CN101671600B - Additives used in compound Chinese herbal medicine cigarette and use thereof - Google Patents

Additives used in compound Chinese herbal medicine cigarette and use thereof Download PDF

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CN101671600B
CN101671600B CN200910196158XA CN200910196158A CN101671600B CN 101671600 B CN101671600 B CN 101671600B CN 200910196158X A CN200910196158X A CN 200910196158XA CN 200910196158 A CN200910196158 A CN 200910196158A CN 101671600 B CN101671600 B CN 101671600B
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cigarette
tobacco
additive
weight
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CN200910196158XA
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CN101671600A (en
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崔秀明
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华宝食用香精香料(上海)有限公司
无锡华海香料有限公司
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Abstract

The invention relates to a preparation method of additives used in the compound Chinese herbal medicine cigarette, additives for the compound Chinese herbal medicine cigarette prepared by the method and a use thereof in the cigarette. The additive for the cigarette is produced by ethanol extracting of Platycodon grandiflorum, loquatleaf, Pummelo Peel, Schisandra chinensis, Momordica grosvenori, fritillaria cirrhosa, and liquorice. The method has the advantages of simple process and low cost. The additives enable cigarette flavors in the cigarettes to be smoother compared with the cigarette flavors produced by the Chinese herbal medicine, and the additives are coordinated with smoky, thereby effectively reducing irritation of smoke on the mouth, and reducing the harm of smoking.

Description

Compound Chinese herb cigarette additive and uses thereof

[technical field]

The present invention relates to the flavouring essence for tobacco technical field.More specifically, the present invention relates to a kind of preparation method of compound Chinese herb cigarette additive, also relate to the compound Chinese herb cigarette additive product that obtains according to this preparation method, and the application of said product in producing tobacco product.

[background technology]

Along with China's accession to the WTO and " Framework Convention on Tobacco Control ", state's inner wrap strip market internationalization trend is obvious day by day, and the requirement of cigarette security is also improved constantly, and Chinese tobacco is faced with more and more serious competition pressure and social pressures.State Tobacco Monopoly Bureau proposes in " the Chinese cigarette development in science and technology outline " of issue in 2003, and the developing direction of Chinese cigarette is " market-oriented, as to greatly develop the Chinese style cigarette ".The gordian technique of development Chinese style cigarette is under the prerequisite that keeps high fragrance, to realize " reducing tar and reducing harm ", the Chinese style cigarette brand of exploitation " high fragrance, low tar, low harm ".

At present; Join article (as adding tobacco sheet and so on low tar content tobacco product) through using cigarette to join, improve cigarette can have been realized reducing tar and reducing harm with physical methods such as auxilliary material, laser boring raising dialysances effect; To fall the negative impact that burnt technology brings also apparent in view but use; Like perfume quantity reduction, suction dried, cigarette flavor quality variation etc.Therefore, the research of reducing cigarette tar and reducing harm reduction must be paid attention to the fragrant jealous compensation that selectivity reduces and low tar hangs down the harm cigarette of cigarette objectionable impurities simultaneously.In the production of cigarettes in the present age, the flavoring and casing technology has become the key point that embodies cigarette products characteristic fragrance, the personalized style of outstanding cigarette product.And by means of the interpolation of characteristic perfume material, thereby improve cigarette smoke concentration and fragrance, constitute low tar product specific fragrance style, be one of key core technology of making by the Chinese style cigarette.

Natural phant or herbal medicine in recent years, are widely used in the cigarette composition as one of very important spices source.Domestic existing result of study shows, contains a large amount of anti-roll cigarette flue gas free radical activity compositions in the herbal medicine, can effectively reduce carcinogenic substance generation in the cigarette smoke, improves the biological safety of cigarette.Patent " CN200610124616.5 " utilizes tarragon, Herba Epimedii, Grosvenor Momordica to obtain a kind of cigarette additive for feedstock production, and can reduce cigarette smoke stimulates, and reduces cigarette harm.

