CN104178356A - Preparation method of mint essence oil microcapsule and application of mint essence oil microcapsule in tobacco - Google Patents
Preparation method of mint essence oil microcapsule and application of mint essence oil microcapsule in tobacco Download PDFInfo
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- CN104178356A CN104178356A CN201410450513.2A CN201410450513A CN104178356A CN 104178356 A CN104178356 A CN 104178356A CN 201410450513 A CN201410450513 A CN 201410450513A CN 104178356 A CN104178356 A CN 104178356A
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- essence oil
- oil microcapsule
- mint essence
- cigarette
- peppermint
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Abstract
The invention discloses a preparation method of a mint essence oil microcapsule and application of the mint essence oil microcapsule in tobaccos, and belongs to the technical field of cigarette processing. The preparation method is characterized in that the mint essence oil microcapsule is obtained through the following steps of adding sodium alginate, chitosan and gelatin with at a weight ratio of (1-3):1:(1-3) to water which accounts for 10%-15% of the weight of the three substances for uniform mixing to prepare a wall material solution at 80-90 DEG C; cooling to 40-50 DEG C, adding mint essence oil which accounts for 15%-30% of the weight of three wall materials, homogenizing at high pressure to form a mint essence oil emulsion, and carrying out spray drying to obtain the mint essence oil microcapsule. The mint essence oil microcapsule prepared through the method disclosed by the invention is 100% dissolved into water and can be applied to a cigarette filter as an additive and then rolled into a cigarette. The mint essence oil microcapsule disclosed by the invention can improve the cigarette quality, reduce the irritation, increase the fragrance and improve the oral cavity wettability.
Description
Technical field
The invention belongs to technical field of cigarette processing, be specifically related to a kind of preparation method of peppermint essence oil microcapsule and the application in tobacco thereof.
Background technology
technology:
Essence spice for cigarette is to specialize in each tobacco articles perfuming flavoring to use, and in production of cigarettes, essence spice for cigarette is abundant in content, various in style.Its Type of aroma and aromatic style are determining class and the grade of tobacco to a certain extent.Conventionally tobacco can produce the organism of some pungent tastes in the time of burning, if add some essence in cigarette, just can cover the sharp flavor producing in result of combustion of tobacco process with fragrance, makes it to produce good flue gas effect in the time burning and sucking.But essence or essential oil are added to the uncertainty that can increase the complicacy of pipe tobacco combustion processes in cigarette shreds and generate product harm, the present invention adds essence in cigarette filter, can avoid this problem.
Peppermint essential oil is soluble in organic solvent, is insoluble in water, and volatility is stronger.The present invention is by microcapsulary, solves peppermint essence oil production volatile, oxidizable problem in storage process.The peppermint essence oil microcapsule of preparation is applied in cigarette filter, can reduce the harm of cigarette, improves cigarette igniting and sucking quality.
By literature search, have no identical with the present invention open source literature report.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of peppermint essence oil microcapsule and the application in tobacco thereof.
The present invention adopts following technical scheme:
A kind of preparation method of peppermint essence oil microcapsule, the sodium alginate that to comprise the steps: wall material mass ratio be 1 ~ 3:1:1 ~ 3, chitosan, gelatin adds the water of these three kinds of material masses 10 ~ 15% to mix, at 70 ~ 80 DEG C, make wall material solution, be cooled to 40 ~ 50 DEG C, add while stirring 15 ~ 30% peppermint essential oil of these three kinds of wall material amounts, after 8000 ~ 10000r/min high-speed stirring 10min, pass into high pressure homogenizer, homogeneous three times under 70 ~ 80 DEG C and pressure 20 ~ 30MPa, each 5min, form the emulsion of uniform particle diameter, it is 150 ~ 200 DEG C in inlet temperature, temperature out is 90 ~ 120 DEG C, atomizing pressure is that under the condition of 0.2 ~ 0.5MPa, spraying is dry, obtain peppermint essence oil microcapsule.
500 ~ 1000 times of distilled water dilutings for peppermint essence oil microcapsule of the present invention, diluting soln joins in cigarette filter with 2% of filter tip weight, and filter tip cigarette is become to cigarette.
Beneficial effect of the present invention is: the solubleness of peppermint essence oil microcapsule in water reaches 100%, uses it in cigarette filter and can improve cigarette quality, reduces and stimulates, and increases fragrance, improves oral cavity wettability.
