CN114468345B - Electronic cigarette liquid with pepper flavor and preparation method thereof - Google Patents
Electronic cigarette liquid with pepper flavor and preparation method thereof Download PDFInfo
- Publication number
- CN114468345B CN114468345B CN202111628468.1A CN202111628468A CN114468345B CN 114468345 B CN114468345 B CN 114468345B CN 202111628468 A CN202111628468 A CN 202111628468A CN 114468345 B CN114468345 B CN 114468345B
- Authority
- CN
- China
- Prior art keywords
- parts
- pepper
- refined
- tobacco
- extraction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/34—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a carbocyclic ring other than a six-membered aromatic ring
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/10—Devices using liquid inhalable precursors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0403—Solvent extraction of solutions which are liquid with a supercritical fluid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D2011/007—Extraction using a solvent in the gas phase
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a single-cigarette tobacco juice with pepper flavor and a preparation method thereof, wherein the electronic cigarette tobacco juice is prepared from the following raw materials in parts by weight: 1 to 10 parts of refined pepper product, 1 to 10 parts of bergamot oil, 1 to 5 parts of peppermint oil, 1 to 5 parts of pine needle oil, 1 to 5 parts of linalool, 0.2 to 1.5 parts of menthyl acetate, 0.5 to 2.5 parts of cooling agent, 5 to 15 parts of refined tobacco product, 1 to 5 parts of ethanol, 5 to 10 parts of water, 15 to 25 parts of propylene glycol and 6 to 68.3 parts of glycerol. The electronic cigarette liquid has the special aroma of the pepper, shows the style characteristics of freshness, refreshing, sweetness and smoothness in the throat, enriches the smoking flavor of the electronic cigarette, has a certain health-care function, and can effectively reduce the potential harm of the electronic cigarette to consumers.
Description
Technical Field
The invention relates to the technical field of tobacco, in particular to electronic cigarette liquid with pepper flavor and a preparation method thereof.
Background
With the growing concern of consumers on health problems, in recent years, various novel tobacco products are emerging at home and abroad, and electronic cigarettes are favored by consumers as an important form of the novel tobacco products. The electronic cigarette generally comprises elements such as a lithium battery, an atomizer and cigarette liquid, and the qualified electronic cigarette does not contain harmful substances such as tar, carbon dioxide, carbon monoxide and hydrocyanic acid, so that the electronic cigarette does not harm human bodies and natural environment. The electronic cigarette heats the cigarette liquid in the atomization bin to generate a smoke effect in the smoking process. The electronic cigarette liquid mainly comprises propylene glycol or glycerol solvent containing nicotine, and essences with different styles and characteristics are added to prepare different tastes so as to meet the requirements of different smokers. At present, the problem of monotonous smoking flavor still exists in the cigarette liquid of the electronic cigarette, and the market of the electronic cigarette is greatly limited.
The pepper is a rutaceae plant, is pungent and warm in taste, enters liver, spleen and stomach meridians, has the effects of resisting tumors, anesthetizing, easing pain, resisting bacteria, killing insects, resisting oxidation and the like, can reduce free radicals with oxidability in a system so as to prevent continuous reaction of the free radicals, and has the advantages that the clearance rate of hydroxyl free radicals is enhanced and the antioxidant activity is increased along with the gradual increase of the adding amount of the pepper volatile oil in a certain range. The essential oil of Zanthoxylum bungeanum has strong inhibiting effect on Escherichia coli, and has effects of improving intestinal function and maintaining health. The chemical components of the pepper mainly comprise volatile oil, alkaloid, amides, flavonoids, coumarins, triterpenes, sterols, hydrocarbons, lignans, fatty acid and other components, and evaluation shows that when the pepper essential oil is added into cigarette products, the spicy substances can influence the smoking taste and have strong irritation. According to the existing research reports, the pepper can bring prickling feeling and numb feeling to people, mainly because the pepper contains amide substances, particularly a series of unsaturated fatty acid amides which are insoluble in cold petroleum ether, so that a large amount of amide substances with irritation can be removed by petroleum ether extraction, the irritation is reduced, and the suction feeling is improved.
