oily, obtain Pericarpium Citri Reticulatae absolute oil.
Above-mentioned gained Pericarpium Citri Reticulatae absolute oil allocates conventional tobacco spice (such as pure tobacco oil) middle xylitol into and glycerol dilutes 100 times
Obtain seasoning liquid, by the 2% of tobacco quality, seasoning liquid is sprayed in tobacco.
Contrast below by main component in gained CHENPI DING of the present invention and the sensory evaluating smoking in Medicated cigarette, illustrate this
The advantage of bright relatively other technologies scheme.
Comparative example 1: take Pericarpium Citri Reticulatae raw material same as in Example 1, CHENPI DING is obtained by extraction with conventional microwave, solvent is second
Alcohol；Microwave extracting power is 500W, and the time is 2h.Solvent is petroleum ether.
Comparative example 2: take Pericarpium Citri Reticulatae raw material same as in Example 1, CHENPI DING is obtained by extraction with conventional ultrasound, solvent is second
Alcohol；Ultrasonic extraction power is 500W, and the time is 2h, carries out at normal temperatures and pressures.Solvent is petroleum ether.
Comparative example 3: take Pericarpium Citri Reticulatae raw material same as in Example 1, extracts with normal reflux and obtains CHENPI DING, and solvent is second
Alcohol, extraction time is 2h.Solvent is petroleum ether.
Comparative example 4: with embodiment 1, only omits step (2).
By examples detailed above 1,2,3 and comparative example 1,2,3,4 gained Pericarpium Citri Reticulatae extract, all with propylene glycol solution (analytical pure)
Being diluted to 100 times, be then sprayed at blank (non-flavoring and casing) the flue-cured tobacco tobacco shred surface of same, addition is tobacco shred weight
1%.Simultaneously with do not spray CHENPI DING flue-cured tobacco tobacco shred for blank sample, subsequent treatment cigarette process routinely is carried out, and is i.e. spraying
After the diluent of CHENPI DING, by flue-cured tobacco tobacco storage 4 hours, then through shredding, dry silk, perfuming, storage silk, cigarette and packaging process
Making cigarette finished product, the group of smokeing panel test being made up of 7 people carries out contrast to above-mentioned sample respectively and smokes panel test, with fragrance, coordination, miscellaneous QI,
Zest and five indexs of pleasant impression, carry out sensory quality assessment, and result see table.
As can be known from the above table, although the reflux, extract, yield of microwave extracting, ultrasonic extraction and routine is higher, but to Pericarpium Citri Reticulatae
In extract, effective aroma component destroys relatively big, especially the heat-sensitive substance such as volatile oil, this perfume in heavy losses Pericarpium Citri Reticulatae,
Reduce Pericarpium Citri Reticulatae extract quality.Embodiment all can increase the rich of flue gas, improves pleasant impression, gives the natural feature of flue gas Pericarpium Citri Reticulatae
Perfume (or spice), is all improved above fragrance, mouthfeel pleasant impression, flue gas quality, and overall imparting Medicated cigarette Pericarpium Citri Reticulatae feature comfortable, natural is fragrant.
Above content is to combine the further description that the present invention is done by concrete preferred embodiment, it is impossible to assert
Being embodied as of the present invention is confined to these explanations.For those skilled in the art, do not taking off
On the premise of present inventive concept, make some replacements or substantially deform, and performance or purposes are identical, all should be considered as this
The protection domain of invention.
Claims (10)
1. the preparation method of a Pericarpium Citri Reticulatae absolute oil, it is characterised in that through following each step:
(1) Pericarpium Citri Reticulatae is pulverized: pulverize dry Pericarpium Citri Reticulatae for Pericarpium Citri Reticulatae grain；
(2) fermentation Pericarpium Citri Reticulatae: 0.1～5% by Pericarpium Citri Reticulatae grain quality take pectase, by 0.1～5% extracting cellulose of Pericarpium Citri Reticulatae grain quality
Enzyme；Step (1) gained Pericarpium Citri Reticulatae grain is placed in the environment of constant temperature and humidity, then adds pectase in material spray mode and cellulase enters
Row fermentation 1～10 day, turning in every 1～2 day is once；
(3) extraction Pericarpium Citri Reticulatae: the petroleum ether mixing adding 2～15 times of volumes in the Pericarpium Citri Reticulatae grain after step (2) gained ferments stirs evenly,
Obtain mixed material；
(4) extract and filter: step (3) gained mixed material be heated at 30～150 DEG C and be incubated 0.5～12h, then passing through
Filter obtains lixiviating solution；
(5) concentrate: step (5) gained lixiviating solution, through being evaporated to extractum, is obtained extract；
(6) precipitate with ethanol: in the extract obtained middle addition 1 of step (5)～the ethanol of 30 times of volumes, seal the most afterwards, then 0
～at-50 DEG C, stand 0.5～48h, obtain mixed liquor；
(7) concentrate: step (6) gained mixed liquor is carried out sucking filtration, concentrates filtrate to oily, obtain Pericarpium Citri Reticulatae absolute oil.
The preparation method of Pericarpium Citri Reticulatae absolute oil the most according to claim 1, it is characterised in that: the Pericarpium Citri Reticulatae of described step (1) is aqueous
Amount is 7～20%.
The preparation method of Pericarpium Citri Reticulatae absolute oil the most according to claim 1, it is characterised in that: the grain of described step (1) Pericarpium Citri Reticulatae grain
Degree is 0.1～5mm.
The preparation method of Pericarpium Citri Reticulatae absolute oil the most according to claim 1, it is characterised in that: constant temperature and humidity in described step (2)
Be temperature be 30～60 DEG C, humidity be 60～90%.
The preparation method of Pericarpium Citri Reticulatae absolute oil the most according to claim 1, it is characterised in that: the filtration of described step (4) is to adopt
Filter with the filter screen of 10～1000 mesh.
The preparation method of Pericarpium Citri Reticulatae absolute oil the most according to claim 1, it is characterised in that: decompression in described step (5) and (7)
The vacuum pressure concentrated is 0.01～0.1MPa.
The preparation method of Pericarpium Citri Reticulatae absolute oil the most according to claim 1, it is characterised in that: concentration of alcohol in described step (6)
For 70v/v%～dehydrated alcohol.
8. according to the preparation method of the arbitrary described Pericarpium Citri Reticulatae absolute oil of claim 1-7, it is characterised in that: gained Pericarpium Citri Reticulatae absolute oil is at volume
Application in cigarette, individually prepares described Pericarpium Citri Reticulatae absolute oil or allocates in conventional tobacco spice, spray in the way of perfuming or charging
Spill in tobacco.
The preparation method of Pericarpium Citri Reticulatae absolute oil the most according to claim 8, it is characterised in that: described Pericarpium Citri Reticulatae absolute oil is individually prepared and is
Pericarpium Citri Reticulatae absolute oil solvent dilution 2～100 times are obtained seasoning liquid.
The preparation method of Pericarpium Citri Reticulatae absolute oil the most according to claim 8, it is characterised in that: described sprinkling is by tobacco
Seasoning liquid is sprayed in tobacco by the 0.01 of quality～2%.
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| CN107802027A (en) * | 2017-09-29 | 2018-03-16 | 昆明坤九香精香料有限公司 | A kind of method that pure tobacco oil is prepared using biology enzyme |
| CN109222212A (en) * | 2017-07-10 | 2019-01-18 | 中国烟草总公司广东省公司 | A kind of fragrance-enhancing tobacco agent containing faenum graecum essential oil |
| CN109280582A (en) * | 2018-09-20 | 2019-01-29 | 云南中烟工业有限责任公司 | A kind of high efficiency preparation method of the dried orange peel absolute oil for tobacco flavoring |
| WO2020258386A1 (en) * | 2019-06-27 | 2020-12-30 | 广东中烟工业有限责任公司 | Slow-release flavorant and application thereof in chinese-flavor tobacco product |
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| CN109280582A (en) * | 2018-09-20 | 2019-01-29 | 云南中烟工业有限责任公司 | A kind of high efficiency preparation method of the dried orange peel absolute oil for tobacco flavoring |
| CN109280582B (en) * | 2018-09-20 | 2021-07-13 | 云南中烟工业有限责任公司 | Efficient preparation method of dried orange peel absolute oil for flavoring tobacco |
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| JP2021530977A (en) * | 2019-06-27 | 2021-11-18 | チャイナ・タバコ・カントン・インダストリアル・カンパニー・リミテッドChina Tobacco Guangdong Industrial Co., Ltd. | Its application in sustained release flavors and Chinese flavored tobacco products |
| JP7177309B2 (en) | 2019-06-27 | 2022-11-24 | チャイナ・タバコ・カントン・インダストリアル・カンパニー・リミテッド | Chinese-flavored tobacco cigarette base material, reconstituted tobacco and heated non-combustible cigarettes |
| CN113264965A (en) * | 2021-05-10 | 2021-08-17 | 杭州云中羽网络科技有限公司 | Method for preparing hesperidin from orange peels |
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