CN105029698A - Radix scrophulariae and glycerol triacetate extracts and application of radix scrophulariae and glycerol triacetate extracts on cigarettes - Google Patents
Radix scrophulariae and glycerol triacetate extracts and application of radix scrophulariae and glycerol triacetate extracts on cigarettes Download PDFInfo
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- CN105029698A CN105029698A CN201510336693.6A CN201510336693A CN105029698A CN 105029698 A CN105029698 A CN 105029698A CN 201510336693 A CN201510336693 A CN 201510336693A CN 105029698 A CN105029698 A CN 105029698A
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- radix scrophulariae
- glycerol triacetate
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- triacetyl glycerine
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Abstract
The invention discloses radix scrophulariae and glycerol triacetate extracts and application of the radix scrophulariae and glycerol triacetate extracts on cigarettes. Radix scrophulariae particles of which the moisture content is 8-10% and the grain size is 20-60 meshes serve as raw materials, and glycerol triacetate serve as extraction agents. The application of the radix scrophulariae and glycerol triacetate extracts on the cigarettes comprises the following steps of extracting in a heating and flow-returning mode; preparing radix scrophulariae glycerol triacetate extracts through microwave extraction; preparing the radix scrophulariae and glycerol triacetate extracts into liquor of which the concentration is 1-3% by using the glycerol triacetate as solvent; uniformly spraying the liquor on diacetate cellulose tows under the condition that the weight percentage of the liquor is 7-8% of that of the diacetate cellulose tows to obtain cigarette filter sticks; and preparing cigarettes with the filter sticks containing effective ingredients of the radix scrophulariae through the conventional cigarette curling process. The salivation promoting and sweet taste of smoke of the cigarettes can be obviously improved by the extracts, fragrance of the cigarettes is natural and strong, and remaining taste is clean and comfortable. A production technology is simple, operability and standardability are high, raw materials are easy to obtain, the cost is low, industrialized production is convenient to implement, and the application prospect is good.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of radix scrophulariae triacetyl glycerine extract.Meanwhile, the invention still further relates to the described application of radix scrophulariae triacetyl glycerine extract in cigarette.
Background technology
Radix scrophulariae taste is sweet, bitter, salty, cold nature, is a kind of traditional for clearing heat and detoxicating medicinal plant, has clearing heat and detoxicating, relieving pain and activating blood circulation, and relieve sore throat reduces phlegm and subside a swelling effect of yin-nourishing.The active ingredient of radix scrophulariae mainly comprises phytosterol, organic acid, flavonoids, carbohydrate, alkaloid, iridoids, Phenylpropanoid Glycosides glycosides, acetone, aliphatic acid and volatilization wet goods, modern medicine study shows, the bioactivator in radix scrophulariae has anti-inflammation, antitumor, develop immunitypty, antifatigue, protects the liver oxidation resistant effect.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus that each tobacco productive corporation is researched and developed.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.The such as application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN103271441A) thereof, a kind of filter stick fiber base material additive and application (CN103126073A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN104161303A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582A) etc., but the filter stick additive described in above-mentioned patent need first by extract or allocate additive again in triacetyl glycerine dissolve add in cigarette, or the additive some being insoluble in triacetyl glycerine is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the solvability of triacetyl glycerine to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in triacetyl glycerine, limit the application of spices in cigarette filter rod perfuming.On the other hand, if be not that medium carries out filter stick perfuming by triacetyl glycerine, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco business in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of Radix Scrophulariae extract prepared using triacetyl glycerine as extractant is provided, this extract is applied to the sweet sense of promoting the production of body fluid that cigarette effectively can increase cigarette, and cigarette perfume (or spice) enriches full, alcohol and clear and rich, excitant and oral cavity is residual alleviates.
The present invention also aims to provide the described embody rule of radix scrophulariae triacetyl glycerine extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage adopted in the present invention is mass percent.
A kind of radix scrophulariae triacetyl glycerine extract, is obtained by the method for following steps:
(1) first by radix scrophulariae coarse crushing, under 50 ~ 70 DEG C of conditions, be dried to moisture is 8 ~ 10%, then pulverizing is 20 ~ 60 object particles further, for subsequent use;
(2) take 500 ~ 1000 parts of radix scrophulariae particles according to weight portion and be placed in round-bottomed flask, glycerol triacetate for tobacco is added as extractant by solid-liquid ratio 1:4 ~ 7, soaking at room temperature is after 4 ~ 10 hours, refluxing extraction is carried out under 70 ~ 120 DEG C of conditions, 4 ~ 9 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 600W, 40kHZ condition, extract 20 ~ 55 minutes, obtain settled solution after excessively filtering filter residue and be required radix scrophulariae triacetyl glycerine extract.
The described application of radix scrophulariae triacetyl glycerine extract in cigarette, it is characterized in that: take triacetyl glycerine as solvent, described radix scrophulariae triacetyl glycerine extract is mixed with the solution that concentration is 1 ~ 3%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the radix scrophulariae triacetyl glycerine extract prepared by the present invention, can dissolve each other in any proportion with triacetyl glycerine, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that radix scrophulariae exists by prior art when filter stick additive is mixed and is fitted in plasticizer.
2. adopt triacetyl glycerine to be that extractant extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in triacetyl glycerine in radix scrophulariae fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to triacetyl glycerine time, the loss of effective efficiency composition.
3. gained radix scrophulariae triacetyl glycerine extract can effectively show cigarette sweet sense of promoting the production of body fluid back, enrich cigarette nature fragrance, have simultaneously and alleviate the residual effect in flue gas excitant and oral cavity.
4. material used herein is food-grade, has higher safety in utilization.
5. production technology of the present invention is simple, operability and normative strong, and raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
First by radix scrophulariae coarse crushing, under 50 DEG C of conditions, be dried to moisture is 8%, then pulverizes further as 20-60 object particle.Take 500g radix scrophulariae particle according to weight portion and be placed in round-bottomed flask, adding solid-liquid ratio is that the glycerol triacetate for tobacco of 1:7 is as extractant, soaking at room temperature is after 10 hours, refluxing extraction is carried out under 70 DEG C of conditions, extraction time is 9 hours, after being cooled to room temperature, radix scrophulariae after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (400W, 40kHZ), extract 45 minutes, cross after filtering filter residue and obtain settled solution, required radix scrophulariae triacetyl glycerine extract can be obtained.
Be that radix scrophulariae triacetyl glycerine extract is mixed with the solution that concentration is 1% by solvent with triacetyl glycerine, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains radix scrophulariae active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the sweet sense of cigarette flue gas adding above-mentioned radix scrophulariae triacetyl glycerine extract is obvious, and oral cavity is promoted the production of body fluid back sweet, and flue gas excitant and assorted gas obviously alleviate, and cigarette perfume (or spice) is fresh and clean.
Embodiment 2
First by radix scrophulariae coarse crushing, under 70 DEG C of conditions, be dried to moisture is 10%, then pulverizes further as 40-60 object particle.Take 800g radix scrophulariae particle according to weight portion and be placed in round-bottomed flask, adding solid-liquid ratio is that the glycerol triacetate for tobacco of 1:4 is as extractant, soaking at room temperature is after 4 hours, refluxing extraction is carried out under 120 DEG C of conditions, extraction time is 4 hours, after being cooled to room temperature, radix scrophulariae after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (600W, 40kHZ), extract 20 minutes, cross after filtering filter residue and obtain settled solution, required radix scrophulariae triacetyl glycerine extract can be obtained.
Be that radix scrophulariae triacetyl glycerine extract is mixed with the solution that concentration is 3% by solvent with triacetyl glycerine, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains radix scrophulariae active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas adding above-mentioned radix scrophulariae triacetyl glycerine extract is pure and fresh sweet, delicate mouthfeel alcohol and, excitant reduce, pleasant impression improve, cigarette perfume (or spice) enriches full.
Embodiment 3
First by radix scrophulariae coarse crushing, under 50 DEG C of conditions, be dried to moisture is 8-10%, then pulverizes further as 20-60 object particle.Take 500g radix scrophulariae particle according to weight portion and be placed in round-bottomed flask, adding solid-liquid ratio is that the glycerol triacetate for tobacco of 1:7 is as extractant, soaking at room temperature is after 4 hours, refluxing extraction is carried out under 70 DEG C of conditions, extraction time is 6 hours, after being cooled to room temperature, radix scrophulariae after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (400W, 40kHZ), extract 20 minutes, cross after filtering filter residue and obtain settled solution, required radix scrophulariae triacetyl glycerine extract can be obtained.
Be that radix scrophulariae triacetyl glycerine extract is mixed with the solution that concentration is 3% by solvent with triacetyl glycerine, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8% and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains radix scrophulariae active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas adding above-mentioned radix scrophulariae triacetyl glycerine extract is sweet smooth and easy, and flue gas excitant obviously reduces, and pleasant impression and oral cavity remain and improve, and cigarette perfume (or spice) is abundanter.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a radix scrophulariae triacetyl glycerine extract, is obtained by the method for following steps:
(1) first by radix scrophulariae coarse crushing, under 50 ~ 70 DEG C of conditions, be dried to moisture is 8 ~ 10%, then pulverizing is 20 ~ 60 object particles further, for subsequent use;
(2) take 500 ~ 1000 parts of radix scrophulariae particles according to weight portion and be placed in round-bottomed flask, glycerol triacetate for tobacco is added as extractant by solid-liquid ratio 1:4 ~ 7, soaking at room temperature is after 4 ~ 10 hours, refluxing extraction is carried out under 70 ~ 120 DEG C of conditions, 4 ~ 9 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 600W, 40kHZ condition, extract 20 ~ 55 minutes, obtain settled solution after excessively filtering filter residue and be required radix scrophulariae triacetyl glycerine extract.
2. the application of radix scrophulariae triacetyl glycerine extract according to claim 1 in cigarette, it is characterized in that: take triacetyl glycerine as solvent, described radix scrophulariae triacetyl glycerine extract is mixed with the solution that concentration is 1 ~ 3%, be sprayed onto on tow by the ratio uniform of acetate fibres beam quality 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
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Cited By (2)
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| CN106539124A (en) * | 2016-10-20 | 2017-03-29 | 云南中烟工业有限责任公司 | A kind of cigarette filter tip additive and preparation method thereof |
| CN106539125A (en) * | 2016-10-20 | 2017-03-29 | 云南中烟工业有限责任公司 | Sweetened humectant additive of a kind of cigarette shreds and preparation method thereof |
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Cited By (4)
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| CN106539124A (en) * | 2016-10-20 | 2017-03-29 | 云南中烟工业有限责任公司 | A kind of cigarette filter tip additive and preparation method thereof |
| CN106539125A (en) * | 2016-10-20 | 2017-03-29 | 云南中烟工业有限责任公司 | Sweetened humectant additive of a kind of cigarette shreds and preparation method thereof |
| CN106539125B (en) * | 2016-10-20 | 2018-05-18 | 云南中烟工业有限责任公司 | A kind of sweetened humectant additive of cigarette shreds and preparation method thereof |
| CN106539124B (en) * | 2016-10-20 | 2018-05-29 | 云南中烟工业有限责任公司 | A kind of preparation method of cigarette filter tip additive |
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