Disclosure of Invention
In order to overcome the technical defects, the invention provides the electronic cigarette liquid with the pepper flavor and the preparation method thereof aiming at the problem of monotonous smoking flavor of the existing electronic cigarette liquid.
In order to achieve the purpose, the invention adopts the following technical scheme:
the invention provides an electronic cigarette liquid with pepper flavor, which is prepared from the following components in parts by weight: 1 to 10 parts of refined pepper product, 1 to 10 parts of bergamot oil, 1 to 5 parts of peppermint oil, 1 to 5 parts of pine needle oil, 1 to 5 parts of linalool, 0.2 to 1.5 parts of menthyl acetate, 0.5 to 2.5 parts of cooling agent, 5 to 15 parts of refined tobacco product, 1 to 5 parts of ethanol, 5 to 10 parts of water, 15 to 25 parts of propylene glycol and 6 to 68.3 parts of glycerol.
The further technical proposal is that the refined product of the pepper is one or more refined products of pepper substances in Chinese tribute pepper, wudu Dahongpao and Hancheng Dahongpao;
the further technical scheme is that the pepper used in the refined pepper product is fresh pepper;
the further technical scheme is that the preparation method of the refined zanthoxylum bungeanum product comprises the following steps: placing fresh pepper in a rotary cage dryer, wherein the drying temperature is 40-50 ℃, and the drying time is 2-4 h; immediately placing the dried pepper in a refrigerator at the temperature of-5 ℃ for cooling for 20-30 min; after standing, taking out the pepper, placing the pepper in a rotary cage dryer, and repeating the steps of heating and drying, cooling and standing for three times; putting the pepper which is cooled and stood for the third time into a freeze dryer, and drying for 12-24 h; separating the dried pericarpium Zanthoxyli from semen Zanthoxyli, pulverizing, and sieving with 50 mesh sieve; collecting pericarpium Zanthoxyli powder, and performing supercritical CO 2 Extracting to obtain pepper essential oil; removing amide substances in the zanthoxylum essential oil by using petroleum ether extraction to obtain a refined zanthoxylum bungeanum product;
the further technical proposal is that the supercritical CO 2 The extraction pressure of the extraction is 20-40 MPa,the extraction temperature is 40-50 ℃, the extraction time is 2-4h 2 The flow rate is controlled to be 25-30L/h;
the further technical scheme is that the proportion of the pepper essential oil to the petroleum ether is 1-3-1, the extraction time is 1-2 h, and the petroleum ether is removed by rotary evaporation after the extraction is finished.
