CN110804497A - Preparation method of saffron extract for tobacco bead blasting - Google Patents
Preparation method of saffron extract for tobacco bead blasting Download PDFInfo
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- CN110804497A CN110804497A CN201911128200.4A CN201911128200A CN110804497A CN 110804497 A CN110804497 A CN 110804497A CN 201911128200 A CN201911128200 A CN 201911128200A CN 110804497 A CN110804497 A CN 110804497A
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- saffron
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- 239000011324 bead Substances 0.000 title claims abstract description 34
- 239000001599 crocus sativus l. flower extract Substances 0.000 title claims abstract description 25
- 229940076591 saffron extract Drugs 0.000 title claims abstract description 25
- 238000005422 blasting Methods 0.000 title claims abstract description 24
- 241000208125 Nicotiana Species 0.000 title claims abstract description 21
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000002994 raw material Substances 0.000 claims abstract description 24
- 239000000243 solution Substances 0.000 claims abstract description 19
- 238000000605 extraction Methods 0.000 claims abstract description 17
- 244000124209 Crocus sativus Species 0.000 claims abstract description 16
- 235000015655 Crocus sativus Nutrition 0.000 claims abstract description 16
- 238000000874 microwave-assisted extraction Methods 0.000 claims abstract description 14
- 238000010992 reflux Methods 0.000 claims abstract description 13
- 238000001914 filtration Methods 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 11
- 239000000706 filtrate Substances 0.000 claims abstract description 9
- 239000003960 organic solvent Substances 0.000 claims abstract description 9
- 238000002791 soaking Methods 0.000 claims abstract description 9
- 239000002904 solvent Substances 0.000 claims abstract description 8
- 238000001816 cooling Methods 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract description 6
- 239000011259 mixed solution Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000004006 olive oil Substances 0.000 claims description 6
- 235000008390 olive oil Nutrition 0.000 claims description 6
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 238000009833 condensation Methods 0.000 claims description 3
- 230000005494 condensation Effects 0.000 claims description 3
- -1 carbon fatty acid ester Chemical class 0.000 claims description 2
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 2
- 229930195729 fatty acid Natural products 0.000 claims description 2
- 239000000194 fatty acid Substances 0.000 claims description 2
- 125000005456 glyceride group Chemical group 0.000 claims 1
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical group CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims 1
- 235000019504 cigarettes Nutrition 0.000 abstract description 17
- 235000013974 saffron Nutrition 0.000 abstract description 9
- 239000004248 saffron Substances 0.000 abstract description 9
- 239000000796 flavoring agent Substances 0.000 abstract description 6
- 235000019634 flavors Nutrition 0.000 abstract description 5
- 239000003205 fragrance Substances 0.000 description 8
- 239000000284 extract Substances 0.000 description 6
- 239000007788 liquid Substances 0.000 description 4
- 239000000779 smoke Substances 0.000 description 4
- 235000004237 Crocus Nutrition 0.000 description 3
- 241000596148 Crocus Species 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 235000019640 taste Nutrition 0.000 description 3
- 235000006679 Mentha X verticillata Nutrition 0.000 description 2
- 235000002899 Mentha suaveolens Nutrition 0.000 description 2
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 206010013911 Dysgeusia Diseases 0.000 description 1
- 208000012895 Gastric disease Diseases 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 241001113425 Iridaceae Species 0.000 description 1
- 206010023126 Jaundice Diseases 0.000 description 1
- 201000005505 Measles Diseases 0.000 description 1
- 241000219000 Populus Species 0.000 description 1
- 206010037660 Pyrexia Diseases 0.000 description 1
- 208000005392 Spasm Diseases 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 206010019847 hepatosplenomegaly Diseases 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 230000007721 medicinal effect Effects 0.000 description 1
- 230000005906 menstruation Effects 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 208000018556 stomach disease Diseases 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a preparation method of a saffron extract for bead blasting of tobacco. The preparation method comprises the following steps: (1) pretreatment: soaking stigma croci in warm water for a period of time, and drying at room temperature; (2) reflux extraction: adding dried stigma croci Sativi raw materials into organic solvent, reflux extracting under normal pressure, and cooling; (3) microwave extraction: adding the solvent and the raw materials in the step (2) into an acetic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction; (4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel; (5) concentration: and (4) carrying out reduced pressure concentration on the filtrate obtained in the step (4) to obtain the saffron extract for the tobacco bead blasting. The method can effectively realize the extraction of the saffron flavor components, effectively improve the flavor of cigarettes and improve the comfortable experience of smokers.
