WO2013097164A1

WO2013097164A1 - Alternative cut tobacco composition and preparation method thereof

Info

Publication number: WO2013097164A1
Application number: PCT/CN2011/084987
Authority: WO
Inventors: 华健; 郭红珍
Original assignee: 深圳梵活生物科技有限公司
Priority date: 2011-12-30
Filing date: 2011-12-30
Publication date: 2013-07-04
Also published as: CN103442601A; CN103442601B

Abstract

Disclosed are an alternative cut tobacco composition and a preparation method thereof. The composition comprises the following components by weight: 10-100 parts of cut tobacco shaped objects, and 1-10 part(s) of a concentrated liquor extracted from pure traditional Chinese medicine to be sprayed on the cut tobacco shaped objects. The cut tobacco shaped objects comprise the following components by weight: 30-40 parts Yunnan Pu-erh tea, 20-30 parts rose flower, 20-30 parts snow tea , 20-30 parts of the Chinese herb Lingdancao , 15-25 parts saffron and 15-25 parts ginkgo leaf. The composition can be adapted to the needs of smokers, and has the effects of clearing the lungs, relieving sore throats, relieving coughs, expelling toxins and helping to quit smoking.

Description

Composition for replacing shredded tobacco and preparation method thereof

Technical field

The invention belongs to the field of health care products, and particularly relates to a health-care cigarette which utilizes natural Chinese herbal medicines and natural foods and natural flavors to be scientifically compatible with the concept of medicine and food, and is a kind of health-care cigarette which has the functions of clearing the lungs, relieving cough, detoxifying and quitting smoking.

BACKGROUND OF THE INVENTION Non-smoke tobacco is one of the development directions of traditional tobacco transformation. It has developed rapidly in recent years and has already formed a certain impact on the traditional smoking concept, and is attracting more and more attention and attention from the whole society, especially In foreign countries, tobacco control and cigarette replacement products have received strong government support. In the past five years, the development of non-tobacco tobacco and new cigarette replacement products in China has also been leaps and bounds. In the next few years, non-tobacco products will inevitably form a new pattern of cigarettes. Patent No. 200310116286.1, entitled "Nine-section tea non-tobacco cigarettes and a preparation method thereof" discloses a nine-section tea non-tobacco cigarette, which utilizes nine tea leaves (grass coral leaves). The technical scheme of the invention is as follows: drying and drying the nine-section tea leaves; vacuum-regenerating the dried nine-section loquat leaves with a vacuum resurgence machine, and steaming with a vacuum pump and a steam jet vacuuming regenerative steaming device, so as to After the re-moisture, the nine-section tea is shredded by a wire cutter and dried, and the water is divided into 12 ± 0.5%. The invention is similar to the tobacco in the same phase. Well, Yi Chengsi is easy to roll on the cigarette machine, and has good smoking characteristics. It is an ideal product for non-tobacco substitutes for cigarette products. Pure tobacco cigarette products contain extremely high levels of harmful components such as nicotine and tar, which are harmful to the human body after smoking. The nine-section tea cigarette products do not contain any tobacco ingredients, and are made of nine-section tea. The product contains nine tea leaves containing coumarone, lactone, flavonoid glycosides, cyanogenic glycosides, volatile oil and tannic acid. It has a health effect on the human body. In particular, the characteristics of the nine-section tea determine that it is close to the complexity of the manufacturing process and process of pure tobacco cigarettes. The inventors found that the current market size:: the composition of the composition of the alternative shredded tobacco is relatively simple, and the effect is not good, it is difficult to adapt to the needs of smokers, but also has the effect of clearing the lungs, relieving pharynx, relieving cough, detoxification, and quitting smoking. . Summary of the invention

The object of the present invention is to provide a composition for replacing shredded tobacco and a preparation method thereof, which can not only meet the needs of smokers, but also have the functions of clearing the lungs, relieving cough, detoxifying, quitting smoking, and having a remarkable clinical effect. The technical solution of the present invention is:

The ratios mentioned in the present invention are all by weight unless otherwise specified.

A composition for replacing shredded tobacco comprising the following components in a weight ratio: 10 to 100 parts of tobacco, 1 to 10 parts of a pure Chinese medicine extract concentrate sprayed on the tobacco, and 0.5 to 1 part of a fragrance, Wherein, the tobacco material comprises the following components by weight: 30 to 40 parts of Yunnan Pu'er tea, 20 to 30 parts of rose, 20 to 30 parts of snow tea, 20 to 30 parts of linden grass, 15 to 25 parts of saffron , Ginkgo biloba leaves 15 to 25 servings.