The further technical proposal is that the tobacco refined substance is one or more of burley tobacco, flue-cured tobacco or cigar tobacco fragment refined substances;
the further technical proposal is that the preparation method of the refined tobacco product comprises the following steps: placing tobacco fragments into a closed extraction tank, vacuumizing, and injecting an extraction solvent into the tank, wherein the extraction solvent is one or more of dimethyl ether, butane and cyclohexane, the volume of the tobacco fragments and the extraction solvent is (1-1); refining the tobacco extract by molecular distillation, and collecting light components to obtain a tobacco refined product;
the further technical proposal is that the molecular distillation conditions are that the feeding speed is 6.0-8.0 mL/min, the vacuum degree is 10-20 Pa, the heating temperature is 40-100 ℃, the cooling temperature is 25-35 ℃, and the film scraping speed is 140-150 r/min;
the invention also provides a preparation method of the electronic cigarette liquid with the pepper flavor, which comprises the following steps:
(1) Preparing a pepper refined product: placing fresh pepper in a rotary cage dryer, wherein the drying temperature is 40-50 ℃, and the drying time is 2-4 h; immediately placing the dried pepper in a refrigerator at the temperature of-5 ℃ for cooling for 20-30 min; standing, taking out the pepper, placing the pepper in a rotary cage dryer, and repeating the steps of heating and drying, cooling and standing for three times; putting the pepper which is cooled and stood for the third time into a freeze dryer, and drying for 12-24 h; separating the dried pericarpium Zanthoxyli from semen Zanthoxyli, pulverizing, and sieving with 50 mesh sieve; collecting pericarpium Zanthoxyli powder, and performing supercritical CO 2 Extracting under 20-40 MPa at 40-50 deg.c for 2-4 hr 2 Controlling the flow at 25-30L/h to obtain the zanthoxylum essential oil; removing amides in fructus Zanthoxyli essential oil by petroleum ether extractionThe mass ratio of the pepper essential oil to the petroleum ether is 1-1;
(2) Preparing a tobacco refined product: placing tobacco fragments into a closed extraction tank, vacuumizing, and injecting an extraction solvent into the tank, wherein the extraction solvent is one or more of dimethyl ether, butane and cyclohexane, the volume of the tobacco fragments and the extraction solvent is 1-5-1, the extraction temperature is 30-50 ℃, the extraction time is 3-5 h, and the obtained sample is a tobacco extract; refining the tobacco extract by molecular distillation, wherein the feeding speed is 6.0-8.0 mL/min, the vacuum degree is 10-20 Pa, the heating temperature is 40-100 ℃, the cooling temperature is 25-35 ℃, the film scraping rotating speed is 140-150 r/min, and collecting light components, namely the refined tobacco product;
(3) Preparing electronic cigarette liquid: the electronic cigarette liquid with the pepper flavor is obtained by fully and uniformly mixing the following raw materials in parts by weight: 1 to 10 parts of refined pepper product, 1 to 10 parts of bergamot oil, 1 to 5 parts of peppermint oil, 1 to 5 parts of pine needle oil, 1 to 5 parts of linalool, 0.2 to 1.5 parts of menthyl acetate, 0.5 to 2.5 parts of cooling agent, 5 to 15 parts of refined tobacco product, 1 to 5 parts of ethanol, 5 to 10 parts of water, 15 to 25 parts of propylene glycol and 6 to 68.3 parts of glycerol.
In the invention, the raw materials providing the fragrance of the pepper mainly comprise refined pepper products, and the refined pepper products have special fragrance of the pepper, but have single fragrance, lack sweet fragrance and cool feeling, and cannot make people feel the mouth and teeth to promote the secretion of body fluid when smelling. The bergamot oil, the peppermint oil, the pine needle oil, the linalool and the cooling agent are used as the blending agent, wherein the bergamot oil has fresh and sweet fruit fragrance similar to lemon and fresh fruit sweet fragrance, the peppermint oil has fresh and strong mint fragrance with little grass smell, the cooling gas can be kept through all the time, the pine needle oil has the characteristic fragrance of pine and cool mint feeling, the linalool has weak citrus fruit fragrance, is soft and transparent, has obvious aftertaste, can increase the cooling feeling and is refreshing to the heart and the spleen; the invention combines the substances with the refined substances of the pepper, increases cool feeling and fresh feeling, and enriches the fragrance of the pepper; the menthyl acetate adds light fragrance to the electronic cigarette oil with the pepper flavor. Through the matching use of the raw materials, the prepared pepper has fresh, sweet and refreshing flavor, is rich in fragrance and makes consumers feel like pictures when smelling.
The electronic cigarette liquid with pepper flavor and the preparation method thereof disclosed by the application can bring beneficial effects including but not limited to:
the electronic cigarette liquid prepared by the invention has obvious pepper characteristic flavor, shows style characteristics of freshness, dainty taste, sweetness and smoothness in the throat, enriches the smoking style of the electronic cigarette, can meet the requirements of different consumer groups, has a certain health care function, and can effectively reduce the potential harm of the electronic cigarette to consumers.
