CN106174684A - The preparation method of a kind of natural perfume material superfine powder and the application in reconstituted tobacoo thereof - Google Patents
The preparation method of a kind of natural perfume material superfine powder and the application in reconstituted tobacoo thereof Download PDFInfo
- Publication number
- CN106174684A CN106174684A CN201610541471.2A CN201610541471A CN106174684A CN 106174684 A CN106174684 A CN 106174684A CN 201610541471 A CN201610541471 A CN 201610541471A CN 106174684 A CN106174684 A CN 106174684A
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- Prior art keywords
- perfume material
- natural perfume
- superfine powder
- spice
- pulp
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- 239000000843 powder Substances 0.000 title claims abstract description 74
- 239000002304 perfume Substances 0.000 title claims abstract description 49
- 239000000463 material Substances 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title claims abstract description 28
- 229920001131 Pulp (paper) Polymers 0.000 claims abstract description 31
- 238000000034 method Methods 0.000 claims abstract description 28
- 235000013599 spices Nutrition 0.000 claims abstract description 21
- 238000001035 drying Methods 0.000 claims abstract description 18
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 17
- 238000003756 stirring Methods 0.000 claims abstract description 10
- 238000003618 dip coating Methods 0.000 claims abstract description 9
- 239000007921 spray Substances 0.000 claims abstract description 9
- 238000004519 manufacturing process Methods 0.000 claims abstract description 8
- 241000628997 Flos Species 0.000 claims description 7
- 210000000582 semen Anatomy 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 241000533293 Sesbania emerus Species 0.000 claims description 3
- FFBHFFJDDLITSX-UHFFFAOYSA-N benzyl N-[2-hydroxy-4-(3-oxomorpholin-4-yl)phenyl]carbamate Chemical compound OC1=C(NC(=O)OCC2=CC=CC=C2)C=CC(=C1)N1CCOCC1=O FFBHFFJDDLITSX-UHFFFAOYSA-N 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 244000025254 Cannabis sativa Species 0.000 claims description 2
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims description 2
- 244000046052 Phaseolus vulgaris Species 0.000 claims description 2
- 240000008474 Pimenta dioica Species 0.000 claims description 2
- 235000006990 Pimenta dioica Nutrition 0.000 claims description 2
- 244000299461 Theobroma cacao Species 0.000 claims description 2
- 235000005764 Theobroma cacao ssp. cacao Nutrition 0.000 claims description 2
- 235000005767 Theobroma cacao ssp. sphaerocarpum Nutrition 0.000 claims description 2
- 235000001046 cacaotero Nutrition 0.000 claims description 2
- 239000004744 fabric Substances 0.000 claims description 2
- 229910052757 nitrogen Inorganic materials 0.000 claims description 2
- 239000000796 flavoring agent Substances 0.000 abstract description 7
- 239000003205 fragrance Substances 0.000 abstract description 6
- 238000004891 communication Methods 0.000 abstract description 5
- 235000019634 flavors Nutrition 0.000 abstract description 4
- 239000008187 granular material Substances 0.000 abstract description 4
- 230000002045 lasting effect Effects 0.000 abstract description 4
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 3
- 239000003546 flue gas Substances 0.000 abstract description 3
- 239000000654 additive Substances 0.000 abstract description 2
- 230000000996 additive effect Effects 0.000 abstract description 2
- 210000000214 mouth Anatomy 0.000 abstract description 2
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 238000010298 pulverizing process Methods 0.000 description 12
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 11
- 241000208125 Nicotiana Species 0.000 description 9
- 239000002994 raw material Substances 0.000 description 6
- 238000005520 cutting process Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 235000013305 food Nutrition 0.000 description 3
- 235000013355 food flavoring agent Nutrition 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 230000000391 smoking effect Effects 0.000 description 3
- 244000061176 Nicotiana tabacum Species 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000012634 fragment Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 239000011343 solid material Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000003500 flue dust Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000012437 perfumed product Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 235000019590 thick flavour Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention provides the preparation method of a kind of natural perfume material superfine powder and the application in reconstituted tobacoo thereof.It comprises the steps: that (1) prepares spice fine powder；(2) superfine comminution at low temperature；(3) spice superfine powder addition paper pulp is copied in front tank, after stirring, paper pulp through manufacturing paper with pulp, drying process form sheets of fibres chip base, then by direct for concentrated solution dip-coating or spray in thin slice chip base, be dried, cut prepared reconstituted tobacoo.The characteristic spice that the present invention utilizes superfine communication technique to prepare has the advantages that aromatic flavor is pure, granule fine and even, dispersibility are preferable, adsorptivity is good, can ensure that the pure natural attribute of product simultaneously；The fragrance applications made by the present invention after medicated cigarette thin slice, abundant perfume quantity, coordinate with cigarette perfume (or spice), the soft exquisiteness of flue gas, alleviates oral cavity residual, reduces and stimulate, cover miscellaneous QI, and fragrance lasting lasting stability, be suitable as a kind of perfume additive and be applied to the perfuming process of thin slice.
