CN105132163A - Moringa seed glycerol triacetate extract and application thereof in cigarettes - Google Patents
Moringa seed glycerol triacetate extract and application thereof in cigarettes Download PDFInfo
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- CN105132163A CN105132163A CN201510336852.2A CN201510336852A CN105132163A CN 105132163 A CN105132163 A CN 105132163A CN 201510336852 A CN201510336852 A CN 201510336852A CN 105132163 A CN105132163 A CN 105132163A
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- glycerol triacetate
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Abstract
The invention discloses a moringa seed glycerol triacetate extract and an application thereof in cigarettes. The moringa seed glycerol triacetate extract is prepared by the steps: taking shelled moringa seed particles with the moisture content of 6%-8% and the particle size of 20-40 mesh as raw material, taking glycerol triacetate as an extraction agent, firstly, extracting by a heating reflux method, and extracting by ultrasonic waves to obtain the moringa seed glycerol triacetate extract. Then with glycerol triacetate as a solvent, the moringa seed glycerol triacetate extract is made into a solution with the concentration of 2-4%, the solution is evenly sprayed onto filter rod tows with the proportion of 7-8% of the weight of the acetate fiber tows, then cigarette filter rods are prepared, and the cigarettes having the filter rods containing moringa seed effective ingredients are prepared through a conventional cigarette rolling process. The extract can significantly enhance the smoke sweet feeling, and makes the sweet taste kept for a longer time in an oral cavity. The moringa seed glycerol triacetate extract has the advantages of simple production process, strong operability and normalization, easily available raw materials, low cost, easy realization of industrialized production, and good application prospect.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of moringa seeds glycerine triacetate extract.Meanwhile, the invention still further relates to the described application of moringa seeds glycerine triacetate extract in cigarette.
Background technology
Moringa, as a kind of torrid zone, subtropics multi-functional plant, has long edible history, comprehensively nutritious.Research shows, Moringa is except rich in proteins, carbohydrate, multivitamin and mineral substance, and its plant different sites also comprises: the multiple bioactive ingredients such as organic acid, ester class, glycoside, sterol, ketone, Polyphenols, carotene, antioxygen element and phytokinin.Moringa seeds is very crisp and sweet, and swallow after slowly tasting, the sweet taste in throat still sustainable some minutes, that now eats other foods all can feel sweet taste.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus that each tobacco productive corporation is researched and developed.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.The such as application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN103271441A) thereof, a kind of filter stick fiber base material additive and application (CN103126073A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN104161303A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582A) etc., but the filter stick additive described in above-mentioned patent mainly first by extract or allocate additive again in glycerine triacetate dissolve add in cigarette, or the additive some being insoluble in glycerine triacetate is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the dissolving power of glycerine triacetate to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in glycerine triacetate, limit the application of additive in cigarette filter rod perfuming.On the other hand, if be not that medium carries out filter stick perfuming by glycerine triacetate, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable Technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco industry in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide a kind of moringa seeds extract prepared using glycerine triacetate as extraction agent, this extract is applied to cigarette effectively can be strengthened cigarette sweet moisture feeling and exquisiteness, enrich cigarette nature fragrance.
The present invention also aims to provide the described embody rule of moringa seeds glycerine triacetate extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage ratio adopted in the present invention is mass percent.
A kind of moringa seeds glycerine triacetate extract, is obtained by the method for following steps:
(1) after being shelled by moringa seeds, under 100 DEG C of conditions, be dried to moisture is 6% ~ 8%, then pulverizing is 20 ~ 40 object particles, for subsequent use;
(2) take 5 ~ 10 parts of moringa seeds particles according to weight part and be placed in round-bottomed flask, add 70 ~ 100 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature is after 3 ~ 5 hours, refluxing extraction is carried out under 80 ~ 150 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 500W, 40kHZ condition, extract 20 ~ 45 minutes, obtain settled solution after excessively filtering filter residue and be required moringa seeds glycerine triacetate extract.
The described application of moringa seeds glycerine triacetate extract in cigarette, it is characterized in that: be that described moringa seeds glycerine triacetate extract is mixed with the solution that concentration is 2 ~ 4% by solvent with glycerine triacetate, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the moringa seeds glycerine triacetate extract prepared by the present invention, can dissolve each other in any proportion with glycerine triacetate, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that moringa seeds exists by prior art when filter stick additive is mixed and is fitted in softening agent.
2. adopt glycerine triacetate to be that extraction agent extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in glycerine triacetate in moringa seeds fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to glycerine triacetate time, the loss of effective efficiency composition.
3. gained moringa seeds glycerine triacetate extract effectively can be given prominence to the fragrant and sweet note of cigarette, enrich cigarette nature fragrance, has the effect reducing flue gas pungency, improve pleasant impression simultaneously.
4. material used herein is food grade, has higher safety in utilization.