Detailed Description
In order to make the objects, technical solutions and advantages of the present application more apparent, the present application is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of and not restrictive on the broad application.
On the contrary, this application is intended to cover any alternatives, modifications, equivalents, and alternatives that may be included within the spirit and scope of the application as defined by the appended claims. Furthermore, in the following detailed description of the present application, certain specific details are set forth in order to provide a thorough understanding of the present application. It will be apparent to one skilled in the art that the present application may be practiced without these specific details.
The following describes the electronic cigarette liquid with pepper flavor and the preparation method thereof according to the embodiments of the present application in detail. It is to be noted that the following examples are only for explaining the present application and do not constitute a limitation to the present application.
Example 1
The electronic cigarette liquid with the pepper flavor comprises the following raw materials in parts by weight: 1 part of refined pepper product, 1 part of bergamot oil, 1 part of peppermint oil, 1 part of pine needle oil, 1 part of linalool, 0.2 part of menthyl acetate, 0.5 part of cooling agent, 5 parts of refined tobacco product, 1 part of ethanol, 5 parts of water, 15 parts of propylene glycol and 68.3 parts of glycerol.
The preparation method comprises the following steps:
1mL of the electronic cigarette liquid prepared from the raw materials and the method is added into an atomizer, and the electronic cigarette liquid is evaluated by professional smoke evaluation personnel to have fresh, sweet and refreshing pepper flavor.
Comparative example 1
The preparation method of the raw materials is the same as that of example 1 except that the raw materials do not contain pepper refined powder.
Example 2
2 parts of refined pepper product, 2 parts of bergamot oil, 2 parts of peppermint oil, 2 parts of pine needle oil, 2 parts of linalool, 0.5 part of menthyl acetate, 1 part of cooling agent, 7 parts of refined tobacco product, 2 parts of ethanol, 5 parts of water, 20 parts of propylene glycol and 54.5 parts of glycerol.
The preparation method comprises the following steps:
1mL of the electronic cigarette liquid prepared from the raw materials and the method is added into an atomizer, and the electronic cigarette liquid is evaluated by professional smoke evaluation personnel to have fresh, sweet and refreshing pepper flavor.
Comparative example 2
The raw materials and preparation method are the same as example 2 except that the raw materials do not contain bergamot oil.
Example 3
5 parts of refined pepper product, 5 parts of bergamot oil, 3 parts of peppermint oil, 3 parts of pine needle oil, 3 parts of linalool, 0.8 part of menthyl acetate, 1.5 parts of cooling agent, 10 parts of refined tobacco product, 3 parts of ethanol, 7 parts of water, 25 parts of propylene glycol and 33.7 parts of glycerol.
The preparation method comprises the following steps:
1mL of the electronic cigarette liquid prepared from the raw materials and the method is added into an atomizer, and the electronic cigarette liquid is evaluated by professional smoke evaluation personnel to have fresh, sweet and refreshing pepper flavor.
Comparative example 3
The raw materials and the preparation method are the same as example 3 except that the raw materials do not contain pine needle oil.
Example 4
7 parts of refined pepper product, 7 parts of bergamot oil, 4 parts of peppermint oil, 4 parts of pine needle oil, 4 parts of linalool, 1 part of menthyl acetate, 2 parts of cooling agent, 12 parts of refined tobacco product, 4 parts of ethanol, 10 parts of water, 25 parts of propylene glycol and 20.0 parts of glycerol.
The preparation method comprises the following steps:
1mL of the electronic cigarette liquid prepared from the raw materials and the method is added into an atomizer, and the electronic cigarette liquid is evaluated by professional smoke evaluation personnel to have fresh, sweet and refreshing pepper flavor.
Comparative example 4
The procedure of example 4 was repeated except that the starting materials contained no menthyl acetate.