Description
Technical field
The present invention relates to cigarette flavors field, the preparation method of a kind of natural perfume material superfine powder and should
The application in tobacco sheets by paper making method of the natural perfume material superfine powder.
Background technology
Superfine communication technique, refers to utilize various special disintegrating apparatus, by certain processing process, to material
Carry out milling, impact, shearing etc., thus the material particles of more than 3mm is crushed to the subparticle of 5-15 μm.As a kind of high
New technique processing method, although micronizing is come out soon, has been widely used for food, health product, medicine and other fields.By
Developing to miniaturization direction in granule, cause material table area and porosity to increase considerably, therefore ultrafine powder has uniqueness
Physicochemical property, such as good dissolubility, dispersibility, adsorptivity etc..Utilize the superfine communication technique can be by spice at low temperature
State lower moment is broken into the ultramicro powder of uniform particle sizes, good fluidity, and the loss of raw material flavor components is less, product thick flavor
Strongly fragrant, pure, and belong to the processing of pure physical technique, it is possible to ensure the pure natural attribute of product.
Tobacco sheets by paper making method is with tobacco leaf fragment, offal, cabo etc. as raw material, with paper technology processing, reconstituted tobacco
And a kind of reconstituted product formed.The use of tobacco sheets by paper making method, is possible not only to improve tobacco material utilization rate to greatest extent,
Reduce production of cigarettes cost, it is also possible to a certain extent the physical property and chemical composition making Medicated cigarette is carried out Reasonable Regulation And Control,
It is effectively improved the interior quality of Medicated cigarette.The industrialized production of domestic tobacco sheets by paper making method, starts from the later stage nineties in last century, mesh
Before in terms of aesthetic quality, generally have that miscellaneous QI is obvious, fragrance is not enough, stimulate relatively big, remain the shortcomings such as heavier.Art technology
Personnel find, in addition to improving production Technology, selecting quality raw materials, interpolation essence and flavoring agent becomes and improves thin slice interior quality
Effective way.At present, the essence being applied to thin slice mainly forms, although it is being covered with monomeric compound for body material allotment
Lid miscellaneous QI, improve the aspect such as mouthfeel and obtain certain effect, but its fragrance is rich poor, there is substantially chemistry breath, fragrant with cigarette
Inharmonious, part essence boiling point is the highest, readily volatilized in application process.Additionally, the safety of chemosynthesis class essence and flavoring agent
Problem highlights day by day.
Under the situation that smoking and health problem cause extensive concern day by day, natural essence spice has become Chinese-style cigarette and has increased
One important directions of fragrant humectation research.Improving tobacco sheets by paper making method aesthetic quality's technical field, seeking the most natural
Essence and flavoring agent is gradually favored by Nicotiana tabacum L. scientific worker.The application of solid spice is concentrated mainly on food, daily use chemicals row
Industry, its applied research in cigarette products is less.At present, domestic superfine communication technique is mainly used in medicine, food, health care
The exploitation of product, about natural perfume material superfine powder applied research in reconstituted tobacoo, there are no report.
Summary of the invention
The purpose of the present invention is aiming at above-mentioned deficiency, it is provided that the preparation method of the superfine powder of a kind of natural perfume material and
Application in reconstituted tobacoo, solves existing reconstituted tobacoo miscellaneous QI obvious, and fragrance is not enough, it is relatively big to stimulate, remain the shortcomings such as heavier,
Improve its availability in cigarette tobacco leaf formulation.