Further illustrate the present invention below in conjunction with embodiment, but the scope of protection of present invention is not limited to following embodiment.
embodiment:
Embodiment 1:
Sodium alginate, chitosan, the gelatin that is 1:1:1 by wall material mass ratio adds the water of these three kinds of material masses 10% to mix, at 90 DEG C, make wall material solution, be cooled to 40 DEG C, add while stirring 15% peppermint essential oil of these three kinds of wall material amounts, after 8000r/min high-speed stirring 10min, pass into high pressure homogenizer, homogeneous three times under 80 DEG C and pressure 20MPa, each 5min, form the emulsion of uniform particle diameter, it is 150 DEG C in inlet temperature, temperature out is 90 DEG C, and under the condition that atomizing pressure is 0.2MPa, spraying is dried, and obtains peppermint essence oil microcapsule.1000 times of distilled water dilutings for the peppermint essence oil microcapsule of gained, diluting soln joins in cigarette filter with 2% of filter tip weight, filter tip cigarette is become to cigarette, carry out sensory evaluating smoking's qualification through perfumer, note in its fragrance increases, and with light peppermint feature note, fragrance is plentiful, abundant, harmony, pungency decreases, and sensation slightly refrigerant on pleasant impression, Hui Tian.
Embodiment 2:
Sodium alginate, chitosan, the gelatin that is 2:1:3 by wall material mass ratio adds the water of these three kinds of material masses 15% to mix, at 80 DEG C, make wall material solution, be cooled to 40 DEG C, add while stirring 20% peppermint essential oil of these three kinds of wall material amounts, after 10000r/min high-speed stirring 10min, pass into high pressure homogenizer, homogeneous three times under 70 DEG C and pressure 25MPa, each 5min, form the emulsion of uniform particle diameter, it is 200 DEG C in inlet temperature, temperature out is 120 DEG C, and under the condition that atomizing pressure is 0.5MPa, spraying is dried, and obtains peppermint essence oil microcapsule.500 times of distilled water dilutings for the peppermint essence oil microcapsule of gained, diluting soln joins in cigarette filter with 2% of filter tip weight, filter tip cigarette is become to cigarette, carry out sensory evaluating smoking's qualification through perfumer, note in its fragrance increases, and with light peppermint feature note, fragrance is plentiful, abundant, harmony, pungency decreases, and on pleasant impression, has the significantly sensation of refrigerant, Hui Tian.
Embodiment 3:
The sodium alginate that is 0 ~ 3:1:1 ~ 3 by wall material mass ratio, chitosan, gelatin adds the water of these three kinds of material masses 12% to mix, at 85 DEG C, make wall material solution, be cooled to 45 DEG C, add while stirring 30% peppermint essential oil of these three kinds of wall material amounts, after 9000r/min high-speed stirring 10min, pass into high pressure homogenizer, homogeneous three times under 75 DEG C and pressure 30MPa, each 5min, form the emulsion of uniform particle diameter, it is 180 DEG C in inlet temperature, temperature out is 100 DEG C, atomizing pressure is that under the condition of 0.3MPa, spraying is dry, obtain peppermint essence oil microcapsule.800 times of distilled water dilutings for the peppermint essence oil microcapsule of gained, diluting soln joins in cigarette filter with 2% of filter tip weight, filter tip cigarette is become to cigarette, carry out sensory evaluating smoking's qualification through perfumer, the note in its fragrance increases, and with light peppermint feature note, fragrance is plentiful, abundant, harmony, and pungency decreases, along with the increase of addition, can slightly suppress the tobacco banksia rose, on pleasant impression, also can slightly bring residual.
Claims (2)
1. the preparation method of a peppermint essence oil microcapsule, it is characterized in that, the sodium alginate that to comprise the steps: wall material mass ratio be 1 ~ 3:1:1 ~ 3, chitosan, gelatin adds the water of these three kinds of material masses 10 ~ 15% to mix, at 80 ~ 90 DEG C, make wall material solution, be cooled to 40 ~ 50 DEG C, add while stirring 15 ~ 30% peppermint essential oil of these three kinds of wall material amounts, after 8000 ~ 10000r/min high-speed stirring 10min, pass into high pressure homogenizer, homogeneous three times under 70 ~ 80 DEG C and pressure 20 ~ 30MPa, each 5min, form the emulsion of uniform particle diameter, it is 150 ~ 200 DEG C in inlet temperature, temperature out is 90 ~ 120 DEG C, atomizing pressure is that under the condition of 0.2 ~ 0.5MPa, spraying is dry, obtain peppermint essence oil microcapsule.