Example 5
10 parts of refined pepper product, 10 parts of bergamot oil, 5 parts of peppermint oil, 5 parts of pine needle oil, 5 parts of linalool, 1.5 parts of menthyl acetate, 2.5 parts of cooling agent, 15 parts of refined tobacco product, 5 parts of ethanol, 10 parts of water, 25 parts of propylene glycol and 6 parts of glycerol.
The preparation method comprises the following steps:
1mL of the electronic cigarette tobacco juice prepared by the raw materials and the method is added into an atomizer, and the electronic cigarette tobacco juice is evaluated by professional smokers, so that the electronic cigarette tobacco juice has fresh, sweet and refreshing pepper flavor.
Comparative example 5
The raw materials and the preparation method are the same as example 5 except that the raw materials do not contain the cooling agent.
According to the cigarette sensory quality evaluation standard GB5606.4-2005, in combination with the sensory characteristics of electronic cigarettes, 6 evaluation indexes and scores are set according to different weights, which are shown in Table 1:
TABLE 1
Sensory evaluation is carried out on the electronic cigarette liquid obtained in the embodiments 1 to 5 and the comparative examples 1 to 5, an arithmetic mean value is obtained according to evaluation results of experts according to the evaluation results, a valid number is reserved in the results, and statistical results are shown in table 2.
TABLE 2
| Sample(s) | Satisfaction feeling | Fragrance | Tuning | Miscellaneous qi | Irritation property | Aftertaste |
| Example 1 | 22.5 | 21.5 | 4.5 | 8.5 | 17.0 | 13.5 |
| Example 2 | 23.5 | 21.5 | 4.5 | 8.5 | 16.5 | 13.0 |
| Example 3 | 23.0 | 22.0 | 4.5 | 8.5 | 16.5 | 14.0 |
| Example 4 | 23.0 | 22.5 | 4.5 | 8.5 | 16.5 | 13.5 |
| Example 5 | 23.5 | 21.5 | 4.5 | 8.5 | 16.5 | 13.0 |
| Comparative example 1 | 20.0 | 19.0 | 4.0 | 8.5 | 17.0 | 13.0 |
| Comparative example 2 | 21.5 | 20.5 | 4.0 | 8.0 | 15.5 | 12.5 |
| Comparative example 3 | 20.5 | 20.0 | 4.0 | 7.5 | 16.0 | 12.5 |
| Comparative example 4 | 21.0 | 20.5 | 4.0 | 8.0 | 15.5 | 12.0 |
| Comparative example 5 | 20.5 | 20.0 | 4.0 | 7.5 | 15.5 | 12.0 |
As can be seen from table 2, sensory evaluation of the electronic cigarette liquids of examples 1 to 5 and comparative examples 1 to 5 clearly shows that the sensory quality evaluation indexes of examples 1 to 5 are superior to those of comparative examples 1 to 5.
The above description is intended to be illustrative of the preferred embodiment of the present invention and should not be taken as limiting the invention, but rather, the intention is to cover all modifications, equivalents, and alternatives falling within the spirit and scope of the invention.
Claims (9)
1. The electronic cigarette liquid with the pepper flavor is characterized by being prepared from the following components in parts by weight: 1-10 parts of refined pepper, 1-10 parts of bergamot oil, 1-5 parts of peppermint oil, 1-5 parts of pine needle oil, 1-5 parts of linalool, 0.2-1.5 parts of menthyl acetate, 0.5-2.5 parts of cooling agent, 5-15 parts of refined tobacco, 1-5 parts of ethanol, 5-10 parts of water, 15-25 parts of propylene glycol and 6-68.3 parts of glycerol;
the preparation method of the refined zanthoxylum bungeanum product comprises the following steps: placing fresh pepper in a rotary cage dryer for drying, immediately placing the dried pepper in a refrigerator at the temperature of-5 ℃ for cooling, wherein the cooling time is 20 to 30min; after standing, taking out the pepper, placing the pepper in a rotary cage dryer, and repeating the steps of heating and drying, cooling and standing for three times; putting the pepper cooled and kept stand for the third time into a freeze dryer, and drying for 12 to 24h; separating dried pericarpium Zanthoxyli from semen Zanthoxyli, pulverizing pericarpium Zanthoxyli, collecting pericarpium Zanthoxyli powder, and subjecting to supercritical CO 2 Extracting to obtain pepper essential oil; removing amide substances in the zanthoxylum essential oil by using petroleum ether extraction to obtain a zanthoxylum refined product.
