CN103966027B - A kind of preparation method of the composite extract of Herba Rosmarini Officinalis - Google Patents
A kind of preparation method of the composite extract of Herba Rosmarini Officinalis Download PDFInfo
- Publication number
- CN103966027B CN103966027B CN201410204635.3A CN201410204635A CN103966027B CN 103966027 B CN103966027 B CN 103966027B CN 201410204635 A CN201410204635 A CN 201410204635A CN 103966027 B CN103966027 B CN 103966027B
- Authority
- CN
- China
- Prior art keywords
- herba rosmarini
- rosmarini officinalis
- extract
- base
- leaf
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000284 extract Substances 0.000 title claims abstract description 62
- 239000002131 composite material Substances 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 238000002481 ethanol extraction Methods 0.000 claims abstract description 28
- 238000000926 separation method Methods 0.000 claims abstract description 23
- 239000000843 powder Substances 0.000 claims abstract description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000004108 freeze drying Methods 0.000 claims abstract description 12
- 238000002156 mixing Methods 0.000 claims abstract description 10
- 238000007710 freezing Methods 0.000 claims abstract description 7
- 230000008014 freezing Effects 0.000 claims abstract description 7
- 238000001556 precipitation Methods 0.000 claims abstract description 7
- 238000003815 supercritical carbon dioxide extraction Methods 0.000 claims abstract description 7
- 239000006228 supernatant Substances 0.000 claims abstract description 7
- 238000000605 extraction Methods 0.000 claims description 29
- 238000000194 supercritical-fluid extraction Methods 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 238000000859 sublimation Methods 0.000 claims description 5
- 230000008022 sublimation Effects 0.000 claims description 5
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 9
- 239000003546 flue gas Substances 0.000 abstract description 9
- 235000019504 cigarettes Nutrition 0.000 abstract description 8
- 239000002304 perfume Substances 0.000 abstract 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 15
- 244000061176 Nicotiana tabacum Species 0.000 description 10
- 241000208125 Nicotiana Species 0.000 description 5
- 241001529742 Rosmarinus Species 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000000341 volatile oil Substances 0.000 description 3
- 239000003963 antioxidant agent Substances 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 description 1
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical group CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 1
- WEEGYLXZBRQIMU-UHFFFAOYSA-N Eucalyptol Chemical compound C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229940025250 camphora Drugs 0.000 description 1
- 239000010238 camphora Substances 0.000 description 1
- 229960005233 cineole Drugs 0.000 description 1
- RFFOTVCVTJUTAD-UHFFFAOYSA-N cineole Natural products C1CC2(C)CCC1(C(C)C)O2 RFFOTVCVTJUTAD-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 150000002628 limonene derivativess Chemical class 0.000 description 1
- 238000013441 quality evaluation Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
Landscapes
- Extraction Or Liquid Replacement (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The preparation method that the invention discloses the composite extract of a kind of Herba Rosmarini Officinalis, preparation method comprises the following steps: (1) takes fresh Herba Rosmarini Officinalis base of leaf, carries out freezing at low ambient temperatures；(2) from refrigerating chamber, Herba Rosmarini Officinalis base of leaf is taken out, by Herba Rosmarini Officinalis base of leaf vacuum lyophilization；(3) Herba Rosmarini Officinalis base of leaf is pulverized；(4) it is stirred Herba Rosmarini Officinalis base of leaf powder ethanol extracting；(5) after extracting, extracting solution is centrifuged, after collecting supernatant concentration, obtains Herba Rosmarini Officinalis ethanol extraction；(6) the Herba Rosmarini Officinalis precipitation after centrifugal is carried out supercritical carbon dioxide extraction；(7) Herba Rosmarini Officinalis extract in flash trapping stage still and the second-order separation still is collected；(8) by composite for the composite extract of Herba Rosmarini Officinalis after ethanol extraction, flash trapping stage extract, the mixing of the second-order separation extract.The composite extract of Herba Rosmarini Officinalis prepared effectively raises perfume quantity and the aroma quality of medicated cigarette, improves the mouthfeel of medicated cigarette, improves the flue gas concentration of medicated cigarette.
