CN104082853B - A kind of electronic cigarette liquid containing tomato extract and preparation method thereof - Google Patents
A kind of electronic cigarette liquid containing tomato extract and preparation method thereof Download PDFInfo
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- CN104082853B CN104082853B CN201410318002.5A CN201410318002A CN104082853B CN 104082853 B CN104082853 B CN 104082853B CN 201410318002 A CN201410318002 A CN 201410318002A CN 104082853 B CN104082853 B CN 104082853B
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Abstract
The invention provides a kind of electronic cigarette liquid containing tomato extract and preparation method thereof.Electronic cigarette liquid containing tomato extract of the present invention obtains after being mixed in proportion by tomato extract, flavoring essence, propane diols, G & W etc.; Wherein tomato extract is through ultrasonic process, alcohol heating reflux extracts and the rotary evaporation that reduces pressure is concentrated obtains.Parts by weight containing component each in the electronic cigarette liquid of tomato extract are: tomato extract is 5-10 part, flavoring essence is 0.1-1 part, propane diols is 1-80 part, glycerine is 1-70 part, and water is 5-30 part.Electronic cigarette liquid of the present invention has good fragrance, mouthfeel and strength, can meet the smoking demand of consumer.
Description
Technical field
The invention belongs to flavouring essence for tobacco field, relate to a kind of electronic cigarette liquid and preparation method thereof, particularly relate to a kind of electronic cigarette liquid containing tomato extract and preparation method thereof.
Technical background
Electronic cigarette has another name called electronic cigarette, has the outward appearance the same with cigarette, the taste approximate with cigarette, even will have more a lot than the taste of general cigarette, also can sucking-off cigarette, sucking-off taste and sensation come as cigarette.Electronic cigarette does not have other harmful components such as tar, suspended particulates in cigarette, produces second-hand-cigarette hardly yet.Electronic cigarette is generally made up of three parts: tobacco rod, atomizer and cigarette bullet.When smoker is by cigarette holder air-breathing, the electronic cigarette liquid in cigarette bullet is become the droplet of about 0.5-1.5um in atomizer by heating atomization, forms simulation smoke.
Fragrance and the mouthfeel of electronic cigarette derive from electronic cigarette liquid, the composition mainly essence and flavoring agent of electronic cigarette liquid, tobacco extract and propane diols, glycerine equal solvent.In order to ensure strength sense during smoking, usually need containing certain density nicotine in electronic cigarette liquid.Except tobacco, in uncivilized nation eggplant, tealeaves, eggplant, potato etc., all contain alkaloid.Therefore in electronic cigarette liquid, add appropriate tomato extract, strength sense during electronic cigarette suction can be improved.
Summary of the invention
the technical problem solved:as the substitute products of cigarette, usually do not contain or only contain the nicotine of seldom amount in electronic cigarette liquid, the strength sense which results in electronic cigarette flue gas is not enough, can not meet the psychological need of smoker.
technical scheme:for above-mentioned technical problem, the invention discloses a kind of electronic cigarette liquid containing tomato extract, the described electronic cigarette liquid containing tomato extract consists of the following composition: tomato extract, flavoring essence, propane diols, G & W.
Preferably, described a kind of parts by weight containing each component in the electronic cigarette liquid of tomato extract are: tomato extract is 5-10 part, flavoring essence is 0.1-1 part, propane diols is 1-80 part, glycerine is 1-70 part, and water is 5-30 part.
Preferably, described a kind of electronic cigarette liquid containing tomato extract is sundown.
Preferably, described a kind of electronic cigarette liquid containing tomato extract, described flavoring essence is edible Mint Essence, eats cacao essence or table grapes essence.
Preferably, described a kind of electronic cigarette liquid containing tomato extract, described tomato extract is the tomato extract with obtaining after alcohol extract.
Preferably, described tomato extract preparation method comprises the following steps: (1) takes clean blue or green tomato, smashs to pieces with tissue mashing machine; (2) add certain density ethanol in proportion, ultrasonic wave extracts three times; (3) merge extract, decompression rotary evaporation is condensed into paste, for subsequent use.
Preferably, in the preparation method of described tomato extract, concentration of alcohol used is 60wt% ~ 90wt%, solid-liquid ratio is 1:8-1:20, supersonic frequency is 50 ~ 400kHz, ultrasonic power is 50 ~ 600W, single ultrasonic extraction time is 10-30min, and the temperature that decompression rotary evaporation concentrates is 50 DEG C, and vacuum is 0.095 Mpa.