5. production technique of the present invention is simple, operability and standardization strong, raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
After being shelled by moringa seeds, under 100 DEG C of conditions, be dried to moisture is 8%, then is crushed to 40 object particles.Take 10 parts of moringa seeds particles according to weight part and be placed in round-bottomed flask, add 100 parts of glycerol triacetate for tobacco and make extraction agent, soaking at room temperature is after 5 hours, refluxing extraction is carried out under 150 DEG C of conditions, extraction time is 8 hours, after being cooled to room temperature, moringa seeds after refluxing extraction and glycerine triacetate mixture are placed in ultrasonic extractor (500W, 40kHZ), extract 45 minutes, cross after filtering filter residue and obtain settled solution, required moringa seeds glycerine triacetate extract can be obtained.
Take glycerine triacetate as solvent, moringa seeds glycerine triacetate extract is mixed with the solution that concentration is 2%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains moringa seeds effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the sweet sense of cigarette flue gas adding above-mentioned moringa seeds glycerine triacetate extract is obvious, and the sweet sense in oral cavity can keep the long period, and flue gas pungency obviously reduces, pleasant impression be improved significantly, cigarette perfume (or spice) is abundanter.
Embodiment 2
After being shelled by moringa seeds, under 100 DEG C of conditions, be dried to moisture is 7%, then pulverizing is 30 object particles.Take 7 parts of moringa seeds particles according to weight part and be placed in round-bottomed flask, the glycerol triacetate for tobacco adding 85 parts makes extraction agent, soaking at room temperature is after 4 hours, refluxing extraction is carried out under 110 DEG C of conditions, extraction time is 6 hours, to be cooled to room temperature, moringa seeds after refluxing extraction and glycerine triacetate mixture are placed in ultrasonic extractor (500W, 40kHZ), extract 32 minutes, cross after filtering filter residue and obtain settled solution, required moringa seeds glycerine triacetate extract can be obtained.
Take glycerine triacetate as solvent, moringa seeds glycerine triacetate extract is mixed with the solution that concentration is 3%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains moringa seeds effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the sweet sense of cigarette flue gas adding above-mentioned moringa seeds glycerine triacetate extract is obvious, and the sweet sense in oral cavity can keep the long period, and flue gas pungency obviously reduces, pleasant impression be improved significantly, cigarette perfume (or spice) is abundanter.
Embodiment 3
After being shelled by moringa seeds, under 100 DEG C of conditions, be dried to moisture is 6%, then pulverizing is 20 object particles.Take 5 parts of moringa seeds particles according to weight part and be placed in round-bottomed flask, the glycerol triacetate for tobacco adding 70 parts makes extraction agent, soaking at room temperature is after 3 hours, refluxing extraction is carried out under 80 DEG C of conditions, extraction time is 4 hours, to be cooled to room temperature, moringa seeds after refluxing extraction and glycerine triacetate mixture are placed in ultrasonic extractor (500W, 40kHZ), extract 20 minutes, cross after filtering filter residue and obtain settled solution, required moringa seeds glycerine triacetate extract can be obtained.
Take glycerine triacetate as solvent, moringa seeds glycerine triacetate extract is mixed with the solution that concentration is 4%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7% and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains moringa seeds effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the sweet sense of cigarette flue gas adding above-mentioned moringa seeds glycerine triacetate extract is obvious, and the sweet sense in oral cavity can keep the long period, and flue gas pungency obviously reduces, pleasant impression be improved significantly, cigarette perfume (or spice) is abundanter.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a moringa seeds glycerine triacetate extract, is obtained by the method for following steps:
(1) after being shelled by moringa seeds, under 100 DEG C of conditions, be dried to moisture is 6% ~ 8%, then pulverizing is 20 ~ 40 object particles, for subsequent use;
(2) take 5 ~ 10 parts of moringa seeds particles according to weight part and be placed in round-bottomed flask, add 70 ~ 100 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature is after 3 ~ 5 hours, refluxing extraction is carried out under 80 ~ 150 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 500W, 40kHZ condition, extract 20 ~ 45 minutes, obtain settled solution after excessively filtering filter residue and be required moringa seeds glycerine triacetate extract.
2. the application of moringa seeds glycerine triacetate extract according to claim 1 in cigarette, it is characterized in that: be that described moringa seeds glycerine triacetate extract is mixed with the solution that concentration is 2 ~ 4% by solvent with glycerine triacetate, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510336852.2A CN105132163A (en) | 2015-06-17 | 2015-06-17 | Moringa seed glycerol triacetate extract and application thereof in cigarettes |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108142983A (en) * | 2018-02-02 | 2018-06-12 | 新智能生活馆（深圳）有限公司 | A kind of electronic atomized liquid composition and its application |
| CN109588760A (en) * | 2018-12-13 | 2019-04-09 | 中国烟草总公司郑州烟草研究院 | A kind of moringa seeds base chewing smokeless tobacco and preparation method thereof |
-
2015
- 2015-06-17 CN CN201510336852.2A patent/CN105132163A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108142983A (en) * | 2018-02-02 | 2018-06-12 | 新智能生活馆（深圳）有限公司 | A kind of electronic atomized liquid composition and its application |
| CN109588760A (en) * | 2018-12-13 | 2019-04-09 | 中国烟草总公司郑州烟草研究院 | A kind of moringa seeds base chewing smokeless tobacco and preparation method thereof |
| CN109588760B (en) * | 2018-12-13 | 2021-03-26 | 中国烟草总公司郑州烟草研究院 | Preparation method of moringa seed-based chewing smokeless tobacco |
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