CN108013507B - Dropping pill for cigarette and preparation method thereof - Google Patents
Dropping pill for cigarette and preparation method thereof Download PDFInfo
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- CN108013507B CN108013507B CN201711263263.1A CN201711263263A CN108013507B CN 108013507 B CN108013507 B CN 108013507B CN 201711263263 A CN201711263263 A CN 201711263263A CN 108013507 B CN108013507 B CN 108013507B
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- calcium chloride
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/18—Mouthpieces for cigars or cigarettes; Manufacture thereof
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Confectionery (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
The invention discloses a dropping pill for tobacco and a preparation method thereof. Comprises calcium chloride, calcium lactate and water-based essence, which are gradually mixed and frozen, and then are respectively dipped in forming liquid and shaping liquid to obtain the dropping pill for cigarettes. The dripping pill adopts aqueous essence which is widely applied, so that the taste types of the dripping pill for the cigarettes are increased, the types of the coating materials of the dripping pill for the cigarettes are expanded, the safety of the dripping pill for the cigarettes is better increased, and the use cost of the essence for the cigarettes is reduced.
Description
Technical Field
The invention relates to the technical field of dropping pills for cigarettes, in particular to a dropping pill for cigarettes and a preparation method thereof.
Background
The addition of the fragrance-moistening dropping pills in the filter stick of the cigarette becomes a common means for improving the taste of the cigarette for each large cigarette brand, and greatly increases the consumption experience of consumers. Traditional moist fragrant dripping pill mainly wraps up oil-soluble essence spices, for example olive oil, caprylic capric acid glyceride etc. but this kind of traditional oil-soluble essence spices volatility is relatively poor, simultaneously because oily stronger, in the cigarette use, the essence spices in the filter rod covers a large amount of smoke and dust, makes the dripping pill discolour, even flows the essence spices that discolours from the filter tip, great influence consumer's result of use, can't satisfy the consumer that has higher demand value to the cigarette. Meanwhile, the variety of the oily essence and flavor is relatively rare, which undoubtedly reduces the variety of the taste of the dripping pill, limits the development of the taste of the dripping pill, improves the research and development production cost and is not beneficial to the wide application of the dripping pill in cigarettes.
Disclosure of Invention
The invention aims to provide a dropping pill for cigarettes and a preparation method thereof aiming at the defects of the prior art, and the dropping pill for cigarettes prepared from water-based essence is provided, so that the types of the tastes of the dropping pills are greatly increased.
The dropping pill for the cigarette comprises the following components in parts by mass:
6-20 parts of calcium chloride;
12-30 parts of calcium lactate;
2-8 parts of water-based essence.
The variety of the water-based essence is far more than that of the oil-based essence, so that the water-based essence replaces the traditional oil-based essence, the taste selection of the dropping pills for the cigarettes is greatly increased, and the requirements of different consumers can be more comprehensively met; meanwhile, most of the aqueous essence is widely applied to beverages and foods, so that the edible safety level is relatively high, and adverse reactions of consumers caused by smoking of the dripping pill essence are avoided; due to the ubiquitous existence of the water-based essence and the wide development of the water-based essence in all communities, the water-based essence has lower use cost.
The calcium chloride and the calcium lactate are used as the solvents of the aqueous essence, so that the fineness and the taste of the cigarette taste can be better improved, and the integral stability of the dripping pill is greatly improved.
Preferably, a surfactant is also included. Aims to better enable the water-based essence to be mutually soluble with a calcium chloride solution and a calcium lactate solution and to ensure that the distribution of the water-based essence is more uniform.
Preferably, the surfactant is one or more of tween, span and succinic acid monoglyceride.
Preferably, an antifreeze is also included. Aims to prevent the dripping pills from being frozen and being unusable because of the over-low external environment temperature in the daily storage process of the cigarettes.
Preferably, the antifreeze agent is propylene glycol. The propylene glycol not only has certain antifreezing property, but also has certain cosolvent property, and can make all the components in the dripping pill be uniformly mixed.
A preparation method of dropping pills for cigarettes comprises the following steps:
dissolving water-based essence in distilled water to prepare a water-based essence solution;
respectively preparing calcium chloride solution and calcium lactate solution from calcium chloride and calcium lactate, adding surfactant and propylene glycol into the aqueous essence solution to obtain mixture solution;
freezing the mixture solution to obtain a frozen matter;
soaking the frozen object in a forming liquid for 10-20 min;
and (3) immersing the frozen matter immersed in the forming liquid in a stabilizing liquid for 2-6 min to obtain the dropping pills for cigarettes.
Preferably, the molding liquid is a sodium alginate solution. The sodium alginate solution has certain viscosity, and is coated on the periphery of the dripping pill to seal the dripping pill and protect the substances in the dripping pill.
Preferably, the sodium alginate solution comprises 10-20 parts of sodium alginate with the viscosity of 150-250 Pa.s, 5-20 parts of sodium alginate with the viscosity of 60-100 Pa.s and a thickening agent. The mixture of two kinds of sodium alginate with different viscosities can achieve better viscosity and simultaneously has certain elasticity.
Preferably, the thickener is one or more of carrageenan, gellan gum, carboxymethyl cellulose, acetylated distarch diacid and xanthan gum.
Preferably, the stabilizing solution is a calcium chloride solution. The purpose is to make the surface treatment of the dropping pill and make the dropping pill form stably.
According to the dropping pill for the cigarettes and the preparation method, the aqueous essence which is widely applied is adopted, the taste types of the dropping pill for the cigarettes are greatly increased, the types of the wrapping materials of the dropping pill for the cigarettes are expanded, meanwhile, the safety of the dropping pill for the cigarettes is better increased, and the use cost of the essence for the cigarettes is reduced.
Detailed Description
The invention will be further illustrated below with reference to specific examples. It should be understood that these examples are for illustrative purposes only and are not intended to limit the scope of the present invention. Furthermore, various changes or modifications of the present invention may be made by those skilled in the art, and equivalents may fall within the scope of the claims of the present application. The proportions in the examples of the invention are by weight.
Example 1
Dissolving 2 parts of aqueous essence in distilled water, and stirring until the aqueous essence is fully dissolved to prepare an aqueous essence solution; respectively preparing calcium chloride solution and calcium lactate solution from 6 parts of calcium chloride and 10 parts of calcium lactate, adding span and propylene glycol into the aqueous essence solution, stirring, and dissolving to obtain mixture solution; after the mixture solution is cooled, injecting the mixture solution into a spherical mold with the outer diameter of 4mm and the inner diameter of 3.6mm, and putting the spherical mold into a refrigerator at the temperature of-10 ℃ to freeze into a large number of small ice balls; soaking the frozen object in a molding solution prepared from 10 parts of sodium alginate with the viscosity of 150Pa.s, 5 parts of sodium alginate with the viscosity of 60Pa.s and carrageenan for 10 min; and then soaking the frozen matter soaked by the forming liquid in a calcium chloride solution for 2min, and taking out to obtain the dropping pill for cigarettes.
Example 2
Dissolving 5 parts of aqueous essence in distilled water, and stirring until the aqueous essence is fully dissolved to prepare an aqueous essence solution; respectively preparing 13 parts of calcium chloride and 15 parts of calcium lactate into calcium chloride solution and calcium lactate solution, adding the calcium chloride solution and the calcium lactate solution together with tween and propylene glycol into the aqueous essence solution, and uniformly stirring until the calcium chloride solution and the calcium lactate solution are fully dissolved to obtain mixture solution; after the mixture solution is cooled, injecting the mixture solution into a spherical mold with the outer diameter of 4mm and the inner diameter of 3.6mm, and putting the spherical mold into a refrigerator at the temperature of-10 ℃ to freeze into a large number of small ice balls; soaking the frozen matter in a molding solution prepared from 10 parts of sodium alginate with the viscosity of 200Pa.s, 5 parts of sodium alginate with the viscosity of 80Pa.s and gellan gum for 10 min; and then soaking the frozen matter soaked by the forming liquid in a calcium chloride solution for 2min, and taking out to obtain the dropping pill for cigarettes.
Example 3
Dissolving 8 parts of water-based essence in distilled water, and stirring until the water-based essence is fully dissolved to prepare a water-based essence solution; respectively preparing 20 parts of calcium chloride and 30 parts of calcium lactate into a calcium chloride solution and a calcium lactate solution, adding the calcium chloride solution and the calcium lactate solution together with succinic acid monoglyceride and propylene glycol into the aqueous essence solution, and uniformly stirring until the calcium chloride solution and the calcium lactate solution are fully dissolved to obtain a mixture solution; after the mixture solution is cooled, injecting the mixture solution into a spherical mold with the outer diameter of 4mm and the inner diameter of 3.6mm, and putting the spherical mold into a refrigerator at the temperature of-10 ℃ to freeze into a large number of small ice balls; soaking the frozen matter in molding liquid prepared from 10 parts of sodium alginate with the viscosity of 250Pa.s, 5 parts of sodium alginate with the viscosity of 100Pa.s and carboxymethyl cellulose for 10 min; and (3) soaking the frozen matter soaked by the forming solution in a calcium chloride solution for 2min, and taking out to obtain the dropping pill for cigarettes.
Example 4
Dissolving 8 parts of water-based essence in distilled water, and stirring until the water-based essence is fully dissolved to prepare a water-based essence solution; respectively preparing 20 parts of calcium chloride and 30 parts of calcium lactate into a calcium chloride solution and a calcium lactate solution, adding the calcium chloride solution and the calcium lactate solution together with tween, span, succinic acid monoglyceride and propylene glycol into the aqueous essence solution, and uniformly stirring until the calcium chloride solution and the calcium lactate solution are fully dissolved to obtain a mixture solution; after the mixture solution is cooled, injecting the mixture solution into a spherical mold with the outer diameter of 4mm and the inner diameter of 3.6mm, and putting the spherical mold into a refrigerator at the temperature of-10 ℃ to freeze into a large number of small ice balls; soaking the frozen matter in a molding solution prepared from 15 parts of sodium alginate with the viscosity of 200Pa.s, 13 parts of sodium alginate with the viscosity of 80Pa.s and acetylated diacid double starch for 10 min; and (3) soaking the frozen matter soaked by the forming solution in a calcium chloride solution for 2min, and taking out to obtain the dropping pill for cigarettes.
Example 5
Dissolving 8 parts of water-based essence in distilled water, and stirring until the water-based essence is fully dissolved to prepare a water-based essence solution; respectively preparing 20 parts of calcium chloride and 30 parts of calcium lactate into calcium chloride solution and calcium lactate solution, adding the calcium chloride solution and the calcium lactate solution together with tween, span and propylene glycol into the aqueous essence solution, and uniformly stirring until the calcium chloride solution and the calcium lactate solution are fully dissolved to obtain mixture solution; after the mixture solution is cooled, injecting the mixture solution into a spherical mold with the outer diameter of 4mm and the inner diameter of 3.6mm, and putting the spherical mold into a refrigerator at the temperature of-10 ℃ to freeze into a large number of small ice balls; soaking the frozen object in a molding solution prepared from 20 parts of sodium alginate with the viscosity of 200Pa.s, 20 parts of sodium alginate with the viscosity of 80Pa.s and xanthan gum for 10 min; and (3) soaking the frozen matter soaked by the forming solution in a calcium chloride solution for 2min, and taking out to obtain the dropping pill for cigarettes.
Example 6
Dissolving 8 parts of water-based essence in distilled water, and stirring until the water-based essence is fully dissolved to prepare a water-based essence solution; respectively preparing 20 parts of calcium chloride and 30 parts of calcium lactate into a calcium chloride solution and a calcium lactate solution, adding the calcium chloride solution and the calcium lactate solution together with succinic acid monoglyceride and propylene glycol into the aqueous essence solution, and uniformly stirring until the calcium chloride solution and the calcium lactate solution are fully dissolved to obtain a mixture solution; after the mixture solution is cooled, injecting the mixture solution into a spherical mold with the outer diameter of 4mm and the inner diameter of 3.6mm, and putting the spherical mold into a refrigerator at the temperature of-10 ℃ to freeze into a large number of small ice balls; soaking the frozen matter in a molding solution prepared from 20 parts of sodium alginate with the viscosity of 200Pa.s, 20 parts of sodium alginate with the viscosity of 80Pa.s and a thickening agent for 15 min; and (3) soaking the frozen matter soaked by the forming solution in a calcium chloride solution for 4min, and taking out to obtain the dropping pill for cigarettes.
Example 7
Dissolving 8 parts of water-based essence in distilled water, and stirring until the water-based essence is fully dissolved to prepare a water-based essence solution; respectively preparing 20 parts of calcium chloride and 30 parts of calcium lactate into a calcium chloride solution and a calcium lactate solution, adding span, succinic acid monoglyceride and propylene glycol into the aqueous essence solution, and stirring uniformly until the calcium chloride solution and the calcium lactate solution are fully dissolved to obtain a mixture solution; after the mixture solution is cooled, injecting the mixture solution into a spherical mold with the outer diameter of 4mm and the inner diameter of 3.6mm, and putting the spherical mold into a refrigerator at the temperature of-10 ℃ to freeze into a large number of small ice balls; soaking the frozen matter in a molding solution prepared from 20 parts of sodium alginate with the viscosity of 200Pa.s, 20 parts of sodium alginate with the viscosity of 80Pa.s, carrageenan, gellan gum and carboxymethyl cellulose for 20 min; and (3) soaking the frozen matter soaked by the forming liquid in a calcium chloride solution for 6min, and taking out to obtain the dropping pill for cigarettes.
Example 8
Dissolving 8 parts of coffee-flavored water-based essence in distilled water, and stirring until the coffee-flavored water-based essence is fully dissolved to prepare a water-based essence solution; preparing 20 parts of calcium chloride and 30 parts of calcium lactate into a calcium chloride solution and a calcium lactate solution respectively, adding the calcium chloride solution and the calcium lactate solution together with tween 80 and propylene glycol into the aqueous essence solution, and stirring uniformly until the calcium chloride solution and the calcium lactate solution are fully dissolved to obtain a mixture solution; after the mixture solution is cooled, injecting the mixture solution into a spherical mold with the outer diameter of 4mm and the inner diameter of 3.6mm, and putting the spherical mold into a refrigerator at the temperature of-10 ℃ to freeze into a large number of small ice balls; soaking the frozen matter in a molding solution prepared from 20 parts of sodium alginate with the viscosity of 200Pa.s, 20 parts of sodium alginate with the viscosity of 80Pa.s and carboxymethyl cellulose for 20 min; and (3) soaking the frozen matter soaked by the forming liquid in a calcium chloride solution for 6min, and taking out to obtain the dropping pill for cigarettes.
Example 9
Dissolving 8 parts of mint-flavored water-based essence in distilled water, and stirring until the mint-flavored water-based essence is fully dissolved to prepare a water-based essence solution; respectively preparing 20 parts of calcium chloride and 30 parts of calcium lactate into a calcium chloride solution and a calcium lactate solution, adding the calcium chloride solution and the calcium lactate solution together with succinic acid monoglyceride and propylene glycol into the aqueous essence solution, and uniformly stirring until the calcium chloride solution and the calcium lactate solution are fully dissolved to obtain a mixture solution; after the mixture solution is cooled, injecting the mixture solution into a spherical mold with the outer diameter of 4mm and the inner diameter of 3.6mm, and putting the spherical mold into a refrigerator at the temperature of-10 ℃ to freeze into a large number of small ice balls; soaking the frozen matter in a molding solution prepared from 20 parts of sodium alginate with the viscosity of 200Pa.s, 20 parts of sodium alginate with the viscosity of 80Pa.s and gellan gum for 20 min; and (3) soaking the frozen matter soaked by the forming liquid in a calcium chloride solution for 6min, and taking out to obtain the dropping pill for cigarettes.
The embodiments of the present invention have been described above by way of example, but the description is only a preferred embodiment of the present invention and should not be construed as limiting the scope of the invention. All equivalent changes and modifications within the scope of the application of the present invention shall fall within the scope of the patent of the present invention.
Claims (3)
1. A preparation method of dropping pills for cigarettes is characterized by comprising the following steps: the method comprises the following steps:
dissolving 2-8 parts of water-based essence in distilled water to prepare a water-based essence solution;
respectively preparing 6-10 parts of calcium chloride and 12-30 parts of calcium lactate into calcium chloride solution and calcium lactate solution, and adding surfactant and propylene glycol into the aqueous essence solution to obtain mixture solution;
freezing the mixture solution to obtain a frozen matter;
soaking the frozen object in a forming liquid for 10-20 min;
immersing the frozen matter immersed in the forming liquid in a stabilizing liquid for 2-6 min to obtain dropping pills for cigarettes;
the forming liquid is a sodium alginate solution, and the sodium alginate solution comprises 10-20 parts of sodium alginate with the viscosity of 150-250 Pa.s, 5-20 parts of sodium alginate with the viscosity of 60-100 Pa.s and a thickening agent.
2. The preparation method of the dropping pill for cigarette as claimed in claim 1, wherein the dropping pill for cigarette comprises the following steps: the thickening agent is one or more of carrageenan, gellan gum, carboxymethyl cellulose, acetylated distarch and xanthan gum.
3. The preparation method of the dropping pill for cigarette as claimed in claim 1, wherein the dropping pill for cigarette comprises the following steps: the stabilizing solution is calcium chloride solution.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711263263.1A CN108013507B (en) | 2017-12-05 | 2017-12-05 | Dropping pill for cigarette and preparation method thereof |
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| CN201711263263.1A CN108013507B (en) | 2017-12-05 | 2017-12-05 | Dropping pill for cigarette and preparation method thereof |
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| CN108013507B true CN108013507B (en) | 2020-05-26 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109536280A (en) * | 2018-11-27 | 2019-03-29 | 湖北中烟工业有限责任公司 | The quick-fried pearl preparation method of cigarette of internal essence further progress Maillard reaction after molding |
| CN111249992A (en) * | 2018-12-03 | 2020-06-09 | 沈欣 | Method for preparing liquid bead pill |
| CN112273713A (en) * | 2019-07-10 | 2021-01-29 | 云南巴菰生物科技有限公司 | Water-soluble substance blasting bead and preparation method thereof |
| CN113088389A (en) * | 2021-04-08 | 2021-07-09 | 武汉黄鹤楼香精香料有限公司 | Water-soluble dropping pill prepared from porous material and preparation method thereof |
| CN113662242B (en) * | 2021-07-27 | 2023-10-20 | 常德市雄鹰科技有限责任公司 | Device and system for preparing and forming explosion beads in cigarette filter tip |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102065989A (en) * | 2008-07-24 | 2011-05-18 | 国立大学法人新泻大学 | Microcapsule, process for production thereof, and food or beverage containing microcapsule |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR100860519B1 (en) * | 2008-03-03 | 2008-09-26 | 주식회사 에스앤텍 | Alginate-calcium-capsule and the method therof |
| CN102488330A (en) * | 2010-03-30 | 2012-06-13 | 广东神农烟科技术有限公司 | Natural plant extract microcapsules and cigarette filter tip containing natural plant extract microcapsules |
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Effective date of registration: 20200814 Address after: 430000 No.4, dailiwan, qilimiao, Hanyang District, Wuhan, Hubei Province Patentee after: HUBEI ZHONGYAN CIGARETTE FACTORY Address before: 430000, Jinshan Road, Dongxihu District, Hubei, Wuhan Province, 1355 Patentee before: WUHAN YELLOW CRANE TOWER NEW MATERIAL TECHNOLOGY DEVELOPMENT Co.,Ltd. |