Description
Technical field
The preparation method that the present invention relates to a kind of tobacco spice, the preparation method particularly relating to the composite extract of a kind of Herba Rosmarini Officinalis.
Background technology
Herba Rosmarini Officinalis is Labiatae Rosmarinus plant, and for evergreen dwarf shrub, original producton location is Europe and Mediterranean.Herba Rosmarini Officinalis, due to the odor characteristic of its uniqueness, is widely used in the middle of Nicotiana tabacum L., fancy soap, cosmetics, toothpaste etc..Additionally, have substantial amounts of antioxidant content in Herba Rosmarini Officinalis, these antioxidant contents have higher antioxidation.
In Field of Tobacco, Herba Rosmarini Officinalis extract application in the middle of Nicotiana tabacum L. is less, rosemary ethereal oil is owing to containing aroma components such as substantial amounts of australene, cineole, Camphora, Borneolum Syntheticum, dipentenes, these nonpolar extracts are applied in the middle of Nicotiana tabacum L., it is possible to can effectively improve concentration and the quality of flue gas.In the middle of current research, to Herba Rosmarini Officinalis the ethanol extraction research that is applied in Nicotiana tabacum L. considerably less, Herba Rosmarini Officinalis ethanol extraction is unclear to the castering action of flue gas, these middle polarity extracts and rudimentary property extract on the mouthfeel of medicated cigarette, flue gas, strength impact still need that we do further research.
Summary of the invention
Solve the technical problem that: conventional extracting method not to Herba Rosmarini Officinalis extract carry out extracting by different level after composite usage in Nicotiana tabacum L., and it is relatively low to extract the Herba Rosmarini Officinalis extract extraction ratio obtained, it is applied in the middle of Nicotiana tabacum L., the lifting of the mouthfeel of Nicotiana tabacum L., flue gas concentration and quality, strength is less, it is impossible to improve the quality of Nicotiana tabacum L. preferably.
Technical scheme: the preparation method that the invention discloses the composite extract of a kind of Herba Rosmarini Officinalis, preparation method comprises the following steps: (1) takes fresh Herba Rosmarini Officinalis base of leaf, carries out freezing at low ambient temperatures；(2) from refrigerating chamber, Herba Rosmarini Officinalis base of leaf is taken out, by Herba Rosmarini Officinalis base of leaf vacuum lyophilization；(3) Herba Rosmarini Officinalis base of leaf is taken out from freezer dryer, pulverize Herba Rosmarini Officinalis base of leaf, be placed in dry environment；(4) take Herba Rosmarini Officinalis base of leaf powder, be stirred Herba Rosmarini Officinalis base of leaf powder ethanol extracting；(5) after extracting, extracting solution is centrifuged, after collecting supernatant concentration, obtains Herba Rosmarini Officinalis ethanol extraction；(6) the Herba Rosmarini Officinalis precipitation after centrifugal is carried out supercritical carbon dioxide extraction；(7) Herba Rosmarini Officinalis extract in flash trapping stage still and the second-order separation still is collected；(8) ethanol extraction, flash trapping stage extract, the second-order separation extract are mixed according to the mass ratio of 1:3:1～1:4:1, composite for the composite extract of Herba Rosmarini Officinalis after mixing.
