CN110037334A - It is a kind of can lifting electrical heating do not burn the rich essence of cigarette flavor and its application - Google Patents
It is a kind of can lifting electrical heating do not burn the rich essence of cigarette flavor and its application Download PDFInfo
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- CN110037334A CN110037334A CN201910388460.9A CN201910388460A CN110037334A CN 110037334 A CN110037334 A CN 110037334A CN 201910388460 A CN201910388460 A CN 201910388460A CN 110037334 A CN110037334 A CN 110037334A
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 47
- 238000010438 heat treatment Methods 0.000 title claims abstract description 15
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 13
- 235000019634 flavors Nutrition 0.000 title claims abstract description 13
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000000341 volatile oil Substances 0.000 claims abstract description 24
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 15
- 235000019502 Orange oil Nutrition 0.000 claims abstract description 8
- 239000001926 citrus aurantium l. subsp. bergamia wright et arn. oil Substances 0.000 claims abstract description 8
- 239000003921 oil Substances 0.000 claims abstract description 8
- 235000019198 oils Nutrition 0.000 claims abstract description 8
- 239000010502 orange oil Substances 0.000 claims abstract description 8
- 235000009421 Myristica fragrans Nutrition 0.000 claims abstract description 7
- 239000001115 mace Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 5
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 17
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 claims description 16
- 102000004190 Enzymes Human genes 0.000 claims description 15
- 108090000790 Enzymes Proteins 0.000 claims description 15
- 229940088598 enzyme Drugs 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 10
- 235000007866 Chamaemelum nobile Nutrition 0.000 claims description 9
- 235000010254 Jasminum officinale Nutrition 0.000 claims description 9
- 244000042664 Matricaria chamomilla Species 0.000 claims description 9
- 235000007232 Matricaria chamomilla Nutrition 0.000 claims description 9
- 238000002360 preparation method Methods 0.000 claims description 8
- 239000001294 propane Substances 0.000 claims description 8
- 230000007071 enzymatic hydrolysis Effects 0.000 claims description 7
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 claims description 7
- 238000000605 extraction Methods 0.000 claims description 7
- 108010059892 Cellulase Proteins 0.000 claims description 5
- 108091005804 Peptidases Proteins 0.000 claims description 5
- 239000004365 Protease Substances 0.000 claims description 5
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 5
- 229940106157 cellulase Drugs 0.000 claims description 5
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 claims description 4
- 238000002525 ultrasonication Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000654 additive Substances 0.000 claims description 2
- 230000000996 additive effect Effects 0.000 claims description 2
- 239000001273 butane Substances 0.000 claims description 2
- 239000001282 iso-butane Substances 0.000 claims description 2
- 235000013847 iso-butane Nutrition 0.000 claims description 2
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims description 2
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 2
- 240000005385 Jasminum sambac Species 0.000 claims 3
- 244000061176 Nicotiana tabacum Species 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 238000009210 therapy by ultrasound Methods 0.000 claims 1
- 238000005485 electric heating Methods 0.000 abstract description 21
- 210000000214 mouth Anatomy 0.000 abstract description 8
- 239000002304 perfume Substances 0.000 abstract description 7
- 125000003118 aryl group Chemical group 0.000 abstract description 5
- 239000003205 fragrance Substances 0.000 description 18
- 241000208125 Nicotiana Species 0.000 description 16
- 235000019441 ethanol Nutrition 0.000 description 10
- 239000000126 substance Substances 0.000 description 9
- 239000004615 ingredient Substances 0.000 description 7
- 241000207840 Jasminum Species 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 235000019658 bitter taste Nutrition 0.000 description 5
- 230000035943 smell Effects 0.000 description 5
- HEVGGTGPGPKZHF-UHFFFAOYSA-N 1-(1,2-dimethyl-3-methylidenecyclopentyl)-4-methylbenzene Chemical compound CC1C(=C)CCC1(C)C1=CC=C(C)C=C1 HEVGGTGPGPKZHF-UHFFFAOYSA-N 0.000 description 4
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 4
- 239000000779 smoke Substances 0.000 description 4
- 238000007865 diluting Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- 239000013049 sediment Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 238000005292 vacuum distillation Methods 0.000 description 3