Description
Technical Field
The invention belongs to the technical field of cigarette additives, and particularly relates to a preparation method of a saffron extract for bead blasting of tobacco.
Background
In the 60's of the 20 th century, tobacco companies began to offer cigarettes with bead-blasting, which means that a small liquid rubber bead embedded in a tobacco filter wrapped with liquids of different types of flavors, smokers could pinch and burst the liquid in the bead during smoking to make the liquid flow out, so that the cigarettes had richer and more fragrant tastes, and the smokers had more comfortable experiences.
The foreign bead for the cigarette mainly takes a mint type as a main material, the domestic bead for the cigarette has great difference, and has different types such as mint, fruit fragrance, wine fragrance, Chinese herbal medicine and the like, however, the development space for perfuming the bead for the bead is huge, and the proper new raw material for the bead for the cigarette is the most important work at present.
Saffron, also called crocus and saffron, is a perennial flower of crocus of iridaceae, originally cultivated manually by greek, mainly distributed in europe, mediterranean, and central asia, where the Ming dynasty introduced into China, it was listed as a drug in compendium of materia Medica, and planted in Zhejiang, etc. China. Saffron is a rare traditional Chinese medicinal material, has strong physiological activity, has medicinal effects of tranquilizing, eliminating phlegm and relieving spasm when stigma croci is used in Asia and Europe, is used for treating gastropathy, menstruation regulation, measles, fever, jaundice, hepatosplenomegaly and the like, is a spice, has sweet flower fragrance when being picked and dried, is fresher, has stronger sweet flower fragrance, can be smelled only in each year of saffron harvesting season, is gradually lightened along with the increase of storage time, and has more and more intense specific fragrance.
Disclosure of Invention
In order to develop a novel raw material for bead blasting for cigarettes, the invention aims to provide a preparation method of a saffron extract for bead blasting for tobaccos. The method can effectively realize the extraction of the saffron flavor components, effectively improve the flavor of cigarettes and improve the comfortable experience of smokers.
In order to achieve the purpose, the invention adopts the following technical scheme:
a preparation method of stigma croci Sativi extract for tobacco bead blasting comprises the following steps:
(1) pretreatment: soaking stigma croci in warm water for a period of time, and drying at room temperature;
(2) reflux extraction: adding dried stigma croci Sativi raw materials into organic solvent, reflux extracting under normal pressure, and cooling;
(3) microwave extraction: adding the solvent and the raw materials in the step (2) into an acetic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction;
(4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel;
(5) concentration: and (4) carrying out reduced pressure concentration on the filtrate obtained in the step (4) to obtain the saffron extract for the tobacco bead blasting.
Further, the soaking time in the step (1) is 30-60 min.
Further, the organic solvent in the step (2) is medium-chain carbon fatty acid ester; preferably, the organic solvent is caprylic capric acid glyceride (ODO).
Further, the mass ratio of the saffron crocus raw material to the organic solvent is 1: (5-15).
Furthermore, the adding amount of the acetic acid solution in the step (3) is 10% of the mass of the solvent and the raw materials in the step (2).
Further, the microwave extraction time in the step (3) is 15-20min, and the microwave frequency is 915 MHz.
Further, the temperature of the reduced pressure concentration is 45 ℃, the rotating speed is 20r/min, and the concentration is carried out until the mass is 5 times of that of the raw materials.
The invention also provides an application of the saffron extract in tobacco bead blasting, which specifically comprises the following steps: adding the saffron crocus extract into olive oil, and then popping the crocus according to a natural condensation process.
Further, the saffron extract accounts for 20% of the mass ratio of the olive oil.
The invention has the following technical characteristics:
1) the invention extracts the saffron extract by the synergy of soaking, refluxing and microwave, and can effectively realize the extraction of the saffron fragrance components.
2) The invention uses the saffron extract in the tobacco bead blasting, can effectively improve the fragrance of cigarettes, has fresh and sweet aroma, conglobation of smoke, soft smoke and rich aftertaste, has better dissolubility than the saffron extract in the market, and can improve the forming rate of bead blasting.