According to the prior art achievement in research; Comprise Grosvenor Momordica, Unibract Fritillary Bulb, Radix Glycyrrhizae, shizandra berry, Radix Angelicae Sinensis, Japanese Honeysuckle etc. to what cigarette smoke had a positive contribution effect; But up to the present; Also do not utilize the said herbal medicine assembly, use the report of modern separation and Extraction and purification technique exploitation cigarette with perfume material.For this reason, the inventor works out the preparation method of compound Chinese herb cigarette additive of the present invention finally through exploring for many years.

[summary of the invention]

[technical problem that will solve]

The preparation method who the purpose of this invention is to provide a kind of compound Chinese herb cigarette additive.

Another object of the present invention provides the compound Chinese herb cigarette additive that obtains according to said method.

Another object of the present invention provides the purposes of the compound Chinese herb cigarette additive that obtains according to said method.

[technical scheme]

The present invention realizes through following technical proposals.

The present invention relates to the preparation method of compound Chinese herb cigarette additive.This method comprises the steps:

(1) 10-30 weight part balloonflower root, 15-35 weight part Loquat Leaf, 10-25 weight part Pummelo Peel, 5-15 weight part shizandra berry, 5-15 weight part Grosvenor Momordica, 0-10 weight part Unibract Fritillary Bulb and 0-10 weight part Radix Glycyrrhizae mix and obtain a kind of mixture;

(2) add 500-1500 weight part 50-80 weight % aqueous ethanolic solution in the mixture that obtains toward 100 weight part steps (1); Under temperature 50-60 ℃, carry out heating and refluxing extraction 2-3 time again; Each 2-4 hour; Extracting solution merges, and filters then, and the filtrating that obtains concentrating obtains 50-150 weight part liquid concentrator;

(3) liquid concentrator that step (2) is obtained is dissolved in the glycerine; Filter then; Filtrating is preheating to temperature 40-70 ℃ in the feeder of molecular distillation apparatus, under the 1.00-2.00torr pressure condition, the light constituent of this filtrating flies to intermediate condenser straight and condenses into liquid with gaseous phase; Get into the collection of light constituent scoop and obtain additive A, it is used to prepare the table essence of tobacco product; Heavy constituent get into the collection of heavy constituent scoop along cylinder inboard wall and obtain additive B, and it is used to prepare the material essence of tobacco product.

A preferred embodiment of the invention, the granularity of said balloonflower root, Loquat Leaf, Pummelo Peel, shizandra berry, Grosvenor Momordica, Unibract Fritillary Bulb and Radix Glycyrrhizae mixture≤200 orders.

According to another kind of preferred implementation of the present invention, described molecular distillation apparatus is selected from KDF-5 type molecular distillation apparatus.

According to another kind of preferred implementation of the present invention, 22-28 ℃ of the condensing surface temperature of the middle control of step (3) molecular distillation apparatus, circulating water temperature 68-72 ℃, knifing rotating speed 150-400r/min, feeding rate 100-300mL/h.

The invention still further relates to the compound Chinese herb cigarette additive A and the additive B that adopt said method to obtain.

The invention still further relates to and use described compound Chinese herb cigarette additive to produce the method for tobacco product, it is characterized in that it comprises the steps:

Add 10-50 weight part natural extract and 2-6 weight part Ucar 35 in the 50-90 weight part additive B according to claim 5 to; The mixture that obtains is dissolved in the warm water, and the equal refining essence that obtains evenly is sprayed onto in pipe tobacco, stem or the tobacco sheet.

Described natural extract is made up of 20-40 weight part Chinese date extract, 20-40 weight part high fructose syrup, 10-20 weight part cocoa extract and 10-20 weight part Fructus Fici medicinal extract.

A preferred embodiment of the invention, the consumption of said material essence are the 0.01-1% of pipe tobacco, stem or tobacco sheet weight.

The invention still further relates to and use described compound Chinese herb cigarette additive to produce the method for tobacco product, it is characterized in that it comprises the steps:

In 50-80 weight part additive A according to claim 5, add 20-50 weight part terpenes, alcohols, aldehydes and ester mixture, the even table essence that obtains adds in pipe tobacco, stem or the tobacco sheet.