The preparation method of the composite extract of a kind of Herba Rosmarini Officinalis, preparation method comprises the following steps: (1) takes fresh Herba Rosmarini Officinalis base of leaf, is launched by Herba Rosmarini Officinalis base of leaf, carries out freezing under the environment that temperature is-6～-9 DEG C, and cooling time is 6h～10h；(2) taking out Herba Rosmarini Officinalis base of leaf from refrigerating chamber, by Herba Rosmarini Officinalis base of leaf vacuum lyophilization, the pressure of vacuum lyophilization is 11Pa～17Pa, and sublimation drying is 5h～7h；(3) being taken out from freezer dryer by Herba Rosmarini Officinalis base of leaf, pulverize Herba Rosmarini Officinalis base of leaf, being crushed to base of leaf powder is 200～300 orders, is placed in dry environment；(4) taking Herba Rosmarini Officinalis base of leaf powder, be stirred Herba Rosmarini Officinalis base of leaf powder ethanol extracting, solid-liquid ratio is 1:6～1:10, and Extracting temperature is 40 DEG C～50 DEG C, and extraction time is 2h～4h；(5) after extracting, extracting solution is centrifuged, after collecting supernatant concentration, obtains Herba Rosmarini Officinalis ethanol extraction；(6) the Herba Rosmarini Officinalis precipitation after centrifugal being carried out supercritical carbon dioxide extraction, supercritical extraction pressure is 21MPa～27MPa, and extraction temperature is 50 DEG C～60 DEG C, and flash trapping stage pressure is 8.5～9MPa, and the second-order separation pressure is 6.5MPa, and extraction time is 4h；(7) Herba Rosmarini Officinalis extract in flash trapping stage still and the second-order separation still is collected；(8) ethanol extraction, flash trapping stage extract, the second-order separation extract are mixed according to the mass ratio of 1:3:1～1:4:1, composite for the composite extract of Herba Rosmarini Officinalis after mixing.
Wherein, described supercritical extraction pressure is preferably 25MPa.By supercritical extraction pressure is preferably 25MPa, flash trapping stage extract and the second-order separation extract extraction ratio that supercritical extraction obtains are obtained for and are effectively improved.
Wherein, flash trapping stage pressure is preferably 9MPa.Flash trapping stage pressure is preferably 9MPa, and after the flash trapping stage extract obtained is composite with ethanol extraction and the second-order separation extract, it is the most obvious to improvement and the castering action of Nicotiana tabacum L..
Wherein, with ethanol extraction time, solid-liquid ratio is preferably 1:10.Solid-liquid ratio is preferably 1:10, effectively raises Herba Rosmarini Officinalis ethanol extraction rate.
Wherein, ethanol extraction, flash trapping stage extract, the second-order separation extract are mixed according to the mass ratio of 1:4:1, composite for the composite extract of Herba Rosmarini Officinalis after mixing.Under this mass ratio, the Herba Rosmarini Officinalis extract obtained castering action in Nicotiana tabacum L. is maximum.
Beneficial effect: in the preparation method of the present invention, Herba Rosmarini Officinalis ethanol extraction rate has been up to 21.5%, in supercritical extraction process, flash trapping stage extraction ratio is up to 6.9%, and two grades of extraction ratios have been up to 4.6%, the extraction ratio greatly prepared higher than conventional vapor distillation or additive method.Additionally, undertaken composite by Herba Rosmarini Officinalis ethanol extraction and supercritical extract, the compound obtained according to the mass ratio of 1:4:1 is readily apparent that to improve the mouthfeel of Medicated cigarette, flue gas concentration and quality, strength etc..
Detailed description of the invention
Embodiment 1
(1) taking fresh Herba Rosmarini Officinalis base of leaf 2kg, launched by Herba Rosmarini Officinalis base of leaf, carry out freezing under the environment that temperature is-9 DEG C, cooling time is 10h；(2) taking out Herba Rosmarini Officinalis base of leaf from refrigerating chamber, by Herba Rosmarini Officinalis base of leaf vacuum lyophilization, the pressure of vacuum lyophilization is 17Pa, and sublimation drying is 5h；(3) being taken out from freezer dryer by Herba Rosmarini Officinalis base of leaf, pulverize Herba Rosmarini Officinalis base of leaf, being crushed to base of leaf powder is 300 orders, is placed in dry environment；(4) taking Herba Rosmarini Officinalis base of leaf powder, be stirred Herba Rosmarini Officinalis base of leaf powder ethanol extracting, solid-liquid ratio is 1:8, and Extracting temperature is 50 DEG C, and extraction time is 2h；(5) after extracting, extracting solution is centrifuged, after collecting supernatant concentration, obtains Herba Rosmarini Officinalis ethanol extraction；(6) the Herba Rosmarini Officinalis precipitation after centrifugal being carried out supercritical carbon dioxide extraction, supercritical extraction pressure is 21MPa, and extraction temperature is 60 DEG C, and flash trapping stage pressure is 8.5MPa, and the second-order separation pressure is 6.5MPa, and extraction time is 4h；(7) Herba Rosmarini Officinalis extract in flash trapping stage still and the second-order separation still is collected；(8) ethanol extraction, flash trapping stage extract, the second-order separation extract are mixed according to the mass ratio of 1:3:1, composite for the composite extract of Herba Rosmarini Officinalis after mixing.
