CN104479871A - Crumbable carbon dioxide solid flavor ball and application of flavor ball in cigarette filter rod - Google Patents
Crumbable carbon dioxide solid flavor ball and application of flavor ball in cigarette filter rod Download PDFInfo
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- CN104479871A CN104479871A CN201410776822.9A CN201410776822A CN104479871A CN 104479871 A CN104479871 A CN 104479871A CN 201410776822 A CN201410776822 A CN 201410776822A CN 104479871 A CN104479871 A CN 104479871A
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- parts
- ball
- carbon dioxide
- extract
- dioxide solid
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- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 title claims abstract description 66
- 239000007787 solid Substances 0.000 title claims abstract description 46
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 41
- 239000001569 carbon dioxide Substances 0.000 title claims abstract description 29
- 229910002092 carbon dioxide Inorganic materials 0.000 title claims abstract description 29
- 239000000796 flavoring agent Substances 0.000 title abstract 10
- 235000019634 flavors Nutrition 0.000 title abstract 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 44
- 239000002245 particle Substances 0.000 claims abstract description 17
- 230000002378 acidificating effect Effects 0.000 claims abstract description 16
- 239000000126 substance Substances 0.000 claims abstract description 16
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims abstract description 13
- 239000001110 calcium chloride Substances 0.000 claims abstract description 13
- 229910001628 calcium chloride Inorganic materials 0.000 claims abstract description 13
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 238000002360 preparation method Methods 0.000 claims abstract description 5
- 239000000284 extract Substances 0.000 claims description 30
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 21
- 238000000034 method Methods 0.000 claims description 20
- 235000013599 spices Nutrition 0.000 claims description 20
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 12
- YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical compound [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 claims description 9
- 235000019691 monocalcium phosphate Nutrition 0.000 claims description 9
- 239000002304 perfume Substances 0.000 claims description 9
- 239000001509 sodium citrate Substances 0.000 claims description 9
- 229920002472 Starch Polymers 0.000 claims description 8
- 239000001506 calcium phosphate Substances 0.000 claims description 8
- 239000001683 mentha spicata herb oil Substances 0.000 claims description 8
- 229910000150 monocalcium phosphate Inorganic materials 0.000 claims description 8
- 239000003921 oil Substances 0.000 claims description 8
- 235000019198 oils Nutrition 0.000 claims description 8
- 235000019721 spearmint oil Nutrition 0.000 claims description 8
- 239000008107 starch Substances 0.000 claims description 8
- 235000019698 starch Nutrition 0.000 claims description 8
- -1 sucrose fatty ester Chemical class 0.000 claims description 8
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 claims description 8
- 229940038773 trisodium citrate Drugs 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 238000001879 gelation Methods 0.000 claims description 7
- 241001116389 Aloe Species 0.000 claims description 6
- 241000416162 Astragalus gummifer Species 0.000 claims description 6
- 235000005976 Citrus sinensis Nutrition 0.000 claims description 6
- 240000002319 Citrus sinensis Species 0.000 claims description 6
- 229920001615 Tragacanth Polymers 0.000 claims description 6
- 235000011399 aloe vera Nutrition 0.000 claims description 6
- 159000000007 calcium salts Chemical class 0.000 claims description 6
- 239000011347 resin Substances 0.000 claims description 6
- 229920005989 resin Polymers 0.000 claims description 6
- 235000010487 tragacanth Nutrition 0.000 claims description 6
- 239000000196 tragacanth Substances 0.000 claims description 6
- 229940116362 tragacanth Drugs 0.000 claims description 6
- 229930006000 Sucrose Natural products 0.000 claims description 5
- 239000005720 sucrose Substances 0.000 claims description 5
- 244000215068 Acacia senegal Species 0.000 claims description 4
- 244000025254 Cannabis sativa Species 0.000 claims description 4
- 241000675108 Citrus tangerina Species 0.000 claims description 4
- 229920000858 Cyclodextrin Polymers 0.000 claims description 4
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 4
- 229920000084 Gum arabic Polymers 0.000 claims description 4