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 description 2
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 description 2
- 244000068485 Convallaria majalis Species 0.000 description 2
- 235000009046 Convallaria majalis Nutrition 0.000 description 2
- XMLSXPIVAXONDL-PLNGDYQASA-N Jasmone Chemical compound CC\C=C/CC1=C(C)CCC1=O XMLSXPIVAXONDL-PLNGDYQASA-N 0.000 description 2
- 244000223014 Syzygium aromaticum Species 0.000 description 2
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 2
- 239000001387 apium graveolens Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 229930007744 linalool Natural products 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- XMLSXPIVAXONDL-UHFFFAOYSA-N trans-jasmone Natural products CCC=CCC1=C(C)CCC1=O XMLSXPIVAXONDL-UHFFFAOYSA-N 0.000 description 2
- 238000002604 ultrasonography Methods 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 240000002943 Elettaria cardamomum Species 0.000 description 1
- 230000005526 G1 to G0 transition Effects 0.000 description 1
- -1 Oxygen alkane Chemical class 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000005300 cardamomo Nutrition 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003571 electronic cigarette Substances 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 239000005350 fused silica glass Substances 0.000 description 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
- JMANVNJQNLATNU-UHFFFAOYSA-N glycolonitrile Natural products N#CC#N JMANVNJQNLATNU-UHFFFAOYSA-N 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229910021420 polycrystalline silicon Inorganic materials 0.000 description 1
- 229920005591 polysilicon Polymers 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000006722 reduction reaction Methods 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention relates to it is a kind of can lifting electrical heating do not burn the rich essence of cigarette flavor and its application, above-mentioned essence is made of following raw material: 8-15 parts of mixed essential oil, 5-8 parts of bergamot oil, 5-8 parts of orange oil, 1-4 parts of mace oil, 30-40 parts of glycerol, 10-40 parts of alcohol, and total weight number is 100 parts.Mixed essential oil, bergamot oil, orange oil, mace oil etc. is selected to be used as raw material in the present invention, so that essence has the characteristics that smell aromatic and nature, to preferably coordinate with cigarette perfume；Mixed essential oil is obtained through subcritical abstraction in the present invention, so that essential oil quality is pure, smell it is fragrant it is abundant, naturally, be applied to electric heating do not burn cigarette when can eliminate conventional extract residual sense in bring oral cavity in suction, so that mouthfeel is pure, comfortable, so as to improve suction impression.
Description
Technical field
The present invention relates to technical field of tobacco, more particularly to it is a kind of can the lifting electrical heating cigarette flavor that do not burn it is rich
Essence and its application.
Background technique
Electric heating is not burnt cigarette, is most fiery new tobacco products in the world in recent years.With electronic cigarette " with electronics device
Part heats tobacco tar, sucks after atomization " it is different, it is " heating tobacco material with electronic device, suck after smoke ".Heating is not burnt
Smoke grenade still belong to the scope of " cigarette ", only to be sucked under the smoking set of " electronization " cooperation.
It is equally sucking smog, traditional cigarette is sucked after lighting tobacco material, and the temperature of cigarette butt is at 600 DEG C -900 DEG C
Between change, thousands of kinds of ingredients in tobacco material have occurred extremely complex physics, chemical reaction, temperature is uncontrollable, various
Oxidation reaction, reduction reaction, the product of cracking reaction are just more uncontrollable；And electric heating is not burnt, the electronic heater of cigarette can
Temperature is accurately controlled in 300 DEG C or so, smoke components are relatively controllable, and harmful substance in contrast will much less.
Since the electric heating cigarette that do not burn mainly generates flue gas and meets smoker's demand, but since electric heating is not burnt
The smoke composition of cigarette is more single compared with traditional cigarette, inevitably will cause that oral cavity comfort is poor, has a bitterness sense, and fragrance is not abundant etc. to ask
Topic, thus the effect of added essence is particularly critical.