The technical scheme that the present invention provides: the preparation method of described a kind of natural perfume material superfine powder, it is characterised in that include
Following steps:
(1) spice fine powder is prepared: put into by solid natural perfume material in the air dry oven of temperature 50 C～60 DEG C, be dried 3
～5 hours, put in pulverizer and pulverize, after sieving, make spice fine powder；Wherein said natural perfume material be Radix Glycyrrhizae, Fructus Jujubae, Fructus Crataegi,
One in Semen Myristicae, Fructus Anisi Stellati, allspice, Flos Caryophylli, coffee bean, cacao bean.
(2) micronizing: put in super micron mill by the spice fine powder that step (1) obtains, in charging rate 1～2kg/
H, carries out micronizing and processes 1～2 time, obtain the natural perfume material superfine powder of particle diameter 8-12 μm under conditions of pressure 0.5～1MPa.
The present invention preferably technical scheme: after the solid natural perfume material in step (1) is pulverized, crosses the screen cloth of 40～80 mesh.
The present invention preferably technical scheme: super micron mill described in step (2) is to have liquid nitrogen auxiliary protection device
Air-stream type ultrafine pulverizer, this super micron mill is existing equipment.
The another kind of technical scheme that the present invention provides: described natural perfume material superfine powder application in reconstituted tobacoo, it is special
Levy and be: above-mentioned natural perfume material superfine powder addition paper pulp is copied in front tank, addition be paper pulp gross weight in pulp tank 0.1～
0.5%, stir；The most just be added with the paper pulp of natural perfume material micropowder through manufacturing paper with pulp, drying process form sheets of fibres
Chip base；Then by direct for concentrated solution dip-coating or spray in thin slice chip base, last drying, cut to prepare and surpass containing natural perfume material
The reconstituted tobacoo of micropowder.
The characteristic spice that the present invention utilizes superfine communication technique to prepare have granule fine and even, dispersibility preferably, absorption
Property good feature, the pure comfortable and natural true to nature of raw material local flavor can be kept well simultaneously；Natural perfume material ultrafine powder
Can reach the granule degree of submicron order, in terms of the fine degree of processing powder perfume, there is unrivaled advantage, by it
Paper process thin slice production process is being applied in paper pulp, it is possible to controllability and the uniformity of addition, spice are effectively ensured
It is difficult to be scattered from the thin slice chip base of molding, it can be ensured that the quality stability of perfumed products, perfume quantity can be enriched simultaneously, with
Cigarette perfume (or spice) is coordinated, the soft exquisiteness of flue gas, alleviates oral cavity residual, reduces and stimulate, cover miscellaneous QI, and fragrance lasting lasting stability, is suitable for
The perfuming being applied to thin slice as a kind of perfume additive processes.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail.
The natural perfume material superfine powder that the present invention provides application in reconstituted tobacoo, is to be added on by natural perfume material superfine powder
Paper pulp is copied in front tank, then uses and is added with the paper pulp of natural perfume material superfine powder to prepare reconstituted tobacoo, the system of its reconstituted tobacoo
Preparation Method is prior art, and the step adding natural perfume material superfine powder is as follows: used by the raw materials such as cabo, offal, tobacco leaf fragment
Water as solvent carries out the cycling extraction of routine, after extraction terminates, carries out solid-liquid separation, obtains solid material A and liquid B；By liquid
Body B makes concentrated solution C after concentrating；Being merged by the raw materials such as solid material A and flue dust rod and carry out slurrying, paper pulp is beaten after too many levels
Enter and copy front tank, the natural perfume material superfine powder prepared is poured into by pulp tank the 0.1 of paper pulp gross weight～the addition of 0.5%
Copy in front tank and stir, then by paper pulp through manufacturing paper with pulp, drying process form chip base, then concentrations C liquid be coated onto on substrate, do
The reconstituted tobacoo containing natural perfume material superfine powder is obtained after dry.
Embodiment 1, the preparation method of a kind of natural perfume material superfine powder, its concrete preparation process is as follows:
(1) commercially available Fructus Crataegi is put in the air dry oven of 50 DEG C and be dried 5 hours, cross 60 eye mesh screens after pulverizing and make Fructus Crataegi
Fine powder.
(2) Fructus Crataegi fine powder is put in air-stream type ultrafine pulverizer, at charging rate 1kg/h, operating pressure 0.8MPa bar
Pulverization process 2 times under part, the Fructus Crataegi superfine powder of collection cut size 8-12 μm.
