CN108395932A - A kind of preparation method of cigarette jasmine oil - Google Patents
A kind of preparation method of cigarette jasmine oil Download PDFInfo
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- CN108395932A CN108395932A CN201810269878.3A CN201810269878A CN108395932A CN 108395932 A CN108395932 A CN 108395932A CN 201810269878 A CN201810269878 A CN 201810269878A CN 108395932 A CN108395932 A CN 108395932A
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- Prior art keywords
- jasmine
- cigarette
- preparation
- jasmine oil
- oil
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Botany (AREA)
- Agronomy & Crop Science (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Health & Medical Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of preparation methods of cigarette jasmine oil.The preparation method of the cigarette jasmine oil of the present invention, includes the following steps:（1）Jasmine raw material is provided, and ultrasonic extraction is carried out to the Jasmine raw material, obtains Jasmine extracting solution；（2）The liquid phase component of the Jasmine extracting solution is subjected to precipitating with alcoholic solvent, obtains precipitating liquid；（3）The precipitating liquid is subjected to molecular distillation, isolated jasmine oil.The preparation method of the present invention uses ultrasonic extraction to new fresh Jasmine, solvent can be made to rapidly enter cell interior, fully be extracted to active ingredient；This method carries out under cryogenic, is avoided that active ingredient by heat damage, improves the aroma quality of product；The present invention carries out precipitating with alcoholic solvent, can more thoroughly remove wax and other impurities ingredient；The present invention isolates and purifies jasmine oil using molecular distillation technique, can the wherein preferable fraction of effect be detached, be collected.
Description
Technical field
The invention belongs to essence spice for cigarette additive preparing technical fields, and in particular to a kind of cigarette jasmine oil
Preparation method.
Background technology
Jasmine fresh flower is due to containing abundant natural perfume ingredient as a kind of ornamental and specialty industries plant and extraction
The raw material of fragrance and obtain extensive plantation.Fragrance main component through chemical analysis Jasmine by：Benzyl acetate, α-linalool, leaf
Alcohol, methyl jasmonate, acetic acid linalool ester, ethyl benzoate, aminobenzoic acid formicester, jasmine lactone, cis-jasmone,
The mixture of tens kinds of organic compounds such as indoles forms.These fragrance components can be widely used in various perfume, perfumed soap, face cream and
In daily cosmetics essence be used as type-odor, also to many flavor essences of international popular such as chypre, violet, bashfully spend
Equal fragrance play modification.China standard GB/T 2760-86 is defined as food additive perfuming agent in terms of food, is mainly used for
Roasting jasmine fragrant flower tea, biscuit, cake, candy, can, drinks, cigarette class and the fragrance addition for training roasting product.In weaving, clothes
There is application in numerous industrial circles such as dress, process hides, medicine, papermaking.Part fragrance has the effects that sterilizing, anti-corrosion, excitement,
It plays a role in health care in clinical medicine and daily chemical industry, purposes is wide.
Invention content
It is an object of the present invention to for the above-mentioned deficiency of the prior art, a kind of preparation of cigarette jasmine oil is proposed
Method.
The preparation method of the cigarette jasmine oil of the present invention, includes the following steps:
（1）Jasmine raw material is provided, and ultrasonic extraction is carried out to the Jasmine raw material, obtains Jasmine extracting solution；
（2）The liquid phase component of the Jasmine extracting solution is subjected to precipitating with alcoholic solvent, obtains precipitating liquid；
（3）The precipitating liquid is subjected to molecular distillation, isolated jasmine oil.
Preferably, in step（1）Later, step（2）Further include before：The liquid phase component of Jasmine extracting solution is carried out dense
Contracting is to obtain medicinal extract shape concentrate.
Preferably, in step（2）Later, step（3）Further include before：Precipitating liquid is concentrated in vacuo.
Preferably, step（1）Described in extraction before be added mass fraction be 1~3 alcohol solvent after use ultrasonic extraction.
Preferably, the frequency of the ultrasonic extraction be 180~220KHz, temperature be 35~40 DEG C, extraction time be 20~
30min is extracted 2~4 times.
Preferably, the aqueous solution of a concentration of 50%~70wt% of the alcohol solvent.
Preferably, the concentration is concentrated using cryogenic vacuum, is concentrated into the 1/8~1/5 of original volume.
Preferably, described be concentrated in vacuo is concentrated using cryogenic vacuum, is concentrated into the 1/5~1/3 of original volume.
Preferably, the temperature of the cryogenic vacuum concentration is 40~50 DEG C.
Preferably, step（2）In the alcoholic solvent be alcohol solvent a concentration of 90%~95wt% aqueous solution.
The preparation method of the cigarette jasmine oil of the present invention uses ultrasonic extraction to new fresh Jasmine, and solvent can be made fast
Speed enters cell interior, is fully extracted to active ingredient；This method carries out under cryogenic, be avoided that active ingredient by
Heat damage improves the aroma quality of product；The present invention with alcoholic solvent carry out precipitating, can more thoroughly remove wax etc. other
Impurity component；The present invention isolates and purifies jasmine oil using molecular distillation technique, can will wherein effect it is preferable
Fraction is detached, is collected.
Specific implementation mode
The following is specific embodiments of the present invention, and technical scheme of the present invention will be further described, but the present invention is simultaneously
It is not limited to these embodiments.
Embodiment 1
The preparation method of the cigarette jasmine oil of the present invention, including step in detail below:
（1）Pre-treatment：New fresh Jasmine is taken, is cleaned, removal holder；
（2）Homogenate：By treated, Jasmine is weighed, and the aqueous solution of 2.5 times of weight is added, and is placed in homogenate equipment, is ground into
Uniform paste；
（3）Ultrasonic extraction：Paste after homogenate is placed in ultrasonic extraction device, 60% alcohol solvent of 2 times of weight is added,
Carry out ultrasonic extraction 3 times, merging filtrate obtains Jasmine extracting solution；Wherein, ultrasonic extraction frequency is 190KHz, temperature 36
DEG C, extraction time 25min.
（4）It is concentrated under reduced pressure：Using Buchner funnel by step（3）Middle extracting solution filtering, cryogenic vacuum are concentrated into the 1/7 of original volume,
Obtain leaching paste extract；Wherein, thickening temperature is set as 60 DEG C.
（5）Alcohol precipitation：By step（4）In the medicinal extract of gained be added 4 times of weight 95% ethanol solution, stirring be placed on 5 DEG C it is low
Temperature is lower to settle 28h；
（6）It is concentrated under reduced pressure：Using Buchner funnel by step（5）Middle sedimentation liquid filtering, cryogenic vacuum are concentrated into the 1/4 of original volume,
Wherein thickening temperature is set as 40 DEG C
（7）Molecular distillation：By step（6）In filtrate carry out molecular distillation, molecular distillation pressure be 0.1 Pa, initial temperature 60
DEG C, 10 DEG C of intervals are distilled, rotor speed 200r/min, and 80mL/h is added dropwise；Collect 80 DEG C of light components below, as jasmine
Extrait.
Embodiment 2
（1）Pre-treatment：New fresh Jasmine is taken, is cleaned, removal holder；
（2）Homogenate：By treated, Jasmine is weighed, and the aqueous solution of 2 times of weight is added, and is placed in homogenate equipment, is ground into
Even paste；
（3）Ultrasonic extraction：Paste after homogenate is placed in ultrasonic extraction device, 50% ethyl alcohol that 1.5 times of weight are added is molten
Agent, carries out ultrasonic extraction 3 times, and merging filtrate obtains Jasmine extracting solution；Wherein, ultrasonic extraction frequency is 190KHz, and temperature is
38 DEG C, extraction time 30min.
（4）It is concentrated under reduced pressure：Using Buchner funnel by step（3）Middle extracting solution filtering, cryogenic vacuum are concentrated into the 1/6 of original volume,
Obtain leaching paste extract；Wherein, thickening temperature is set as 50 DEG C.
（5）Alcohol precipitation：By step（4）In the medicinal extract of gained be added 4 times of weight 95% ethanol solution, stirring be placed on 4 DEG C it is low
Temperature is lower to settle 25h；
（6）It is concentrated under reduced pressure：Using Buchner funnel by step（5）Middle sedimentation liquid filtering, cryogenic vacuum are concentrated into the 1/5 of original volume,
Wherein thickening temperature is set as 45 DEG C
（7）Molecular distillation：By step（6）In filtrate carry out molecular distillation, molecular distillation pressure be 0.1 Pa, initial temperature 50
DEG C, 10 DEG C of intervals are distilled, rotor speed 220r/min, and 85 mL/h are added dropwise；Collect 80 DEG C of light components below, as jasmine
Jasmine extrait.
Embodiment 3
（1）Pre-treatment：New fresh Jasmine is taken, is cleaned, removal holder；
（2）Homogenate：By treated, Jasmine is weighed, and the aqueous solution of 3 times of weight is added, and is placed in homogenate equipment, is ground into
Even paste；
（3）Ultrasonic extraction：Paste after homogenate is placed in ultrasonic extraction device, 70% alcohol solvent of 3 times of weight is added,
Carry out ultrasonic extraction 4 times, merging filtrate obtains Jasmine extracting solution；Wherein, ultrasonic extraction frequency is 200KHz, temperature 40
DEG C, extraction time 20min.
（4）It is concentrated under reduced pressure：Using Buchner funnel by step（3）Middle extracting solution filtering, cryogenic vacuum are concentrated into original volume
1/5, obtain leaching paste extract；Wherein, thickening temperature is set as 70 DEG C.
（5）Alcohol precipitation：By step（4）In the medicinal extract of gained be added 4 times of weight 95% ethanol solution, stirring be placed on 2 DEG C it is low
Temperature is lower to settle 30h；
（6）It is concentrated under reduced pressure：Using Buchner funnel by step（5）Middle sedimentation liquid filtering, cryogenic vacuum are concentrated into the 1/3 of original volume,
Wherein thickening temperature is set as 42 DEG C
（7）Molecular distillation：By step（6）In filtrate carry out molecular distillation, molecular distillation pressure be 0.1 Pa, initial temperature 45
DEG C, 10 DEG C of intervals are distilled, rotor speed 250r/min, and 90mL/h is added dropwise；Collect 80 DEG C of light components below, as jasmine
Extrait.
Embodiment 4
（1）Pre-treatment：New fresh Jasmine is taken, is cleaned, removal holder；
（2）Homogenate：By treated, Jasmine is weighed, and the aqueous solution of 2 times of weight is added, and is placed in homogenate equipment, is ground into
Even paste；
（3）Ultrasonic extraction：Paste after homogenate is placed in ultrasonic extraction device, 65% alcohol solvent of 3 times of weight is added,
Carry out ultrasonic extraction 4 times, merging filtrate obtains Jasmine extracting solution；Wherein, ultrasonic extraction frequency is 200KHz, temperature 38
DEG C, extraction time 28min.
（4）It is concentrated under reduced pressure：Using Buchner funnel by step（3）Middle extracting solution filtering, cryogenic vacuum are concentrated into original volume
1/5, obtain leaching paste extract；Wherein, thickening temperature is set as 70 DEG C.
（5）Alcohol precipitation：By step（4）In the medicinal extract of gained be added 4 times of weight 95% ethanol solution, stirring be placed on 6 DEG C it is low
Temperature is lower to settle 35h；
（6）It is concentrated under reduced pressure：Using Buchner funnel by step（5）Middle sedimentation liquid filtering, cryogenic vacuum are concentrated into the 2/9 of original volume,
Wherein thickening temperature is set as 50 DEG C
（7）Molecular distillation：By step（6）In filtrate carry out molecular distillation, molecular distillation pressure be 0.1 Pa, initial temperature 45
DEG C, 10 DEG C of intervals are distilled, rotor speed 240r/min, and 90mL/h is added dropwise；Collect 80 DEG C of light components below, as jasmine
Extrait.
Cigarette is smoked panel test experiment with effect：The cigarette green tea absolute oil that is prepared in above-mentioned 4 embodiments is added according to 0.1% respectively
Add ratio, sprinkling in the tobacco, rolls into cigarette, and to be not added with the cigarette of cigarette jasmine oil product as a contrast.Choose 9
The name personnel that smoke panel test smoke panel test.Smoking result shows that the cigarette flavor feature for being added to cigarette jasmine oil is apparent, Neng Goufeng
Rich cigarette perfume promotes aroma quality, improves oral cavity pleasant impression, and assign cigarette idiosyncrasy feature.Specific smoking result such as following table：
Effect table is commented in the suction of cigarette jasmine oil
In said effect table, aroma quality effect is better, and score value is higher, and full marks 10 divide；Perfume quantity effect more good grades are higher, full marks
10 points；Smoke behavior is better, and score value is higher, and full marks 10 divide；The miscellaneous fewer score value of gas is higher, and full marks 10 divide；The smaller score value of irritation is got over
Height, full marks 10 divide；Pleasant impression is more comfortable, and score value is higher, and full marks 10 divide.