2. The electronic cigarette liquid with the pepper flavor as claimed in claim 1, wherein the pepper refined product is one or more refined products of pepper substances from Chinese tribute pepper, wudu dahongpao and Hancheng dahongpao.
3. The electronic cigarette liquid with the pepper flavor as claimed in claim 1, wherein the pepper used in the pepper refined product is fresh pepper.
4. The electronic cigarette liquid with pepper flavor according to claim 1, characterized in that the supercritical CO 2 The extraction pressure of the extraction is 20 to 40MPa, the extraction temperature is 40 to 50 ℃, the extraction time is 2 to 4 hours 2 The flow rate is controlled to be 25 to 30L/h.
5. The electronic cigarette liquid with the pepper flavor as claimed in claim 1, wherein the ratio of the pepper essential oil to the petroleum ether is 1 to 1, the extraction time is 1 to 2 hours, and the petroleum ether is removed by rotary evaporation after the extraction is finished.
6. The electronic cigarette liquid with the pepper flavor according to claim 1, wherein the tobacco refined substance is one or more of burley tobacco, flue-cured tobacco or cigar tobacco fragment refined substances.
7. The electronic cigarette liquid with the pepper flavor as claimed in claim 1, wherein the preparation method of the tobacco refined product comprises the following steps: placing tobacco fragments into a closed extraction tank, vacuumizing, and injecting an extraction solvent into the tank, wherein the extraction solvent is one or more of dimethyl ether, butane and cyclohexane, the volume ratio of the tobacco fragments to the extraction solvent is (1) - (5) - (1), the extraction temperature is 30) - (50 ℃, and the extraction time is 3) - (5 h, so that the obtained sample is the tobacco extract; refining the tobacco extract by molecular distillation, and collecting light components to obtain the tobacco refined product.
8. The electronic cigarette liquid with pepper flavor as claimed in claim 7, wherein the molecular distillation conditions are that the feeding speed is 6.0-8.0 mL/min, the vacuum degree is 10-20 Pa, the heating temperature is 40-100 ℃, the cooling temperature is 25-35 ℃, and the film scraping rotation speed is 140-150 r/min.
9. A preparation method of electronic cigarette liquid with pepper flavor is characterized by comprising the following steps:
(1) Preparing a pepper refined product: placing fresh pepper in a rotary cage dryer, wherein the drying temperature is 40 to 50 ℃, and the drying time is 2 to 4 hours; immediately placing the dried pepper in a refrigerator at the temperature of-5 ℃ for cooling, wherein the cooling time is 20 to 30min; after standing, taking out the pepper, placing the pepper in a rotary cage dryer, and repeating the steps of heating and drying, cooling and standing for three times; putting the pepper cooled and kept stand for the third time into a freeze dryer, and drying for 12 to 24h; separating the dried pericarpium Zanthoxyli from semen Zanthoxyli, pulverizing, and sieving with 50 mesh sieve; collecting pericarpium Zanthoxyli powder, and performing supercritical CO 2 Extracting under the extraction pressure of 20 to 40MPa, at the extraction temperature of 40 to 50 ℃ for 2 to 4 hours 2 Controlling the flow at 25 to 30L/h to obtain the pepper essential oil; using stonesExtracting with oil ether to remove amide substances in the zanthoxylum essential oil, wherein the proportion of the zanthoxylum essential oil to the petroleum ether is 1 to 3 to 1, the extraction time is 1 to 2 hours, and after the extraction is finished, removing the petroleum ether by rotary evaporation to obtain a zanthoxylum refined substance;