- 244000061176 Nicotiana tabacum Species 0.000 claims description 4
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 4
- 235000010489 acacia gum Nutrition 0.000 claims description 4
- 239000000205 acacia gum Substances 0.000 claims description 4
- NEEHYRZPVYRGPP-IYEMJOQQSA-L calcium gluconate Chemical compound [Ca+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O NEEHYRZPVYRGPP-IYEMJOQQSA-L 0.000 claims description 4
- FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical compound [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 claims description 4
- 235000010418 carrageenan Nutrition 0.000 claims description 4
- 229920001525 carrageenan Polymers 0.000 claims description 4
- 150000004676 glycans Chemical class 0.000 claims description 4
- 239000000419 plant extract Substances 0.000 claims description 4
- 229920001282 polysaccharide Polymers 0.000 claims description 4
- 239000005017 polysaccharide Substances 0.000 claims description 4
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 claims description 4
- 229940095064 tartrate Drugs 0.000 claims description 4
- 239000000341 volatile oil Substances 0.000 claims description 4
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 2
- 229920002101 Chitin Polymers 0.000 claims description 2
- PHOQVHQSTUBQQK-SQOUGZDYSA-N D-glucono-1,5-lactone Chemical compound OC[C@H]1OC(=O)[C@H](O)[C@@H](O)[C@@H]1O PHOQVHQSTUBQQK-SQOUGZDYSA-N 0.000 claims description 2
- 244000153234 Hibiscus abelmoschus Species 0.000 claims description 2
- 235000015511 Liquidambar orientalis Nutrition 0.000 claims description 2
- 229920000161 Locust bean gum Polymers 0.000 claims description 2
- 240000007673 Origanum vulgare Species 0.000 claims description 2
- 235000004383 Origanum vulgare subsp. vulgare Nutrition 0.000 claims description 2
- 239000004870 Styrax Substances 0.000 claims description 2
- 244000028419 Styrax benzoin Species 0.000 claims description 2
- 235000000126 Styrax benzoin Nutrition 0.000 claims description 2
- 240000004584 Tamarindus indica Species 0.000 claims description 2
- 235000004298 Tamarindus indica Nutrition 0.000 claims description 2
- 244000126002 Ziziphus vulgaris Species 0.000 claims description 2
- 229920000392 Zymosan Polymers 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 claims description 2
- 239000001527 calcium lactate Substances 0.000 claims description 2
- 229960002401 calcium lactate Drugs 0.000 claims description 2
- 235000011086 calcium lactate Nutrition 0.000 claims description 2
- 239000004833 fish glue Substances 0.000 claims description 2
- 235000012209 glucono delta-lactone Nutrition 0.000 claims description 2
- 229960003681 gluconolactone Drugs 0.000 claims description 2
- 235000010420 locust bean gum Nutrition 0.000 claims description 2
- 239000001367 polianthes tuberosa l. flower oil Substances 0.000 claims description 2
- 235000010413 sodium alginate Nutrition 0.000 claims description 2
- 239000000661 sodium alginate Substances 0.000 claims description 2
- 229940005550 sodium alginate Drugs 0.000 claims description 2
- 229940092665 tea leaf extract Drugs 0.000 claims description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims 1
- 239000011575 calcium Substances 0.000 claims 1
- 229960005069 calcium Drugs 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 230000000391 smoking effect Effects 0.000 abstract description 10
- 238000003756 stirring Methods 0.000 abstract description 4
- 239000002131 composite material Substances 0.000 abstract description 3
- 238000003860 storage Methods 0.000 abstract description 3
- 239000000945 filler Substances 0.000 abstract 2
- 239000011230 binding agent Substances 0.000 abstract 1
- 230000003247 decreasing effect Effects 0.000 abstract 1
- 229910017053 inorganic salt Inorganic materials 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- 235000011837 pasties Nutrition 0.000 abstract 1
- 238000004321 preservation Methods 0.000 abstract 1
- 159000000000 sodium salts Chemical class 0.000 abstract 1
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 10
- 235000011089 carbon dioxide Nutrition 0.000 description 8
- 238000005516 engineering process Methods 0.000 description 8
- 239000000243 solution Substances 0.000 description 7
- 239000007864 aqueous solution Substances 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 6
- 239000003205 fragrance Substances 0.000 description 5
- 235000017557 sodium bicarbonate Nutrition 0.000 description 5
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 5
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 4
- 239000003546 flue gas Substances 0.000 description 4