A preferred embodiment of the invention, described terpenes, alcohols, aldehydes and ester mixture are made up of 0.1-0.4 Chong Liang Fen limonene, 0.2-0.7 weight part phenyl aldehyde, 1.0-9.0 weight part phantol, 0.1-0.5 weight part safranal, 2.0-25.0 weight part tobacco cleaned oil, 1.0-9.0 weight part dorinone, 0.1-50.0 weight part Ethylisovalerate and 10.0-50.0 weight part 95 weight % aqueous ethanolic solutions.

A preferred embodiment of the invention, the consumption of said table essence are the 0.01-1% of pipe tobacco, stem or tobacco sheet weight.

Below the present invention will be described in more detail.

The present invention relates to a kind of preparation method of compound Chinese herb cigarette additive, it is characterized in that this method may further comprise the steps:

(1) 10-30 weight part balloonflower root, 15-35 weight part Loquat Leaf, 10-25 weight part Pummelo Peel, 5-15 weight part shizandra berry, 5-15 weight part Grosvenor Momordica, 0-10 weight part Unibract Fritillary Bulb and 0-10 weight part Radix Glycyrrhizae mix, and the mixture that obtains is through grinding and sieving.

According to the prior art achievement in research, theoretical in conjunction with traditional Chinese medicine, discover that balloonflower root is the dried roots of campanulaceae Platycodon grandiflouorum, bitter, suffering, slightly warm in nature.Go into lung channel.The ability expelling phlegm for arresting cough, and a surname's lung, apocenosis effect are arranged.Balloonflower root contains multiple saponin(e, is mainly platycodin, and multiple mixing saponin(e has platycodigenin, senegeninic acid and a spot of platycogenic acid also to contain synanthrin, plant sterol etc. in addition through the sapogenin that complete hydrolysis produced.Contained platycodin makes the sputum dilution to the direct stimulation of oral cavity, throat, stomach mucous membrane thereby reflectivity ground increases the tunica mucosa bronchiorum hypersecretion, is easy to discharge.

Loquat Leaf, hardship is slightly cold, and returns lung, the stomach warp.Cure mainly the cough due to lung-heat, the circulation of vital energy in the wrong direction is breathed heavily urgency, gastropyretic vomiting, hiccup.Loquat Leaf contains multiple volatile oil, and like peruviol, farnesol, α, beta pinene, amphene, myrcene, former kinds is typical rose fragrance.

Pummelo Peel, warm in nature, flavor is hot, bitter.Fruit contains naringin, naringin unit; Pericarp contains citral Geraniol, phantol, phosphorus Methyl anthranilate etc.The effect that cold, the eliminating dampness of loosing, sharp gas and dissolving phlegm being arranged, it is many etc. to be used to treat cough due to wind and cold, the larynx phlegm of itching.

Shizandra berry, warm in nature; Sour, sweet; Return lung, the heart, kidney channel.Shizandra berry contains rich organic acid, VITAMINs, flavonoid, plant sterol and the lignan of strong effect reactivation (for example schisandrin, Wuweizisu B or shizandra berry fat are plain) is arranged; It also is one of minority medicinal material that has concurrently essence, gas, refreshing three big helps, the strong liver of the beneficial gas of ability, the efficient of promoting the cells exclude refuse, supply more oxygen, construction and uses energy, memory and property stamina.

Grosvenor Momordica, cool in nature, it is sweet to distinguish the flavor of.Return lung, large intestine channel.Mainly contain triterpene compound, flavonoid glycoside compound, fructose, amino acid, N.F,USP MANNITOL, VITAMINs etc.; Wherein, the Grosvenor Momordica saponin(e is a topmost effective constituent in the Grosvenor Momordica, is used for lung-fire cough caused by dryness; Diseases such as swelling and pain in the throat aphonia; Its smoking result that adds in the cigarette is shown that the cigarette smoke exquisiteness is mellow and full, and throat is comfortable.

