CN112251290A - Thyme and benzoin composite essence for cigarettes and preparation method and application thereof - Google Patents
Thyme and benzoin composite essence for cigarettes and preparation method and application thereof Download PDFInfo
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- CN112251290A CN112251290A CN202011117307.1A CN202011117307A CN112251290A CN 112251290 A CN112251290 A CN 112251290A CN 202011117307 A CN202011117307 A CN 202011117307A CN 112251290 A CN112251290 A CN 112251290A
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- thyme
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
Abstract
The invention relates to the field of tobacco additives and tobacco essences, in particular to a thyme and benzoin composite tobacco essence as well as a preparation method and application thereof; the thyme and benzoin composite essence for cigarettes is prepared from the following components in percentage by mass: 40-80% of thyme essential oil, 5-30% of benzoin resin, 5-30% of propylene glycol, 1-2% of benzyl benzoate and 0.5-1% of soybean lecithin; the essence can not only embody the sweet fragrance of the herb fragrance and the benzoin of the thyme, but also cover up the uncoordinated smell brought by independently adding the thyme essential oil; the compound tobacco essence is added with thyme, benzoin and benzyl benzoate, and all components are mutually coordinated, so that the cigarette is endowed with a unique cigarette aroma style containing mutually-coordinated herb aroma, sweet aroma and tobacco aroma, the cigarette brand recognition degree is improved, the cigarette aroma quality and the aroma quantity are improved, the cigarette smoking taste is effectively improved, and the taste is fresh, fine, clean and comfortable; the essence of the invention has simple preparation method and low cost, and is suitable for industrial production.
Description
Technical Field
The invention relates to the field of tobacco additives and tobacco essences, in particular to a thyme and benzoin composite tobacco essence as well as a preparation method and application thereof.
Background
The Chinese style cigarette aroma comprises licorice aroma, sweet aroma, normal sweet aroma, burnt sweet aroma, green aroma, costustoot, bean aroma, nut aroma, burnt aroma, spicy aroma, fruit aroma, herb aroma, flower aroma, resin aroma and flower aroma at present. The essence with the aroma of the herbs is rare all the time, because most of the substances containing the herbs have strong odor, and the original aroma structure can be damaged when the essence is directly added into cigarettes, so that the inconsistent smell is brought. However, the aroma of the herbal medicine is easy to capture and has a special style, and the development of the essence with the aroma of the herbal medicine is beneficial to highlighting the style of cigarette products and improving the identification degree of consumers, thereby improving the competitiveness of cigarette brands.
The thyme is the whole herb of the thyme of the Labiatae, has faint scent, is native to coastal areas of the Mediterranean sea, and is planted in northwest, North China and northeast China. The whole herb of thyme in full bloom stage contains 0.8-1.2% of volatile oil, the volatile oil mainly contains thymol, carvacrol and the like, can promote movement of trachea cilia, is beneficial to secretion of trachea mucus, has the effect of eliminating phlegm, also has better antiseptic, antibacterial and anthelmintic effects, and is commonly used for relieving cough and reducing sputum, killing insects, and sterilizing oral cavity and throat. At present, thyme is mainly used as a spice for preparing cough syrup, chewing gum, spice, perfume, toothpaste and other fields. Benzoin is dry resin of a plant benzoin tree, is in an irregular rapid shape by pressing spherical particles under a natural state, is orange yellow on the surface, is thick and heavy dark brownish red after being heated, has fragrant and strong smell, has the peculiar sweet smell of benzoin resin, is like vanilla, has the effects of inducing resuscitation and refreshing mind, promoting qi and activating blood, relieving pain and the like, and is commonly used for traditional Chinese medicines and spices.