Embodiment 2
(1) taking fresh Herba Rosmarini Officinalis base of leaf 1kg, launched by Herba Rosmarini Officinalis base of leaf, carry out freezing under the environment that temperature is-6 DEG C, cooling time is 6h；(2) taking out Herba Rosmarini Officinalis base of leaf from refrigerating chamber, by Herba Rosmarini Officinalis base of leaf vacuum lyophilization, the pressure of vacuum lyophilization is 14Pa, and sublimation drying is 7h；(3) being taken out from freezer dryer by Herba Rosmarini Officinalis base of leaf, pulverize Herba Rosmarini Officinalis base of leaf, being crushed to base of leaf powder is 200 orders, is placed in dry environment；(4) taking Herba Rosmarini Officinalis base of leaf powder, be stirred Herba Rosmarini Officinalis base of leaf powder ethanol extracting, solid-liquid ratio is 1:6, and Extracting temperature is 40 DEG C, and extraction time is 4h；(5) after extracting, extracting solution is centrifuged, after collecting supernatant concentration, obtains Herba Rosmarini Officinalis ethanol extraction；(6) the Herba Rosmarini Officinalis precipitation after centrifugal being carried out supercritical carbon dioxide extraction, supercritical extraction pressure is 25MPa, and extraction temperature is 50 DEG C, and flash trapping stage pressure is 9MPa, and the second-order separation pressure is 6.5MPa, and extraction time is 4h；(7) Herba Rosmarini Officinalis extract in flash trapping stage still and the second-order separation still is collected；(8) ethanol extraction, flash trapping stage extract, the second-order separation extract are mixed according to the mass ratio of 1:4:1, composite for the composite extract of Herba Rosmarini Officinalis after mixing.
Embodiment 3
(1) taking fresh Herba Rosmarini Officinalis base of leaf 3kg, launched by Herba Rosmarini Officinalis base of leaf, carry out freezing under the environment that temperature is-8 DEG C, cooling time is 8h；(2) taking out Herba Rosmarini Officinalis base of leaf from refrigerating chamber, by Herba Rosmarini Officinalis base of leaf vacuum lyophilization, the pressure of vacuum lyophilization is 11Pa, and sublimation drying is 6h；(3) being taken out from freezer dryer by Herba Rosmarini Officinalis base of leaf, pulverize Herba Rosmarini Officinalis base of leaf, being crushed to base of leaf powder is 250 orders, is placed in dry environment；(4) taking Herba Rosmarini Officinalis base of leaf powder, be stirred Herba Rosmarini Officinalis base of leaf powder ethanol extracting, solid-liquid ratio is 1:10, and Extracting temperature is 45 DEG C, and extraction time is 3h；(5) after extracting, extracting solution is centrifuged, after collecting supernatant concentration, obtains Herba Rosmarini Officinalis ethanol extraction；(6) the Herba Rosmarini Officinalis precipitation after centrifugal being carried out supercritical carbon dioxide extraction, supercritical extraction pressure is 27MPa, and extraction temperature is 55 DEG C, and flash trapping stage pressure is 8.5MPa, and the second-order separation pressure is 6.5MPa, and extraction time is 4h；(7) Herba Rosmarini Officinalis extract in flash trapping stage still and the second-order separation still is collected；(8) ethanol extraction, flash trapping stage extract, the second-order separation extract are mixed according to the mass ratio of 1:3:1, composite for the composite extract of Herba Rosmarini Officinalis after mixing.