3) Compared with saffron oil-soluble essence, the invention is added into the bead blasting product, so that the fragrance is more harmonious and no fat powder smell exists.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions of the embodiments of the present invention will be clearly and completely described below. It is to be understood that the embodiments described are only a few embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the described embodiments of the invention without any inventive step, are within the scope of protection of the invention.
Unless defined otherwise, technical or scientific terms used herein shall have the ordinary meaning as understood by one of ordinary skill in the art to which this invention belongs.
Example 1:
a preparation method of stigma croci Sativi extract for tobacco bead blasting comprises the following steps:
(1) pretreatment: soaking stigma croci in warm water for 30min, and drying at room temperature;
(2) reflux extraction: adding dried saffron crocus raw material into ODO solution with the mass of 10 times, carrying out reflux extraction for 1 hour under normal pressure, and finally cooling;
(3) microwave extraction: adding the solvent and the raw materials in the step (2) into an acetic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction for 15min, wherein the microwave frequency is 915 MHz;
(4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel;
(5) concentration: and (4) carrying out reduced pressure concentration on the filtrate obtained in the step (4) until the mass of the filtrate is 5 times that of the raw material, setting the concentration temperature at 45 ℃ and the rotating speed at 20r/min, and obtaining the saffron extract for tobacco bead blasting.
Example 2:
a preparation method of stigma croci Sativi extract for tobacco bead blasting comprises the following steps:
(1) pretreatment: soaking stigma croci in warm water for 40min, and drying at room temperature;
(2) reflux extraction: adding dried saffron crocus raw material into ODO solution with 5 times of the mass, refluxing and extracting for 1 hour under normal pressure, and finally cooling;
(3) microwave extraction: adding the solvent and the raw materials in the step (2) into an acetic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction for 20min, wherein the microwave frequency is 915 MHz;
(4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel;
(5) concentration: and (4) carrying out reduced pressure concentration on the filtrate obtained in the step (4) until the mass of the filtrate is 5 times that of the raw material, setting the concentration temperature at 45 ℃ and the rotating speed at 20r/min, and obtaining the saffron extract for tobacco bead blasting.
Example 3:
a preparation method of stigma croci Sativi extract for tobacco bead blasting comprises the following steps:
(1) pretreatment: soaking stigma croci in warm water for 60min, and drying at room temperature;
(2) reflux extraction: adding dried saffron crocus raw material into ODO solution with the mass 15 times that of the saffron crocus raw material, carrying out reflux extraction for 1 hour under normal pressure, and finally cooling;
(3) microwave extraction: adding the solvent and the raw materials in the step (2) into an acetic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction for 15min, wherein the microwave frequency is 915 MHz;
(4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel;
(5) concentration: and (4) carrying out reduced pressure concentration on the filtrate obtained in the step (4) until the mass of the filtrate is 5 times that of the raw material, setting the concentration temperature at 45 ℃ and the rotating speed at 20r/min, and obtaining the saffron extract for tobacco bead blasting.
Example 4:
adding the saffron extract obtained in the examples 1-3 into olive oil, and then preparing into populus according to a natural condensation method process, wherein the saffron extract accounts for 20% of the mass ratio of the olive oil. And adding the prepared puffed beads into a cigarette holder, and enabling a cigarette flavoring agent to evaluate smoking according to the national standard GB 5606.4-2005. The comparison reference samples are cigarettes without bead blasting and cigarettes with saffron essence bead blasting. The evaluation results are shown in tables 1 and 2.
TABLE 1 evaluation of cigarettes containing saffron extract exploded beads and without exploded beads
TABLE 2 evaluation of aroma, smoke and taste of cigarettes containing saffron extract
As can be seen from the experimental results in tables 1 and 2, the popped bead cigarette containing the saffron extract has better performance in aroma, smoke and taste, and can enable smokers to obtain more comfortable experience.
The above description of the embodiments is only intended to facilitate the understanding of the method of the invention and its core ideas. It should be noted that, for those skilled in the art, it is possible to make various improvements and modifications to the present invention without departing from the principle of the present invention, and those improvements and modifications also fall within the scope of the claims of the present invention.