- 239000000470 constituent Substances 0.000 description 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 230000005802 health problem Effects 0.000 description 2
- 235000019633 pungent taste Nutrition 0.000 description 2
- 235000019263 trisodium citrate Nutrition 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 241000282412 Homo Species 0.000 description 1
- 239000008896 Opium Substances 0.000 description 1
- 208000004224 Opium Dependence Diseases 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229940062672 calcium dihydrogen phosphate Drugs 0.000 description 1
- 229910000389 calcium phosphate Inorganic materials 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000004868 gas analysis Methods 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229960001027 opium Drugs 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
- 239000007901 soft capsule Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
- A24D3/048—Tobacco smoke filters characterised by their shape or structure containing additives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Confectionery (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses crumbable carbon dioxide solid flavor balls as well as a preparation method and application of the flavor ball in a cigarette filter rod. The crumbable carbon dioxide solid flavor ball is prepared from the following raw materials in parts by weight: 20-80 parts of composite filler, 5-15 parts of a binder, 2-10 parts of a natural flavor and 10-30 parts of water. The preparation method comprises the following steps of sequentially and rapidly adding sodium salt, inorganic salt, an acidic substance, calcium chloride and the filler into a stirring container filled with hot water, carrying out heat preservation, and stirring to be uniform and viscous pasty to obtain a paste; and preparing particles of which the sizes are smaller than 20 meshes in squeezing and granulating manners through a 20-mesh sieve, placing the particles into a microwave oven, and treating the particles for 3-15 minutes at a microwave power density of 10-40 kilowatts/m<2> to obtain the flavor ball. By the flavor ball, the irritation of the cigarette is effectively decreased, and the smoking quality of the cigarette is improved; since the flavor ball has low mixture content, the storage time is longer, the influences caused by moisture and temperature are smaller and thus the flavor ball is hardly deformed and softened.
Description
Technical field
The present invention relates to solid spice ball, and containing the cigarette filter rod of this solid spice ball, refer to a kind of carbon dioxide solid Flavouring ball of pinching brokenly and the application in cigarette filter rod thereof particularly.
Background technology
Smoking is one of important environmental factors of harm humans health, and smoking and health problem are worldwide important topics.Due to smoking, human consumer is numerous, and ban on opium-smoking and the opium trade is difficult to realize comprehensively, reduces the hazardness of cigarette smoke to human body and becomes the effective way alleviating smoking and health problem.In recent years, for reducing cigarette hazardness, protect the health of smoking human consumer better, researcher has expanded in Harm reduction techniques gain field and has studied widely.How to make the tar of cigarette and objectionable constituent thereof reduce, keep again cigarette odor-absorbing to make human consumer obtain physiology simultaneously and meet, be the gordian technique difficult problem that Cigarette design faces.
The application of current cigarette flavouring harm reduction additive is very extensive, falls burnt and compensating aroma important role at Harm reduction techniques.Tobacco aromatics using mainly adds in pipe tobacco by prior art, can participate in burning, may produce new objectionable impurities because of cracking along with the suction of cigarette; If be added in filter stick, may be difficult to dissolve each other with filter stick softening agent, or easily cause dust raising phenomenon, be difficult to realize compound and add.Separately there is the method that cotton thread adsorbs, also have difficult quantitation, addition instability, skewness, easily the defect such as to scatter and disappear.Therefore cause being difficult to realize the industrial applications in cigarette.Have the soft capsule of parcel essence in prior art, what in smoking process, be subject to flue gas moisture and temperature affects deliquescing, is difficult to make the capsule in filter stick broken by finger pressure.