Summary of the invention
For the above problem present in winding development, now provide one kind can the lifting electrical heating cigarette flavor that do not burn it is abundant
Property essence and its application, it is intended to effectively increase cigarette perfume, mitigate oral cavity bitterness sense, while promoting the sweet sense in oral cavity.
Specific technical solution is as follows:
The first aspect of the invention be to provide it is a kind of can lifting electrical heating do not burn the rich essence of cigarette flavor, tool
There is such feature, be made of following raw material: 8-15 parts of mixed essential oil, 5-8 parts of bergamot oil, 5-8 parts of orange oil, meat
1-4 parts of cardamom oil, 30-40 parts of glycerol, 10-40 parts of alcohol, total weight number are 100 parts；
Wherein, mixed essential oil is obtained by chamomile and Jasmine extraction.
Above-mentioned essence, also has the feature that, mixed essential oil the preparation method comprises the following steps: by chamomile dried flower and Jasmine
It is ground into after dried flower mixing and spends end, end will be spent to be added to the water and mixed enzyme is added after being ultrasonically treated thereto again, then made in ultrasound
With lower enzymatic hydrolysis, extractant is added into the feed liquid after enzymatic hydrolysis and carries out subcritical abstraction, feed liquid extracted is evaporated under reduced pressure, is centrifuged
It separates, filter to obtain mixed essential oil.
Above-mentioned essence, also has the feature that, is in mass ratio that 1:1 is mixed by chamomile dried flower and dry jasmine flower
It is ground into partial size afterwards and spends end for 80 mesh.
Above-mentioned essence, also has the feature that, end will be spent to mix with water by mass volume ratio for 1:2-3 and at ultrasound
Mixed enzyme is added thereto again after reason 10-15min.
Above-mentioned essence, also has the feature that, the mass volume ratio of mixed enzyme and water is 1:10, and enzymolysis time is
50-70min。
Above-mentioned essence, also has the feature that, mixed enzyme is that 1:1 is mixed with cellulase by protease in mass ratio
It forms.
Above-mentioned essence, also has the feature that, the mass volume ratio of Hua Moyu extractant is 1:6-10.
Above-mentioned essence, also has the feature that, extractant is selected from one of propane, butane or iso-butane or several
Kind.
Above-mentioned essence, also has the feature that, subcritical abstraction temperature is 50-100 DEG C, extracting pressure 1-
1.5Mpa, extraction time 1-1.5h.
Sonification power is 150-200w, frequency 20-400Hz in the present invention.
The second aspect of the invention is to provide a kind of application of essence in cigarette, has the feature that, essence exists
It is added in pipe tobacco, additive amount is the 0.05-0.10% of pipe tobacco weight.
The beneficial effect of above scheme is:
1), mixed essential oil, bergamot oil, orange oil, mace oil etc. is selected to be used as raw material in the present invention, so that essence has
Have the characteristics that smell aromatic and nature, to preferably coordinate with cigarette perfume；
2), mixed essential oil is obtained through subcritical abstraction in the present invention, and essential oil quality is pure in the present invention, smells fragrant enrich, certainly
So, do not burn applied to electric heating cigarette when can eliminate conventional extract suction when bring oral cavity residual sense so that mouthfeel
It is pure, comfortable, so as to improve suction impression.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, those of ordinary skill in the art's every other embodiment obtained without creative labor,
It shall fall within the protection scope of the present invention.
It should be noted that in the absence of conflict, the feature in embodiment and embodiment in the present invention can phase
Mutually combination.
The present invention is further explained in the light of specific embodiments, but not as the limitation of the invention.
Embodiment 1
It is a kind of can lifting electrical heating do not burn the rich essence of cigarette flavor, preparation includes the following steps: to weigh mixed
Close 15 parts of essential oil, 5 parts of bergamot oil, 5 parts of orange oil, 1 part of mace oil, 34 parts of glycerol, 40 parts of alcohol, by alcohol, glycerol according to
In secondary addition blend tank and after stirring 20min, remaining component is added into blend tank, stands 2d after stirring 2.5h, then with hole
The filter membrane that diameter is 0.8 μm filter off the obtained filtrate of sediment to get it is a kind of can the lifting electrical heating cigarette flavor that do not burn it is rich
Essence；
Wherein, mixed essential oil the preparation method comprises the following steps: by chamomile dried flower and dry jasmine flower be in mass ratio 1:1 mix after
End is spent after being ground into, end and water will will be spent to be mixed and sonicated after 10min again by mass volume ratio for 1:2, and addition is mixed thereto
Synthase (mixed enzyme is mixed in mass ratio for 1:1 by protease with cellulase, and the mass volume ratio of mixed enzyme and water is 1:
10) 50min, then under ultrasonication is digested, extractant (propane, the quality of Hua Moyu propane are added into the feed liquid after enzymatic hydrolysis
Volume ratio is 1:6) carrying out subcritical abstraction, (subcritical abstraction temperature is 50 DEG C, extracting pressure 1Mpa, extraction time are
1h), feed liquid extracted through vacuum distillation, centrifuge separation, filter to obtain mixed essential oil.
Perfume ingredient is detected using GC-MS method in the present invention.
GC condition: chromatographic column: middle polarity fused-silica capillary column, stationary phase are (14% cyanogen propyl)-methyl polysilicon
Oxygen alkane, 30m × 0.25mm × 0.25 μm.
MS condition: ion source: the source EI；Ion source temperature: 230 DEG C；Electron energy: 70eV；Scan pattern: full scan.
The results show that more aroma substance is produced in essence provided by the invention, increased specific substance and content
It is as shown in the table:
| Chemical name | Content (%) | Odor type |
| Laurene | 0.21 | Light face cream sample fragrance |
| Carypohyllene | 0.1 | Mild cloves sample fragrance |
| Linalool | 0.31 | Like lily of the valley fragrance |
| Jasmone | 0.09 | Like celery seed sample fragrance |
As seen from the above table, the ingredient of a large amount of great natural faint scents and mellowness is increased in essence provided by the invention, thus
The fragrance of essence can be greatly enriched, so that essence has the characteristics that smell aromatic and nature.
Reconstituted tobacco is sprayed directly on after diluting the essence that above-described embodiment obtains with 70% ethyl alcohol in the present invention to be made
Pipe tobacco on, placed 2 hours in 40 DEG C of drying boxes, electric heating be then made and does not burn new cigarette, wherein essence in cigarette
Account for the 0.05% of pipe tobacco weight.
Essence provided by the invention is not added by what new cigarette and conventional commercial were not burnt in above-mentioned electric heating in the present invention
The electric heating cigarette that do not burn smoked panel test by the 9 people groups of smokeing panel test, final result is using majority's opinion as final result, knot of smokeing panel test
Fruit show electric heating provided by the invention do not burn cigarette compared with the electric heating of conventional commercial do not burn cigarette significantly increase it is strong
Fragrance of a flower fragrance, mouthfeel is pure, comfortable when and slightly alleviating oral cavity bitterness sense, while aspirating.