Claims (10)
1. A preparation method of a saffron extract for tobacco bead blasting is characterized by comprising the following steps:
(1) pretreatment: soaking stigma croci in warm water for a period of time, and drying at room temperature;
(2) reflux extraction: adding dried stigma croci Sativi raw materials into organic solvent, reflux extracting under normal pressure, and cooling;
(3) microwave extraction: adding the solvent and the raw materials in the step (2) into an acetic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction;
(4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel;
(5) concentration: and (4) carrying out reduced pressure concentration on the filtrate obtained in the step (4) to obtain the saffron extract for the tobacco bead blasting.
2. The preparation method according to claim 1, wherein the soaking time in the step (1) is 30-60 min.
3. The method according to claim 1, wherein the organic solvent in the step (2) is a medium-chain carbon fatty acid ester.
4. The method according to claim 3, wherein the organic solvent is caprylic/capric glyceride (ODO).
5. The preparation method according to claim 1, wherein the mass ratio of saffron crocus raw material to organic solvent is 1: (5-15).
6. The preparation method according to claim 1, wherein the amount of the acetic acid solution added in the step (3) is 10% of the mass of the solvent and the raw materials in the step (2).
7. The method according to claim 1, wherein the microwave extraction time in step (3) is 15-20min, and the microwave frequency is 915 MHz.
8. The method according to claim 1, wherein the concentration under reduced pressure is carried out at a temperature of 45 ℃ and at a rotation speed of 20r/min, and the concentration is carried out to 5 times the mass of the raw material.
9. The use of saffron extract in tobacco beading according to claims 1-8, wherein said saffron extract is added to olive oil and then the beading is performed according to the natural condensation process.
10. Use according to claim 9, characterized in that said saffron extract represents 20% by mass of said olive oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911128200.4A CN110804497A (en) | 2019-11-18 | 2019-11-18 | Preparation method of saffron extract for tobacco bead blasting |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911128200.4A CN110804497A (en) | 2019-11-18 | 2019-11-18 | Preparation method of saffron extract for tobacco bead blasting |
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| Publication Number | Publication Date |
|---|---|
| CN110804497A true CN110804497A (en) | 2020-02-18 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201911128200.4A Pending CN110804497A (en) | 2019-11-18 | 2019-11-18 | Preparation method of saffron extract for tobacco bead blasting |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114736736A (en) * | 2022-04-15 | 2022-07-12 | 甘肃烟草工业有限责任公司 | Saffron spice and preparation method and application thereof |
Citations (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005013138A (en) * | 2003-06-27 | 2005-01-20 | Kiyomitsu Kawasaki | Method for producing spice flavor |
| CN103387489A (en) * | 2013-07-11 | 2013-11-13 | 苏州大学 | Preparation method of high pure crocin and geniposide |
| US20140010774A1 (en) * | 2011-03-18 | 2014-01-09 | Firmenich Sa | Saffron odorants |
| CN103525553A (en) * | 2013-10-23 | 2014-01-22 | 红云红河烟草(集团)有限责任公司 | Tobacco and spice plant mixing essence and application thereof |
| CN103550433A (en) * | 2013-11-01 | 2014-02-05 | 王颖 | Extraction method of saffron crocus essence substances |
| CN103805340A (en) * | 2012-11-15 | 2014-05-21 | 大连捌伍捌创新工场科技服务有限公司 | Method for extracting saffron crocus essential oil |
| CN104178354A (en) * | 2014-09-04 | 2014-12-03 | 南京标科生物科技有限公司 | Method for extracting stigma croci essential oil |
| CN105079325A (en) * | 2015-09-23 | 2015-11-25 | 成都艾比科生物科技有限公司 | Method for extracting essence substances of saffron crocus |
| CN106266299A (en) * | 2015-05-24 | 2017-01-04 | 张凌 | Stigma Croci extract |
| CN106957880A (en) * | 2016-10-13 | 2017-07-18 | 湖北中烟工业有限责任公司 | A kind of immobilization beta glucuroide prepares method of the cigarette with safranine flower extract |
| CN107474958A (en) * | 2017-08-16 | 2017-12-15 | 湖北中烟工业有限责任公司 | A kind of method of infiltration evaporation film preparation safflower extract |
| CN107474963A (en) * | 2017-09-01 | 2017-12-15 | 云南巴菰生物科技有限公司 | A kind of cordate houttuynia essential oil cigarette is with quick-fried pearl and preparation method thereof |
| CN107927901A (en) * | 2017-11-22 | 2018-04-20 | 湖北中烟工业有限责任公司 | It is a kind of that the method for tobacco aromaticss and its application in the quick-fried pearl of cigarette are prepared using Glycerin, mixed triester with caprylic acid capric acid |
| CN108218692A (en) * | 2018-02-26 | 2018-06-29 | 南阳泰瑞生物科技股份有限公司 | Utilize the method for cape jasmine fruit production crocetin |
| CN108285830A (en) * | 2018-01-24 | 2018-07-17 | 云南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl herbal essential oil and quick-fried pearl preparation method |
| CN109468173A (en) * | 2018-11-16 | 2019-03-15 | 湖北中烟工业有限责任公司 | Quick-fried pearl base oil and preparation method thereof with natural cream perfume (or spice) note |
| CN109776370A (en) * | 2017-11-11 | 2019-05-21 | 原海彦 | The method of carrotene is extracted in a kind of safflower |
-
2019
- 2019-11-18 CN CN201911128200.4A patent/CN110804497A/en active Pending
Patent Citations (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005013138A (en) * | 2003-06-27 | 2005-01-20 | Kiyomitsu Kawasaki | Method for producing spice flavor |
| US20140010774A1 (en) * | 2011-03-18 | 2014-01-09 | Firmenich Sa | Saffron odorants |
| CN103805340A (en) * | 2012-11-15 | 2014-05-21 | 大连捌伍捌创新工场科技服务有限公司 | Method for extracting saffron crocus essential oil |
| CN103387489A (en) * | 2013-07-11 | 2013-11-13 | 苏州大学 | Preparation method of high pure crocin and geniposide |
| CN103525553A (en) * | 2013-10-23 | 2014-01-22 | 红云红河烟草(集团)有限责任公司 | Tobacco and spice plant mixing essence and application thereof |
| CN103550433A (en) * | 2013-11-01 | 2014-02-05 | 王颖 | Extraction method of saffron crocus essence substances |
| CN104178354A (en) * | 2014-09-04 | 2014-12-03 | 南京标科生物科技有限公司 | Method for extracting stigma croci essential oil |
| CN106266299A (en) * | 2015-05-24 | 2017-01-04 | 张凌 | Stigma Croci extract |
| CN105079325A (en) * | 2015-09-23 | 2015-11-25 | 成都艾比科生物科技有限公司 | Method for extracting essence substances of saffron crocus |
| CN106957880A (en) * | 2016-10-13 | 2017-07-18 | 湖北中烟工业有限责任公司 | A kind of immobilization beta glucuroide prepares method of the cigarette with safranine flower extract |
| CN107474958A (en) * | 2017-08-16 | 2017-12-15 | 湖北中烟工业有限责任公司 | A kind of method of infiltration evaporation film preparation safflower extract |
| CN107474963A (en) * | 2017-09-01 | 2017-12-15 | 云南巴菰生物科技有限公司 | A kind of cordate houttuynia essential oil cigarette is with quick-fried pearl and preparation method thereof |
| CN109776370A (en) * | 2017-11-11 | 2019-05-21 | 原海彦 | The method of carrotene is extracted in a kind of safflower |
| CN107927901A (en) * | 2017-11-22 | 2018-04-20 | 湖北中烟工业有限责任公司 | It is a kind of that the method for tobacco aromaticss and its application in the quick-fried pearl of cigarette are prepared using Glycerin, mixed triester with caprylic acid capric acid |
| CN108285830A (en) * | 2018-01-24 | 2018-07-17 | 云南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl herbal essential oil and quick-fried pearl preparation method |
| CN108218692A (en) * | 2018-02-26 | 2018-06-29 | 南阳泰瑞生物科技股份有限公司 | Utilize the method for cape jasmine fruit production crocetin |
| CN109468173A (en) * | 2018-11-16 | 2019-03-15 | 湖北中烟工业有限责任公司 | Quick-fried pearl base oil and preparation method thereof with natural cream perfume (or spice) note |
Non-Patent Citations (1)
| Title |
|---|
| 王亮: "《精油的科学》", 31 December 2018, 东南大学出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114736736A (en) * | 2022-04-15 | 2022-07-12 | 甘肃烟草工业有限责任公司 | Saffron spice and preparation method and application thereof |
| CN114736736B (en) * | 2022-04-15 | 2023-08-04 | 甘肃烟草工业有限责任公司 | Saffron perfume and preparation method and application thereof |
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