The natural plant essential oil is extracted by organic solvent extraction, steam distillation, supercritical carbon dioxide extraction, etc. On one hand, the extraction rate of the organic solvent extraction method is low, and on the other hand, redundant organic solvent needs to be removed, so that the environment is polluted. In addition, because the tobacco essence belongs to food-grade essence and has higher safety requirement, the non-toxicity and the harmlessness need to be paid attention to when selecting the solvent, thereby further increasing the difficulty of extraction. The steam distillation method has the advantages that due to the limitation of temperature, some substances in the volatile oil are easy to oxidize or decompose, so that the yield is reduced; the method can destroy essential oil components of thyme, especially oxidation of phenols. The supercritical carbon dioxide extraction method can be carried out at the condition close to room temperature, effectively prevents the dissipation of heat sensitivity and volatile substances, has no residual solvent because no organic solvent is used in the whole process, is nontoxic and harmless in the whole process, and is simple and easy to operate. But due to high-efficiency extraction, part of substances which have negative influence on the smoke of the cigarettes are extracted together.
Disclosure of Invention
The invention provides an essence for thyme and benzoin composite cigarettes and a preparation method thereof, aiming at overcoming the defects of the prior art.
In order to solve the technical problems, the technical scheme adopted by the invention is as follows:
the thyme and benzoin composite essence for cigarettes is prepared from the following components in percentage by mass: 40-80% of thyme essential oil, 5-30% of benzoin resin, 5-30% of propylene glycol, 1-2% of benzyl benzoate and 0.5-1% of soybean lecithin.
The thyme has strong herb smell and special fragrance characteristics, is difficult to harmoniously mix with the fragrance with other fragrance characteristics, and the thyme essential oil directly added into the cigarette can enrich the cigarette fragrance, but can destroy the original cigarette fragrance state and introduce discordant smell. Experimenters find that the thyme essential oil and the benzoin are matched and added into the tobacco shreds according to a proper proportion by matching different fragrant raw materials with the thyme essential oil, the benzoin, the cigarette smoke concentration can be obviously improved, the cigarette fragrance fullness is improved, the fragrance of the cigarette is enriched, and the fragrance characteristics of special herb fragrance can be endowed to the cigarette products.
A preparation method of thyme and benzoin composite essence for cigarettes comprises the following steps:
1) drying Thymus vulgaris in shade, pulverizing, and sieving with 40, 50, and 80 mesh sieve respectively to obtain 40, 50, and 80 mesh Thymus vulgaris powder;
2) shaking thyme powder with acid solution, filtering,
3) vacuum drying the filter residue to obtain treated thyme powder;
4) putting the obtained thyme powder into an extraction kettle, and heating the extraction kettle to 30-50 ℃;
5) opening of CO2The gas storage tank controls the flow rate to be 1-5L/h, and pressurizes the extraction kettle;
6) when the pressure of the extraction kettle reaches 18-22 MPa, keeping the temperature and the pressure, extracting for 3-4 h, and collecting thyme essential oil;
7) uniformly mixing the thyme essential oil, the benzoin resin, the propylene glycol, the benzyl benzoate and the soybean lecithin obtained in the step 6) according to the mass percentage to prepare the thyme and benzoin composite essence for cigarettes.
Further, the acidic solution in step 2) is an acetic acid solution.
Further, the mass concentration of the acetic acid solution used in the step 2) is 3% -10%, and the shaking time is 2-4 h.
The invention is further improved on the technology of supercritical carbon dioxide extraction. As the aroma components in the thyme mainly come from the volatile oil in the thyme, the main components of the volatile oil are thymol, carvacrol and the like. The prepared thyme powder is subjected to shaking extraction by using a dilute acid solution, the main purpose of the step is to change bound phenol into free phenol, so that the yield of the thyme oil for cigarettes is improved, and in addition, some water-soluble pigments and other water-soluble substances can be removed, so that the purity (usability) of the thyme oil for cigarettes is improved. Filtering after the oscillation extraction is finished, drying filter residues, and extracting the dried powder with supercritical carbon dioxide. At present, the thyme essential oil for cigarettes prepared by the supercritical carbon dioxide technology is not reported.