2. the application of peppermint essence oil microcapsule according to claim 1 in tobacco, is characterized in that, 500 ~ 1000 times of distilled water dilutings for peppermint essence oil microcapsule, and diluting soln joins in cigarette filter with 2% of filter tip weight, and filter tip cigarette is become to cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410450513.2A CN104178356A (en) | 2014-09-05 | 2014-09-05 | Preparation method of mint essence oil microcapsule and application of mint essence oil microcapsule in tobacco |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410450513.2A CN104178356A (en) | 2014-09-05 | 2014-09-05 | Preparation method of mint essence oil microcapsule and application of mint essence oil microcapsule in tobacco |
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| CN104178356A true CN104178356A (en) | 2014-12-03 |
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| CN201410450513.2A Pending CN104178356A (en) | 2014-09-05 | 2014-09-05 | Preparation method of mint essence oil microcapsule and application of mint essence oil microcapsule in tobacco |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107630259A (en) * | 2017-09-30 | 2018-01-26 | 金华市纳德棠生物科技有限公司 | Multi-functional summer is with the preparation method of refrigerant sense fabric |
| CN107675560A (en) * | 2017-05-24 | 2018-02-09 | 湖北中烟工业有限责任公司 | Cigarette aluminium-foil paper preparation method with slow controlled release cool feeling essence |
| CN107774205A (en) * | 2017-11-10 | 2018-03-09 | 昆明理工大学 | A kind of fragrant plant dries the apparatus and method of coproduction microcapsule essence |
| CN107904014A (en) * | 2017-11-28 | 2018-04-13 | 戴凤 | A kind of composite plant essential oil microcapsules and preparation method thereof |
| CN108967520A (en) * | 2018-05-24 | 2018-12-11 | 中北大学 | A kind of preparation method and applications of Fructus Perillae quintessence oil micro-capsule |
| CN110150742A (en) * | 2018-02-13 | 2019-08-23 | 湖南中烟工业有限责任公司 | A kind of packet capsule with diuresis promoting function and its one-step shaping preparation method and the application in cigarette |
| CN111449278A (en) * | 2020-04-01 | 2020-07-28 | 上海应用技术大学 | Preparation method of menthone microcapsule and application of menthone microcapsule in chewing tobacco |
| CN111496951A (en) * | 2020-05-14 | 2020-08-07 | 东北林业大学 | Microcapsule technology-based environment-friendly plywood capable of releasing fragrance of machilus serrulata essential oil |
| CN114081204A (en) * | 2021-11-26 | 2022-02-25 | 福建中烟工业有限责任公司 | Cinnamyl alcohol microcapsule and preparation method thereof, tobacco granules and preparation method thereof, filter stick or filter tip, tobacco product and application |
-
2014
- 2014-09-05 CN CN201410450513.2A patent/CN104178356A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107675560A (en) * | 2017-05-24 | 2018-02-09 | 湖北中烟工业有限责任公司 | Cigarette aluminium-foil paper preparation method with slow controlled release cool feeling essence |
| CN107630259A (en) * | 2017-09-30 | 2018-01-26 | 金华市纳德棠生物科技有限公司 | Multi-functional summer is with the preparation method of refrigerant sense fabric |
| CN107774205A (en) * | 2017-11-10 | 2018-03-09 | 昆明理工大学 | A kind of fragrant plant dries the apparatus and method of coproduction microcapsule essence |
| CN107774205B (en) * | 2017-11-10 | 2024-02-02 | 昆明理工大学 | Device and method for drying aromatic plants and co-producing microcapsule essence |
| CN107904014A (en) * | 2017-11-28 | 2018-04-13 | 戴凤 | A kind of composite plant essential oil microcapsules and preparation method thereof |
| CN110150742A (en) * | 2018-02-13 | 2019-08-23 | 湖南中烟工业有限责任公司 | A kind of packet capsule with diuresis promoting function and its one-step shaping preparation method and the application in cigarette |
| CN108967520A (en) * | 2018-05-24 | 2018-12-11 | 中北大学 | A kind of preparation method and applications of Fructus Perillae quintessence oil micro-capsule |
| CN111449278A (en) * | 2020-04-01 | 2020-07-28 | 上海应用技术大学 | Preparation method of menthone microcapsule and application of menthone microcapsule in chewing tobacco |
| CN111496951A (en) * | 2020-05-14 | 2020-08-07 | 东北林业大学 | Microcapsule technology-based environment-friendly plywood capable of releasing fragrance of machilus serrulata essential oil |
| CN114081204A (en) * | 2021-11-26 | 2022-02-25 | 福建中烟工业有限责任公司 | Cinnamyl alcohol microcapsule and preparation method thereof, tobacco granules and preparation method thereof, filter stick or filter tip, tobacco product and application |
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20141203 |
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| WD01 | Invention patent application deemed withdrawn after publication |