The pure Chinese medicine extraction concentrate comprises the following components by weight fraction: 10 to 20 parts of valerian, 20 to 30 parts of honeysuckle, 15 to 25 parts of tribute, 20 to 30 parts of dandelion, 15 to 25 parts of lavender, 15 to 25 parts of lotus leaf, 10 to 20 parts of arborvitae leaves, 10 to 20 parts of wood butterfly, 15 to 25 parts of generational flowers, 15 to 25 parts of light bamboo leaves, and 10 to 20 parts of musk.

The pure Chinese medicine extract concentrate may further comprise an extract of the following parts by weight: 10 to 20 parts of Radix Scutellariae, 10 to 20 parts of aloe, 15 to 25 parts of Suzi, 15 to 25 parts of Rhodiola, 15 to 25 parts of Magnolia, 10 to 20 parts of fig, 15 to 25 parts of Astragalus, 10 to 20 parts of Sanqi, 10 to 20 parts of Angelica, 15 to 25 parts of licorice, 15 to 25 parts of clove, 20 to 30 parts of platycodon, 10 to 20 parts of Pueraria, 20 to 30 parts of American ginseng, 20 to 30 parts of lily, 20 to 30 parts of Luo Han Guo, 10 to 20 parts of glutinous rice, 10 to 20 parts of fat sea, 15 to 25 parts of orange, 15 to 25 20 parts, 15 to 25 parts of Polygonatum, 15 to 25 parts of yellow mustard, 10 to 20 parts of Rhizoma Imperata, 15 to 25 parts of white, 10 to 20 parts of Ophiopogon, 10 to 20 parts of Rhizoma Chuanxiong, 15 to 25 parts of Coix seed, 10 to 20 parts of almonds, 15 to 30 parts of dried tangerine peel, 15 to 25 parts of agarwood, and 10 to 20 parts of Ganoderma lucidum.

Preferably, the pure Chinese medicine extract concentrate may further comprise extracts A and B mixed in any proportion as follows;

Extract A: An extract containing the following parts by weight, 10 to 20 parts of valerian, 20 to 30 parts of honeysuckle, 15 to 25 parts of tribute, 20 to 30 parts of dandelion, 15 to 25 parts of lavender, 15 leaves of lotus leaf ~25 parts, 10~20 parts of arborvitae leaves, 10~20 parts of wood butterfly, 15~25 parts of generational flowers, 15~25 parts of light bamboo leaves, 10~20 parts of musk;

Extract B: The extract containing the following parts by weight, 10 to 20 parts of Radix Scutellariae, 10 to 20 parts of aloe, 15 to 25 parts of Suzi, 15 to 25 parts of Rhodiola, and 15 to 25 of Magnolia 10 parts, 10 parts of figs, 15 to 25 parts of astragalus, 10 to 20 parts of scutellaria, 10 to 20 parts of angelica, 15 to 25 parts of licorice, 15 to 25 parts of cloves, 20 to 30 parts of platycodon, 10 to 20 parts of puerarin 20~30 parts of American ginseng, 20~30 parts of lily, 20~30 parts of Luo Han Guo, 10~20 parts of glutinous rice, 10~20 parts of fat sea, 15~25 parts of orange red, 10~20 parts of Sichuan Fritillaria, Polygonatum odoratum 15~25 parts, 15~25 parts of yellow mustard, 10~20 parts of Rhizoma Imperatae, 15~25 parts of medlar white, 10~20 parts of Ophiopogon, 10~20 parts of Chuanxiong, 15~25 parts of Coix seed, 10~20 parts of almond 15 to 30 servings of dried tangerine peel, 15 to 25 servings of agarwood, and 10 to 20 parts of Ganoderma lucidum.

Further, the fragrance may further comprise an extract of mint leaves.

A method for preparing a composition for replacing shredded tobacco comprises the following steps: (1) preparing a tobacco product, mixing the components of the tobacco filament with alcohol, stirring and moistening, maintaining a room temperature between 20 and 30 degrees, sealing fermentation for 3 days, drying, and then using a cutting machine to mix the mixture Cut into a tobacco of about 5 mm and air dry.

(2) preparing a pure Chinese medicine extract concentrate, uniformly spraying the pure Chinese medicine extract concentrate onto the tobacco obtained in the first step, at a low temperature and drying;

(3) A fragrance is prepared, which is sprayed onto the tobacco obtained in the second step.

Preferably, the step (2) comprises the following steps: weighing 10 to 20 parts of valerian, 20 to 30 parts of honeysuckle, 15 to 25 parts of tribute, 20 to 30 parts of dandelion, and 15 to 30 parts of lavender according to the weight ratio. 25 parts, lotus leaf 15~25 parts, arborvitae leaves 10~20 parts, wood butterfly 10~20 parts, generational flowers 15~25 parts, light bamboo leaves 15~25 parts, musk 10~20 parts, evenly mixed, Adding to 50%~80% ethanol, first heating and refluxing for 40 min, filtering; second heating and refluxing for 20 min, filtering, combining the filtrate; concentrating to a pure Chinese medicine extract concentrate with a density of 1.20~130.

Preferably, the step (2) further comprises the following steps: weighing 10 to 20 parts of the northern sand ginseng, 10 to 20 parts of the aloe, 15 to 25 parts of the sage, and 15 to 25 parts of the sedum according to the weight ratio. Parts, Magnolia 15~25 parts, fig 10~20 parts, Astragalus 15~25 parts, Sanqi 10~20 parts, Angelica 10~20 parts, Licorice 15~25 parts, Clove 15~25 parts, Campanulaceae 20~30 Parts, 10 to 20 parts of Pueraria, 20 to 30 parts of American ginseng, 20 to 30 parts of lily, 20 to 30 parts of Luo Han Guo, 10 to 20 parts of glutinous rice, 10 to 20 parts of fat sea, 15 to 25 parts of orange, 15 10~20 parts, 15~25 parts of Polygonatum, 15~25 parts of yellow mustard, 10~20 parts of Rhizoma Imperatae, 15~25 parts of white peony, 10~20 parts of Ophiopogon, 10~20 parts of Chuanxiong, 15~25 of Huanren 10 parts, almonds, 10 to 20 parts, 15 to 30 parts of dried tangerine peel, 15 to 25 parts of agarwood, 10 to 20 parts of Ganoderma lucidum, uniformly mixed, crushed, sieved through a 50 mesh, placed in a 1 L extraction vessel, and added with a co-extractant ethanol. Extraction pressure 15~45Mpa, extraction temperature 30~50°C, separation tank pressure 10~30Mpa, separation temperature 30~60°C, C02 flow rate 1L~3L /min, Extraction time 1. 0h~3. 0h. Filter to obtain the extract.

Further, the step (2) may further comprise the steps of mixing the filtrate obtained in the above two steps in an arbitrary ratio and concentrating to a pure Chinese medicine refining concentrate having a density of 1.20 to 1.30.

Preferably, the step (3) comprises: extracting the mint leaves in parts by weight, pulverizing, and taking the powder into the extraction vessel at an extraction pressure of 6.0 to 9. OMPa, the extraction temperature is 30 ° C to 55, The C02 flow rate was 1 L to 3 L/min, and C02 supercritical extraction was carried out for 1.0 to 2.0 h. The peppermint oil was collected, dehydrated with anhydrous sodium sulfate, filtered, filtered, and diluted with 95% ethanol.

Preferably, the step (3) comprises: weighing the golden silk jujube by weight ratio, adding 70% ethanol to reflux for 2 hours, and filtering.

The invention also discloses the use of the tobacco as a tobacco substitute. Further, the invention also discloses the application of the pure Chinese medicine extraction concentrate as a spray additive for tobacco substitute.

Further, the present invention also discloses the use of the extract of the mint leaf as a flavor on a tobacco substitute.

The beneficial effects of the invention are as follows: The main ingredient of the present invention, Yunnan Pu'er tea, is a product of warm stomach, lipid-lowering, anti-cancer, anti-cancer and nourishing. Pu'er tea contains caffeine, a kind of xanthine alkaloid compound, which is a central nervous system stimulant that stimulates the central nervous system of the brain, prolongs brain waking time and relieves fatigue. The tea polyphenols, tannic acid, and vitamins in tea have an adsorption complex for nicotine, which can eliminate the nicotine content in the body and play a role in quitting smoking. Studies have shown that the ingredients contained in tea can also make the flue gas sweet, delicate and soft, cover up the gas, reduce irritation, burn easily, and not extinguish the flame. So it can be used as a substitute for tobacco.

The invention can also be applied to lung diseases caused by various factors such as smoking, and most of the smokers have smoked for a long time, and the clinical manifestations are: less cough, uncomfortable cough, sputum and difficulty, dry throat or upper breath. The traditional Chinese medicine combination of the invention mainly includes Fritillaria, Lilium, Rhizoma Imperatae, Ophiopogon japonicus, Reed Rhizome, and Luo Han Guo, which have the functions of clearing away heat and phlegm, moistening the lungs and relieving cough, and setting the asthma, and matching the fat sea, the wood butterfly, the generation flower, and the jade. Bamboo, light bamboo leaves, Rhizoma Imperatae, white peony, Magnolia, and eucalyptus leaves enhance the power of clearing away phlegm, relieving cough and moistening dryness. (《Medicine in the West" (volume in the book) 痰痰 because of spleen deficiency, due to qi stagnation, so use 茯苓, 薏苡健 spleen and spleen, to the source of Dusheng ;; orange red, orange peel, tamping, agarwood The figs are qi and phlegm, so that the qi stagnation can be eliminated; then the platycodon, almonds, and scorpions are used to declare the lungs, phlegm and cough, so that the lungs can be declared to the right, and the combination of the spleen and the spleen can be used to clear the lungs. The Lord, and Run does not obstruct the phlegm, phlegm and phlegm without hurting the lungs, so that the lungs are clear and dry and self-sufficient, and the right to declare is reduced and the cough is self-leveling. The method of use of the invention is as follows:

1. Using the principle of "Chinese medicine fumigation therapy", by burning the shredded tobacco of the present invention instead of the composition, the flue gas is generated through the oral cavity, the respiratory tract, and the lung tissue, and the drug ions are directly absorbed and utilized, thereby improving the bioavailability of the drug. At the same time, it avoids the damage of the drug to the liver and kidney and the first-pass effect. The natural pure Chinese medicine of the invention is green, safe, reliable and has unique curative effect, and has the health care function that the internal medicine can not play in the cough, phlegm, chronic obstructive pulmonary disease and smoking cessation.

2. The invention can also play the role of relieving cough, phlegm, chronic obstructive pulmonary disease and quitting smoking through tea drinking and oral administration.

3. The invention extracts components by C02 supercritical extraction method, and the C02 supercritical extraction method is a new technology which integrates extraction and separation, and basically does not use organic solvent. The principle of C02 supercritical fluid extraction (SFE) separation process is to use the relationship between the solubility of supercritical fluid and its density, that is, the use of pressure And the effect of temperature on the solubility of supercritical fluids. In the supercritical state, C02 is a single phase between liquid and gas. It has a density close to that of liquid. The diffusion coefficient is 10~100 times that of liquid, and it has good permeability and solubility to materials. When the supercritical fluid is in contact with the substance to be separated, it selectively extracts the components of the polarity, the boiling point, and the molecular weight. Of course, the extract obtained for each pressure range cannot be single, but it is possible to control the conditions to obtain the optimum proportion of the mixed components, and then to make the supercritical fluid into a normal gas by means of decompression and temperature rise, and the extracted material is Completely or substantially precipitated to achieve separation and purification

C02 Supercritical extraction of the active ingredients of Chinese herbal medicines outstanding advantages: 1 can work at near room temperature, to prevent some of the heat-labile Chinese herbal ingredients from being destroyed or escaped, 2 extracts have a natural plant pure aroma, 3 extracts The active ingredient is fully retained, the color is good, the purity is high, the extraction rate is high, the energy is saved, the organic solvent is almost eliminated in the extraction process, the organic solvent is not left in the extract, and the environment is harmless. 6 C02 itself is inert and can be recycled. , cheap price.

Drug toxicity test

Eighteen Kunming mice were selected and divided into three groups, namely A, B, and C, each with 6 rats, half male and half female, weighing 18~20g. Fasted for 12 hours. Group A mice were each injected with 2 ml of a concentrate of conventional cigarettes. Group B mice were each injected with 2 ml of a concentrate of the non-tobacco cigarette of the present invention. Group C was injected with 2 ml of physiological saline. After 2 hours, all mice in group A died. Group B mice were more active and mentally active than before injection, and none of them died. Group C mice were normal and had no change compared with before injection. The conclusion of the acute toxicity test indicates that the traditional cigarette is toxic, and the non-tobacco cigarette of the present invention is not only non-toxic, but also has an effect of enhancing immunity.

clinical information

In 2009, in this city, 80 smokers who voluntarily quit smoking were found in the city, aged between 35 and 70, and the smoking period was more than 10 years. The 80 smokers were randomly divided into 4 groups of 20 people each. The first group A smokers smoke the non-tobacco cigarettes of the invention; the second group B smokers smoke the traditional tobacco cigarettes; the third group C smokers tea the non-tobacco cigarettes of the invention; the fourth group D is the non-smokers suction The present invention is a non-tobacco cigarette. They were also examined for related items: nicotine content in the urine, lung color, lung fibrosis, and chronic obstructive pulmonary disease. See the table below for the results. Results of the inspection results of each item inspection table group (0 days) Inspection results (after 1 year) The average amount of nicotine in urine is 2.3ug/ml _{; the} average amount of nicotine in urine is 0.5ug/ml, and the color of smoking lungs is black~ Dark black; 15 cases reached 100%; normal lung color accounted for pulmonary fibrosis; 18 cases were 96%; pulmonary fibrosis cure rate accounted for 98;

A 20 varying degrees of chronic obstructive pulmonary disease. Chronic obstructive pulmonary disease cure rate

98%.

The average amount of nicotine in the urine is 2.5ug/ml _{; the} average amount of nicotine in the urine is 3.0ug/ml, the color of the lung is black ~ dark black; the rate of smoke is 10%; the color of the lung is dark black. Fibrosis; 17 cases increased by 60%; pulmonary fibrosis accounted for

B 20 Different degrees of chronic obstructive pulmonary disease. 90%; different degrees of chronic obstructive pulmonary disease accounted for 100%. The average amount of nicotine in urine was 2.3ug/ml _{; the} average amount of nicotine in urine was 0.5ug/ml, the color of lung was black ~ dark black; there were 13 cases of tobacco People account for 100%; lung color becomes normal

C 20

Pulmonary fibrosis occurred; 17 cases were not 98%; pulmonary fibrosis cure rate was 100%; slow same degree of chronic obstructive pulmonary disease. The cure rate of obstructive pulmonary disease was 98%.

The amount of nicotine in the urine Oug/ml; the amount of nicotine in the urine of the lungs Oug / ml; the color of the lungs is close to normal 90%; the lungs are close to normal 100% in 2 cases; 0 cases of pulmonary fibrosis;

D 20

Fibrosis; 2 cases of chronic 0 cases of chronic obstructive pulmonary disease.

Obstructive pulmonary disease. Ei particles, smoke impregnated, repair lung tissue, treat chronic obstructive pulmonary disease, quit smoking and reach smoking cessation rate

98% The invention can meet the physiological and psychological needs of smokers for traditional cigarettes, and can be both aspirated and tea-drinked, and still has certain curative effect on non-smoker lung diseases.

detailed description

The invention will be further described below in conjunction with the embodiments.

Example 1

According to the weight ratio, weigh 30~40 copies of Yunnan Pu'er tea, 20~30 parts of rose, 20~30 parts of snow tea, 20~30 parts of Lingdan grass, 15~25 parts of saffron, 15~25 parts of ginkgo leaves, The alcohol was mixed evenly, stirred and moistened, kept at room temperature for 20 days at 30 to 30 degrees, and dried for drying. The above items were cut into filaments of about 5 mm by a cutting machine, and air-dried.

2, weigh 10 to 20 parts by weight, 10 to 30 parts of honeysuckle, 15 to 25 parts of tribute, 20 to 30 parts of dandelion, 15 to 25 parts of lavender, 15 to 25 parts of lotus leaf, arborvitae leaves 10~20 parts, 10~20 parts of wood butterfly, 15~25 parts of generational flowers, 15~25 parts of light bamboo leaves, 10~20 parts of musk, mixed evenly, added to 50%~80% ethanol, first The mixture was heated to reflux for 40 min, and filtered; the second heating was refluxed for 20 min, filtered, and the filtrate was combined and used.

3. Weigh 10~20 parts of Beisha ginseng, 10~20 parts of aloe vera, 15~25 parts of Suzi, 15~25 parts of Rhodiola, 15~25 parts of Magnolia, 10~20 parts of fig, according to the weight ratio. Astragalus 15~25 parts, Sanqi 10~20 parts, Angelica 10~20 parts, Licorice 15~25 parts, Clove 15~25 parts, Campanulaceae 20~30 parts, Pueraria 10~20 parts, American ginseng 20~30 parts, Lily 20~30 parts, 20~30 parts of Luo Han Guo, 10~20 parts of glutinous rice, 10~20 parts of fat sea, 15~25 parts of orange, 15~20 parts of Fritillaria, 15~25 parts of Polygonatum, Yellow mustard 15 ~25 parts, 10~20 parts of Rhizoma Imperatae, 15~25 parts of medlar white, 10~20 parts of Ophiopogon japonicus, 10~20 parts of Chuanxiong, 15~25 parts of Coix seed, 10~20 parts of almond, 15~30 parts of dried tangerine peel, Agarwood 15~25 parts, Ganoderma lucidum 10~20 parts are mixed evenly, crushed, passed through 50 mesh sieve, placed in 1L extraction kettle, added with co-extraction agent ethanol, set extraction pressure 15~45Mpa, extraction temperature 30~50°C, separation 0h〜3. 0h。 The pressure is 10~ 30Mpa, the separation temperature is 30~60°C, the flow rate of C02 is 1L~3L/min, and the extraction time is 1. 0h~3. 0h. After filtration, the extract was obtained.

4. Combine the two extracts of the above 2 and 3, and concentrate to a density of 1.20~1.30 for use.

5. The above concentrated liquid is evenly sprayed onto the above 1, dried in the shade, and rolled into an ultra-low tar finished product by using a ZB45 cigarette machine. Example 2 1. According to the weight ratio, weigh Yunnan Pu'er tea 30~40, rose 20~30, snow tea 20~30, Lingdan grass 20~30, saffron 15~25, ginkgo leaf 15~25, mix evenly with alcohol, Stirring and moistening, keeping the room temperature between 20 and 30 degrees for 3 days in a closed fermentation, drying, and then cutting the above-mentioned articles into a filament of about 5 mm with a cigarette cutter, and drying it by air flow.

2. Weigh 10~20 parts of valerian, 20~30 parts of honeysuckle, 15~25 parts of tribute, 20~30 parts of dandelion, 15~25 parts of lavender, 15~25 parts of lotus leaf, and arborvitae leaves 10 according to the weight ratio ~20 parts, 10~20 parts of wood butterfly, 15~25 parts of generational flowers, 15~25 parts of light bamboo leaves, 10~20 parts of musk, mixed evenly, added to 50%~80% ethanol, first time The mixture was heated to reflux for 40 min, filtered; the second heating was refluxed for 20 min, filtered, and the filtrate was combined.

3. Weigh 10~20 parts of Beisha ginseng, 10~20 parts of aloe vera, 15~25 parts of Suzi, 15~25 parts of Rhodiola, 15~25 parts of Magnolia, 10~20 parts of fig, according to the weight ratio. Astragalus 15~25 parts, Sanqi 10~20 parts, Angelica 10~20 parts, Licorice 15~25 parts, Clove 15~25 parts, Campanulaceae 20~30 parts, Pueraria 10~20 parts, American ginseng 20~30 parts, Lily 20~30 parts, 20~30 parts of Luo Han Guo, 10~20 parts of glutinous rice, 10~20 parts of fat sea, 15~25 parts of orange, 15~20 parts of Fritillaria, 15~25 parts of Polygonatum, Yellow mustard 15 ~25 parts, 10~20 parts of Rhizoma Imperatae, 15~25 parts of medlar white, 10~20 parts of Ophiopogon japonicus, 10~20 parts of Chuanxiong, 15~25 parts of Coix seed, 10~20 parts of almond, 15~30 parts of dried tangerine peel, Agarwood 15~25 parts, Ganoderma lucidum 10~20 parts are mixed evenly, crushed, passed through 50 mesh sieve, placed in 1L extraction kettle, added with co-extraction agent ethanol, set extraction pressure 15~45Mpa, extraction temperature 30~50°C, separation 0h〜3. 0h。 The pressure is 10~ 30Mpa, the separation temperature is 30~60°C, the flow rate of C02 is 1L~3L/min, and the extraction time is 1. 0h~3. 0h. Filtered to obtain an extract;

4. Combine the two extracts of the above 2 and 3, and concentrate to a density of 1.20~1.30 for use;

5. uniformly spraying the above concentrated liquid onto the tobacco obtained in the above step 1;

6. Weigh the mint leaves by weight ratio, pulverize, and take the powder into the extraction kettle. The extraction pressure is 6.0~ 9.0MPa, the extraction temperature is 30°C~55, and the C02 flow rate is lL~3L/min. Using C02 supercritical extraction 1.0~2.0 h, the peppermint oil was collected, dehydrated with anhydrous sodium sulfate, filtered, filtered, and diluted with 95% ethanol. The tobacco obtained in step 1 is dried in the shade and made into an ultra-low tar finished product by using ZB45 cigarette machine equipment. Example 3

The first five steps are the same as in the second embodiment.

6. Weigh the gold silk jujube by weight ratio, add 70% ethanol and heat to reflux for 2h, filter, spray the filtrate onto the tobacco obtained in step 1, dry it, use ZB45 cigarette machine equipment to make ultra low tar. Finished product. Example 4

1. Weigh 40 copies of Yunnan Pu'er tea, 25 parts of rose, 25 parts of snow tea, 20 parts of Lingdan grass, 20 parts of saffron, and 15 parts of ginkgo leaves by weight ratio. Mix well with alcohol, stir and moist, keep room temperature. The mixture was sealed and fermented for 20 days between 20 and 30 degrees, dried, and then cut into a filament of about 5 mm by a cutting machine, and air-dried.

2. Weigh 15 parts of valerian, 25 parts of honeysuckle, 20 parts of tribute, 20 parts of dandelion, 15 parts of lavender, 15 parts of lotus leaf, 20 parts of oriental arborvitae, 15 parts of wood butterfly, 15 parts of generational flowers. 15 parts of light bamboo leaves, 15 parts of musk, mixed evenly, added to 60% ethanol, first heated to reflux for 40min, filtered; second heated reflux for 20min, filtered, combined filtrate, spare.

3. Weigh 15 parts of Radix Scutellariae, 15 parts of Aloe Vera, 20 parts of Suzi, 15 parts of Rhodiola, 15 parts of Magnolia, 10 parts of fig, 20 parts of Astragalus, 15 parts of Sanqi, 15 parts of Angelica by weight ratio 15 parts of licorice, 15 parts of cloves, 20 parts of platycodon, 10 parts of pueraria, 30 parts of ginseng, 20 parts of lily, 20 parts of mangosteen, 15 parts of glutinous rice, 15 parts of fat sea, 20 parts of citrus red, 20 parts of chuanbei, 15 parts of Polygonatum, 15 parts of yellow mustard, 20 parts of Rhizoma Imperata, 15 parts of white peony, 15 parts of medlar, 15 parts of Ophiopogon japonicus, 15 parts of Chuanxiong, 15 parts of Coix seed, 15 parts of almond, 155 parts of dried tangerine peel, 155 parts of agarwood, 15 parts of Ganoderma lucidum , pulverize, pass 50 mesh sieve, place in 1L extraction kettle, add co-extractant ethanol, set extraction pressure 25Mpa, extraction temperature 45 °C, separation kettle pressure 15Mpa, separation temperature 50 °C, C02 flow rate 2L / min, 5小时。 Extraction time 1. 5h. Filtered to obtain an extract;

4. Combine the two extracts of the above 2 and 3, and concentrate to a density of 1.25 for use;

6. Weigh 0.6kg of mint leaves, crush, and take the powder into the extraction kettle. Under the conditions of extraction pressure of 8.5 MPa, extraction temperature of 40 °C and C02 flow rate of 2 L/min, the CO2 supercritical extraction was used for 1.5 h, the peppermint oil was collected, dehydrated with anhydrous sodium sulfate, filter paper, filtered, and appropriate amount. Dilute with 95% ethanol and spray the tobacco obtained in step 1.

7. Weigh the gold silk jujube by weight ratio, add 70% ethanol and heat to reflux for 2h, filter, and spray the filtrate onto the tobacco obtained in step 1. Dry it and use ZB45 cigarette machine to make ultra low tar. Finished product. The invention may be summarized in other specific forms without departing from the spirit or essential characteristics of the invention. Therefore, the above-described embodiments of the present invention are intended to be illustrative only and not to limit the scope of the invention, and the scope of the invention , _ the equivalent meaning and any changes within the scope of the request shall be considered to be included in the scope of the present invention.

Claims

Claim

A composition for replacing cut tobacco comprising the following components in a weight ratio: 10 to 100 parts of tobacco, and 1 to 10 parts of pure Chinese medicine extract concentrate sprayed on the tobacco, wherein The tobacco material comprises the following components by weight: 30~40 parts of Yunnan Pu'er tea, 20~30 parts of rose, 20~30 parts of snow tea, 20~30 parts of Lingdan grass, 15~25 parts of saffron , Ginkgo biloba leaves 15 to 25 servings.

The composition for replacing shredded tobacco according to claim 1, further comprising 0.5 to 1 part by weight of the perfume.

The composition for replacing shredded tobacco according to claim 1 or 2, wherein the pure Chinese medicine extract concentrate comprises the following components by weight fraction: 10 to 20 parts of valerian, 20 to 30 of honeysuckle Parts, Gongju 15~25 parts, dandelion 20~30 parts, lavender 15~25 parts, lotus leaf 15~25 parts, arborvitae leaves 10~20 parts, wood butterfly 10~20 parts, generation generation flowers 15~25 parts , 15 to 25 parts of light bamboo leaves, 10 to 20 parts of musk.

The composition for replacing shredded tobacco according to claim 1 or 2, wherein the pure Chinese medicine extract concentrate further comprises an extract of the following parts by weight: Beisha 10-20 parts, aloe vera 10~20 parts, 15~25 parts of Suzi, 15~25 parts of Rhodiola, 15~25 parts of Magnolia, 10~20 parts of fig, 15~25 parts of Astragalus, 10~20 parts of Sanqi, 10~20 of Angelica Parts, licorice 15~25 parts, clove 15~25 parts, platycodon 20~30 parts, puerarin 10~20 parts, American ginseng 20~30 parts, lily 20~30 parts, Luo Han Guo 20~30 parts, 茯苓10~20 parts, 10 to 20 parts of fat sea, 15 to 25 parts of orange, 15 to 20 parts of Fritillaria, 15 to 25 parts of Polygonatum, 15 to 25 parts of yellow mustard, 10 to 20 parts of Rhizoma Imperata, 15 to 25 parts of white, 10~20 parts of Ophiopogon, 10~20 parts of Chuanxiong, 15~25 parts of Coix seed, 10~20 parts of almond, 15~30 parts of tangerine peel, 15~25 parts of agarwood, 10~20 parts of Ganoderma lucidum.

The composition for replacing shredded tobacco according to claim 1 or 2, wherein the pure Chinese medicine extracting concentrate comprises the following extracts A and B mixed in any ratio;

6. A composition for replacing shredded tobacco according to claim 2, wherein: said flavor comprises

Correction page (Article 91) The extract of the golden silk jujube of the claims.

7. A composition for replacing shredded tobacco according to claim 2, wherein: said flavor comprises an extract of mint leaves.

The composition for replacing shredded tobacco according to claim 2, wherein the flavor comprises an extract of the golden silk jujube mixed in an arbitrary ratio and an extract of mint leaves.

9. A method of preparing a composition for replacing shredded tobacco according to claim 1 or 2, comprising the steps of:

(1) preparing a tobacco product, mixing the tobacco-like component of claim 1 with alcohol, stirring and moistening, maintaining a room temperature between 20 and 30 degrees, sealing fermentation for 3 days, drying, and then cutting the tobacco. The mixture was cut into a tobacco of about 5 mm and air dried.

(2) preparing a pure Chinese medicine extract concentrate, uniformly spraying the pure Chinese medicine extract concentrate onto the tobacco obtained in the first step, low temperature and drying;

(3) A fragrance is prepared, and the fragrance is sprayed onto the tobacco obtained in the second step.

The preparation method according to claim 9, wherein the step (2) comprises: weighing 10 to 20 parts of valerian, 20 to 30 parts of honeysuckle, and 15 to 25 parts of tribute by weight ratio. 20~30 parts of dandelion, 15~25 parts of lavender, 15~25 parts of lotus leaf, 10~20 parts of arborvitae leaves, 10~20 parts of wood butterfly, 15~25 parts of generational flowers, 15~25 parts of light bamboo leaves, 10~20 parts of musk, mixed evenly, added to 50%~80% ethanol, first heated to reflux for 40min, filtered; second heated reflux for 20min, filtered, combined filtrate; concentrated to a density of 1.20~1.30 pure Chinese medicine extract concentrate.

The preparation method according to claim 9, wherein the step (2) comprises: weighing 10 to 20 parts of the northern sand ginseng, 10 to 20 parts of the aloe vera, and 15 to 20 parts of the aloe vera according to the weight ratio. 25 parts, Rhodiola 15~25 parts, Magnolia 15~25 parts, fig 10~20 parts, Astragalus 15~25 parts, Sanqi 10~20 parts, Angelica 10~20 parts, Licorice 15~25 parts, clove 15~25 parts, 20~30 parts of Campanulaceae, 10~20 parts of Pueraria, 20~30 parts of American ginseng, 20~30 parts of lily, 20~30 parts of Luo Han Guo, 10~20 parts of glutinous rice, 10~20 parts of fat sea, orange 15 to 25 parts of red, 10 to 20 parts of Fritillaria, 15 to 25 parts of Polygonatum, 15 to 25 parts of yellow mustard, 10 to 20 parts of Rhizoma Imperata, 15 to 25 parts of white peony, 10 to 20 parts of Ophiopogon, 10 to 20 parts of Ophiopogon japonicus ~20 parts, 15 to 25 parts of coix seed, 10 to 20 parts of almonds, 15 to 30 parts of dried tangerine peel, 15 to 25 parts of agarwood, 10 to 20 parts of Ganoderma lucidum, uniformly mixed, crushed, sieved through 50 mesh, placed in a 1 L extraction kettle Adding co-extraction agent ethanol, setting extraction pressure 15~45Mpa, extraction temperature 30~50Ό, separation tank pressure 10~ 30Mpa, separation temperature 30~60°C, C02 flow rate 1L~3L /min, extraction time 1. 0h~3. 0h. After filtration, the extract was obtained.

The preparation method according to claim 10 or 11, wherein the step (2) comprises: mixing the filtrate obtained in the steps of claim 10 and claim 11 in an arbitrary ratio, and concentrating

12 Correction page (Article 91) A pure Chinese medicine extraction concentrate having a density of 1.20 to 1.30 is claimed.

The preparation method according to claim 9, wherein the step (3) comprises: weighing the mint leaves in parts by weight, pulverizing, and taking the powder into the extraction kettle at an extraction pressure of 6.0 to 9 OMPa, extraction temperature is 30 ° C ~ 55, CO2 flow rate is lL ~ 3L / min, using CO2 supercritical extraction L0~2. 0 h, collecting peppermint oil, dehydrated with anhydrous sodium sulfate, filter paper filter, Dilute with 95% ethanol.

The preparation method according to claim 9, wherein the step (3) comprises: weighing the golden silk jujube by weight ratio, heating and refluxing with 70% ethanol for 2 hours, and filtering to obtain a filtrate.

15. Use of the tobacco as claimed in claim 9 as a substitute for cut tobacco.

16. Use of a pure traditional Chinese medicine extract concentrate according to claim 10 or 11 as a spray additive for tobacco substitute.

Use of an extract of the golden silk jujube and mint leaves according to claim 11 or 12 as a flavor of tobacco substitute.

13 Correction page (Article 91)