The Fructus Crataegi superfine powder product of preparation in embodiment 1 being added paper pulp and copies in front tank, addition is paper pulp in pulp tank
The 0.3% of gross weight, after stirring, paper pulp process is manufactured paper with pulp, drying process forms sheets of fibres chip base, then that concentrated solution is straight
Connect dip-coating or spray in thin slice chip base, last drying, cutting and prepare containing the reconstituted tobacoo of Fructus Crataegi superfine powder.
Embodiment 2, the preparation method of a kind of natural perfume material superfine powder, its concrete preparation process is as follows:
(1) commercially available Fructus Jujubae is put in the air dry oven of 55 DEG C and be dried 4 hours, cross 40 eye mesh screens after pulverizing and make Fructus Jujubae
Fine powder.
(2) Fructus Jujubae fine powder is put in air-stream type ultrafine pulverizer, in charging rate 1.5kg/h, operating pressure 0.5MPa
Under the conditions of pulverization process 2 times, the Fructus Jujubae superfine powder of collection cut size 8-12 μm.
The Fructus Jujubae superfine powder product of preparation in embodiment 2 being added paper pulp and copies in front tank, addition is paper pulp in pulp tank
The 0.5% of gross weight, after stirring, paper pulp process is manufactured paper with pulp, drying process forms sheets of fibres chip base, then that concentrated solution is straight
Connect dip-coating or spray in thin slice chip base, last drying, cutting and prepare containing the reconstituted tobacoo of Fructus Jujubae superfine powder.
Embodiment 3, the preparation method of a kind of natural perfume material superfine powder, its concrete preparation process is as follows:
(1) commercially available Radix Glycyrrhizae is put in the air dry oven of 50 DEG C and be dried 5 hours, cross 60 eye mesh screens after pulverizing and make Radix Glycyrrhizae
Fine powder.
(2) Radix Glycyrrhizae fine powder is put in air-stream type ultrafine pulverizer, in charging rate 1.0kg/h, operating pressure 1.0MPa
Under the conditions of pulverization process 1 time, the Radix Glycyrrhizae superfine powder of collection cut size 8-12 μm.
The Radix Glycyrrhizae superfine powder product of preparation in embodiment 3 being added paper pulp and copies in front tank, addition is paper pulp in pulp tank
The 0.2% of gross weight, after stirring, paper pulp process is manufactured paper with pulp, drying process forms sheets of fibres chip base, then that concentrated solution is straight
Connect dip-coating or spray in thin slice chip base, last drying, cutting and prepare containing the reconstituted tobacoo of Radix Glycyrrhizae superfine powder.
Embodiment 4, the preparation method of a kind of natural perfume material superfine powder, its concrete preparation process is as follows:
(1) commercially available Semen Myristicae is put in the air dry oven of 60 DEG C and be dried 4 hours, cross 80 eye mesh screens after pulverizing and make meat
Fructus Amomi Rotundus fine powder.
(2) Semen Myristicae fine powder is put in air-stream type ultrafine pulverizer, in charging rate 1.5kg/h, operating pressure
Pulverization process 2 times under the conditions of 0.5MPa, the Semen Myristicae superfine powder of collection cut size 8-12 μm.
The Semen Myristicae superfine powder product of preparation in embodiment 4 being added paper pulp and copies in front tank, addition is paper in pulp tank
The 0.1% of slurry gross weight, after stirring, paper pulp process is manufactured paper with pulp, drying process forms sheets of fibres chip base, then by concentrated solution
Directly dip-coating or spray in thin slice chip base, last drying, cuts and prepares the reconstituted tobacoo containing Semen Myristicae superfine powder.
Embodiment 5, the preparation method of a kind of natural perfume material superfine powder, its concrete preparation process is as follows:
(1) commercially available Flos Caryophylli is put in the air dry oven of 50 DEG C and be dried 4.5 hours, cross 40 eye mesh screens after pulverizing and make fourth
Fragrant fine powder.
(2) Flos Caryophylli fine powder is put in air-stream type ultrafine pulverizer, in charging rate 1.0kg/h, operating pressure 1.0MPa
Under the conditions of pulverization process 1 time, the Flos Caryophylli superfine powder of collection cut size 8-12 μm.
The Flos Caryophylli superfine powder product of preparation in embodiment 5 being added paper pulp and copies in front tank, addition is paper pulp in pulp tank
The 0.25% of gross weight, after stirring, paper pulp process is manufactured paper with pulp, drying process forms sheets of fibres chip base, then by concentrated solution
Directly dip-coating or spray in thin slice chip base, last drying, cuts and prepares the reconstituted tobacoo containing Flos Caryophylli superfine powder.
Embodiment 6, the preparation method of a kind of natural perfume material superfine powder, its concrete preparation process is as follows:
(1) commercially available coffee bean is put in the air dry oven of 55 DEG C and be dried 4 hours, cross 60 eye mesh screens after pulverizing and make coffee
Coffee fine powder.
(2) coffee fine powder is put in air-stream type ultrafine pulverizer, in charging rate 2.0kg/h, operating pressure 1.0MPa
Under the conditions of pulverization process 2 times, the coffee superfine powder of collection cut size 8-12 μm.
The coffee superfine powder product of preparation in embodiment 6 being added paper pulp and copies in front tank, addition is paper pulp in pulp tank
The 0.4% of gross weight, after stirring, paper pulp process is manufactured paper with pulp, drying process forms sheets of fibres chip base, then that concentrated solution is straight
Connect dip-coating or spray in thin slice chip base, last drying, cutting and prepare containing the reconstituted tobacoo of coffee superfine powder.
By the shredding respectively of the reconstituted tobacoo containing spice superfine powder described in the embodiment of the present invention 1 to 6, after being rolled into cigarette
Being positioned in thermo-humidistat cabinet balance 48h, the group of smokeing panel test that the cigarette after balance is made up of 9 people is smoked panel test, to be not added with the cigarette of spice
Grass thin slice as comparison, sensory evaluating smoking's result such as following table:
From sensory evaluating smoking's result, being added in reconstituted tobacoo by spice superfine powder, its application effect is: abundant cigarette
Perfume (or spice), coordinates with cigarette perfume (or spice), the soft exquisiteness of flue gas, alleviates residual, and pleasant impression is the most comfortable, reduces and stimulates, covers miscellaneous QI.
Claims (4)
1. the preparation method of a natural perfume material superfine powder, it is characterised in that comprise the following steps:
(1) spice fine powder is prepared: put into by solid natural perfume material in the air dry oven of temperature 50 C～60 DEG C, be dried 3～5 little
Time, put in pulverizer and pulverize, sieve and make spice fine powder；Wherein said natural perfume material be Radix Glycyrrhizae, Fructus Jujubae, Fructus Crataegi, Semen Myristicae,
One in Fructus Anisi Stellati, allspice, Flos Caryophylli, coffee bean, cacao bean；
(2) micronizing: put in super micron mill by the spice fine powder that step (1) obtains, in charging rate 1～2kg/h, pressure
Carry out micronizing under conditions of power 0.5～1MPa to process 1～2 time, obtain the natural perfume material superfine powder of particle diameter 8-12 μm.
The preparation method of a kind of natural perfume material superfine powder the most according to claim 1, it is characterised in that: in step (1)
After solid natural perfume material is pulverized, cross the screen cloth of 40～80 mesh.
A kind of method that natural perfume material superfine powder is applied to reconstituted tobacoo the most according to claim 1, it is characterised in that:
Described in step (2), super micron mill is the air-stream type ultrafine pulverizer with liquid nitrogen auxiliary protection device.