Containing a preparation method for the electronic cigarette liquid of tomato extract, comprise the steps: that (1) takes clean blue or green tomato, smash to pieces with tissue mashing machine; (2) add ethanol, ultrasonic wave extracts three times, and concentration of alcohol is 60wt% ~ 90wt%, and solid-liquid ratio is 1:8-1:20, and supersonic frequency is 50 ~ 400kHz, and ultrasonic power is 50 ~ 600W, and single ultrasonic extraction time is 10-30min; (3) merge extract, decompression rotary evaporation is condensed into paste, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, for subsequent use after concentrated; (4) get that tomato extract is 5-10 part, flavoring essence is 0.1-1 part, propane diols is 1-80 part, glycerine is 1-70 part, water is 5-30 part, will mentioned component mix after prepare electronic cigarette liquid containing tomato extract.
Preferably, the preparation method of described a kind of electronic cigarette liquid containing tomato extract, described flavoring essence is edible Mint Essence, eats cacao essence or table grapes essence.
beneficial effect:the electronic cigarette liquid containing tomato extract prepared by preparation method of the present invention is sundown, overcome in electronic cigarette liquid the nicotine usually not containing or only contain seldom amount, the strength sense which results in electronic cigarette flue gas is not enough, the shortcoming of the psychological need of smoker can not be met, electronic cigarette liquid of the present invention can provide good fragrance, mouthfeel and moderate strength sense when aspirating, and the preparation method of described electronic cigarette liquid is easy, constant product quality, can be widely used in electronic cigarette product.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described.
Embodiment 1
(1) take a certain amount of clean blue or green tomato, smash to pieces with tissue mashing machine; Adding the ethanol of 70wt% according to solid-liquid ratio 1:12, is 200 kHz in supersonic frequency, and power is ultrasonic extraction three times under the condition of 300 W, each 30 min; Merge extract after filtration, temperature be 50 DEG C, the vacuum rotary evaporation that reduces pressure under being 0.095 Mpa is condensed into paste, for subsequent use.(2) tomato extract 9 parts, edible Mint Essence 0.5 part, propane diols 40 parts, glycerine 45 parts and 5 parts, water are mixed, obtain the electronic cigarette liquid containing tomato extract.
Embodiment 2
(1) take a certain amount of clean blue or green tomato, smash to pieces with tissue mashing machine; Adding the ethanol of 60wt% according to solid-liquid ratio 1:8, is 50 kHz in supersonic frequency, and power is ultrasonic extraction three times under the condition of 50 W, each 15 min; Merge extract after filtration, temperature be 50 DEG C, the vacuum rotary evaporation that reduces pressure under being 0.095 Mpa is condensed into paste, for subsequent use.(2) tomato extract 10 parts, edible cacao essence 0.1 part, propane diols 1 part, glycerine 70 parts and 15 parts, water are mixed, obtain the electronic cigarette liquid containing tomato extract.
Embodiment 3
(1) take a certain amount of clean blue or green tomato, smash to pieces with tissue mashing machine; Adding the ethanol of 90wt% according to solid-liquid ratio 1:20, is 400 kHz in supersonic frequency, and power is ultrasonic extraction three times under the condition of 600 W, each 10 min; Merge extract after filtration, temperature be 50 DEG C, the vacuum rotary evaporation that reduces pressure under being 0.095 Mpa is condensed into paste, for subsequent use.(2) tomato extract 5 parts, 1 part, table grapes essence, propane diols 80 parts, glycerine 1 part and 30 parts, water are mixed, obtain the electronic cigarette liquid containing tomato extract.
The electronic cigarette liquid containing tomato extract of the embodiment 1 prepared, embodiment 2, embodiment 3 is got 0.5mL to be added in electronic cigarette, and separately get after medicinal extract that cloud and mist alcohol extract obtains is diluted to 1wt%, the 1wt% yunyan extract dilution getting 0.5mL is added in electronic cigarette, as a comparison case, integrated sensory's quality evaluation is carried out.Result is as follows:
Embodiment 1: flue gas is full, full aroma, mouthfeel are moderate, pleasant impression is better, strength is moderate.
Embodiment 2: flue gas is strong, full aroma, delicate mouthfeel, pleasant impression are comfortable, strength is moderate.
Embodiment 3: aromatic strongly fragrant, the fragrance of cigarette is coordinated, mouthfeel is moderate, strength is moderate.
Comparative example: flue gas is strong, fragrance is coordinated, strength is moderate.
Can find out from result, the electronic cigarette liquid containing tomato extract prepared by preparation method of the present invention has good fragrance, mouthfeel and moderate strength sense, the smoking result identical with cloud and mist ethanol extract can be reached, and not containing nicotine in electronic cigarette liquid of the present invention, the impact of tobacco on health is also reduced when effective guarantee strength and mouthfeel, and the preparation method of described electronic cigarette liquid is easy, constant product quality, can be widely used in electronic cigarette product.
Claims (1)
1., containing a preparation method for the electronic cigarette liquid of tomato extract, it is characterized in that comprising the steps: that (1) takes a certain amount of clean blue or green tomato, smash to pieces with tissue mashing machine; Adding the ethanol of 70wt% according to solid-liquid ratio 1:12, is 200 kHz in supersonic frequency, and power is ultrasonic extraction three times under the condition of 300 W, each 30 min; Merge extract after filtration, temperature be 50 DEG C, the vacuum rotary evaporation that reduces pressure under being 0.095 Mpa is condensed into paste, for subsequent use;
(2) tomato extract 9 parts, edible Mint Essence 0.5 part, propane diols 40 parts, glycerine 45 parts and 5 parts, water are mixed, obtain the electronic cigarette liquid containing tomato extract.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410318002.5A CN104082853B (en) | 2014-07-07 | 2014-07-07 | A kind of electronic cigarette liquid containing tomato extract and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410318002.5A CN104082853B (en) | 2014-07-07 | 2014-07-07 | A kind of electronic cigarette liquid containing tomato extract and preparation method thereof |
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| Publication Number | Publication Date |
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| CN104082853A CN104082853A (en) | 2014-10-08 |
| CN104082853B true CN104082853B (en) | 2015-10-21 |
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| CN201410318002.5A Expired - Fee Related CN104082853B (en) | 2014-07-07 | 2014-07-07 | A kind of electronic cigarette liquid containing tomato extract and preparation method thereof |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104585872A (en) * | 2015-01-20 | 2015-05-06 | 川渝中烟工业有限责任公司 | Electronic cigarette liquid containing water soluble propolis and preparation method thereof |
| CN104939310A (en) * | 2015-06-17 | 2015-09-30 | 云南中烟工业有限责任公司 | Black tomato glycerol triacetate extract and application thereof in cigarettes |
| CN105559145A (en) * | 2015-12-17 | 2016-05-11 | 立场电子科技发展（上海）有限公司 | E-cigarette flavor and preparation method thereof |
| CN107373775A (en) * | 2017-09-04 | 2017-11-24 | 周金成 | A kind of solid tobacco particle and novel baking electronic cigarette device |
| CN109757782A (en) * | 2019-03-05 | 2019-05-17 | 铂德（深圳）科技有限公司 | Grape extract solution, grape electronics tobacco tar and preparation method thereof |
| CN113545509A (en) * | 2021-08-12 | 2021-10-26 | 深圳波顿香料有限公司 | Strengthening agent for electronic cigarette oil |
| CN115005495B (en) * | 2022-06-21 | 2024-01-19 | 河南中烟工业有限责任公司 | Cigar-flavored heating non-combustible cigarette |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20120325228A1 (en) * | 2011-06-23 | 2012-12-27 | Williams Jonnie R | Alkaloid composition for e-cigarette |
| CN102864103B (en) * | 2012-09-05 | 2013-10-09 | 湖北中烟工业有限责任公司 | Composite fermentation spice including tobacco leaf, trigonella foenum-graecum L., capsicum annuum and solanum lycopersicum and application thereof to recombinant tobacco leaf |
| CN103070472A (en) * | 2013-01-25 | 2013-05-01 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid capable of effectively improving sensory quality of electronic cigarette |
| CN103054172A (en) * | 2013-01-25 | 2013-04-24 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid prepared from strong-flavor tobacco |
| CN103054173A (en) * | 2013-01-25 | 2013-04-24 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid prepared from discarded tobacco |
| CN103351951B (en) * | 2013-08-02 | 2014-12-03 | 华宝食用香精香料（上海）有限公司 | Cigarette essence capable of improving quality of cigarettes |
| CN103555424B (en) * | 2013-11-04 | 2015-01-07 | 成都宏亿实业集团有限公司 | Tomato essence |
| CN103865651A (en) * | 2014-03-26 | 2014-06-18 | 安徽中烟工业有限责任公司 | Preparation method of melon and fruit perfume for cigarettes |
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