CN108285830A - A kind of cigarette quick-fried pearl herbal essential oil and quick-fried pearl preparation method - Google Patents
A kind of cigarette quick-fried pearl herbal essential oil and quick-fried pearl preparation method Download PDFInfo
- Publication number
- CN108285830A CN108285830A CN201810068216.XA CN201810068216A CN108285830A CN 108285830 A CN108285830 A CN 108285830A CN 201810068216 A CN201810068216 A CN 201810068216A CN 108285830 A CN108285830 A CN 108285830A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- cigarette
- parts
- quick
- fried pearl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/281—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed
- A24B15/283—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed by encapsulation of the chemical substances
- A24B15/284—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed by encapsulation of the chemical substances the additive being bound to a host by chemical, electrical or like forces, e.g. use of precursors, inclusion complexes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/285—Treatment of tobacco products or tobacco substitutes by chemical substances characterised by structural features, e.g. particle shape or size
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/12—Use of materials for tobacco smoke filters of ion exchange materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/028—Flow sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0288—Applications, solvents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
Abstract
The invention discloses a kind of cigarette quick-fried pearl herbal essential oil and quick-fried pearl preparation methods.Grape-fruit seed oil, Rosemary Oil, Geranium Essential, clove oil, ginseng extract, safflower essential oil, Radix Scrophulariae extract and fat solvent are mixed evenly to prepare quick-fried pearl essential oil.Routinely the quick-fried pearl of cigarette is made in technique again.The essential oil has pure and fresh herbal, enriches the quick-fried pearl odor type feature of style type, while meeting personalization and the multiple demand of consumer, also has resolving stagnation for tranquilization, reinforces the spleen to benefit the lung, promotes the production of body fluid to quench thirst, alleviate abscess of throat and other effects.The present invention is applied to cigarette, and the essential oil released can be such that the rich increase of flue gas, sophistication is promoted, and essential oil fragrance is coordinated naturally with cigarette perfume itself, and throat's refrigerant sense and sweet sense are apparent, and irritation reduces, and can be obviously improved the suction comfort of cigarette.
Description
Technical field
The invention belongs to technical field of cigarette flavors, are specifically related to a kind of quick-fried pearl essence of the cigarette with herbal
Oil.Meanwhile the invention further relates to the methods for preparing the quick-fried pearl of cigarette using the essential oil.
Background technology
Low coking has been the inexorable trend of tobacco business development, but the cigarette smoking mouthfeel that low coking is brought reduces, fragrance
The problems such as insufficient, is also increasingly prominent.How to capture influences tobacco aroma quality, the key technology of perfume quantity, just becomes and improves cigarette life
Where the core for producing competitiveness.Essence spice for cigarette is added in cigarette shreds, is a kind of conventional, required supplement fragrance
Technological means, but the space of its promotion cigarette quality is relatively limited, therefore from the non-burning section of cigarette, it finds relevant novel
Material improves, is promoted the fragrance of cigarette, reduces cigarette smoke irritation and has become new development trend.Wherein, it is filtered in cigarette
The quick-fried pearl of cigarette is added in stick, is a kind of effective and feasible mode by application attestation.Quick-fried pearl is one made an addition in filter tip
Or the more flavored capsules by pinching brokenly release content, to realize artificial controllable characteristic fragrance during smoking property of cigarette
Release reduces external environment and is lost to the influence essence with caused by for inhaling taste, plays abundant smoking property of cigarette taste, realization was sucked
The effects that flavouring humectation of journey.Start to make up smoke perfume loss, more and more brands caused by tar content reduces
Use " quick-fried pearl addition " technology as auxiliary flavoring means.
But the quick-fried pearl of cigarette is usually to be made of some macromolecule organics, glue class, cellulose and some auxiliary materials, these groups
Bring bad breath in varying degrees at ingredient.During the quick-fried pearl of cigarette pinches brokenly, wall material is destroyed, solvent release,
Chemical breath obviously aggravates during this, influences the sensory experience of consumer.
Meanwhile common quick-fried pearl cigarette, essence and flavoring agents that mainly some and cigarette smoke differ greatly in quick-fried pearl, example
Such as minty note, aroma, fruit perfume (or spice), these quick-fried pearls change the odor characteristic of cigarette itself larger.Also have in the prior art
Some are close to the quick-fried pearl of cigarette smoke aromatic style, although cigarette can be made to have certain fragrance in absorption, there is also quick-fried
Pearl fragrance is not merged with the fragrance of cigarette itself, and effect is bad, cannot fundamentally make up that cigarette perfume is insufficient and moisture feeling is insufficient asks
Topic.Moreover, as people are to diversification and personalized all the more pursuit, present quick-fried pearl type has been unable to meet public consumption
Demand.Therefore, carry out removal for the quick-fried pearl of cigarette or cover the technical research of adverse chemical breath, the novel quick-fried pearl of Persisting exploitation and
The quick-fried pearl essence of new style, it has also become the emphasis direction of the quick-fried pearl research and development of cigarette.
Invention content
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide one kind can enrich the quick-fried pearl odor type feature of cigarette,
It covers bad breath, coordinate with cigarette cigarette perfume, the quick-fried pearl essential oil of the cigarette with herbal.
The present invention also aims to provide a kind of method preparing the quick-fried pearl of cigarette using the essential oil.
The purpose of the present invention is achieved by following technical proposals.
Unless otherwise indicated, percentage of the present invention is mass percent.
A kind of cigarette quick-fried pearl herbal essential oil, which is characterized in that be mixed evenly to prepare by the raw material of following mass parts：Shaddock
1~2.5 part of oil, 1.8~3 parts of Rosemary Oil, 1.2~2 parts of Geranium Essential, 0.5~1.5 part of clove oil, ginseng extraction
78~88 parts of 3~5 parts of object, 2.5~4 parts of safflower essential oil, 2~4 parts of Radix Scrophulariae extract and fat solvent.
Preferably, the ginseng extract, is prepared by following methods：
(1) ginseng is dry, crushing, by the ethanol water of 10~20 times of addition concentration 70%~95% of Ginseng Root Powder quality
Solution, 60~80 DEG C of 1~3h of circumfluence distillation；
(2) extracting solution filters while hot, and being then concentrated into volume under the conditions of 45~65 DEG C, 60~90kPa no longer changes, i.e.,
Obtain ginseng extract.
The Radix Scrophulariae extract, is prepared by following methods：
(1) radix scrophulariae is dry, crushing, by the ethanol water of 10~20 times of addition concentration 70%~95% of Figwort Root quality
Solution, 60~80 DEG C of 1~3h of circumfluence distillation；
(2) extracting solution filters while hot, and being then concentrated into volume under the conditions of 45~65 DEG C, 60~90kPa no longer changes, i.e.,
Obtain Radix Scrophulariae extract.
The safflower essential oil, is prepared by following methods：
(1) after cleaning safflower, drying in the shade, it was crushed to 80~150 mesh sieve；
(2) saffron crocus powder is placed in 10~25 times of 70%~95% ethanol water, impregnates 12~48h；
(3) saffron crocus powder soak 30~60min of ultrasound is taken, 35~50W of ultrasonic power, filtrate is 45~60 after suction filtration
DEG C, be concentrated into volume under the conditions of 60~90kPa and no longer change to get safflower essential oil.
The fat solvent is：By 24 degree of palm oils and Glycerin, mixed triester with caprylic acid capric acid according to mass ratio 5:1 mixing, then by mixing
0.5%~0.8% addition sorbester p17 of object gross mass, is mixed evenly to prepare.
The cigarette quick-fried pearl method of herbal essential oil is prepared, is included the following steps：
(1) mass parts are pressed by grape-fruit seed oil, Rosemary Oil, Geranium Essential, clove oil, ginseng extract, Tibetan
Safflower essential oil and Radix Scrophulariae extract are uniformly mixed, and obtain essence；
(2) by 24 degree of palm oils and Glycerin, mixed triester with caprylic acid capric acid according to mass ratio 5:1 mixing, then by mixture gross mass
0.5%~0.8% addition sorbester p17, stirring at normal temperature are slowly added to essence obtained by step (1) in whipping process, after essence adds
Continue 0.5~1.5h of stirring, standing waits for lather collapse to get to required cigarette quick-fried pearl herbal essential oil.
The quick-fried pearl of the cigarette is with the preferred raw material proportioning of herbal essential oil：2 parts of grape-fruit seed oil, 2.2 parts of Rosemary Oil,
1.8 parts of Geranium Essential, 1.3 parts of clove oil, 3.2 parts of ginseng extract, 3.5 parts of safflower essential oil, 3 parts of Radix Scrophulariae extract,
83 parts of fat solvent.
The present invention also provides a kind of methods preparing the quick-fried pearl of cigarette with the medicinal herbs essential oil, include the following steps：
(1) the medicinal herbs essential oil is added in the hopper of pill dripping machine；
(2) dripping pill lapping is added in the rubber cement tank of pill dripping machine, keeps 70 DEG C of temperature；
(3) it is put into calcium ion salts solution solidifying agent in containing dripping pill device；
(4) pill dripping machine is opened, so that medicinal herbs essential oil and dripping pill lapping is oozed respectively from discharge port and gum outlet, medicinal herbs
Essential oil is wrapped in dripping pill lapping, and cured dose of curing molding, obtains the quick-fried pearl of cigarette.
The dripping pill lapping is made of the raw material of following mass parts：6~20 parts of sodium alginate, Arabic gum 0.1
~3 parts, 77~95 parts of water；Wherein, the viscosity of sodium alginate is 5~40Pa.s；The viscosity of Arabic gum is 80~140cP；It will
Each raw material, which is placed in retort, to be stirred, 70 DEG C of reaction temperature, after material melting, is kept the temperature 1~2h, is stood, after foam floating,
It filters and obtains under the conditions of 70 DEG C of heat preservation.
During cigarette filter wire-beam forming, prepared quick-fried pearl positioning is applied in filter rod, you can roll into
Quick-fried pearl type cigarette with herbal.
Compared with the existing technology, the invention has the advantages that：
1, the quick-fried pearl of cigarette of the present invention is safflower essential oil, ginseng and Radix Scrophulariae extract with the main component of herbal essential oil,
With pure and fresh herbal, the quick-fried pearl odor type feature of style type is enriched, personalization and the multiple demand of consumer can be also met,
Also there is resolving stagnation for tranquilization simultaneously, reinforce the spleen to benefit the lung, promote the production of body fluid to quench thirst, alleviate abscess of throat and other effects.
2, the perfume ingredient in essential oil can dissolve each other with fat solvent, and aromatic flavour is naturally, quick-fried Zhu Bi can be hidden well
The bad breath that material and solvent bank come.
3, the quick-fried pearl of the present invention is added in cigarette filter tip, is pinched brokenly quick-fried pearl in aspiration procedure, the essential oil released can make
The rich increase of flue gas, sophistication are promoted, and essential oil fragrance is coordinated naturally with cigarette perfume itself, and throat's refrigerant sense and sweet sense are apparent,
Irritation reduces, and can be obviously improved the suction comfort of cigarette.
4, preparation method of the present invention is simple, and raw material is easy to get, of low cost, is easy to implement industrialized production, there is good answer
With value.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is described in further detail.It should be appreciated that described herein, specific examples are only used to explain the present invention, is not to this hair
The restriction of bright technical solution.
Embodiment 1
1. the preparation of yuan gas explosion pearl essential oil
(1) preparation of ginseng extract
Dry ginseng 1kg is crushed by pulverizer, is sieved with 100 mesh sieve；75% that 10kg is added into Ginseng Root Powder is dense
Ethyl alcohol is spent, circumfluence distillation 3h at 60 DEG C；It filters while hot, 60 DEG C, carry out vacuum-concentrcted under the conditions of 70kPa to volume no longer
Variation is to get ginseng extract.
(2) preparation of Radix Scrophulariae extract
Dry radix scrophulariae 1.5kg is crushed by pulverizer, crosses 120 mesh sieve；The 80% of 20kg is added into Figwort Root
Concentration ethanol, circumfluence distillation 2h at 60 DEG C；It filters while hot, 50 DEG C, carry out vacuum-concentrcted under the conditions of 80kPa to volume not
Change again to get Radix Scrophulariae extract.
(3) preparation of safflower essential oil
Safflower is cleaned, is dried in the shade, is crushed with pulverizer, 150 mesh sieve is crossed；Safflower quality is added into saffron crocus powder
15 times of 80% ethyl alcohol impregnates for 24 hours；Take above-mentioned saffron crocus powder soak ultrasound 40min, ultrasonic power 40W；Ultrasound is laggard
Row filters.Filtrate is concentrated into volume at 50 DEG C, under the conditions of 70kPa and no longer changes, and obtains safflower essential oil.
(2) preparation of first gas explosion pearl essence
2 parts of grape-fruit seed oil, 2.2 parts of Rosemary Oil, 1.8 parts of Geranium Essential, clove oil 1.3 are weighed by mass fraction
Part, 3.2 parts of ginseng extract, 3.5 parts of safflower essential oil, 3 parts of Radix Scrophulariae extract are uniformly mixed and are configured to first gas explosion pearl essence.
(3) preparation of first gas explosion pearl essential oil
By 24 degree of palm oils and Glycerin, mixed triester with caprylic acid capric acid according to mass ratio 5:1 mixed preparing obtains fat solvent；24 degree of palm fibres are pressed again
0.8% addition sorbester p17 of palmitic acid oil and Glycerin, mixed triester with caprylic acid capric acid gross mass, stirs evenly at normal temperatures；It is 83 parts to weigh mass fraction
The above-mentioned fat solvent containing sorbester p17, first gas explosion pearl essence is slowly added in whipping process so that the vigour finally obtained
Fat solvent in quick-fried pearl essential oil：The mass percent of first gas explosion pearl essence is 83:17, essence continues to stir 1.5h after adding, quiet
It sets and waits for lather collapse to get first gas explosion pearl essential oil.
2. the cigarette preparation of first gas explosion pearl, includes the following steps：
It prepares in glue 500ml addition Sandwich pots and stirs by listed proportioning in table 1, steam jacket is heated to 70 DEG C, makes it
Fusing keeps the temperature 2 hours, stands after foam floating, and heat preservation filtering obtains dripping pill lapping；Dripping pill lapping is added
In the rubber cement tank of pill dripping machine, and the temperature of 70 DEG C of holding.First gas explosion pearl essential oil 600g is weighed, is added in the hopper of pill dripping machine, is contained
10% calcium chloride water is put into dripping pill device as curing agent.Quality, which is made, using the small capsule and pill dropping-pill machine of DWJSYJ-I types is
The cigarette of 18mg, crushing strength 2.5kPa, 250 μm of rubber thickness, a diameter of 3.6mm use first gas explosion pearl.
1 dripping pill lapping glue of table is with tabulation
| Specification | Parts by weight | |
| Sodium alginate | Viscosity (Pa.s) 10 | 15 |
| Arabic gum | Viscosity (cP) 120 | 1.5 |
| Water | Pure water | 83.5 |
3. application and evaluation of the cigarette with first gas explosion pearl in cigarette
During cigarette filter wire-beam forming, by the first gas explosion pearl positioning of the cigarette of preparation be applied in filter rod to get
Containing the cigarette cigarette of first gas explosion pearl.Cigarette not add the quick-fried pearl is that control carries out sensory evaluating smoking, Analyses Methods for Sensory Evaluation Results table
It is bright：Compared with the control, the cigarette flue gas for being added to the first gas explosion pearl of cigarette has pure and fresh herbal, quick-fried pearl fragrance and cigarette perfume itself
Naturally coordinate, flue gas is rich to be dramatically increased, and throat's irritation significantly reduces, and Tianjin moisture feeling is obviously improved, and pleasant impression is comfortable.
Embodiment 2
1. the preparation of yuan gas explosion pearl essential oil
(1) preparation of ginseng extract
Dry ginseng 2kg is crushed by pulverizer, crosses 120 mesh sieve；80% that 25kg is added into Ginseng Root Powder is dense
Ethyl alcohol is spent, circumfluence distillation 2h at 70 DEG C；It filters while hot, 55 DEG C, carry out vacuum-concentrcted under the conditions of 60kPa to volume no longer
Variation is to get ginseng extract.
(2) preparation of Radix Scrophulariae extract
Dry radix scrophulariae 1kg is crushed by pulverizer, is sieved with 100 mesh sieve；75% that 15kg is added into Figwort Root is dense
Ethyl alcohol is spent, circumfluence distillation 3h at 65 DEG C；It filters while hot, 60 DEG C, carry out vacuum-concentrcted under the conditions of 80kPa to volume no longer
Variation is to get Radix Scrophulariae extract.
(3) preparation of safflower essential oil
Safflower is cleaned, is dried in the shade, is crushed with pulverizer, 120 mesh sieve is crossed；Safflower quality is added into saffron crocus powder
20 times of 85% ethyl alcohol impregnates for 24 hours；Take above-mentioned saffron crocus powder soak ultrasound 60min, ultrasonic power 45W；Ultrasound is laggard
Row filters.Filtrate is concentrated into volume at 55 DEG C, under the conditions of 80kPa and no longer changes, and obtains safflower essential oil.
(4) preparation of first gas explosion pearl essence
It is 1.5 parts of grape-fruit seed oil, 2.5 parts of Rosemary Oil, 2 parts of Geranium Essential, clove oil 1.5 to weigh mass fraction
Part, 3 parts of ginseng extract, 3 parts of safflower essential oil, 2.5 parts of Radix Scrophulariae extract various essence and flavoring agents be uniformly mixed be configured to member
Gas explosion pearl essence.
(5) preparation of first gas explosion pearl essential oil
By 24 degree of palm oils and Glycerin, mixed triester with caprylic acid capric acid according to mass ratio 5:1 mixed preparing obtains fat solvent；24 degree of palm fibres are pressed again
0.7% addition sorbester p17 of palmitic acid oil and neodecanoic acid glyceride gross mass, stirs evenly at normal temperatures；It is 84 parts to weigh mass fraction
The above-mentioned fat solvent containing sorbester p17, first gas explosion pearl essence is slowly added in whipping process so that the vigour finally obtained
Fat solvent in quick-fried pearl essential oil：The mass percent of first gas explosion pearl essence is 84:16, quick-fried pearl essence continues to stir after adding
1.5h, standing wait for lather collapse to get first gas explosion pearl essential oil.
2. the cigarette preparation of first gas explosion pearl, includes the following steps：
It prepares in glue 500ml addition Sandwich pots and stirs by listed proportioning in table 2, steam jacket is heated to 70 DEG C, makes it
Fusing keeps the temperature 2 hours, stands after foam floating, and heat preservation filtering obtains dripping pill lapping；Dripping pill lapping is added
In the rubber cement tank of pill dripping machine, and kept for 70 DEG C.First gas explosion pearl essential oil 650g is weighed, is added in the hopper of pill dripping machine, dripping pill is contained
8% Dicalcium Phosphate aqueous solution is put into device as curing agent.Quality, which is made, using the small capsule and pill dropping-pill machine of DWJSYJ-I types is
The cigarette of 20mg, crushing strength 3.0kPa, 300 μm of rubber thickness, a diameter of 3.8mm use first gas explosion pearl.
2 dripping pill lapping glue of table is with tabulation
| Specification | Parts by weight | |
| Sodium alginate | Viscosity (Pa.s) 30 | 10 |
| Arabic gum | Viscosity (cP) 100 | 0.2 |
| Water | Pure water | 89.8 |
3. application and evaluation of the cigarette with first gas explosion pearl in cigarette
During cigarette filter wire-beam forming, by the first gas explosion pearl positioning of the cigarette of preparation be applied in filter rod to get
Containing the cigarette cigarette of first gas explosion pearl.Cigarette not add above-mentioned quick-fried pearl is that control carries out sensory evaluating smoking, Analyses Methods for Sensory Evaluation Results table
It is bright：Compared with the control, the quick-fried pearl fragrance for being added to the first gas explosion pearl cigarette of cigarette is coordinated naturally with cigarette perfume itself, and flue gas is rich aobvious
Increase is write, flue gas sophistication is promoted, and alcohol is moistened in flue gas more Tianjin and obviously, irritation reduction can be bright for throat's refrigerant sense and time sweet sense
The aobvious suction comfort for improving cigarette.
Claims (9)
1. a kind of cigarette quick-fried pearl herbal essential oil, which is characterized in that be mixed evenly to prepare by the raw material of following mass parts：Grape-fruit seed oil
1~2.5 part, 1.8~3 parts of Rosemary Oil, 1.2~2 parts of Geranium Essential, 0.5~1.5 part of clove oil, ginseng extract 3
78~88 parts of~5 parts, 2.5~4 parts of safflower essential oil, 2~4 parts of Radix Scrophulariae extract and fat solvent.
2. cigarette quick-fried pearl herbal essential oil according to claim 1, which is characterized in that preferably raw material proportioning is：Shaddock
2 parts of seed oil, 2.2 parts of Rosemary Oil, 1.8 parts of Geranium Essential, 1.3 parts of clove oil, 3.2 parts of ginseng extract, safflower
83 parts of 3.5 parts of essential oil, 3 parts of Radix Scrophulariae extract and fat solvent.
3. cigarette quick-fried pearl herbal essential oil according to claim 1, which is characterized in that the ginseng extract, by
Following methods are prepared：
(1) ginseng is dry, crushing, the ethyl alcohol by 10~20 times of addition concentration 70%~95% of Ginseng Root Powder quality are water-soluble
Liquid, 60~80 DEG C of 1~3h of circumfluence distillation；
(2) extracting solution filters while hot, and being then concentrated into volume under the conditions of 45~65 DEG C, 60~90kPa no longer changes to get people
Conopsea extraction.
4. cigarette quick-fried pearl herbal essential oil according to claim 1, which is characterized in that the Radix Scrophulariae extract, by
Following methods are prepared：
(1) radix scrophulariae is dry, crushing, the ethyl alcohol by 10~20 times of addition concentration 70%~95% of Figwort Root quality are water-soluble
Liquid, 60~80 DEG C of 1~3h of circumfluence distillation；
(2) extracting solution filters while hot, and being then concentrated into volume under the conditions of 45~65 DEG C, 60~90kPa no longer changes to get profound
Conopsea extraction.
5. cigarette quick-fried pearl herbal essential oil according to claim 1, which is characterized in that the safflower essential oil, by
Following methods are prepared：
(1) after cleaning safflower, drying in the shade, it was crushed to 80~150 mesh sieve；
(2) saffron crocus powder is placed in 10~25 times of 70%~95% ethanol water, impregnates 12~48h；
(3) take saffron crocus powder soak 30~60min of ultrasound, 35~50W of ultrasonic power, after suction filtration filtrate 45~60 DEG C,
Volume is concentrated under the conditions of 60~90kPa no longer to change to get safflower essential oil.
6. cigarette quick-fried pearl herbal essential oil according to claim 1, which is characterized in that the fat solvent is：It will
24 degree of palm oils and Glycerin, mixed triester with caprylic acid capric acid are according to mass ratio 5:1 mixing, then 0.5%~0.8% addition by mixture gross mass
Sorbester p17 is mixed evenly to prepare.
7. preparing the cigarette quick-fried pearl method of herbal essential oil described in claims 1 or 2, include the following steps：
(1) mass parts are pressed by grape-fruit seed oil, Rosemary Oil, Geranium Essential, clove oil, ginseng extract, safflower
Essential oil and Radix Scrophulariae extract are uniformly mixed, and obtain essence；
(2) by 24 degree of palm oils and Glycerin, mixed triester with caprylic acid capric acid according to mass ratio 5:1 mixing, then by mixture gross mass 0.5%~
0.8% addition sorbester p17, stirring at normal temperature are slowly added to essence obtained by step (1) in whipping process, and essence continues to stir after adding
0.5~1.5h, standing wait for lather collapse to get to required cigarette quick-fried pearl herbal essential oil.
8. the method for preparing the quick-fried pearl of cigarette using claims 1 or 22 or the 3 or 4 or 5 or 6 medicinal herbs essential oil, including following step
Suddenly：
(1) the medicinal herbs essential oil is added in the hopper of pill dripping machine；
(2) dripping pill lapping is added in the rubber cement tank of pill dripping machine, keeps 70 DEG C of temperature；
(3) it is put into calcium ion salts solution solidifying agent in containing dripping pill device；
(4) pill dripping machine is opened, so that medicinal herbs essential oil and dripping pill lapping is oozed respectively from discharge port and gum outlet, medicinal herbs essence
Oil is wrapped in dripping pill lapping, and cured dose of curing molding, obtains the quick-fried pearl of cigarette.
9. preparation method according to claim 8, it is characterised in that：The dripping pill lapping is by following mass parts
Raw material is made：6~20 parts of sodium alginate, 0.1~3 part of Arabic gum, 77~95 parts of water；Wherein, the viscosity of sodium alginate be 5~
40Pa.s；The viscosity of Arabic gum is 80~140cP；Each raw material is placed in retort and is stirred, 70 DEG C of reaction temperature waits for material
After fusing, 1~2h is kept the temperature, is stood, after foam floating, filters and obtains under the conditions of 70 DEG C of heat preservation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810068216.XA CN108285830A (en) | 2018-01-24 | 2018-01-24 | A kind of cigarette quick-fried pearl herbal essential oil and quick-fried pearl preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810068216.XA CN108285830A (en) | 2018-01-24 | 2018-01-24 | A kind of cigarette quick-fried pearl herbal essential oil and quick-fried pearl preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108285830A true CN108285830A (en) | 2018-07-17 |
Family
ID=62835765
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810068216.XA Pending CN108285830A (en) | 2018-01-24 | 2018-01-24 | A kind of cigarette quick-fried pearl herbal essential oil and quick-fried pearl preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108285830A (en) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109022152A (en) * | 2018-08-30 | 2018-12-18 | 湖北中烟工业有限责任公司 | A kind of rosemary tobacco aromaticss and its preparation method and application |
| CN110079393A (en) * | 2019-04-29 | 2019-08-02 | 亿利耐雀生物科技有限公司 | A kind of quick-fried pearl essential oil and its preparation method and application |
| CN110760387A (en) * | 2019-10-31 | 2020-02-07 | 湖北中烟工业有限责任公司 | Magnolia officinalis and pearl burst essential oil and preparation method thereof |
| CN110804497A (en) * | 2019-11-18 | 2020-02-18 | 湖北中烟工业有限责任公司 | Preparation method of saffron extract for tobacco bead blasting |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
| CN111084409A (en) * | 2019-11-27 | 2020-05-01 | 贵州中烟工业有限责任公司 | Dried orange peel type composite extract for cigarette bead blasting and preparation method thereof |
| CN111449274A (en) * | 2020-04-09 | 2020-07-28 | 福建中烟工业有限责任公司 | Ginseng extract and preparation method and application thereof |
| CN112251290A (en) * | 2020-10-19 | 2021-01-22 | 甘肃烟草工业有限责任公司 | Thyme and benzoin composite essence for cigarettes and preparation method and application thereof |
| CN113142646A (en) * | 2021-05-14 | 2021-07-23 | 云南热丽康生物科技有限公司 | Sweet and fragrant type vetiver root composite extract for cigarettes and application thereof |
| CN114052283A (en) * | 2021-11-25 | 2022-02-18 | 云南中烟新材料科技有限公司 | Abelmoschus manihot bead-blasting essence and preparation method and application thereof |
| CN115406983A (en) * | 2022-08-16 | 2022-11-29 | 浙江中烟工业有限责任公司 | Method for measuring breaking time of blasting beads in cigarette filter |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102108136A (en) * | 2009-12-25 | 2011-06-29 | 湖北中烟工业有限责任公司 | Tobacco additive dropping pill wrapping material, dropping pill wrapped thereby and application of dropping pill |
| CN106753787A (en) * | 2016-11-29 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette quick-fried pearl lemon-mint essential oil and its preparation method and application |
| CN107090356A (en) * | 2017-04-27 | 2017-08-25 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl American Ginseng essence and its application in cigarette |
| CN107115485A (en) * | 2017-04-17 | 2017-09-01 | 曹涛 | A kind of quick-fried pearl of Chinese herbal medicine and quick-fried pearl cigarette holder |
-
2018
- 2018-01-24 CN CN201810068216.XA patent/CN108285830A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102108136A (en) * | 2009-12-25 | 2011-06-29 | 湖北中烟工业有限责任公司 | Tobacco additive dropping pill wrapping material, dropping pill wrapped thereby and application of dropping pill |
| CN106753787A (en) * | 2016-11-29 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette quick-fried pearl lemon-mint essential oil and its preparation method and application |
| CN107115485A (en) * | 2017-04-17 | 2017-09-01 | 曹涛 | A kind of quick-fried pearl of Chinese herbal medicine and quick-fried pearl cigarette holder |
| CN107090356A (en) * | 2017-04-27 | 2017-08-25 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl American Ginseng essence and its application in cigarette |
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109022152A (en) * | 2018-08-30 | 2018-12-18 | 湖北中烟工业有限责任公司 | A kind of rosemary tobacco aromaticss and its preparation method and application |
| CN110079393B (en) * | 2019-04-29 | 2021-12-28 | 亿利耐雀生物科技有限公司 | Pearl blasting essential oil and preparation method and application thereof |
| CN110079393A (en) * | 2019-04-29 | 2019-08-02 | 亿利耐雀生物科技有限公司 | A kind of quick-fried pearl essential oil and its preparation method and application |
| CN110760387A (en) * | 2019-10-31 | 2020-02-07 | 湖北中烟工业有限责任公司 | Magnolia officinalis and pearl burst essential oil and preparation method thereof |
| CN110760387B (en) * | 2019-10-31 | 2023-01-31 | 湖北中烟工业有限责任公司 | Magnolia officinalis and pearl burst essential oil and preparation method thereof |
| CN110804497A (en) * | 2019-11-18 | 2020-02-18 | 湖北中烟工业有限责任公司 | Preparation method of saffron extract for tobacco bead blasting |
| CN111084409A (en) * | 2019-11-27 | 2020-05-01 | 贵州中烟工业有限责任公司 | Dried orange peel type composite extract for cigarette bead blasting and preparation method thereof |
| CN111084409B (en) * | 2019-11-27 | 2022-11-22 | 贵州中烟工业有限责任公司 | Dried orange peel type composite extract for cigarette bead blasting and preparation method thereof |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
| CN111449274A (en) * | 2020-04-09 | 2020-07-28 | 福建中烟工业有限责任公司 | Ginseng extract and preparation method and application thereof |
| CN112251290A (en) * | 2020-10-19 | 2021-01-22 | 甘肃烟草工业有限责任公司 | Thyme and benzoin composite essence for cigarettes and preparation method and application thereof |
| CN113142646A (en) * | 2021-05-14 | 2021-07-23 | 云南热丽康生物科技有限公司 | Sweet and fragrant type vetiver root composite extract for cigarettes and application thereof |
| CN114052283A (en) * | 2021-11-25 | 2022-02-18 | 云南中烟新材料科技有限公司 | Abelmoschus manihot bead-blasting essence and preparation method and application thereof |
| CN115406983A (en) * | 2022-08-16 | 2022-11-29 | 浙江中烟工业有限责任公司 | Method for measuring breaking time of blasting beads in cigarette filter |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108285830A (en) | A kind of cigarette quick-fried pearl herbal essential oil and quick-fried pearl preparation method | |
| CN108219943A (en) | A kind of quick-fried pearl essential oil of cigarette and the method for preparing quick-fried pearl | |
| CN103989244B (en) | A kind of Chinese style tobacco juice for electronic smoke and preparation method thereof | |
| EP2786664A1 (en) | Pulp preparation method for electronic smoking set and traditional hookah | |
| CN108179066B (en) | Honeysuckle mint essential oil for cigarette bead blasting and preparation method and application thereof | |
| KR20010079406A (en) | A making method of the cigars or the cigarettes of added with caffeine. | |
| CN105861154A (en) | A method of directionally separating aroma substances from tobacco by utilizing supercritical extraction and molecule distillation and applications of the aroma substances | |
| CN104839883A (en) | Electronic cigarette liquid with characteristics of tobaccos for tobacco pipes | |
| CN102524932B (en) | Method for applying natural solid flavors and fragrances to papermaking-reconstructed tobacco sheets | |
| JP7182805B2 (en) | HNB herb aroma bomb flakes, filaments, filament cuts, recipes and production methods for herb aroma bombs | |
| CN103783660A (en) | Supercritical extraction method of aroma substances in tobacco leaf fragments and application of aroma substances | |
| CN104256892A (en) | Method for extracting Pu-Er raw tea essential oil and purpose of Pu-Er raw tea essential oil in cigarette filter stick | |
| CN101731743B (en) | Flavouring essence perfume for tobacco and preparation method thereof | |
| CN106281690A (en) | A kind of flavoring essence improving bamboo pulp Chip Quality and application thereof | |
| CN105011353B (en) | Natural bio-chemical agent used for cigar fermentation and quality improvement and application thereof | |
| CN105852197A (en) | Raw material formula for healthcare cigarettes with fructus mori and folium mori and method for manufacturing healthcare cigarettes | |
| CN101606756A (en) | Green tea cigarette and production method thereof | |
| CN101637303A (en) | Lemon extract, preparation method thereof and application thereof in cigarette flavoring | |
| CN106723276B (en) | A kind of tobacco aromaticss and preparation method thereof | |
| CN107057856B (en) | Preparation method of liquorice sweetening and moisturizing essence for filter tip | |
| CN111718797A (en) | Method for finely extracting tobacco essence | |
| CN108113049B (en) | Herbal tea flavor liquid essence, microcapsule essence and application of herbal tea flavor liquid essence and microcapsule essence in cigarettes | |
| CN110122921A (en) | A kind of preparation method of the quick-fried pearl of black tea | |
| CN100486469C (en) | Medicated cigarette-type smoking quitting product and production method thereof | |
| CN102703216A (en) | Method for making momordica grosvenori tobacco flavor |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180717 |