4. by the natural perfume material superfine powder of preparation application in reconstituted tobacoo in claim 1 or 2 or 3, it is characterised in that: will
Above-mentioned natural perfume material superfine powder adds paper pulp and copies in front tank, and addition is in pulp tank the 0.1～0.5% of paper pulp gross weight, stirs
Mix uniformly；The most just be added with the paper pulp of natural perfume material micropowder through manufacturing paper with pulp, drying process form sheets of fibres chip base；Then
By direct for concentrated solution dip-coating or spray in thin slice chip base, last drying, cut and prepare the cigarette containing natural perfume material superfine powder
Grass thin slice.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610541471.2A CN106174684A (en) | 2016-07-12 | 2016-07-12 | The preparation method of a kind of natural perfume material superfine powder and the application in reconstituted tobacoo thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610541471.2A CN106174684A (en) | 2016-07-12 | 2016-07-12 | The preparation method of a kind of natural perfume material superfine powder and the application in reconstituted tobacoo thereof |
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|---|---|
| CN106174684A true CN106174684A (en) | 2016-12-07 |
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| CN201610541471.2A Pending CN106174684A (en) | 2016-07-12 | 2016-07-12 | The preparation method of a kind of natural perfume material superfine powder and the application in reconstituted tobacoo thereof |
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| CN107183778A (en) * | 2017-07-03 | 2017-09-22 | 中烟施伟策（云南）再造烟叶有限公司 | A kind of papermaking-method reconstituted tobaccos preparation method of the natural plant powder containing ultra micro |
| CN107232639A (en) * | 2017-06-22 | 2017-10-10 | 中烟施伟策（云南）再造烟叶有限公司 | A kind of reconstituted tobacco of the powder of plum containing ultra micro and preparation method thereof |
| CN107594618A (en) * | 2017-11-08 | 2018-01-19 | 湖北中烟工业有限责任公司 | Sustained release pellet based on natural perfume material Ultramicro-powder and preparation method thereof |
| CN107746748A (en) * | 2017-11-08 | 2018-03-02 | 湖北中烟工业有限责任公司 | A kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and the application in cigarette |
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| CN109393543A (en) * | 2018-12-21 | 2019-03-01 | 云南巴菰生物科技有限公司 | A kind of ultra-micro powder plantflakesare and preparation method thereof |
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| CN111257522A (en) * | 2020-04-01 | 2020-06-09 | 中烟施伟策（云南）再造烟叶有限公司 | Method for rapidly evaluating and identifying internal sensory quality of tobacco raw material |
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| CN112971194A (en) * | 2021-04-19 | 2021-06-18 | 云南中烟工业有限责任公司 | Tobacco flavor loading process |
| CN113455692A (en) * | 2020-03-31 | 2021-10-01 | 中烟施伟策（云南）再造烟叶有限公司 | Cocoa-containing auxiliary material for cigarettes and tobacco product |
| CN113455693A (en) * | 2020-03-31 | 2021-10-01 | 中烟施伟策（云南）再造烟叶有限公司 | Method for preparing non-tobacco-cocoa type tobacco material by wet papermaking technology |
| CN114732147A (en) * | 2021-01-08 | 2022-07-12 | 中烟施伟策（云南）再造烟叶有限公司 | Method for preparing non-tobacco-cocoa type cigarette material by wet papermaking powder forming technology |
| CN114747789A (en) * | 2021-01-08 | 2022-07-15 | 中烟施伟策（云南）再造烟叶有限公司 | Wet-process powder forming preparation method containing cocoa tobacco auxiliary materials and tobacco product |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20000021999A (en) * | 1998-09-30 | 2000-04-25 | 전창호 | Tobacco composition generating vitamins and fragrance when smoking tobacco using the same |
| CN101331934A (en) * | 2008-07-31 | 2008-12-31 | 天津春发食品配料有限公司 | Preparation method of spice superfines |
| CN102021074A (en) * | 2009-09-16 | 2011-04-20 | 崔举峰 | Thermally sensitive plant-aromatic controlled-release granules and preparation method thereof |
| CN103355739A (en) * | 2013-08-06 | 2013-10-23 | 湖北中烟工业有限责任公司 | Method for manufacturing recombined tobacco leaves through paper-making mode |
| CN103549646A (en) * | 2013-11-11 | 2014-02-05 | 云南烟草科学研究院 | Orally-disintegrating-tablet-type smokeless tobacco product containing tobacco ultra-micro powder and preparation method thereof |
| CN105105314A (en) * | 2015-08-18 | 2015-12-02 | 云南中烟工业有限责任公司 | Powder spray agent containing tobacco components and preparation method thereof |
| CN105192876A (en) * | 2015-10-20 | 2015-12-30 | 贵州中烟工业有限责任公司 | Oral smokeless tobacco composition added with plant composition and application of oral smokeless tobacco composition |
-
2016
- 2016-07-12 CN CN201610541471.2A patent/CN106174684A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20000021999A (en) * | 1998-09-30 | 2000-04-25 | 전창호 | Tobacco composition generating vitamins and fragrance when smoking tobacco using the same |
| CN101331934A (en) * | 2008-07-31 | 2008-12-31 | 天津春发食品配料有限公司 | Preparation method of spice superfines |
| CN102021074A (en) * | 2009-09-16 | 2011-04-20 | 崔举峰 | Thermally sensitive plant-aromatic controlled-release granules and preparation method thereof |
| CN103355739A (en) * | 2013-08-06 | 2013-10-23 | 湖北中烟工业有限责任公司 | Method for manufacturing recombined tobacco leaves through paper-making mode |
| CN103549646A (en) * | 2013-11-11 | 2014-02-05 | 云南烟草科学研究院 | Orally-disintegrating-tablet-type smokeless tobacco product containing tobacco ultra-micro powder and preparation method thereof |
| CN105105314A (en) * | 2015-08-18 | 2015-12-02 | 云南中烟工业有限责任公司 | Powder spray agent containing tobacco components and preparation method thereof |
| CN105192876A (en) * | 2015-10-20 | 2015-12-30 | 贵州中烟工业有限责任公司 | Oral smokeless tobacco composition added with plant composition and application of oral smokeless tobacco composition |
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| CN107232639A (en) * | 2017-06-22 | 2017-10-10 | 中烟施伟策（云南）再造烟叶有限公司 | A kind of reconstituted tobacco of the powder of plum containing ultra micro and preparation method thereof |
| CN107183778A (en) * | 2017-07-03 | 2017-09-22 | 中烟施伟策（云南）再造烟叶有限公司 | A kind of papermaking-method reconstituted tobaccos preparation method of the natural plant powder containing ultra micro |
| CN107594618A (en) * | 2017-11-08 | 2018-01-19 | 湖北中烟工业有限责任公司 | Sustained release pellet based on natural perfume material Ultramicro-powder and preparation method thereof |
| CN107746748A (en) * | 2017-11-08 | 2018-03-02 | 湖北中烟工业有限责任公司 | A kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and the application in cigarette |
| CN108077993A (en) * | 2017-12-18 | 2018-05-29 | 中科国思生物科技研究（广州）有限公司 | A kind of application of hawthorn in health care reconstituted tobacoo |
| CN109393543B (en) * | 2018-12-21 | 2021-07-20 | 云南巴菰生物科技有限公司 | Ultra-micro powder plant slice and preparation method thereof |
| CN109393543A (en) * | 2018-12-21 | 2019-03-01 | 云南巴菰生物科技有限公司 | A kind of ultra-micro powder plantflakesare and preparation method thereof |
| CN109875095A (en) * | 2019-02-01 | 2019-06-14 | 湖北中烟工业有限责任公司 | It can be used for the ultralow temperature preparation method of the cumin Ultramicro-powder of cigarette product flavoring and casing |
| CN113455692A (en) * | 2020-03-31 | 2021-10-01 | 中烟施伟策（云南）再造烟叶有限公司 | Cocoa-containing auxiliary material for cigarettes and tobacco product |
| CN113455693A (en) * | 2020-03-31 | 2021-10-01 | 中烟施伟策（云南）再造烟叶有限公司 | Method for preparing non-tobacco-cocoa type tobacco material by wet papermaking technology |
| CN111257523A (en) * | 2020-04-01 | 2020-06-09 | 中烟施伟策（云南）再造烟叶有限公司 | Evaluation and identification method for internal sensory quality of non-tobacco raw materials |
| CN111257522A (en) * | 2020-04-01 | 2020-06-09 | 中烟施伟策（云南）再造烟叶有限公司 | Method for rapidly evaluating and identifying internal sensory quality of tobacco raw material |
| CN114732147A (en) * | 2021-01-08 | 2022-07-12 | 中烟施伟策（云南）再造烟叶有限公司 | Method for preparing non-tobacco-cocoa type cigarette material by wet papermaking powder forming technology |
| CN114747789A (en) * | 2021-01-08 | 2022-07-15 | 中烟施伟策（云南）再造烟叶有限公司 | Wet-process powder forming preparation method containing cocoa tobacco auxiliary materials and tobacco product |
| CN112971194A (en) * | 2021-04-19 | 2021-06-18 | 云南中烟工业有限责任公司 | Tobacco flavor loading process |
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