Summary of the invention
Technical problem to be solved by this invention is just to provide a kind of carbon dioxide solid Flavouring ball pinched brokenly and preparation method thereof and the application in cigarette filter rod, because the even carbonic acid gas bubble structure that this solid spice ball contains, before suction, human consumer can pinch and break light sound, slowly-releasing goes out the fragrance of natural perfume, human consumer can be touched and hear, has and clearly feel; When cigarette burning is to back segment, larger heat, by mouth rod, can make the carbonic acid gas bubble inside solid spice ball break further, send slight crackling, makes human consumer produce unique sense and novel sense; And the content of the objectionable constituent such as the phenol in flue gas can be reduced, effectively reduce cigarette pungency, improve cigarette smoking quality, because its water content is low, storage time is longer, and the impact by moisture and temperature is less, is not easy to be out of shape deliquescing.
For solving the problems of the technologies described above, a kind of carbon dioxide solid Flavouring ball pinched brokenly provided by the invention, the raw materials by weight portion of described solid spice ball forms than the water of meter by the compounded mix of 20 ~ 80 parts, the tackiness agent of 5 ~ 15 parts, the natural perfume of 2 ~ 10 parts and 10 ~ 30 parts; Wherein, described compounded mix is made up of sodium bicarbonate, acidic substance, weighting material and calcium salt.
Further, the weight ratio of described sodium bicarbonate, acidic substance, weighting material is: 1 ︰ 1 ~ 3 ︰ 1 ~ 3 ︰ 0.1 ~ 1.
Again further, described acidic substance be in monocalcium phosphate, tartrate, oxysuccinic acid, citric acid, Gluconolactone, sucrose fatty ester, tartarus, Trisodium Citrate any one.
Again further, described weighting material is starch, wheat-flour or cyclodextrin.
Again further, described calcium salt be in calcium chloride, secondary calcium phosphate, calglucon and calcium lactate any one.
When sodium bicarbonate and acidic substance effect can produce carbonic acid gas, acidic substance can also in and the basic salt that formed in carbonic acid gas production process, and the speed that regulation of carbon dioxide produces, makes bubble distribution even.Different according to its proportioning, the made carbonic acid gas bubble amount contained by solid spice ball is different with distribution consistency degree.
Again further, described tackiness agent is any one or a few in tamarind seed gum, Viscogum BE, Tragacanth, carob bean gum, maleic resin, carrageenin, gum arabic, celestial grass polysaccharide, extract solution from aloe, chitin, zymosan, fish glue and sodium alginate.
Again further, described natural perfume is selected from natural plant extracts and volatile oil, described natural plant extracts is coffee extract, in jujube extract, Fructus Fici extract, Radix Glycyrrhizae extract, Paraquay tea leaf extract, Moschus extract, sweet orange extract, plum extract and tobacco extract any one, volatile oil is any one or a few in spearmint oil, wild marjoram oil, Oleum Menthae Rotundifoliae, styrax oil, tangerine oil, tuberose oil.
Again further, described solid spice ball raw materials by weight portion than meter by 10 parts sodium bicarbonate, the Trisodium Citrate of 5 parts, the monocalcium phosphate of 5 parts, the starch of 5 parts, the calcium chloride of 1 part, the Tragacanth of 10 parts, the maleic resin of 5 parts, the sweet orange extract of 8 parts, the spearmint oil of 2 parts and 20 parts water form.
The invention provides a kind of carbon dioxide solid Flavouring ball preparation method pinched brokenly, comprise the following steps:
1) compounded mix, tackiness agent, natural perfume, water is taken by the ratio of weight and number of above-mentioned raw materials; For subsequent use, wherein, described compounded mix is made up of sodium bicarbonate, acidic substance, weighting material;
2) stirred vessel that hot water is housed is heated to 80 ~ 90 DEG C, respectively by sodium bicarbonate, acidic substance, calcium salt with hot water dissolving, add in stirred vessel by sodium bicarbonate, acidic substance, calcium chloride water and weighting material successively, insulated and stirred, to even thick-pasty, obtains mashed prod;
3) by step 2) obtain mashed prod reduction temperature to normal temperature, be less than 20 object particles by 20 eye mesh screen extruder grain modes are obtained, above-mentioned particle put into microwave oven, with 10 ~ 40 kilowatts/m
2microwave Power Density process 3 ~ 15 minutes, make mashed prod gelation shape and be dried into the carbon dioxide solid Flavouring ball that can pinch brokenly, water content is less than 8%.
Present invention also offers a kind of application of carbon dioxide solid Flavouring ball in cigarette filter rod of pinching brokenly, the amount of Flavouring ball is added in cigarette filter rod according to the addition of 10 ~ 50mg/10mm tow, in management process, these cigarette do not discharge the fragrance of spices, but pinch brokenly Flavouring ball before aspirating this cigarette, and in aspiration procedure, give out the fragrance of spices Absorbable organic halogens.
Beneficial effect of the present invention is:
This carbon dioxide solid Flavouring ball that can pinch brokenly is by the compounded mix (other materials such as sodium bicarbonate, acidic substance, weighting material) of certain proportioning, natural perfume, tackiness agent, water etc., constantly stir at a certain temperature, form the short texture of inner how fine and closely woven carbonic acid gas bubble, cross screen cloth by extruder grain mode at a certain temperature and obtain Flavouring ball, make this solid spice ball water content lower than 8% by microwave drying, there are certain hardness and fragility, can pinch brokenly and send the sound and slowly-releasing fragrance; This solid spice ball locates applying one or many in the wire-beam forming process of filter tip stick, and the general filter stick formation Technology once shaped adopting prior art is a meta structure filter stick or multi-factor structure filter stick, then rolls into cigarette.Because the even carbonic acid gas bubble structure that this solid spice ball contains, before suction, human consumer can pinch and break light sound, and slowly-releasing goes out the fragrance of natural perfume, human consumer can be touched and hear, has and clearly feel; When cigarette burning is to back segment, larger heat, by mouth rod, can make the carbonic acid gas bubble inside solid spice ball break further, send slight crackling, makes human consumer produce unique sense and novel sense; And the content of the objectionable constituent such as the phenol in flue gas can be reduced, effectively reduce cigarette pungency, improve cigarette smoking quality, because its water content is low, storage time is longer, and the impact by moisture and temperature is less, is not easy to be out of shape deliquescing.
Embodiment
In order to explain the present invention better, illustrate main contents of the present invention further below in conjunction with specific embodiment, but content of the present invention is not only confined to following examples.
Embodiment 1
1) sodium bicarbonate of 20g, the tartrate of 20g, the wheat-flour of 20g, the calcium chloride of 20g, the extract solution from aloe of 5g, the Radix Glycyrrhizae extract of 2g is taken, water 25mL;
2) stirred vessel that hot water is housed is heated to 84 DEG C, sodium bicarbonate, calcium chloride are used a small amount of hot water dissolving, successively sodium bicarbonate aqueous solution, tartrate, calcium chloride water, wheat-flour, extract solution from aloe, Radix Glycyrrhizae extract are added rapidly in the hot water in stirred vessel, insulated and stirred, to even thick-pasty, obtains mashed prod; Water amounts to 25mL;
3) by step 2) obtain mashed prod reduction temperature to normal temperature, be less than 20 object particles by 20 eye mesh screen extruder grain modes are obtained, above-mentioned particle put into microwave oven, with 40 kilowatts/m
2microwave Power Density process 5 minutes, make mashed prod gelation shape and be dried into the carbon dioxide solid Flavouring ball 1 that can pinch brokenly, water content is less than 8%.
The amount of Flavouring ball is added in cigarette filter rod according to the addition of 10mg/10mm tow, this solid spice ball locates applying in the wire-beam forming process of filter tip stick, the general filter stick formation Technology once shaped adopting prior art is a meta structure filter stick, then rolls into cigarette 1.
Embodiment 2
1) sodium bicarbonate of 10g, the Trisodium Citrate of 5g, the monocalcium phosphate of 5g, the starch of 5g, the calcium chloride of 1g, the Tragacanth of 10g, the maleic resin of 5g, the sweet orange extract of 8g, the spearmint oil of 2g is taken, water 20mL;
2) stirred vessel that hot water is housed is heated to 88 DEG C, sodium bicarbonate, Trisodium Citrate, monocalcium phosphate are used a small amount of hot water dissolving respectively, and successively sodium bicarbonate aqueous solution, sodium citrate aqueous solution, calcium dihydrogen phosphate aqueous solution, starch, Tragacanth, maleic resin, sweet orange extract, spearmint oil are added rapidly in the hot water of stirred vessel, insulated and stirred, to even thick-pasty, obtains mashed prod; Water amounts to 20mL;
3) by step 2) obtain mashed prod reduction temperature to normal temperature, be less than 20 object particles by 20 eye mesh screen extruder grain modes are obtained, above-mentioned particle put into microwave oven, with 10 kilowatts/m
2microwave Power Density process 10 minutes, make mashed prod gelation shape and be dried into the carbon dioxide solid Flavouring ball 2 that can pinch brokenly, water content is less than 8%.
The amount of Flavouring ball is added in cigarette filter rod according to the addition of 20mg/10mm tow, this solid spice ball locates applying in the wire-beam forming process of filter tip stick, the general filter stick formation Technology once shaped adopting prior art is a meta structure filter stick, then rolls into cigarette 2.
Embodiment 3
1) sodium bicarbonate, the citric acid of 15g, the calglucon of 10g, the cyclodextrin of 15g, the gum arabic of 5g, the celestial grass polysaccharide of 5g, the extract solution from aloe of 5g, the coffee extract of 5g, the 30mL water of 15g;
2) stirred vessel that hot water is housed is heated to 85 DEG C, sodium bicarbonate, citric acid, calglucon are used a small amount of hydrothermal solution respectively, and the above-mentioned aqueous solution and cyclodextrin, gum arabic, celestial grass polysaccharide, extract solution from aloe, coffee extract are added rapidly in the hot water of stirred vessel successively do not stop insulated and stirred to even thick-pasty, obtain mashed prod; Water amounts to 30mL;
3) by step 2) obtain mashed prod reduction temperature to normal temperature, be less than 20 object particles by 20 eye mesh screen extruder grain modes are obtained, above-mentioned particle put into microwave oven, with 10 ~ 40 kilowatts/m
2microwave Power Density process 15 minutes, make mashed prod gelation shape and be dried into the carbon dioxide solid Flavouring ball 3 that can pinch brokenly, water content is less than 8%.
The amount of Flavouring ball is added in cigarette filter rod according to the addition of 30mg/10mm tow, this solid spice ball locates applying in the wire-beam forming process of filter tip stick, the general filter stick formation Technology once shaped adopting prior art is a meta structure filter stick, then rolls into cigarette 3.
Embodiment 4
1) tartarus, the sucrose fatty ester of 10g, the calcium chloride of 10g, the wheat-flour of 20g, 1g spearmint oil, 1g Oleum Menthae Rotundifoliae, the 30mL water of 18g sodium bicarbonate, 10g;
2) stirred vessel that hot water is housed is heated to 90 DEG C, sodium bicarbonate, tartarus, sucrose fatty ester, calcium chloride are used a small amount of hydrothermal solution respectively, to stir while add rapidly in stirred vessel according to tartarus, sucrose fatty ester, calcium chloride, wheat-flour, spearmint oil, Oleum Menthae Rotundifoliae successively, insulated and stirred, to even thick-pasty, obtains mashed prod;
3) by step 2) obtain mashed prod reduction temperature to normal temperature, be less than 20 object particles by 20 eye mesh screen extruder grain modes are obtained, above-mentioned particle put into microwave oven, with 20 kilowatts/m
2microwave Power Density process 15 minutes, make mashed prod gelation shape and be dried into the carbon dioxide solid Flavouring ball that can pinch brokenly, water content is less than 8%.
The amount of Flavouring ball is added in cigarette filter rod according to the addition of 40mg/10mm tow, this solid spice ball locates applying in the wire-beam forming process of filter tip stick, the general filter stick formation Technology once shaped adopting prior art is a meta structure filter stick, then rolls into cigarette 4.
Embodiment 5
1) sodium bicarbonate, the Trisodium Citrate of 10g, the monocalcium phosphate of 15g, the secondary calcium phosphate of 1.5g, the starch of 10g, the carrageenin of 8g, the tangerine oil of 6g of 15g, 25mL water;
2) stirred vessel that hot water is housed is heated to 82 DEG C, the secondary calcium phosphate of sodium bicarbonate, Trisodium Citrate, monocalcium phosphate and 1.5g is used a small amount of hot water dissolving respectively, the above-mentioned aqueous solution and starch, carrageenin, tangerine oil are added rapidly in stirred vessel successively, insulated and stirred, to even thick-pasty, obtains mashed prod;
3) by step 2) obtain mashed prod reduction temperature to normal temperature, be less than 20 object particles by 20 eye mesh screen extruder grain modes are obtained, above-mentioned particle put into microwave oven, with 30 kilowatts/m
2microwave Power Density process 6 minutes, make mashed prod gelation shape and be dried into the carbon dioxide solid Flavouring ball that can pinch brokenly, water content is less than 8%.
The amount of Flavouring ball is added in cigarette filter rod according to the addition of 10mg/10mm tow, this solid spice ball locates applying in the wire-beam forming process of filter tip stick, the general filter stick formation Technology once shaped of employing prior art is the ternary structural filter stick of filter stick-Flavouring ball-filter stick, rolls into cigarette 5.
Table 1: the composite filter cigarette and the contrast smoking result thereof that add the carbon dioxide solid Flavouring ball that can pinch brokenly
Table 2 composite filter cigarette and control sample flue gas analysis result
Other unspecified part is prior art.Although above-described embodiment is to invention has been detailed description; but it is only the present invention's part embodiment; instead of whole embodiment, people can also obtain other embodiments according to the present embodiment under without creative prerequisite, and these embodiments all belong to scope.
Claims (10)
1. the carbon dioxide solid Flavouring ball can pinched brokenly, is characterized in that: the raw materials by weight portion of described solid spice ball forms than the water of meter by the compounded mix of 20 ~ 80 parts, the tackiness agent of 5 ~ 15 parts, the natural perfume of 2 ~ 10 parts and 10 ~ 30 parts; Wherein, described compounded mix is made up of sodium bicarbonate, acidic substance, weighting material and calcium salt.
2. the carbon dioxide solid Flavouring ball can pinched brokenly according to claim 1, is characterized in that: the weight ratio of described sodium bicarbonate, acidic substance, weighting material is: 1 ︰ 1 ~ 3 ︰ 1 ~ 3 ︰ 0.1 ~ 1.
3. the carbon dioxide solid Flavouring ball can pinched brokenly according to claim 1 or 2, is characterized in that: described acidic substance be in monocalcium phosphate, tartrate, oxysuccinic acid, citric acid, Gluconolactone, sucrose fatty ester, tartarus, Trisodium Citrate any one.
4. the carbon dioxide solid Flavouring ball can pinched brokenly according to claim 1 or 2, is characterized in that: described weighting material is starch, wheat-flour or cyclodextrin.
5. the carbon dioxide solid Flavouring ball can pinched brokenly according to claim 1 or 2, is characterized in that: described calcium salt be in calcium chloride, secondary calcium phosphate, calglucon and calcium lactate any one.
6. the carbon dioxide solid Flavouring ball can pinched brokenly according to claim 1 or 2, is characterized in that: described tackiness agent is any one or a few in tamarind seed gum, Viscogum BE, Tragacanth, carob bean gum, maleic resin, carrageenin, gum arabic, celestial grass polysaccharide, extract solution from aloe, chitin, zymosan, fish glue and sodium alginate.
7. the carbon dioxide solid Flavouring ball can pinched brokenly according to claim 1 or 2, it is characterized in that: described natural perfume is selected from natural plant extracts and volatile oil, described natural plant extracts be coffee extract, in jujube extract, Fructus Fici extract, Radix Glycyrrhizae extract, Paraquay tea leaf extract, Moschus extract, sweet orange extract, plum extract and tobacco extract any one, volatile oil is any one or a few in spearmint oil, wild marjoram oil, Oleum Menthae Rotundifoliae, styrax oil, tangerine oil, tuberose oil.
8. the carbon dioxide solid Flavouring ball can pinched brokenly according to claim 1 or 2, is characterized in that: the raw materials by weight portion of described solid spice ball than meter by 10 parts sodium bicarbonate, the Trisodium Citrate of 5 parts, the monocalcium phosphate of 5 parts, the starch of 5 parts, the calcium chloride of 1 part, the Tragacanth of 10 parts, the maleic resin of 5 parts, the sweet orange extract of 8 parts, the spearmint oil of 2 parts and 20 parts water form.
9. the carbon dioxide solid Flavouring ball preparation method that can pinch brokenly described in claim 1, is characterized in that: comprise the following steps:
1) compounded mix, tackiness agent, natural perfume, water is taken by the ratio of weight and number of above-mentioned raw materials; For subsequent use, wherein, described compounded mix is made up of sodium bicarbonate, acidic substance, weighting material;
2) stirred vessel that hot water is housed is heated to 80 ~ 90 DEG C, respectively by sodium bicarbonate, acidic substance, calcium salt with hot water dissolving, add in stirred vessel by sodium bicarbonate, acidic substance, calcium saline solution and weighting material successively, insulated and stirred, to even thick-pasty, obtains mashed prod;
3) by step 2) obtain mashed prod reduction temperature to normal temperature, be less than 20 object particles by 20 eye mesh screen extruder grain modes are obtained, above-mentioned particle put into microwave oven, with 10 ~ 40 kilowatts/m
2microwave Power Density process 3 ~ 15 minutes, make mashed prod gelation shape and be dried into the carbon dioxide solid Flavouring ball that can pinch brokenly, water content is less than 8%.
10. the application of carbon dioxide solid Flavouring ball in cigarette filter rod can pinched brokenly described in claim 1, is characterized in that: added in cigarette filter rod by the addition of the amount of Flavouring ball according to 10 ~ 50mg/10mm tow.
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| CN106509979A (en) * | 2016-12-26 | 2017-03-22 | 福建中烟工业有限责任公司 | Composition and method for preparing tobacco extract by using composition |
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| CN109497611A (en) * | 2018-12-12 | 2019-03-22 | 湖北中烟工业有限责任公司 | One kind is improved to heat the cigarette cooling mouth stick that do not burn |
| CN109497611B (en) * | 2018-12-12 | 2021-03-16 | 湖北中烟工业有限责任公司 | Improved cooling filter tip for heating non-combustion cigarette |
| CN111700301A (en) * | 2020-06-18 | 2020-09-25 | 吕品华 | A health cigarette containing Chinese medicinal materials, and its preparation method |
| CN112956736A (en) * | 2021-03-17 | 2021-06-15 | 河南中烟工业有限责任公司 | Preparation method of sweet particles for cigarette filter stick and sweet filter stick |
| CN114621818A (en) * | 2022-03-09 | 2022-06-14 | 山东省食品发酵工业研究设计院 | Nano essence particles for cigarette filter stick and preparation method thereof |
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