In addition, the invention also provides application of the thyme and benzoin composite essence for cigarettes.
Further, the application of the thyme and benzoin composite essence for cigarettes is that when the thyme and benzoin composite essence for cigarettes is used, the composite essence for cigarettes is added into cigarette tobacco shreds according to the mass ratio of 0.03% -0.4%, and the specific steps are as follows: weighing the composite tobacco essence according to the corresponding mass proportion, adding a 70% ethanol solution with the volume being 2 times that of the composite tobacco essence, uniformly spraying the mixture on tobacco shreds, sealing the mixture for 2-4 hours at normal temperature, and preparing a cigarette sample after the essence is fully absorbed by the tobacco shreds.
The newly developed thyme and benzoin composite essence for cigarettes not only can embody the sweet fragrance of the herb fragrance and the benzoin of thyme, but also can cover up the uncoordinated smell brought by adding the thyme essential oil alone. After the cigarette is added, the smoke concentration can be improved, the plumpness of the cigarette fragrance can be improved, the cigarette fragrance can be well combined with the tobacco fragrance, the fragrance of the cigarette is enriched, and a unique cigarette fragrance style containing the herbal fragrance, the sweet fragrance and the tobacco fragrance which are mutually harmonious is formed. The essence has simple preparation method and low cost, and is suitable for industrial production.
Compared with the prior art, the invention has the following beneficial effects:
the thyme and benzoin composite essence for cigarettes, which is newly developed by the invention, not only can embody the sweet fragrance of the herb fragrance and the benzoin of the thyme, but also can cover up the uncoordinated smell brought by independently adding the thyme essential oil. According to the composite essence for cigarettes, thyme, benzoin and benzyl benzoate are added, and the components are mutually coordinated, so that the cigarettes are endowed with a unique cigarette aroma style containing mutually-coordinated herbal aroma, sweet aroma and tobacco aroma, the brand recognition degree of the cigarettes is improved, the cigarette aroma quality and the aroma quantity are improved, the cigarette smoking taste is effectively improved, and the taste is fresh, fine, clean and comfortable. The essence of the invention has simple preparation method and low cost, and is suitable for industrial production.
The invention adopts the dilute acid solution with the mass concentration of 3-10% to pretreat the thyme powder, changes the phenol in the combined state into the phenol in the free state, increases the yield of the thyme oil for cigarettes, and can remove some water-soluble pigments and other water-soluble substances, thereby improving the purity (availability) of the thyme oil for cigarettes. The use of acetic acid solution is more beneficial to the extraction of phenolic substances, and a small amount of small molecular acetic acid has the effects of softening cigarette smoke and reducing cigarette irritation.
The method is simple to operate, low in cost and suitable for cigarette enterprises.
Detailed Description
The present invention is further illustrated by the following specific examples.
Example 1.
A preparation method of thyme and benzoin composite essence for cigarettes comprises the following steps:
1) drying thyme in the dark, pulverizing, and sieving with 40 mesh sieve to obtain thyme powder;
2) oscillating thyme powder with 5% acetic acid solution for 2h, and performing suction filtration;
3) vacuum drying the filter residue to obtain treated thyme powder;
4) putting the obtained thyme powder into an extraction kettle, and heating the extraction kettle to 40 ℃;
5) opening of CO2The gas storage tank controls the flow rate to be 3L/h and pressurizes the extraction kettle;
6) when the pressure of the extraction kettle reaches 18MPa, keeping the temperature and the pressure, extracting for 4h, and collecting thyme essential oil;
7) according to the mass percentage, 57.5 percent of thyme extract, 20 percent of benzoin resin, 20 percent of propylene glycol, 2 percent of benzyl benzoate and 0.5 percent of soybean lecithin are mixed and evenly mixed to prepare the thyme benzoin cigarette essence.