(2) Preparing a tobacco refined product: placing tobacco fragments into a closed extraction tank, vacuumizing, and injecting an extraction solvent into the tank, wherein the extraction solvent is one or more of dimethyl ether, butane and cyclohexane, the volume ratio of the tobacco fragments to the extraction solvent is (1) - (5) - (1), the extraction temperature is 30) - (50 ℃, and the extraction time is 3) - (5 h, so that the obtained sample is the tobacco extract; refining the tobacco extract by molecular distillation, wherein the feeding speed is 6.0-8.0 mL/min, the vacuum degree is 10-20 Pa, the heating temperature is 40-100 ℃, the cooling temperature is 25-35 ℃, the film scraping speed is 140-150 r/min, and collecting light components, namely the refined tobacco product;
(3) Preparing electronic cigarette liquid: the electronic cigarette liquid with the pepper flavor is obtained by fully and uniformly mixing the following raw materials in parts by weight: 1-10 parts of refined pepper, 1-10 parts of bergamot oil, 1-5 parts of peppermint oil, 1-5 parts of pine needle oil, 1-5 parts of linalool, 0.2-1.5 parts of menthyl acetate, 0.5-2.5 parts of cooling agent, 5-15 parts of refined tobacco, 1-5 parts of ethanol, 5-10 parts of water, 15-25 parts of propylene glycol and 6-68.3 parts of glycerol.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111628468.1A CN114468345B (en) | 2021-12-28 | 2021-12-28 | Electronic cigarette liquid with pepper flavor and preparation method thereof |
| KR1020220181127A KR20230100643A (en) | 2021-12-28 | 2022-12-21 | Tobacco liquid of electronic cigarette having peppermint taste and manufacturing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111628468.1A CN114468345B (en) | 2021-12-28 | 2021-12-28 | Electronic cigarette liquid with pepper flavor and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN114468345A CN114468345A (en) | 2022-05-13 |
| CN114468345B true CN114468345B (en) | 2022-11-15 |
Family
ID=81495732
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202111628468.1A Active CN114468345B (en) | 2021-12-28 | 2021-12-28 | Electronic cigarette liquid with pepper flavor and preparation method thereof |
Country Status (2)
| Country | Link |
|---|---|
| KR (1) | KR20230100643A (en) |
| CN (1) | CN114468345B (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101961300A (en) * | 2010-09-29 | 2011-02-02 | 重庆市超临界精细化工生产力促进中心有限公司 | Perfume composition containing pepper aroma essential oil and preparation method thereof |
| CN110358630A (en) * | 2019-06-25 | 2019-10-22 | 河南中烟工业有限责任公司 | A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette |
| CN110419765A (en) * | 2019-08-12 | 2019-11-08 | 四川三联新材料有限公司 | A kind of preparation method and preparation facilities of electronic cigarette tobacco tar |
| CN110540899A (en) * | 2019-09-18 | 2019-12-06 | 成都中医药大学 | Zanthoxylum bungeanum flavor essence for cigarette bead blasting and application of zanthoxylum bungeanum flavor essence in cigarettes |
| CN110575413A (en) * | 2019-10-24 | 2019-12-17 | 山东花物堂生物科技有限公司 | Preparation method of pepper extract and application of pepper extract in cosmetics |
| CN113633017A (en) * | 2020-05-11 | 2021-11-12 | 中国烟草总公司郑州烟草研究院 | Tobacco extract, preparation method and application thereof, and tobacco product |
| WO2021234034A1 (en) * | 2020-05-20 | 2021-11-25 | V.F.P. France | Vaping compositions |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20170172204A1 (en) * | 2015-12-18 | 2017-06-22 | Altria Client Services Llc | Strength enhancers and method of achieving strength enhancement in an electronic vapor device |
-
2021
- 2021-12-28 CN CN202111628468.1A patent/CN114468345B/en active Active
-
2022
- 2022-12-21 KR KR1020220181127A patent/KR20230100643A/en unknown
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101961300A (en) * | 2010-09-29 | 2011-02-02 | 重庆市超临界精细化工生产力促进中心有限公司 | Perfume composition containing pepper aroma essential oil and preparation method thereof |
| CN110358630A (en) * | 2019-06-25 | 2019-10-22 | 河南中烟工业有限责任公司 | A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette |
| CN110419765A (en) * | 2019-08-12 | 2019-11-08 | 四川三联新材料有限公司 | A kind of preparation method and preparation facilities of electronic cigarette tobacco tar |
| CN110540899A (en) * | 2019-09-18 | 2019-12-06 | 成都中医药大学 | Zanthoxylum bungeanum flavor essence for cigarette bead blasting and application of zanthoxylum bungeanum flavor essence in cigarettes |
| CN110575413A (en) * | 2019-10-24 | 2019-12-17 | 山东花物堂生物科技有限公司 | Preparation method of pepper extract and application of pepper extract in cosmetics |
| CN113633017A (en) * | 2020-05-11 | 2021-11-12 | 中国烟草总公司郑州烟草研究院 | Tobacco extract, preparation method and application thereof, and tobacco product |
| WO2021234034A1 (en) * | 2020-05-20 | 2021-11-25 | V.F.P. France | Vaping compositions |
Also Published As
| Publication number | Publication date |
|---|---|
| CN114468345A (en) | 2022-05-13 |
| KR20230100643A (en) | 2023-07-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105146739B (en) | The preparation method of a kind of mao of cigarette quintessence oil and application thereof | |
| CN101548797B (en) | Cigarette and preparation method thereof | |
| JPS6024172A (en) | Production of tobacco flavor | |
| CN102793264B (en) | Preparation method of magnolia fruit extract and application thereof in cigarette | |
| WO2021223319A1 (en) | Flavor additive for cigarettes and preparation method therefor | |
| CN105112161A (en) | Casing flavor for cigarette paper of cigars | |
| CN111671134A (en) | Mint flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid | |
| CN111418892A (en) | Cigarette filter stick additive and application thereof | |
| CN109259296B (en) | Electronic cigarette oil with tea baking fragrance and preparation method and application thereof | |
| CN101637303A (en) | Lemon extract, preparation method thereof and application thereof in cigarette flavoring | |
| CN108618192A (en) | A kind of 15 are formulated electronic cigarette tobacco tar and preparation method thereof | |
| CN114468345B (en) | Electronic cigarette liquid with pepper flavor and preparation method thereof | |
| CN114085711B (en) | Plant essence for electronic atomized liquid and preparation method thereof | |
| CN114410376A (en) | Cigarette bead-blasting essential oil with pepper flavor and preparation method thereof | |
| CN109452684B (en) | Electronic cigarette liquid with pineapple-flavor fragrance and preparation method thereof | |
| CN115558548A (en) | Rosin-flavored essence for cigarettes as well as preparation method and application thereof | |
| CN114098141A (en) | Electronic atomized liquid containing borneol plant components and preparation method thereof | |
| CN113693264A (en) | Licorice root and mixed fruit tobacco tar and preparation method thereof | |
| CN115721683A (en) | Electronic atomized liquid and preparation and use methods thereof | |
| CN110804497A (en) | Preparation method of saffron extract for tobacco bead blasting | |
| KR101724825B1 (en) | Helpful agent contaiend chicory and aconitie tuber for prohibit smoking | |
| CN110720658B (en) | Preparation method of acacia flower extract for tobacco bead blasting | |
| CN114680362B (en) | Electronic cigarette liquid with refreshing function | |
| CN115428980B (en) | Tobacco essence suitable for heating non-combustible tobacco products | |
| CN113862081B (en) | Composite extract for cigar spice and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |