CN110720658B - Preparation method of acacia flower extract for tobacco bead blasting - Google Patents
Preparation method of acacia flower extract for tobacco bead blasting Download PDFInfo
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- CN110720658B CN110720658B CN201911128130.2A CN201911128130A CN110720658B CN 110720658 B CN110720658 B CN 110720658B CN 201911128130 A CN201911128130 A CN 201911128130A CN 110720658 B CN110720658 B CN 110720658B
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- acacia
- extraction
- flower extract
- acacia flower
- bead blasting
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- 235000010643 Leucaena leucocephala Nutrition 0.000 title claims abstract description 56
- 239000011324 bead Substances 0.000 title claims abstract description 33
- 239000000284 extract Substances 0.000 title claims abstract description 33
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 23
- 238000005422 blasting Methods 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title abstract description 10
- 240000007472 Leucaena leucocephala Species 0.000 title 1
- 244000061176 Nicotiana tabacum Species 0.000 title 1
- 241000220479 Acacia Species 0.000 claims abstract description 55
- 239000002994 raw material Substances 0.000 claims abstract description 25
- 238000000605 extraction Methods 0.000 claims abstract description 23
- 241000208125 Nicotiana Species 0.000 claims abstract description 22
- 239000000243 solution Substances 0.000 claims abstract description 19
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000000874 microwave-assisted extraction Methods 0.000 claims abstract description 15
- 238000010992 reflux Methods 0.000 claims abstract description 14
- 238000001914 filtration Methods 0.000 claims abstract description 12
- 239000000706 filtrate Substances 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims abstract description 9
- 239000003960 organic solvent Substances 0.000 claims abstract description 9
- 235000014655 lactic acid Nutrition 0.000 claims abstract description 8
- 239000004310 lactic acid Substances 0.000 claims abstract description 8
- 238000002791 soaking Methods 0.000 claims abstract description 8
- 239000002904 solvent Substances 0.000 claims abstract description 8
- 238000001816 cooling Methods 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract description 6
- 239000011259 mixed solution Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000004006 olive oil Substances 0.000 claims description 6
- 235000008390 olive oil Nutrition 0.000 claims description 6
- 238000009833 condensation Methods 0.000 claims description 3
- 230000005494 condensation Effects 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- -1 carbon fatty acid ester Chemical class 0.000 claims description 2
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 2
- 229930195729 fatty acid Natural products 0.000 claims description 2
- 239000000194 fatty acid Substances 0.000 claims description 2
- 125000005456 glyceride group Chemical group 0.000 claims 1
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical group CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims 1
- 235000019504 cigarettes Nutrition 0.000 abstract description 22
- 239000003205 fragrance Substances 0.000 abstract description 10
- 239000000779 smoke Substances 0.000 abstract description 5
- 239000007788 liquid Substances 0.000 description 4
- 241000628997 Flos Species 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 235000019640 taste Nutrition 0.000 description 3
- 240000007185 Albizia julibrissin Species 0.000 description 2
- 235000011468 Albizia julibrissin Nutrition 0.000 description 2
- 235000006679 Mentha X verticillata Nutrition 0.000 description 2
- 235000002899 Mentha suaveolens Nutrition 0.000 description 2
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 241000272525 Anas platyrhynchos Species 0.000 description 1
- 235000007650 Aralia spinosa Nutrition 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241001092473 Quillaja Species 0.000 description 1
- 235000009001 Quillaja saponaria Nutrition 0.000 description 1
- 241000949456 Zanthoxylum Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000010692 aromatic oil Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a preparation method of an acacia flower extract for bead blasting of tobacco. The preparation method comprises the following steps: (1) pretreatment: soaking the acacia flowers in warm water for a period of time, and then drying at room temperature; (2) reflux extraction: adding dried acacia flower raw material into an organic solvent, carrying out reflux extraction under normal pressure, and finally cooling; (3) microwave extraction: adding the solvent and the raw materials in the step (2) into a lactic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction; (4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel; (5) concentration: and (4) concentrating the filtrate obtained in the step (4) under reduced pressure to obtain the acacia flower extract for the tobacco bead blasting. The method can effectively realize the extraction of the flower fragrance components of the acacia, so that the cigarette has the fragrance of the acacia, the smoke of the cigarette is fine and smooth and long, and the dry feeling is reduced.
Description
Technical Field
The invention belongs to the technical field of cigarette additives, and particularly relates to a preparation method of an acacia flower extract for bead blasting of tobacco.
Background
In the 60's of the 20 th century, tobacco companies began to offer cigarettes with bead-blasting, which means that a small liquid rubber bead embedded in a tobacco filter wrapped with liquids of different types of flavors, smokers could pinch and burst the liquid in the bead during smoking to make the liquid flow out, so that the cigarettes had richer and more fragrant tastes, and the smokers had more comfortable experiences.
The foreign bead for the cigarette mainly takes a mint type as a main material, the domestic bead for the cigarette has great difference, and has different types such as mint, fruit fragrance, wine fragrance, Chinese herbal medicine and the like, however, the development space for perfuming the bead for the bead is huge, and the proper new raw material for the bead for the cigarette is the most important work at present.
Acacia, alias duck Quillaja, Roxburgh pricklyash, Mediterranean tree, etc., shrub or small arbor plant, 2-4 m high; the bark is coarse, brown, and has many branches, and the branches are usually bent like a Chinese character 'zhi', and have small bark holes. The acacia flower has extremely fragrant and rich flower fragrance, and can be used for extracting essence and extracting aromatic oil to be used as raw materials of cosmetics such as high-grade perfume and the like.
The article of 'analysis of aroma components of acacia flowers and application of the acacia flowers in cigarettes' published by Ningzhengxing and the like adopts a solvent extraction method to extract chemical components of the acacia flowers, and a cigarette flavoring experiment is carried out by spraying the extract on tobacco shreds. However, there is no study on the addition of acacia flower extract to, for example, a tobacco bead. The above extraction method is inefficient and cannot efficiently extract all the aroma components.
Disclosure of Invention
In order to develop the acacia flower fragrance bead for cigarette, the invention aims to provide a preparation method of the acacia flower extract for the tobacco bead. The method can effectively realize the extraction of the flower fragrance components of the acacia, so that the cigarette has the fragrance of the acacia, the smoke of the cigarette is fine and smooth and long, and the dry feeling is reduced.
In order to achieve the purpose, the invention adopts the following technical scheme:
a preparation method of an acacia flower extract for tobacco bead blasting comprises the following steps:
(1) pretreatment: soaking the acacia flowers in warm water for a period of time, and then drying at room temperature;
(2) reflux extraction: adding dried acacia flower raw material into an organic solvent, carrying out reflux extraction under normal pressure, and finally cooling;
(3) microwave extraction: adding the solvent and the raw materials in the step (2) into a lactic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction;
(4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel;
(5) concentration: and (4) concentrating the filtrate obtained in the step (4) under reduced pressure to obtain the acacia flower extract for the tobacco bead blasting.
Further, the soaking time in the step (1) is 30-60 min.
Further, the organic solvent in the step (2) is medium-chain carbon fatty acid ester; preferably, the organic solvent is caprylic capric acid glyceride (ODO).
Further, the mass ratio of the acacia flower raw material to the organic solvent is 1: (5-10), and the reflux extraction time is 2 hours.
Furthermore, the addition amount of the lactic acid solution in the step (3) is 10% of the mass of the solvent and the raw materials in the step (2).
Further, the microwave extraction time in the step (3) is 20-30min, and the microwave frequency is 915 MHz.
Further, the temperature of the reduced pressure concentration is 50 ℃, the rotating speed is 20r/min, and the concentration is carried out until the mass is 3 times of that of the raw materials.
The invention also provides an application of the acacia flower extract in tobacco bead blasting, which specifically comprises the following steps: adding the acacia flower extract into olive oil, and then carrying out bead blasting according to a natural condensation process.
Further, the acacia flower extract accounts for 10% of the olive oil by mass.
The invention has the following technical characteristics:
1) the method can effectively realize the extraction of the flower fragrance components of the acacia by extracting the acacia flower extract through the soaking-refluxing-microwave synergistic manner.
2) The acacia flower extract is used in the tobacco bead blasting, so that the acacia flower aroma of the cigarette can be increased, the cigarette has fresh and sweet aroma, the smoke is fine and long, and the dry feeling is reduced; meanwhile, the acacia flower extract has good dissolubility, and can effectively improve the bead explosion forming rate.
3) Compared with the acacia oil-soluble essence, the invention is added into the exploded bead product, so that the fragrance is more harmonious and the smell of fat powder is avoided.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions of the embodiments of the present invention will be clearly and completely described below. It is to be understood that the embodiments described are only a few embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the described embodiments of the invention without any inventive step, are within the scope of protection of the invention.
Unless defined otherwise, technical or scientific terms used herein shall have the ordinary meaning as understood by one of ordinary skill in the art to which this invention belongs.
Example 1:
a preparation method of an acacia flower extract for tobacco bead blasting comprises the following steps:
(1) pretreatment: soaking flos Acaciae Farnesianae in warm water for 30min, and drying at room temperature;
(2) reflux extraction: adding dried acacia flower raw material into ODO solution with the mass 5 times that of the acacia flower raw material, carrying out reflux extraction for 2 hours under normal pressure, and finally cooling;
(3) microwave extraction: adding the solvent and the raw materials in the step (2) into a lactic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction for 20min, wherein the microwave frequency is 915 MHz;
(4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel;
(5) concentration: and (4) carrying out reduced pressure concentration on the filtrate obtained in the step (4) until the mass of the filtrate is 3 times that of the raw material, setting the concentration temperature at 50 ℃ and the rotating speed at 20r/min, and obtaining the acacia flower extract for the tobacco popping.
Example 2:
a preparation method of an acacia flower extract for tobacco bead blasting comprises the following steps:
(1) pretreatment: soaking flos Acaciae Farnesianae in warm water for 50min, and drying at room temperature;
(2) reflux extraction: adding dried acacia flower raw material into ODO solution with the mass 5 times that of the acacia flower raw material, carrying out reflux extraction for 2 hours under normal pressure, and finally cooling;
(3) microwave extraction: adding the solvent and the raw materials in the step (2) into a lactic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction for 25min, wherein the microwave frequency is 915 MHz;
(4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel;
(5) concentration: and (4) carrying out reduced pressure concentration on the filtrate obtained in the step (4) until the mass of the filtrate is 3 times that of the raw material, setting the concentration temperature at 50 ℃ and the rotating speed at 20r/min, and obtaining the acacia flower extract for the tobacco popping.
Example 3:
a preparation method of an acacia flower extract for tobacco bead blasting comprises the following steps:
(1) pretreatment: soaking flos Acaciae Farnesianae in warm water for 60min, and drying at room temperature;
(2) reflux extraction: adding dried acacia flower raw material into ODO solution with the mass being 10 times that of the raw material, carrying out reflux extraction for 2 hours under normal pressure, and finally cooling;
(3) microwave extraction: adding the solvent and the raw materials in the step (2) into a lactic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction for 30min, wherein the microwave frequency is 915 MHz;
(4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel;
(5) concentration: and (4) carrying out reduced pressure concentration on the filtrate obtained in the step (4) until the mass of the filtrate is 3 times that of the raw material, setting the concentration temperature at 50 ℃ and the rotating speed at 20r/min, and obtaining the acacia flower extract for the tobacco popping.
Example 4:
the acacia flower extract obtained in examples 1 to 3 was added to olive oil, and then the beads were popped according to the natural condensation process, and the acacia flower extract accounted for 10% by mass of the olive oil. And then adding the prepared popping beads into a cigarette filter tip, and evaluating by a cigarette flavoring agent according to the national standard GB 5606.4-2005. The comparative reference samples are cigarettes without the bead blasting and cigarettes with the bead blasting of the acacia essence. The evaluation results are shown in tables 1 and 2.
TABLE 1 evaluation of cigarettes containing extracts of Albizzia julibrissin Durazz
TABLE 2 evaluation of the aroma, smoke and taste of cigarettes containing the extract of Albizzia julibrissin Durazz
As can be seen from the experimental results in tables 1 and 2, the cigarettes containing the acacia flower extract have better performances in aroma, smoke and taste, and can enable smokers to obtain more comfortable experience.
The above description of the embodiments is only intended to facilitate the understanding of the method of the invention and its core ideas. It should be noted that, for those skilled in the art, it is possible to make various improvements and modifications to the present invention without departing from the principle of the present invention, and those improvements and modifications also fall within the scope of the claims of the present invention.
Claims (8)
1. The application of the acacia flower extract in the tobacco bead blasting is characterized in that the acacia flower extract is added into olive oil and then is made into the bead blasting according to a natural condensation method process;
the acacia flower extract for the tobacco bead blasting comprises the following steps:
(1) pretreatment: soaking the acacia flowers in warm water for a period of time, and then drying at room temperature;
(2) reflux extraction: adding dried acacia flower raw material into an organic solvent, carrying out reflux extraction under normal pressure, and finally cooling;
(3) microwave extraction: adding the solvent and the raw materials in the step (2) into a lactic acid solution with the mass percentage of 10%, and then placing the mixed solution into microwave extraction equipment for further extraction;
(4) and (3) filtering: filtering the extracting solution in the step (3) by using a Buchner funnel;
(5) concentration: and (4) concentrating the filtrate obtained in the step (4) under reduced pressure to obtain the acacia flower extract for the tobacco bead blasting.
2. Use according to claim 1, wherein the acacia flower extract represents 10% by mass of the olive oil.
3. The use of claim 1, wherein the soaking time in step (1) is 30-60 min.
4. The use according to claim 1, wherein the organic solvent of step (2) is a medium-chain carbon fatty acid ester.
5. Use according to claim 3, characterized in that the organic solvent is caprylic capric glyceride (ODO).
6. The use as claimed in claim 1, wherein the weight ratio of the acacia flower raw material to the organic solvent is 1: (5-10), and refluxing and extracting for 2 hours.
7. The use according to claim 1, wherein the amount of the lactic acid solution added in step (3) is 10% of the mass of the solvent and the raw materials in step (2).
8. The use according to claim 1, wherein the microwave extraction time of step (3) is 20-30min, and the frequency of microwave extraction is 915 MHz.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911128130.2A CN110720658B (en) | 2019-11-18 | 2019-11-18 | Preparation method of acacia flower extract for tobacco bead blasting |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911128130.2A CN110720658B (en) | 2019-11-18 | 2019-11-18 | Preparation method of acacia flower extract for tobacco bead blasting |
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| Publication Number | Publication Date |
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| CN110720658A CN110720658A (en) | 2020-01-24 |
| CN110720658B true CN110720658B (en) | 2021-11-05 |
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Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1058858C (en) * | 1994-06-14 | 2000-11-29 | 荆树汉 | Health-care cigarette |
| US20060204599A1 (en) * | 2005-03-14 | 2006-09-14 | Wheat Jared R | Dietary supplement and method of using same |
| CN102936535B (en) * | 2012-11-23 | 2014-02-12 | 中国烟草总公司郑州烟草研究院 | Preparation method and application of natural tobacco aroma enhancer |
| CN104814912B (en) * | 2015-05-08 | 2017-06-30 | 福建春辉生物工程有限公司 | A kind of hand lotion containing wild tea oil |
| CN105062676B (en) * | 2015-07-29 | 2018-11-23 | 湖北中烟工业有限责任公司 | A kind of Acacia tobacco aromaticss and preparation method thereof |
| CN106957873A (en) * | 2016-10-13 | 2017-07-18 | 武汉黄鹤楼香精香料有限公司 | A kind of fixing lactic acid bacteria prepares method of the cigarette with Acacia extract |
| CN107927901A (en) * | 2017-11-22 | 2018-04-20 | 湖北中烟工业有限责任公司 | It is a kind of that the method for tobacco aromaticss and its application in the quick-fried pearl of cigarette are prepared using Glycerin, mixed triester with caprylic acid capric acid |
| CN108060014A (en) * | 2017-12-12 | 2018-05-22 | 湖北中烟工业有限责任公司 | For the preparation method of the Flos Caryophylli extract of quick-fried pearl base oil |
| CN109609278A (en) * | 2019-01-25 | 2019-04-12 | 云南巴菰生物科技有限公司 | A kind of fritillary-loquat essence and its preparing purposes of the cigarette in quick-fried pearl |
| CN109868185A (en) * | 2019-01-31 | 2019-06-11 | 广西中烟工业有限责任公司 | A kind of faenum graecum cigarette quick-fried pearl essence and its application in cigarette |
| CN109868184A (en) * | 2019-01-31 | 2019-06-11 | 广西中烟工业有限责任公司 | A kind of Radix Glycyrrhizae cigarette quick-fried pearl essence and its application in cigarette |
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