Embodiment 2
It is a kind of can lifting electrical heating do not burn the rich essence of cigarette flavor, preparation includes the following steps: to weigh mixed
Close 11 parts of essential oil, 6 parts of bergamot oil, 8 parts of orange oil, 3 parts of mace oil, 40 parts of glycerol, 32 parts of alcohol, by alcohol, glycerol according to
In secondary addition blend tank and after stirring 20min, remaining component is added into blend tank, stands 2d after stirring 2.5h, then with hole
The filter membrane that diameter is 0.8 μm filters off the obtained filtrate of sediment, as it is a kind of can the lifting electrical heating cigarette flavor that do not burn it is rich
Essence；
Wherein, mixed essential oil the preparation method comprises the following steps: by chamomile dried flower and dry jasmine flower be in mass ratio 1:1 mix after
End is spent after being ground into, and end and water will will be spent to be mixed and sonicated after 13min by mass volume ratio for 1:2.5 and be added thereto again
(mixed enzyme is mixed in mass ratio for 1:1 by protease with cellulase mixed enzyme, and the mass volume ratio of mixed enzyme and water is
1:10), then under ultrasonication 60min is digested, extractant (propane, the matter of Hua Moyu propane is added into the feed liquid after enzymatic hydrolysis
Amount volume ratio is 1:8) carrying out subcritical abstraction, (subcritical abstraction temperature is 70 DEG C, extracting pressure 1.2Mpa, extraction time
For 1.3h), feed liquid extracted through vacuum distillation, centrifuge separation, filter to obtain mixed essential oil.
Perfume ingredient is detected referring to test method in embodiment 1 in the present embodiment, the results show that essence provided by the invention
In produce more aroma substance, increased specific substance and content are as shown in the table:
| Chemical name | Content (%) | Odor type |
| Laurene | 0.01 | Light face cream sample fragrance |
| Carypohyllene | 0.05 | Mild cloves sample fragrance |
| Linalool | 0.23 | Like lily of the valley fragrance |
| Jasmone | 0.19 | Like celery seed sample fragrance |
As seen from the above table, the ingredient of a large amount of great natural faint scents and mellowness is increased in essence provided by the invention, thus
The fragrance of essence can be greatly enriched, so that essence has the characteristics that smell aromatic and nature.
Reconstituted tobacco is sprayed directly on after diluting the essence that above-described embodiment obtains with 70% ethyl alcohol in the present invention to be made
Pipe tobacco on, placed 3 hours in 40 DEG C of drying boxes, electric heating be then made and does not burn new cigarette, wherein essence in cigarette
Account for the 0.08% of pipe tobacco weight.
Essence provided by the invention is not added by what new cigarette and conventional commercial were not burnt in above-mentioned electric heating in the present invention
The electric heating cigarette that do not burn smoked panel test by the 9 people groups of smokeing panel test, final result is using majority's opinion as final result, knot of smokeing panel test
Fruit show electric heating provided by the invention do not burn cigarette compared with the electric heating of conventional commercial do not burn cigarette significantly increase it is strong
Fragrance of a flower fragrance, mouthfeel is pure, comfortable when and slightly alleviating oral cavity bitterness sense, while aspirating.
Embodiment 3
It is a kind of can lifting electrical heating do not burn the rich essence of cigarette flavor, preparation includes the following steps: to weigh mixed
8 parts of essential oil, 7 parts of bergamot oil, 8 parts of orange oil, 4 parts of mace oil, 37 parts of glycerol, 36 parts of alcohol are closed, successively by alcohol, glycerol
It is added in blend tank and after stirring 20min, remaining component is added into blend tank, stand 2d after stirring 2.5h, then with aperture
For 0.8 μm of filter membrane filter off the obtained filtrate of sediment to get it is a kind of can lifting electrical heating do not burn the rich perfume (or spice) of cigarette flavor
Essence；
Wherein, mixed essential oil the preparation method comprises the following steps: by chamomile dried flower and dry jasmine flower be in mass ratio 1:1 mix after
End is spent after being ground into, end and water will will be spent to be mixed and sonicated after 15min again by mass volume ratio for 1:2, and addition is mixed thereto
Synthase (mixed enzyme is mixed in mass ratio for 1:1 by protease with cellulase, and the mass volume ratio of mixed enzyme and water is 1:
10) 50min, then under ultrasonication is digested, extractant (propane, the quality of Hua Moyu propane are added into the feed liquid after enzymatic hydrolysis
Volume ratio is 1:10) carrying out subcritical abstraction, (subcritical abstraction temperature is 100 DEG C, extracting pressure 1.5Mpa, extraction time
For 1.5h), feed liquid extracted through vacuum distillation, centrifuge separation, filter to obtain mixed essential oil.
Perfume ingredient is detected referring to test method in embodiment 1 in the present embodiment, the results show that essence provided by the invention
In produce more aroma substance, increased specific substance and content are as shown in the table:
As seen from the above table, the ingredient of a large amount of great natural faint scents and mellowness is increased in essence provided by the invention, thus
The fragrance of essence can be greatly enriched, so that essence has the characteristics that smell aromatic and nature.
Reconstituted tobacco is sprayed directly on after diluting the essence that above-described embodiment obtains with 70% ethyl alcohol respectively in the present invention
It on manufactured pipe tobacco, is placed 4 hours in 40 DEG C of drying boxes, electric heating is then made and does not burn new cigarette, wherein in cigarette
Essence accounts for the 0.10% of pipe tobacco weight.
Essence provided by the invention is not added by what new cigarette and conventional commercial were not burnt in above-mentioned electric heating in the present invention
The electric heating cigarette that do not burn smoked panel test by the 9 people groups of smokeing panel test, final result is using majority's opinion as final result, knot of smokeing panel test
Fruit show electric heating provided by the invention do not burn cigarette compared with the electric heating of conventional commercial do not burn cigarette significantly increase it is strong
Fragrance of a flower fragrance, and slightly alleviate oral cavity bitterness sense.
The above is only preferred embodiments of the present invention, are not intended to limit the implementation manners and the protection scope of the present invention, right
For those skilled in the art, it should can appreciate that all with equivalent replacement made by present specification and aobvious
And the obtained scheme of variation being clear to, it should all be included within the scope of the present invention.
Claims (10)
1. one kind can lifting electrical heating do not burn the rich essence of cigarette flavor, which is characterized in that by following raw material
Composition: 8-15 parts of mixed essential oil, 5-8 parts of bergamot oil, 5-8 parts of orange oil, 1-4 parts of mace oil, 30-40 parts of glycerol, alcohol
10-40 parts, total weight number is 100 parts；
Wherein, the mixed essential oil is obtained by chamomile and Jasmine extraction.
2. essence according to claim 1, which is characterized in that the mixed essential oil the preparation method comprises the following steps: chamomile is done
It is ground into after the mixing of colored and dry jasmine flower and spends end, end will be spent to be added to the water and mixed enzyme is added thereto again after being ultrasonically treated,
It is digested under ultrasonication again, extractant is added into the feed liquid after enzymatic hydrolysis and carries out subcritical abstraction, feed liquid extracted is through subtracting
The mixed essential oil is distilled, is centrifugated, filtering and to be obtained to pressure.
3. essence according to claim 2, which is characterized in that by chamomile dried flower and dry jasmine flower be in mass ratio 1:
It is ground into after 1 mixing and spends end.
4. essence according to claim 2, which is characterized in that end will be spent to mix simultaneously by mass volume ratio for 1:2-3 with water
Mixed enzyme is added thereto again after ultrasonic treatment 10-15min.
5. essence according to claim 3, which is characterized in that the mass volume ratio of mixed enzyme and water is 1:10, when enzymatic hydrolysis
Between be 50-70min.
6. essence according to claim 5, which is characterized in that the mixed enzyme by protease and cellulase in mass ratio
It is mixed for 1:1.
7. essence according to claim 2, which is characterized in that the mass volume ratio of Hua Moyu extractant is 1:6-10.
8. essence according to claim 7, which is characterized in that extractant is selected from one of propane, butane or iso-butane
Or it is several.
9. essence according to claim 2, which is characterized in that subcritical abstraction temperature is 50-100 DEG C, extracting pressure is
1-1.5Mpa, extraction time 1-1.5h.
10. application of the essence described in claim 1 in cigarette, which is characterized in that essence adds in the tobacco, and additive amount is cigarette
The 0.05-0.10% of silk weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
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| CN115251450A (en) * | 2022-08-22 | 2022-11-01 | 东莞市鸿馥生物科技有限公司 | Bergamot essential oil applied to electronic cigarette and preparation method thereof |
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