The tobacco essence is added into tobacco shreds of cigarettes according to the mass ratio of 0.05%. Weighing the essence according to a corresponding mass ratio, adding a 70% ethanol solution with the volume 2 times that of the essence, uniformly spraying the solution on tobacco shreds, packaging the tobacco shreds with a valve bag, and sealing for 4 hours at normal temperature to ensure that the essence is fully absorbed by the tobacco shreds to prepare the cigarette. And (3) carrying out comparative smoking and evaluation on the sample and a control blank cigarette sample by 9 or more persons with tobacco sensory evaluation qualification.
The cigarette evaluation results of example 1 show that: compared with a blank cigarette, the cigarette flavored by the composite cigarette essence has a unique cigarette aroma style with mutually-matched herbal aroma, sweet aroma and tobacco aroma, and has the advantages of fresh aroma, good comfortable sensation, less miscellaneous odor, reduced irritation, improved smoke concentration and cigarette aroma fullness, and improved aftertaste.
Example 2.
A preparation method of thyme and benzoin composite essence for cigarettes comprises the following steps:
1) drying herba Thymi vulgaris in shade, pulverizing, and sieving with 80 mesh sieve to obtain herba Thymi vulgaris powder;
2) oscillating thyme powder with 5% acetic acid solution for 4h, and performing suction filtration;
3) vacuum drying the filter residue to obtain treated thyme powder;
4) putting the obtained thyme powder into an extraction kettle, and heating the extraction kettle to 50 ℃;
5) opening of CO2The gas storage tank controls the flow rate to be 1L/h and pressurizes the extraction kettle;
6) when the pressure of the extraction kettle reaches 20MPa, keeping the temperature and the pressure, extracting for 3h, and collecting thyme essential oil;
7) according to the mass percentage, 72 percent of thyme extract, 12.5 percent of benzoin resin, 12.5 percent of propylene glycol, 1.5 percent of benzyl benzoate and 1.5 percent of soybean lecithin are evenly mixed to prepare the thyme benzoin cigarette essence.
The tobacco essence is added into tobacco shreds of cigarettes according to the mass ratio of 0.1%. Weighing the essence according to a corresponding mass ratio, adding a 70% ethanol solution with the volume 2 times that of the essence, uniformly spraying the solution on tobacco shreds, packaging the tobacco shreds with a valve bag, and sealing for 2 hours at normal temperature to ensure that the essence is fully absorbed by the tobacco shreds to prepare the cigarette. And (3) carrying out comparative smoking and evaluation on the sample and a control blank cigarette sample by 9 or more persons with tobacco sensory evaluation qualification.
Example 2 the cigarette evaluation results are: compared with a control blank cigarette, the cigarette flavored by the composite cigarette essence has fresh aroma, has slight aroma lasting appeal with the aroma characteristic of vanilla flavor, has moderate sample concentration, is harmoniously mixed with the tobacco aroma with the aroma lasting appeal with full tobacco aroma, obvious elegant feeling, good satisfaction and pure and comfortable aftertaste.
Example 3.
A preparation method of thyme and benzoin composite essence for cigarettes comprises the following steps:
1) drying herba Thymi vulgaris in shade, pulverizing, and sieving with 50 mesh sieve to obtain herba Thymi vulgaris powder;
2) oscillating thyme powder by using a 5% acetic acid solution for 3 hours, and then carrying out suction filtration;
3) vacuum drying the filter residue to obtain treated thyme powder;
4) putting the obtained thyme powder into an extraction kettle, and heating the extraction kettle to 30 ℃;
5) opening of CO2The gas storage tank controls the flow rate to be 2L/h and pressurizes the extraction kettle;
6) when the pressure of the extraction kettle reaches 22MPa, keeping the temperature and the pressure, extracting for 3h, and collecting thyme essential oil;
7) according to the mass percentage, 66.5 percent of thyme extract, 16 percent of benzoin resin, 15 percent of propylene glycol, 2 percent of benzyl benzoate and 0.5 percent of soybean lecithin are evenly mixed to prepare the thyme benzoin cigarette essence.