Embodiment 1, embodiment 2, the ethanol extraction rate of embodiment 3, one-level extraction ratio, two grades of extraction ratio results are as follows.
Ethanol extraction rate: ethanol concentrate quality/Herba Rosmarini Officinalis gross mass × 100%
One-level extraction ratio: one-level extract quality/Herba Rosmarini Officinalis gross mass × 100%
Two grades of extraction ratios: two grades of extract quality/Herba Rosmarini Officinalis gross mass × 100%
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Ethanol extraction rate | 11.8% | 15.6% | 21.5% |
| One-level extraction ratio | 4.6% | 6.9% | 6.7% |
| Two grades of extraction ratios | 1.4% | 4.6% | 4.2% |
The solid-liquid ratio of embodiment 3 is 1:10 as can be seen from the table, and the ethanol extraction quality that it prepares is also the highest.Additionally, the supercritical extraction pressure in embodiment 2 is preferably 25MPa, one-level extraction ratio and two grades of extraction ratios are all higher than the 27MPa of embodiment 3, are different from the phenomenon that in the supercritical extraction of routine, the more big extraction ratio of pressure is more big.
By embodiment 1, embodiment 2, embodiment 3 the composite extract acetic acid ethyl dissolution of Herba Rosmarini Officinalis, the composite extract concentrations of Herba Rosmarini Officinalis is 1wt%, is uniformly sprayed on tobacco shred, and fountain height is the 0.5wt% of tobacco shred weight, makes Medicated cigarette and smoke panel test after balance.Reference examples is with the addition of the Medicated cigarette of the rosemary ethereal oil that vapor distillation method obtains, and the concentration of rosemary ethereal oil is also 1wt%, and fountain height is also the 0.5wt% of tobacco shred weight, and integrated sensory's quality evaluation result is as follows:
Embodiment 1: flue gas is full, full aroma, mouthfeel are moderate, pleasant impression is better, Titian effect is comparatively obvious.
Embodiment 2: flue gas is strong, full aroma, coordination and elegant, delicate mouthfeel is soft and smooth, pleasant impression is comfortable, Titian effect clearly.
Embodiment 3: aromatic strongly fragrant, the fragrance of cigarette is coordinated, mouthfeel is moderate, Titian effect is comparatively obvious.
Reference examples: flue gas slightly increases, fragrance slightly promotes, mouthfeel is general, pleasant impression is poor, Titian effect does not highlight.
Claims (5)
1. the preparation method of the composite extract of Herba Rosmarini Officinalis, it is characterised in that preparation method comprises the following steps: (1) takes fresh Herba Rosmarini Officinalis base of leaf, launches Herba Rosmarini Officinalis base of leaf, carries out freezing under the environment that temperature is-6～-9 DEG C, and cooling time is 6h～10h；(2) taking out Herba Rosmarini Officinalis base of leaf from refrigerating chamber, by Herba Rosmarini Officinalis base of leaf vacuum lyophilization, the pressure of vacuum lyophilization is 11Pa～17Pa, and sublimation drying is 5h～7h；(3) being taken out from freezer dryer by Herba Rosmarini Officinalis base of leaf, pulverize Herba Rosmarini Officinalis base of leaf, being crushed to base of leaf powder is 200～300 orders, is placed in dry environment；(4) taking Herba Rosmarini Officinalis base of leaf powder, be stirred Herba Rosmarini Officinalis base of leaf powder ethanol extracting, solid-liquid ratio is 1:6～1:10, and Extracting temperature is 40 DEG C～50 DEG C, and extraction time is 2h～4h；(5) after extracting, extracting solution is centrifuged, after collecting supernatant concentration, obtains Herba Rosmarini Officinalis ethanol extraction；(6) the Herba Rosmarini Officinalis precipitation after centrifugal being carried out supercritical carbon dioxide extraction, supercritical extraction pressure is 21MPa～27MPa, and extraction temperature is 50 DEG C～60 DEG C, and flash trapping stage pressure is 8.5～9MPa, and the second-order separation pressure is 6.5MPa, and extraction time is 4h；(7) Herba Rosmarini Officinalis extract in flash trapping stage still and the second-order separation still is collected；(8) ethanol extraction, flash trapping stage extract, the second-order separation extract are mixed according to the mass ratio of 1:3:1～1:4:1, composite for the composite extract of Herba Rosmarini Officinalis after mixing.
2. the preparation method of the composite extract of a kind of Herba Rosmarini Officinalis according to claim 1, it is characterised in that described supercritical extraction pressure is 25MPa.
3. the preparation method of the composite extract of a kind of Herba Rosmarini Officinalis according to claim 1, it is characterised in that flash trapping stage pressure is 9MPa.
4. the preparation method of the composite extract of a kind of Herba Rosmarini Officinalis according to claim 1, it is characterised in that during with ethanol extraction, solid-liquid ratio is 1:10.
5. the preparation method of the composite extract of a kind of Herba Rosmarini Officinalis according to claim 1, it is characterized in that mixing ethanol extraction, flash trapping stage extract, the second-order separation extract according to the mass ratio of 1:4:1, composite for the composite extract of Herba Rosmarini Officinalis after mixing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410204635.3A CN103966027B (en) | 2014-05-15 | 2014-05-15 | A kind of preparation method of the composite extract of Herba Rosmarini Officinalis |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410204635.3A CN103966027B (en) | 2014-05-15 | 2014-05-15 | A kind of preparation method of the composite extract of Herba Rosmarini Officinalis |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103966027A CN103966027A (en) | 2014-08-06 |
| CN103966027B true CN103966027B (en) | 2016-06-29 |
Family
ID=51236036
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410204635.3A Expired - Fee Related CN103966027B (en) | 2014-05-15 | 2014-05-15 | A kind of preparation method of the composite extract of Herba Rosmarini Officinalis |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103966027B (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104164455A (en) * | 2014-08-19 | 2014-11-26 | 云南中烟工业有限责任公司 | Rosmarinus officinalis L. fermentation broth extract as well as preparation method and application thereof |
| CN104397362A (en) * | 2014-12-15 | 2015-03-11 | 昆山市畜牧兽医站 | Preparation technology for rosemary powder and application of rosemary powder to laying hen feed |
| CN105686067A (en) * | 2016-03-11 | 2016-06-22 | 李贵生 | Rosemary type cigarette |
| CN108753461A (en) * | 2018-06-05 | 2018-11-06 | 佛山皖阳生物科技有限公司 | A kind of preparation method of biology peptide composite antioxidant |
| CN109022152A (en) * | 2018-08-30 | 2018-12-18 | 湖北中烟工业有限责任公司 | A kind of rosemary tobacco aromaticss and its preparation method and application |
| CN115486530B (en) * | 2022-10-21 | 2024-03-26 | 湖南祥民制药有限公司 | Freeze-drying method of rosemary |
| CN116019219A (en) * | 2022-12-30 | 2023-04-28 | 东莞市吉纯生物技术有限公司 | A buccal product containing herba Rosmarini officinalis extract and its preparation method |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1316494A (en) * | 2000-04-06 | 2001-10-10 | 张高 | Process for extracting antioxidizing agent and perfume from rosemary |
| CN1781545A (en) * | 2001-02-09 | 2006-06-07 | 新纪元公司 | Method for extracting herbal medicine |
| CN102199092A (en) * | 2010-03-26 | 2011-09-28 | 禹州市森源本草天然产物有限公司 | Production technology for acquiring two antioxidant agents from Rosmarinus officinalis L. |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH03293001A (en) * | 1990-04-11 | 1991-12-24 | Chisso Corp | Method for deodorizing antioxidant component extracted from natural resouce |
-
2014
- 2014-05-15 CN CN201410204635.3A patent/CN103966027B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1316494A (en) * | 2000-04-06 | 2001-10-10 | 张高 | Process for extracting antioxidizing agent and perfume from rosemary |
| CN1781545A (en) * | 2001-02-09 | 2006-06-07 | 新纪元公司 | Method for extracting herbal medicine |
| CN102199092A (en) * | 2010-03-26 | 2011-09-28 | 禹州市森源本草天然产物有限公司 | Production technology for acquiring two antioxidant agents from Rosmarinus officinalis L. |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103966027A (en) | 2014-08-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103966027B (en) | A kind of preparation method of the composite extract of Herba Rosmarini Officinalis | |
