CN105029699A - Mint glycerol triacetate extract and application thereof in cigarette - Google Patents
Mint glycerol triacetate extract and application thereof in cigarette Download PDFInfo
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- CN105029699A CN105029699A CN201510336731.8A CN201510336731A CN105029699A CN 105029699 A CN105029699 A CN 105029699A CN 201510336731 A CN201510336731 A CN 201510336731A CN 105029699 A CN105029699 A CN 105029699A
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- peppermint
- glycerol triacetate
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Abstract
The invention discloses a mint glycerol triacetate extract and application thereof in cigarette. The mint glycerol triacetate extract is prepared from mint which is cleaned and dried and is ground to 20-40 meshes and is prepared by taking glycerol triacetate as an extracting agent through the following steps: firstly, carrying out heating reflux extraction, and then, carrying out ultrasonic extraction so as to obtain the mint glycerol triacetate extract. Then, the mint glycerol triacetate extract is prepared into a solution which is 0.5-3% in concentration by taking glycerol triacetate as a solvent; the prepared solution is uniformly sprayed on filter rod tows according to 7-8% of the weight of the filter rod tows so as to prepare a cigarette filter rod; and through a conventional cigarette rolling process, a cigarette containing mint effective components in the filter rod is prepared. The extract can be used for significantly improving the smoking smell of the cigarette, bringing about fresh and natural cooling feeling of mint to the cigarette, and enhancing the comfort in the mouth and throat of a smoker. The mint glycerol triacetate extract disclosed by the invention is simple in production process, strong in operability and normalization, conducive to the achievement of industrial production and good in application prospect, and the raw materials are easily available and are low in cost.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of peppermint triacetyl glycerine extract.Meanwhile, the invention still further relates to the described application of peppermint triacetyl glycerine extract in cigarette.
Background technology
Not only peppermint is Labiatae mint, is a kind of important fragrant plant but also is one of traditional Chinese herbal medicine of China.Peppermint taste cool in nature is pungent, returns lung, Liver Channel.Taste is refreshing, has medical and edible dual-use function.The peppermint of fresh harvesting can as the fresh vegetable on dining table, clearly good to eat, has effect of the improving eyesight that clears away heart-fire, wind-dispelling heat-dissipating, removing toxic substances with peppermint for tea.Containing number of chemical composition in peppermint: volatile oil, comprises alcohol, ketone, ester, terpenes and terpane class etc.; Flavone compound; Terpene and steroid compound; Organic acid and phenolic acid; Amino acid and some other functional components, contained many property materials have good biologically active.The volatile oil contained because of it in peppermint stem and leaf has strong mint flavored, also has been widely used in production of cigarettes.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus that each tobacco productive corporation is researched and developed.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.The such as application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN103271441A) thereof, a kind of filter stick fiber base material additive and application (CN103126073A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN104161303A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582A) etc., but the filter stick additive described in above-mentioned patent need first by extract or allocate additive again in triacetyl glycerine dissolve add in cigarette, or the additive some being insoluble in triacetyl glycerine is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the solvability of triacetyl glycerine to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in triacetyl glycerine, limit the application of spices in cigarette filter rod.On the other hand, if be not that medium carries out filter stick perfuming by triacetyl glycerine, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco business in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, there is provided a kind of mint extract prepared using triacetyl glycerine as extractant, this extract is applied to the refrigerant sense that cigarette can give cigarette peppermint, and coordinates with cigarette cigarette perfume, improve suction comfortableness, cover assorted gas, taste is inhaled in rectification.
The present invention also aims to provide the described application of peppermint triacetyl glycerine extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage adopted in the present invention is mass percent.
A kind of peppermint triacetyl glycerine extract, is obtained by the method for following steps:
(1) fresh mint is cleaned, dry in the shade, pulverized 20 ~ 40 mesh sieves, for subsequent use;
(2) take peppermint powder and be placed in round-bottomed flask, add the glycerol triacetate for tobacco of peppermint powder weight 5 ~ 10 times as extractant, soaking at room temperature, after 3 ~ 5 hours, carries out refluxing extraction under 50 ~ 100 DEG C of conditions, 3 ~ 6 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 600W, 40kHZ condition, extract 10 ~ 40 minutes, obtain settled solution after excessively filtering filter residue and be required peppermint triacetyl glycerine extract.
The described application of peppermint triacetyl glycerine extract in cigarette, it is characterized in that: take triacetyl glycerine as solvent, described peppermint triacetyl glycerine extract is mixed with the solution that concentration is 0.5 ~ 3%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the peppermint triacetyl glycerine extract prepared by the present invention, can dissolve each other in any proportion with triacetyl glycerine, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that peppermint exists by prior art when filter stick additive is mixed and is fitted in plasticizer.
2. adopt triacetyl glycerine to be that extractant extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in triacetyl glycerine in peppermint fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to triacetyl glycerine time, the loss of effective efficiency composition.
3. gained peppermint triacetyl glycerine extract effectively can promote the oral cavity of smoker, the comfort level of throat, makes cigarette taste fresh and clean, coordinates, have the effect alleviating flue gas excitant, improve pleasant impression simultaneously with cigarette perfume.
4. material used herein is food-grade, has higher safety in utilization.
5. production technology of the present invention is simple, operability and normative strong, and raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
Fresh peppermint is cleaned, dry in the shade, pulverized 40 mesh sieves, the peppermint powder taking a certain amount of pulverizing is placed in round-bottomed flask, add the glycerol triacetate for tobacco of raw material 5 times amount (V/W) as extractant, soaking at room temperature is after 5 hours, refluxing extraction is carried out under 70 DEG C of conditions, extraction time is 3 hours, to be cooled to room temperature, peppermint after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (400W, 40kHZ), extract 20 minutes, cross after filtering filter residue and obtain settled solution, required peppermint triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, peppermint triacetyl glycerine extract is mixed with the solution that concentration is 2%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains peppermint active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas adding above-mentioned peppermint triacetyl glycerine extract has obvious refrigerant sense, and the oral cavity of smoker and the comfort level of throat are increased, and flue gas excitant and pleasant impression obviously improve, and sucking quality promotes.
Embodiment 2
Fresh peppermint is cleaned, dry in the shade, pulverized 20 mesh sieves, the peppermint powder taking a certain amount of pulverizing is placed in round-bottomed flask, add the glycerol triacetate for tobacco of raw material 80 times amount (V/W) as extractant, after room temperature soaks 5 hours, refluxing extraction is carried out under 50 DEG C of conditions, extraction time is 6 hours, to be cooled to room temperature, peppermint after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (600W, 40kHZ), extract 40 minutes, cross after filtering filter residue and obtain settled solution, required peppermint triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, peppermint triacetyl glycerine extract is mixed with the solution that concentration is 0.5%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains peppermint active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and add the refrigerant sense of the imparting flue gas peppermint of above-mentioned peppermint triacetyl glycerine extract, flue gas is fresh and clean, and cigarette excitant reduces, pleasant impression improves.
Embodiment 3
Fresh peppermint is cleaned, dry in the shade, pulverized 40 mesh sieves, the peppermint powder taking a certain amount of pulverizing is placed in round-bottomed flask, add the glycerol triacetate for tobacco of raw material 10 times amount (V/W) as extractant, soaking at room temperature is after 5 hours, refluxing extraction is carried out under 100 DEG C of conditions, extraction time is 6 hours, to be cooled to room temperature, peppermint after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (400W, 40kHZ), extract 10 minutes, cross after filtering filter residue and obtain settled solution, required peppermint triacetyl glycerine extract can be obtained.
Be that peppermint triacetyl glycerine extract is mixed with the solution that concentration is 3% by solvent with triacetyl glycerine, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7% and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains peppermint active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas adding above-mentioned peppermint triacetyl glycerine extract has the refrigerant sense of obvious peppermint, and flue gas is fresh and clean, and assorted gas and excitant obviously reduce, and pleasant impression and suction comfortableness are obviously improved.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a peppermint triacetyl glycerine extract, is obtained by the method for following steps:
(1) fresh mint is cleaned, dry in the shade, pulverized 20 ~ 40 mesh sieves, for subsequent use;
(2) take peppermint powder and be placed in round-bottomed flask, add the glycerol triacetate for tobacco of peppermint powder weight 5 ~ 10 times as extractant, soaking at room temperature, after 3 ~ 5 hours, carries out refluxing extraction under 50 ~ 100 DEG C of conditions, 3 ~ 6 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 600W, 40kHZ condition, extract 10 ~ 40 minutes, obtain settled solution after excessively filtering filter residue and be required peppermint triacetyl glycerine extract.
2. the application of peppermint triacetyl glycerine extract according to claim 1 in cigarette, it is characterized in that: take triacetyl glycerine as solvent, described peppermint triacetyl glycerine extract is mixed with the solution that concentration is 0.5 ~ 3%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
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| CN201510336731.8A CN105029699A (en) | 2015-06-17 | 2015-06-17 | Mint glycerol triacetate extract and application thereof in cigarette |
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| CN201510336731.8A CN105029699A (en) | 2015-06-17 | 2015-06-17 | Mint glycerol triacetate extract and application thereof in cigarette |
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Cited By (3)
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| CN105686076A (en) * | 2016-03-25 | 2016-06-22 | 湖北中烟工业有限责任公司 | Method for preparing cigarette filter tip containing temperature sensibility controlled-released cool essence |
| CN108179062A (en) * | 2017-12-27 | 2018-06-19 | 广东中烟工业有限责任公司 | A kind of composition containing natural extracts and its application in functionalization filter stick plasticizer is prepared |
| CN111418892A (en) * | 2020-05-20 | 2020-07-17 | 云南如茨生物科技有限公司 | Cigarette filter stick additive and application thereof |
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| CN105686076A (en) * | 2016-03-25 | 2016-06-22 | 湖北中烟工业有限责任公司 | Method for preparing cigarette filter tip containing temperature sensibility controlled-released cool essence |
| CN108179062A (en) * | 2017-12-27 | 2018-06-19 | 广东中烟工业有限责任公司 | A kind of composition containing natural extracts and its application in functionalization filter stick plasticizer is prepared |
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