The tobacco essence is added into tobacco shreds of cigarettes according to the mass ratio of 0.4%. Weighing the essence according to a corresponding mass ratio, adding a 70% ethanol solution with the volume 2 times that of the essence, uniformly spraying the solution on tobacco shreds, packaging the tobacco shreds with a valve bag, and sealing for 2 hours at normal temperature to ensure that the essence is fully absorbed by the tobacco shreds to prepare the cigarette. And (3) carrying out comparative smoking and evaluation on the sample and a control blank cigarette sample by 9 or more persons with tobacco sensory evaluation qualification.
Example 3 the cigarette smoking results are: compared with the control blank cigarette, the cigarette flavored by the composite cigarette essence has rich aroma of the medicinal herb sample and obvious characteristic of the unique medicinal herb sample aroma.
Example 4.
A preparation method of thyme and benzoin composite essence for cigarettes comprises the following steps:
1) drying herba Thymi vulgaris in shade, pulverizing, and sieving with 50 mesh sieve to obtain herba Thymi vulgaris powder;
2) oscillating thyme powder by using a 3% acetic acid solution for 3 hours, and then carrying out suction filtration;
3) vacuum drying the filter residue to obtain treated thyme powder;
4) putting the obtained thyme powder into an extraction kettle, and heating the extraction kettle to 30 ℃;
5) opening of CO2The gas storage tank controls the flow rate to be 4L/h and pressurizes the extraction kettle;
6) when the pressure of the extraction kettle reaches 22MPa, keeping the temperature and the pressure, extracting for 3h, and collecting thyme essential oil;
7) according to the mass percentage, 40 percent of thyme extract, 30 percent of benzoin resin, 27 percent of propylene glycol, 2 percent of benzyl benzoate and 1 percent of soybean lecithin are evenly mixed to prepare the thyme benzoin cigarette essence.
The tobacco essence is added into tobacco shreds of cigarettes according to the mass ratio of 0.03 percent. Weighing the essence according to a corresponding mass ratio, adding a 70% ethanol solution with the volume 2 times that of the essence, uniformly spraying the solution on tobacco shreds, packaging the tobacco shreds with a valve bag, and sealing for 2 hours at normal temperature to ensure that the essence is fully absorbed by the tobacco shreds to prepare the cigarette. And (3) carrying out comparative smoking and evaluation on the sample and a control blank cigarette sample by 9 or more persons with tobacco sensory evaluation qualification.
Example 4 the cigarette smoking results are: compared with the control blank cigarette, the cigarette flavored by the composite cigarette essence has rich aroma of the medicinal herb sample and obvious characteristic of the unique medicinal herb sample aroma.
Example 5.
A preparation method of thyme and benzoin composite essence for cigarettes comprises the following steps:
1) drying herba Thymi vulgaris in shade, pulverizing, and sieving with 80 mesh sieve to obtain herba Thymi vulgaris powder;
2) oscillating thyme powder with 10% acetic acid solution for 4h, and performing suction filtration;
3) vacuum drying the filter residue to obtain treated thyme powder;
4) putting the obtained thyme powder into an extraction kettle, and heating the extraction kettle to 50 ℃;
5) opening of CO2The gas storage tank controls the flow rate to be 5L/h and pressurizes the extraction kettle;
6) when the pressure of the extraction kettle reaches 20MPa, keeping the temperature and the pressure, extracting for 3h, and collecting thyme essential oil;
7) according to the mass percentage, 80 percent of thyme extract, 5 percent of benzoin resin, 12.5 percent of propylene glycol, 1 percent of benzyl benzoate and 1.5 percent of soybean lecithin are evenly mixed to prepare the thyme benzoin cigarette essence.
The tobacco essence is added into tobacco shreds of cigarettes according to the mass ratio of 0.2%. Weighing the essence according to a corresponding mass ratio, adding a 70% ethanol solution with the volume 2 times that of the essence, uniformly spraying the solution on tobacco shreds, packaging the tobacco shreds with a valve bag, and sealing for 2 hours at normal temperature to ensure that the essence is fully absorbed by the tobacco shreds to prepare the cigarette. And (3) carrying out comparative smoking and evaluation on the sample and a control blank cigarette sample by 9 or more persons with tobacco sensory evaluation qualification.
Example 5 the cigarette evaluation results are: compared with a control blank cigarette, the cigarette flavored by the composite cigarette essence has fresh aroma, has slight aroma lasting appeal with the aroma characteristic of vanilla flavor, has moderate sample concentration, is harmoniously mixed with the tobacco aroma with the aroma lasting appeal with full tobacco aroma, obvious elegant feeling, good satisfaction and pure and comfortable aftertaste.
Claims (6)
1. The essence for the thyme and benzoin composite cigarettes is characterized by being prepared from the following components in percentage by mass: 40-80% of thyme essential oil, 5-30% of benzoin resin, 5-30% of propylene glycol, 1-2% of benzyl benzoate and 0.5-1% of soybean lecithin.
2. The preparation method of the essence for thyme and benzoin composite cigarettes as claimed in claim 1, comprising the following steps:
1) drying Thymus vulgaris in shade, pulverizing, and sieving with 40, 50, and 80 mesh sieve respectively to obtain 40, 50, and 80 mesh Thymus vulgaris powder;
2) shaking thyme powder with acid solution, filtering,
3) vacuum drying the filter residue to obtain treated thyme powder;
4) putting the obtained thyme powder into an extraction kettle, and heating the extraction kettle to 30-50 ℃;
5) opening of CO2The gas storage tank controls the flow rate to be 1-5L/h, and pressurizes the extraction kettle;
6) when the pressure of the extraction kettle reaches 18-22 MPa, keeping the temperature and the pressure, extracting for 3-4 h, and collecting thyme essential oil;
7) uniformly mixing the thyme essential oil, the benzoin resin, the propylene glycol, the benzyl benzoate and the soybean lecithin obtained in the step 6) according to the mass percentage to prepare the thyme and benzoin composite essence for cigarettes.
3. The method for preparing the thyme and benzoin composite essence for cigarettes as claimed in claim 2, wherein the acidic solution in step 2) is an acetic acid solution.
4. The preparation method of the thyme and benzoin composite essence for cigarettes as claimed in claim 3, wherein the mass concentration of the acetic acid solution used in the step 2) is 3% -10%, and the shaking time is 2-4 h.
5. The use of the thyme and benzoin composite essence for cigarettes as claimed in claim 1.
6. The application of the thyme and benzoin composite essence for cigarettes as claimed in claim 5, wherein the composite essence for cigarettes is added into cut tobacco of cigarettes according to the mass ratio of 0.03% -0.4%, and the specific steps are as follows: weighing the composite tobacco essence according to the corresponding mass proportion, adding a 70% ethanol solution with the volume being 2 times that of the composite tobacco essence, uniformly spraying the mixture on tobacco shreds, sealing the mixture for 2-4 hours at normal temperature, and preparing a cigarette sample after the essence is fully absorbed by the tobacco shreds.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115558548A (en) * | 2022-10-28 | 2023-01-03 | 延边天翊科技有限公司 | Rosin-flavored essence for cigarettes as well as preparation method and application thereof |
| CN115820341A (en) * | 2022-10-28 | 2023-03-21 | 延边天翊科技有限公司 | Essence for costustoot rhyme, preparation method and application thereof |
| CN115558548B (en) * | 2022-10-28 | 2023-12-08 | 延边天翊科技有限公司 | Rosin-flavored essence for cigarettes and preparation method and application thereof |
| CN115820341B (en) * | 2022-10-28 | 2024-02-02 | 延边天翊科技有限公司 | Essence for costustoot charm cigarettes, and preparation method and application thereof |
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