It can be seen that come since the preparation method of cigarette jasmine oil of the invention is to new by said effect contrast table
Fresh Jasmine uses ultrasonic extraction, solvent can be made to rapidly enter cell interior, fully be extracted to active ingredient；This method
It carries out under cryogenic, is avoided that active ingredient by heat damage, improves the aroma quality of product；The present invention with alcoholic solvent into
Row precipitating can more thoroughly remove wax and other impurities ingredient；The present invention is using molecular distillation technique to jasmine oil
It is isolated and purified, can the wherein preferable fraction of effect be detached, be collected.It is added to four kinds of the preparation in the present invention
Cigarette odor characteristic after different cigarette cigarette jasmine oils is apparent, and aroma quality is promoted, and perfume quantity increases, miscellaneous gas and stimulation
Property reduce, pleasant impression is more comfortable.
It is not directed to place above, is suitable for the prior art.
Although some specific embodiments of the present invention are described in detail by example, the skill of this field
Art personnel it should be understood that above example merely to illustrate, the range being not intended to be limiting of the invention, belonging to the present invention
Those skilled in the art can make various modifications or additions to described specific embodiment or use class
As mode substitute, but without departing from the direction or beyond the scope of the appended claims of the present invention.Ability
Domain it is to be understood by the skilled artisans that it is every according to the technical essence of the invention to made by embodiment of above it is any modification, etc.
With replacement, improvement etc., protection scope of the present invention should be included in.
Claims (10)
1. a kind of preparation method of cigarette jasmine oil, it is characterised in that：Include the following steps:
（1）Jasmine raw material is provided, and ultrasonic extraction is carried out to the Jasmine raw material, obtains Jasmine extracting solution；
（2）The liquid phase component of the Jasmine extracting solution is subjected to precipitating with alcoholic solvent, obtains precipitating liquid；
（3）The precipitating liquid is subjected to molecular distillation, isolated jasmine oil.
2. a kind of preparation method of cigarette jasmine oil as described in claim 1, it is characterised in that：In step（1）Later,
Step（2）Further include before：The liquid phase component of Jasmine extracting solution is concentrated to obtain medicinal extract shape concentrate.
3. a kind of preparation method of cigarette jasmine oil as described in claim 1, it is characterised in that：In step（2）Later,
Step（3）Further include before：Precipitating liquid is concentrated in vacuo.
4. a kind of preparation method of cigarette jasmine oil as described in claim 1, it is characterised in that：Step（1）Described in
Ultrasonic extraction is used after the alcohol solvent that mass fraction is 1~3 is added before extraction.
5. a kind of preparation method of cigarette jasmine oil as claimed in claim 4, it is characterised in that：The ultrasonic extraction
Frequency is 180~220KHz, and temperature is 35~40 DEG C, and extraction time is 20~30min, is extracted 2~4 times.
6. a kind of preparation method of cigarette jasmine oil as claimed in claim 4, it is characterised in that：The alcohol solvent
The aqueous solution of a concentration of 50%~70wt%.
7. a kind of preparation method of cigarette jasmine oil as claimed in claim 2, it is characterised in that：The concentration is using low
Temperature is concentrated in vacuo, and is concentrated into the 1/8~1/5 of original volume.
8. a kind of preparation method of cigarette jasmine oil as claimed in claim 3, it is characterised in that：The vacuum concentration is adopted
It is concentrated with cryogenic vacuum, is concentrated into the 1/5~1/3 of original volume.
9. a kind of preparation method of cigarette jasmine oil as claimed in claim 8, it is characterised in that：The cryogenic vacuum is dense
The temperature of contracting is 40~50 DEG C.
10. a kind of preparation method of cigarette jasmine oil as described in claim 1, it is characterised in that：Step（2）In institute
State the aqueous solution for a concentration of 90%~95wt% that alcoholic solvent is alcohol solvent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810269878.3A CN108395932A (en) | 2018-03-29 | 2018-03-29 | A kind of preparation method of cigarette jasmine oil |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810269878.3A CN108395932A (en) | 2018-03-29 | 2018-03-29 | A kind of preparation method of cigarette jasmine oil |
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| Publication Number | Publication Date |
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Family
ID=63096866
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| CN201810269878.3A Pending CN108395932A (en) | 2018-03-29 | 2018-03-29 | A kind of preparation method of cigarette jasmine oil |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109181882A (en) * | 2018-11-02 | 2019-01-11 | 陈艳影 | A kind of extracting method of jasmine essential oil |
| CN117756620A (en) * | 2023-12-18 | 2024-03-26 | 昆山亚香香料股份有限公司 | Preparation method of cis-jasmone |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109181882A (en) * | 2018-11-02 | 2019-01-11 | 陈艳影 | A kind of extracting method of jasmine essential oil |
| CN117756620A (en) * | 2023-12-18 | 2024-03-26 | 昆山亚香香料股份有限公司 | Preparation method of cis-jasmone |
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