Unibract Fritillary Bulb, bitter, sweet, be slightly cold.Return lung, the heart channel of Hang-Shaoyin.Mainly contain Peimine, verticinone, peimisine, cloud shellfish ketone, demissidine and thymidine and adenosine etc.; Have clearing heat and moistening lung, the effect of preventing phlegm from forming and stopping coughing shows its smoking result that adds in the cigarette; It can increase the concentration of flue gas, but can increase the pungency of flue gas slightly.

Radix Glycyrrhizae, property is flat, and it is sweet to distinguish the flavor of, and returns 12 warps.Radix Glycyrrhizae mainly contains the sylvite or the calcium salt of Potenlini, claims glycyrrhizin again, has the effect of expelling phlegm for arresting cough, relieving spasm to stop pain.The Radix Glycyrrhizae tincture is one of the most frequently used kind of tobacco, is important sweetener, has the sweet effect of promoting the production of body fluid back, also is the medicine of the mediation in the prescriptions of traditional Chinese medicine.Its smoking result that adds in the cigarette is shown it has the effect that reduces the cigarette smoke pungency, strengthens the sense of promoting the production of body fluid.

Described these raw materials need pass through pulverizing, so that improve extraction efficiency.The disintegrating apparatus that uses is a normally used equipment in the Chinese medicinal materials processing, for example multi-functional crusher.The granularity of said balloonflower root, Loquat Leaf, Pummelo Peel, shizandra berry, Grosvenor Momordica, Unibract Fritillary Bulb and Radix Glycyrrhizae mixture≤200 orders after pulverizing.

(2) add 500-1500 weight part 50-80 weight % aqueous ethanolic solution in the mixture that obtains toward 100 weight part steps (1); Under temperature 50-60 ℃, carry out heating and refluxing extraction 2-3 time again; Each 2-4 hour; Extracting solution merges, and filters then, and the filtrating that obtains concentrating obtains 50-150 weight part liquid concentrator;

Usually adopt pickling process, percolation process, decocting method, reflux extraction etc. during with the solvent extraction medicinal herb components.In the present invention, reflux extraction is preferred.Therefore, the process for extracting that the present invention relates to is the method that the technician in present technique field knows.

According to a kind of preferred embodiment, the reflux temperature is 50-60 ℃, preferably 52-58 ℃.The extracting solution that obtains temperature 65-75 ℃ with pressure 0.07-0.09MPa under concentrate and obtain liquid concentrator.

Extracting with concentrating the equipment that uses in the present invention all is the normally used equipment of technician in present technique field, and for example extraction equipment is multi-function extractor; Thickening equipment is a plate-type evaporator.

(3) liquid concentrator that step (2) is obtained is dissolved in the glycerine; Filter then; Filtrating is preheating to temperature 40-70 ℃ in the feeder of molecular distillation apparatus, under the 1.00-2.00torr pressure condition, the light constituent of this filtrating flies to intermediate condenser straight and condenses into liquid with gaseous phase; Get into the collection of light constituent scoop and obtain additive A, it is used to prepare the table essence of tobacco product; Heavy constituent get into the collection of heavy constituent scoop along cylinder inboard wall and obtain additive B, and it is used to prepare the material essence of tobacco product.

According to a kind of preferred embodiment; According to another kind of preferred implementation of the present invention, the well heater preheating temperature of control molecular distillation apparatus is controlled at 50-60 ℃, working pressure 1.20-1.80torr in the step (3); 24-26 ℃ of condensing surface temperature; 70 ℃ of circulating water temperatures, knifing rotating speed 150-400r/min, feeding rate 100-300mL/h.

In the present invention, described molecular distillation apparatus is selected from KDF-5 type molecular distillation apparatus.

KDF-5 type molecular distillation apparatus is that the model of being produced by German UIC company is a Specificati on KDF-5 type short-path distillation.

The invention still further relates to the compound Chinese herb cigarette additive A and the additive B that adopt said method to obtain.

The invention still further relates to and use described compound Chinese herb cigarette additive to produce the method for tobacco product, it is characterized in that it comprises the steps:

Add 10-50 weight part natural extract and 2-6 weight part Ucar 35 in the 50-90 weight part additive B according to claim 5 to; The mixture that obtains is dissolved in the warm water, and the equal refining essence that obtains evenly is sprayed onto in pipe tobacco, stem or the tobacco sheet.

Wherein, described natural extract is made up of 20-40 weight part Chinese date extract, 20-40 weight part high fructose syrup, 10-20 weight part cocoa extract and 10-20 weight part Fructus Fici medicinal extract.

The effective constituent of described Chinese date extract is the acid of nucleolus mandarin orange, folic acid, iron, oligose, vitamins C etc.Main effect is antitumor, promote sleep, enhancing human immune, the anaemia of improving.Adding the Chinese date extract can cover assorted gas, improve and inhale flavor.The Chinese date extract that the present invention uses can be the normally used product of technician in present technique field, for example available from the product of precious emblem, Gansu plant biochemistry ltd of industry group.

Described high fructose syrup is used in and can makes smoke sweet-smelling fragrance more in the tobacco as widely used sweeting agent in the foodstuffs industry, inhales the dry puckery bitter taste that oral cavity, throat are reduced in the back.The high fructose syrup that the present invention uses can be the normally used product of technician in present technique field, for example available from the product of Guangdong Bao Fuli crystal diabetin ltd.

Described cocoa extract can increase this perfume (or spice) of tobacco, alleviates to do the thorn sense.The cocoa extract that the present invention uses can be the normally used product of technician in present technique field, for example available from the product of Da Ermei perfumery, Tianjin.

Described Fructus Fici medicinal extract can make flue gas matter that bigger improvement is arranged, and mainly showing increases flue-cured tobacco fragrance, covers assorted gas, improves aspects such as pleasant impression and smell.The Fructus Fici medicinal extract that the present invention uses can be the normally used product of technician in present technique field, for example available from the product of Guangzhou daily use chemicals chemical industry ltd.

A preferred embodiment of the invention, the consumption of said material essence are the 0.01-1% of pipe tobacco, stem or tobacco sheet weight.

The invention still further relates to and use described compound Chinese herb cigarette additive to produce the method for tobacco product, it is characterized in that it comprises the steps:

In 50-80 weight part additive A according to claim 5, add 20-50 weight part terpenes, alcohols, aldehydes and ester mixture, the even table essence that obtains adds in pipe tobacco, stem or the tobacco sheet.

Wherein, described terpenes, alcohols, aldehydes and ester mixture are made up of 0.1-0.4 Chong Liang Fen limonene, 0.2-0.7 weight part phenyl aldehyde, 1.0-9.0 weight part phantol, 0.1-0.5 weight part safranal, 2.0-25.0 weight part tobacco cleaned oil, 1.0-9.0 weight part dorinone, 0.1-50.0 weight part Ethylisovalerate and 10.0-50.0 weight part 95 weight % aqueous ethanolic solutions.

Limonene described in it dissolves in ethanol, can mix with most of oil, has pleasant type of lemonish fragrance, the smell of no camphor and rosin.

Described phantol like coriander appearance fragrance, increases the blue or green perfume (or spice) and the banksia rose, and natural flavor is modified and corrected to the hot note flavor of promoting or transferring with the fragrant harmony of cigarette,, and it is soft to inhale flavor.

Described safranal has the banksia rose, Xin Xiang, medicine is fragrant, powder is fragrant, can be used for allocating the food flavour of old nurse, Fructus Fici, tealeaves and banksia rose odor type, medicinal herbs odor type.

Described dorinone has the blue or green fragrant and sweet gas of recalling rose, and it is fragrant and sweet in cigarette, to give flue gas green grass or young crops, uses as the cigarette flavor synergistic agent, gives into the cured tobacco characteristic perfume.

Described tobacco cleaned oil is that a type of tobacco characteristic perfume of having that from tobacco plant (flue-cured tobacco, burley tobaccos, Turkish tobaccos), extracts causes aroma compounds; It can promote the characteristic perfume of tobacco; Make flue gas full with improve fragrant the passing through of cigarette and send out a property, and can reduce stimulation, the removal gas of mixing; Improve the class of cigarette, be considered to the optimal additive of tobacco product.The tobacco cleaned oil that the present invention uses can be the normally used product of technician in present technique field, for example available from the product of Yunnan Reascend Tobacco Tech.(Group) Co., Ltd..

A preferred embodiment of the invention, the consumption of said table essence are the 0.01-1% of pipe tobacco, stem or tobacco sheet weight.

Be sprayed at pipe tobacco to these material essences and table essence or be coated on the tobacco sheet according to the processing sequence of conventional perfuming; Seal and play cigarette or chopping after 2 hours and beat cigarette and process cigarette and prop up; The cigarette that rolls into props up (relative humidity 60% ± 5% in climatic chamber; 22 ℃ ± 2 ℃ of temperature) balance is 24 hours, lets the perfumer adopt the blind method of commenting to carry out sensory evaluating smoking's evaluation then.Sensory evaluating smoking's content mainly is several aspects such as fragrance quality and quantity, hamony, assorted gas, stimulation, strength and pleasant impression.

According to the regulation of Law of the People's Republic of China on Tobacco Monopoly, described tobacco product is cigarette, cigar, pipe tobacco, redried leaf tobacco.

[beneficial effect]

Owing to adopted solvent method leaching and short-path distillation purified separation and purification mode; It is that the tobacco aromatics using of raw material production is pure and mild with the herbal medicine that the tobacco aromatics using of gained adds more general in the cigarette, coordinates with cigarette is fragrant, and flue gas is nature easily; Fine and smooth, soft; Fragrance pass through to send out, elegant, graceful, the comfortable pungent stimulation that reduces flue gas to the oral cavity effectively in oral cavity alleviates harm of smoking.This cigarette additive preparation technology is simple, and cost is low, has good market outlook and using value.

[embodiment]

Embodiment 1:

Present embodiment adopts following steps to prepare novel Chinese herb feed additive and it is carried out cigarette use sensory evaluation:

(1) gets balloonflower root 50 grams, Loquat Leaf 30 grams, Pummelo Peel 50 grams, shizandra berry 20 grams, Grosvenor Momordica 10 grams, Unibract Fritillary Bulb 20 grams and Radix Glycyrrhizae 20 grams totally 200 grams, pulverize the back and cross 200 mesh sieves.

(2) get the mixture that step (1) obtains, add the 55 weight % aqueous ethanolic solutions of 5 times (weight), 55 ℃ of following heating and refluxing extraction 3 times, each 2 hours.Merge and filter, leach the dregs of a decoction.Under 55 ℃ bath temperature, be condensed into 50mL liquid.

(3) liquid concentrator that step (2) is obtained is dissolved in 100 gram glycerine, filters then, leaches insolubles, then adds the interior preheating of feeder of KDF-5 type molecular distillation apparatus.The well heater preheating temperature is controlled at 50 ℃, and working pressure 1.20torr, 25 ℃ of condensing surface temperature, 70 ℃ of circulating water temperatures, knifing rotating speed are that 200r/min, feeding rate are 200mL/h.Under the effect of blade applicator, be distributed in evaporator surface equably, the water surface of evaporation temperature is accurately controlled by thermal oil.Under high vacuum condition, light constituent flies to intermediate condenser straight and condenses into liquid with gaseous phase, gets into the light constituent scoop, is additive A; Heavy constituent get into the heavy constituent scoop along cylinder inboard wall, are additive B.

Subsequently additive A that makes and additive B are prepared cigarette with table essence and material essence, its step is following:

(1) gets 85 weight part additive Bs; Add the Ucar 35 of 10 weight part natural extracts and 5 weight parts, wherein natural extract is made up of 30 weight part Chinese date extracts, 30 weight part high fructose syrups, 20 weight part cocoa extracts, 20 weight part Fructus Fici medicinal extract.The mixture that obtains is dissolved in the warm water, and as material essence M1, according to 0.5% of pipe tobacco weight, the processing sequence that accordings to conventional perfuming evenly is sprayed onto in the pipe tobacco.

(2) get 80 weight part additive A; Add terpenes, alcohols, aldehydes and the ester mixture of totally 20 weight parts, wherein this mixture is made up of 0.3 Chong Liang Fen limonene, 0.5 weight part phenyl aldehyde, 6.0 weight part phantols, 0.4 weight part safranal, 25.0 weight part tobacco cleaned oils, 8.0 weight part dorinones, 30.0 weight part Ethylisovalerates and 29.8 weight parts, 95 weight % aqueous ethanolic solutions.The mixture that obtains, adds in the cigarette product according to the processing sequence of conventional perfuming according to 0.1% of pipe tobacco weight as table essence N1.

After material essence M1 adds in the pipe tobacco with table essence N1; Seal 2 hours; Playing cigarette or chopping again beats cigarette and processes cigarette and prop up; The cigarette that rolls into propped up in climatic chamber (relative humidity 60% ± 5%, 22 ℃ ± 2 ℃ of temperature) balance 24 hours, let the perfumer adopt the blind method of commenting to carry out sensory evaluating smoking's evaluation then.Sense organ evaluation and analysis result shows that this product has reduced the pungent stimulation of flue gas to oral cavity and throat, coordinates with cigarette is fragrant, and fragrance passes through, elegant, gracefulness, and flue gas is fine and smooth, soft, smooth and easy, and pleasant impression is comfortable, promotes the production of body fluid.

Embodiment 2:

Repeat embodiment 1, difference is that the knifing rotating speed in the step (3) is that 250r/min, feeding rate are 150mL/h, and the gained material is fragrant to be respectively M2 and N2 with the table essence.The sense organ evaluation and analysis is the result show, this product and cigarette are fragrant to be coordinated, and has effectively covered the wooden assorted gas of stem, and fragrance passes through and sends out, opens and raise, and flue gas is fine and smooth, soft, and it is comfortable to the pungent stimulation pleasant impression of oral cavity and throat to have reduced flue gas.

Embodiment 3:

Repeat embodiment 1, difference is that the knifing rotating speed in the step (3) is that 300r/min, feeding rate are 120mL/h, and the gained material is fragrant to be respectively M3 and N3 with the table essence.Sense organ evaluation and analysis result shows that this rich choice of products cigarette is fragrant, improves flue gas matter, has reduced the pungent stimulation of flue gas to oral cavity and throat, and pleasant impression is comfortable.

Application implementation example 1:

Get the B of Zhoukou City, Henan 2F pipe tobacco, Fujian X 2F, Yunnan C 3F, Guizhou C 3Each 30g/ part of F; Evenly be tiled in the Stainless Steel Disc; Material essence M1 among the embodiment 1 is dissolved in an amount of 95 weight % aqueous ethanolic solutions and water; Respectively in 0.02%, 0.05%, 0.1%, 0.25% the ratio that accounts for the pipe tobacco total amount, add in perfuming not tobacco shred, process cigarette respectively behind the sealing 2h; With the pipe tobacco that does not add any additives equally add with above-mentioned cigarette as control samples.More than all cigarette Zhi Jun through the comprehensive test platform check, its condition is cigarette length 84mm, weight in average is 0.9g/cig, pressure drop average out to 1150Kpa.The cigarette that rolls into props up (relative humidity 60% ± 5%, 22 ℃ ± 2 ℃ of temperature) balance 24h in climatic chamber.Organize the expert that smokes panel test that each test cigarette is compared and smoke panel test, the result is as shown in table 1 below.

Table 1 is carried out the application experiment of different amounts to four kinds of pipe tobaccos

Claims (9)

1. the preparation method of compound Chinese herb cigarette additive is characterized in that this method comprises the steps:
(1) 10-30 weight part balloonflower root, 15-35 weight part Loquat Leaf, 10-25 weight part Pummelo Peel, 5-15 weight part shizandra berry, 5-15 weight part Grosvenor Momordica, 0-10 weight part Unibract Fritillary Bulb and 0-10 weight part Radix Glycyrrhizae mix and obtain a kind of mixture;
(2) add 500-1500 weight part 50-80 weight % aqueous ethanolic solution in the mixture that obtains toward 100 weight part steps (1); Under temperature 50-60 ℃, carry out heating and refluxing extraction 2-3 time again; Each 2-4 hour; Extracting solution merges, and filters then, and the filtrating that obtains concentrating obtains 50-150 weight part liquid concentrator;
(3) liquid concentrator that step (2) is obtained is dissolved in the glycerine; Filter then; Filtrating is preheating to temperature 40-70 ℃ in the feeder of molecular distillation apparatus, under the 1.00-2.00torr pressure condition, the light constituent of this filtrating flies to intermediate condenser straight and condenses into liquid with gaseous phase; Get into the collection of light constituent scoop and obtain additive A, it is used to prepare the table essence of tobacco product; Heavy constituent get into the collection of heavy constituent scoop along cylinder inboard wall and obtain additive B, and it is used to prepare the material essence of tobacco product.
2. method according to claim 1 is characterized in that granularity≤200 orders of said balloonflower root, Loquat Leaf, Pummelo Peel, shizandra berry, Grosvenor Momordica, Unibract Fritillary Bulb and Radix Glycyrrhizae mixture.
3. method according to claim 1 is characterized in that described molecular distillation apparatus is selected from KDF-5 type molecular distillation apparatus.
4. method according to claim 1 is characterized in that 22-28 ℃ of the condensing surface temperature of control molecular distillation apparatus in the step (3), circulating water temperature 68-72 ℃, and knifing rotating speed 150-400r/min, feeding rate 100-300mL/h.
5. the compound Chinese herb cigarette additive A and the additive B that obtain according to the said method of each claim among the claim 1-4.
6. use compound Chinese herb cigarette additive according to claim 5 to produce the method for tobacco product, it is characterized in that it comprises the steps:
Add 10-50 weight part natural extract and 2-6 weight part Ucar 35 in the 50-90 weight part additive B according to claim 5 to; The mixture that obtains is dissolved in the warm water, and the equal refining essence that obtains evenly is sprayed onto in pipe tobacco, stem or the tobacco sheet;
Described natural extract is made up of 20-40 weight part Chinese date extract, 20-40 weight part high fructose syrup, 10-20 weight part cocoa extract and 10-20 weight part Fructus Fici medicinal extract.
7. method according to claim 6, the consumption that it is characterized in that said material essence are the 0.01-1% of pipe tobacco, stem or tobacco sheet weight.
8. use compound Chinese herb cigarette additive according to claim 5 to produce the method for tobacco product, it is characterized in that it comprises the steps:
In 50-80 weight part additive A according to claim 5, add 20-50 weight part terpenes, alcohols, aldehydes and ester mixture, the even table essence that obtains adds in pipe tobacco, stem or the tobacco sheet;
Described terpenes, alcohols, aldehydes and ester mixture are made up of 0.1-0.4 Chong Liang Fen limonene, 0.2-0.7 weight part phenyl aldehyde, 1.0-9.0 weight part phantol, 0.1-0.5 weight part safranal, 2.0-25.0 weight part tobacco cleaned oil, 1.0-9.0 weight part dorinone, 0.1-50.0 weight part Ethylisovalerate and 10.0-50.0 weight part 95 weight % aqueous ethanolic solutions.
9. method according to claim 8, the consumption that it is characterized in that said table essence are the 0.01-1% of pipe tobacco, stem or tobacco sheet weight.
CN200910196158XA 2009-09-23 2009-09-23 Additives used in compound Chinese herbal medicine cigarette and use thereof CN101671600B (en)

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