| CN103396885B (en) | Method for preparing pepper aromatic oil | |
| CN103525558B (en) | Tea flower essence with fruity flavor characteristic and application thereof to cigarettes | |
| CN106174683B (en) | A kind of composition and the tobacco juice for electronic smoke containing said composition | |
| CN103263370B (en) | Production method for jasmine flower perfume | |
| CN103484247B (en) | A kind of Tea Flower stage extraction thing, its preparation method and the application in cigarette thereof | |
| CN101586057A (en) | Essence for cigarette mouth building adhesive and preparing and using method thereof | |
| CN104082853B (en) | A kind of electronic cigarette liquid containing tomato extract and preparation method thereof | |
| CN101735888A (en) | Extraction method to produce dendrobium flowers volatile oil | |
| CN103300182A (en) | Method for extracting aromatic substances and tea polyphenols from tea leaves step by step | |
| CN103484248A (en) | Tea flower essence with fresh and sweet characteristics, and application of essence in cigarettes | |
| CN103919274A (en) | Electronic cigarette atomized liquid | |
| KR101799027B1 (en) | Perfume composition for expressing the fragrance of Citrus unshiu of Jeju island the composition for skin external application containing the same | |
| CN103952239A (en) | Method for extracting essential oil from fresh bergamot and application of essential oil in cigarettes | |
| CN103126062B (en) | One grows tobacco composition extracting method | |
| CN106635418A (en) | Preparation method of high-purity citrus aurantium flower essential oil and flavor addition essence used for cigarettes and blended with high-purity citrus aurantium flower essential oil | |
| KR101694484B1 (en) | Perfume composition for expressing the fragrance of flowery oriental medicine | |
| CN202543170U (en) | Novel fragrance recovery equipment | |
| CN105011368A (en) | Glycerol triacetate extract of momordica grosvenori and application thereof to cigarette | |
| CN110037334A (en) | It is a kind of can lifting electrical heating do not burn the rich essence of cigarette flavor and its application | |
| CN105272824A (en) | Preparation method of natural cinnamomum camphora aromatic material | |
| CN105534751A (en) | Refreshing perfume | |
| CN101342010B (en) | Petroleum ether extracted white tea extract, preparation and application thereof | |
| CN108395932A (en) | A kind of preparation method of cigarette jasmine oil | |
| CN109498826A (en) | A kind of agalloch eaglewood champignon volatilization liquid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Wang Xu Inventor before: Yin Fei Inventor before: Han Ting Inventor before: Hu Zhonghao |
|
| COR | Change of bibliographic data | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20160526 Address after: 266000 Shandong province Qingdao City, Shandong Road No. 109 Building No. 3 3102 Taiwan Jing Applicant after: QINGDAO JINZHI HIGH AND NEW TECHNOLOGY CO., LTD. Address before: 108 room 1, building 522, 314000 Asia Pacific Road, Zhejiang, Jiaxing Applicant before: Jiaxing City obtains encyclopaedia novel material Science and Technology Ltd. |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information |
Inventor after: Tang Wenjun Inventor before: Wang Xu |
|
| CB03 | Change of inventor or designer information | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170719 Address after: 518000 Guangdong city of Shenzhen province Luohu District city streets East Road No. 1028 building 1808 Shichu customs Patentee after: Shenzhen Tianxiang Fu Biotechnology Co. Ltd. Address before: 266000 Shandong province Qingdao City, Shandong Road No. 109 Building No. 3 3102 Taiwan Jing Patentee before: QINGDAO JINZHI HIGH AND NEW TECHNOLOGY CO., LTD. |
|
| TR01 | Transfer of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160629 Termination date: 20200515 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |